CN106176480A - A kind of food grade compositions with antiseptic activity and the application in cosmetics thereof - Google Patents
A kind of food grade compositions with antiseptic activity and the application in cosmetics thereof Download PDFInfo
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- CN106176480A CN106176480A CN201610778566.6A CN201610778566A CN106176480A CN 106176480 A CN106176480 A CN 106176480A CN 201610778566 A CN201610778566 A CN 201610778566A CN 106176480 A CN106176480 A CN 106176480A
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- cosmetics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of food grade compositions with antiseptic activity and the application in cosmetics thereof, said composition is made up of glycerol caprylate, p anisic acid, Magnolia bark extract.Three sections of raw materials used by the present invention are food stage, are widely used in food as natural plant food preservative.Three sections of raw material sources are in natural plants, and safety is high, non-stimulated.The present composition can effectively suppress antibacterial, mycete, yeast in cosmetics, extends the life-span of product, it is ensured that the safety of product, and prevents user from causing possible infection because using the product polluted by microorganism.Said composition not only has antisepsis, also has effect of skin moistening, Sage Extract, anti-acne, slow down aging.
Description
Technical field
The present invention relates to cosmetics processing technique field, be specifically related to a kind of food grade compositions with antiseptic activity and
Its application in cosmetics.
Background technology
Adding preservative in cosmetics, its effect is to stop growth of microorganism, extends life of product, prevents consumer
Employ because of the product of microorganism pollution infected.In this demand, on market, most products are anti-by adding chemistry
Rotten agent is to reach preservative efficacy, and product can be played a protective role by these chemical preservatives, but is likely to induce skin simultaneously
Stimulate.The side effect of preservative reduces consumer's degree of belief to product, becomes consumer and is reluctant to be continuing with beauty and make-up
The big factors of product.Under this trend, there is preservative efficacy and don't the human body irritating preservative of generation has just been become change
The new lover of cosmetic circle.Natural plant preservative, extracts effective antipathogenic composition in natural plants, adds with rational collocation
In cosmetic formulations, the growth of suppression microorganism, plays the effect of protection cosmetics, also eliminates simultaneously and lack skin irritant
Point.
Summary of the invention
Have problems in prior art, it is an object of the invention to provide a kind of food stage group with antiseptic activity
Compound and the application in cosmetics thereof.This invention is raw materials used is food stage, and it derives from natural plants, safety
High, non-stimulated.The present invention effectively suppresses antibacterial, mycete, yeast in cosmetics, prevents growth of microorganism, plays product
Protective effect.Cortex Magnoliae Officinalis tree extract in the present invention contains abundant Magnolol and Honokiol, not only has strong antibacterial effect
Really, also having antiinflammatory, anti-acne, moistening effect, to DPPH free radical, hydroxy radical all has scavenging action, plays anti-oxidation efficacy,
Can delaying skin aging.
First purpose realizing the present invention can reach by adopting the following technical scheme that:
A kind of food grade compositions with antiseptic activity, it is characterised in that include the as follows of weight percentage
Component:
Glycerol caprylate 10-80%
P-anisic acid 10-60%
Cortex Magnoliae Officinalis tree extract 5-60%；
The weight percentage sum of said components is 100%, and wherein, described Cortex Magnoliae Officinalis tree extract is with effective solid content group
Divide meter.
As preferably, there is the food grade compositions of antiseptic activity, including the following component of weight percentage:
Glycerol caprylate 15-80%
P-anisic acid 15-55%
Cortex Magnoliae Officinalis tree extract 5-56%；
The weight percentage sum of said components is 100%, and wherein, described Cortex Magnoliae Officinalis tree extract is with effective solid content group
Divide meter.
As preferably, there is the food grade compositions of antiseptic activity, including the following component of weight percentage:
Glycerol caprylate 30-60%
P-anisic acid 30%
Cortex Magnoliae Officinalis tree extract 10-40%；
The weight percentage sum of said components is 100%, and wherein, described Cortex Magnoliae Officinalis tree extract is with effective solid content group
Divide meter.
As preferably, there is the food grade compositions of antiseptic activity, including the following component of weight percentage:
Glycerol caprylate 30%
P-anisic acid 30%
Cortex Magnoliae Officinalis tree extract 40%.
As preferably, there is the food grade compositions of antiseptic activity, including the following component of weight percentage:
Glycerol caprylate 60%
P-anisic acid 30%
Cortex Magnoliae Officinalis tree extract 10%.
The preparation method of the described food grade compositions with antiseptic activity: according to formulation ratio by glycerol caprylate, p-
Anisic acid, Cortex Magnoliae Officinalis tree extract mix homogeneously and get final product.
The application in cosmetics of a kind of food grade compositions with antiseptic activity, said composition adding in cosmetics
Dosage is the 0.01%-3.00% of cosmetics gross weight.
As preferably, said composition addition in cosmetics is the 0.3%-2.0% of cosmetics gross weight.
As preferably, said composition addition in cosmetics is the 0.5%-1.5% of cosmetics gross weight.
As preferably, said composition addition in cosmetics is the 0.6-1.2% of cosmetics gross weight.
As preferably, described cosmetics are facial film class cosmetics, water preparation class cosmetics, type of latex type cosmetics or cream kind
Cosmetic.
The preparation method of described cosmetics is conventional preparation method.
The beneficial effects of the present invention is:
The present composition is made up of glycerol caprylate, p-anisic acid, Magnolia bark extract, optimize them simultaneously it
Between proportion relation, by numerous studies, the present invention finds that three kinds of raw materials have Synergistic in antisepsis each other and make
With.Three sections of raw materials used by the present invention are food stage, are widely used in food as natural plant food preservative.Three sections
Raw material sources are in natural plants, and safety is high, non-stimulated.The present composition can effectively suppress in the cosmetics antibacterial,
Mycete, yeast, extend the life-span of product, it is ensured that the safety of product, and prevents user because using the product polluted by microorganism
Product and cause possible infection.Cortex Magnoliae Officinalis tree extract in the present invention contains abundant Magnolol and Honokiol, not only has
Strong antibacterial effect, also has antiinflammatory, anti-acne, moistening effect, and to DPPH free radical, hydroxy radical all has scavenging action, plays
Anti-oxidation efficacy, can delaying skin aging.Said composition not only has antisepsis, also has antiinflammatory, anti-acne, moisturizing, delays
Old and feeble effect.
Accompanying drawing explanation
Fig. 1 is that zest test tested material A or B are added in the left side, and the right control wells is the photo of the speckle examination device of blank；
Fig. 2 is that zest tests tested material A or B is pasted on the photo on skin equably；
Fig. 3 is the arm the using zest test tested material A photo through 24 hours patch tests；
In Fig. 3, A is test position, and B is blank position.
Fig. 4 is the arm the using zest test tested material B photo through 24 hours patch tests.
In Fig. 4, C is test position, and D is blank position.
Detailed description of the invention
In order to make technical scheme and advantage become apparent from understanding, the present invention is the most furtherly
Bright, but declare specific embodiment described in the invention at this and be only intended to illustrate, it is not intended to limit the present invention.This
Employed in invention, raw material is all commercially available.
Embodiment 1-8:
A kind of food grade compositions with antiseptic activity, including the following component of weight percentage, is specifically shown in
Table 1.
Table 1
| Glycerol caprylate | P-anisic acid | Cortex Magnoliae Officinalis tree extract | |
| Embodiment 1 (Wt%) | 80 | 15 | 5 |
| Embodiment 2 (Wt%) | 70 | 10 | 20 |
| Embodiment 3 (Wt%) | 60 | 30 | 10 |
| Embodiment 4 (Wt%) | 50 | 40 | 10 |
| Embodiment 5 (Wt%) | 40 | 10 | 50 |
| Embodiment 6 (Wt%) | 30 | 30 | 40 |
| Embodiment 7 (Wt%) | 20 | 20 | 60 |
| Embodiment 8 (Wt%) | 10 | 60 | 30 |
The preparation method of the described food grade compositions with antiseptic activity: according to formulation ratio by glycerol caprylate, p-
Anisic acid, Cortex Magnoliae Officinalis tree extract mix homogeneously and get final product.
Table 2 below is the dosage that examples detailed above 1-8 adds 1% in cosmetics cream, carries out anti-corrosive properties challenge test
Result, can confirm that the different proportion collocation that has in the food grade compositions of antiseptic activity of the present invention is respectively provided with preferable anticorrosion
Effect.
Table 2 anti-corrosive properties challenge test result
Table 3
Table 4 below is the dosage that above-mentioned comparative example 1-6 adds 1% in cosmetics cream, carries out anti-corrosive properties challenge
Property test as a result, it is possible to find, there is between these three raw material good anticorrosion synergy, only three is compounding just can be relatively
Good reaches comprehensive antisepsis.
Table 4 anti-corrosive properties challenge test result
Application Example 1-3:
The application in facial film class cosmetics of a kind of food grade compositions with antiseptic activity, described facial film class cosmetics
Including the following component of weight percentage, specifically it is shown in Table 5.
Table 5 facial film system example
Application Example 4-6:
The application in water preparation class cosmetics of a kind of food grade compositions with antiseptic activity, described water preparation class cosmetics
Including the following component of weight percentage, specifically it is shown in Table 6.
Table 6 water preparation system example
Application Example 7-9:
The application in type of latex type cosmetics of a kind of food grade compositions with antiseptic activity, described type of latex type cosmetics
Including the following component of weight percentage, specifically it is shown in Table 7.
Table 7 emulsion system example
Application Example 10-12:
The application in cream kind cosmetics of a kind of food grade compositions with antiseptic activity, described cream kind cosmetics
Including the following component of weight percentage, specifically it is shown in Table 8.
Table 8 cream system example
One, product stability evaluation:
In order to confirm the stability of the embodiment above, evaluate product over 1 month by doing the experiment of cold-resistant, heat-resisting, room temperature
Stability, concrete outcome is shown in Table 9.
Table 9 stability result
Table 10 below is that anti-corrosive properties challenge result, can confirm that the food grade compositions with antiseptic activity of the present invention is being changed
Cosmetic serves antiseptical effect.
Table 10 anti-corrosive properties challenge test result
Zest is tested:
Skin irritation is tested by sealing patch experimental verification.Select 18-25 year Pass Test require volunteer
As study subject.Number is 40 examples.Hereinafter the food grade compositions with antiseptic activity for the present invention is applied to cosmetics
Formula, with this as tested material.
Zest test tested material A: glycerol caprylate, p-anisic acid, Cortex Magnoliae Officinalis tree extract are with weight percent 80:
15:5 forms, and adds 1.2% above-mentioned additive in tested material.
Zest test tested material B: glycerol caprylate, p-anisic acid, Cortex Magnoliae Officinalis tree extract are with weight percent 80:
15:5 forms, and adds 2% above-mentioned additive in tested material.
Table 11 zest test tested material formula
| Composition | Zest test tested material A | Zest test tested material B |
| Water | 86% | 84.5% |
| Glycerol | 5% | 5% |
| Glycerin polyether-26 | 3% | 3% |
| Allantoin | 0.1% | 0.1% |
| Herba portulacae extract | 1% | 1% |
| Xanthan gum | 0.08% | 0.08% |
| Pectin | 1% | 1% |
| Hydrolyzed vegetable protein | 0.8% | 0.8% |
| Tremella extract | 1% | 1% |
| Beta glucan | 1% | 1% |
| Hyaluronate sodium | 0.1% | 0.1% |
| Carbomer | 0.08% | 0.08% |
| Potassium hydroxide | In right amount | In right amount |
| Food grade compositions described in embodiment 1 | 1.2% | 2% |
Test method:
1) inside arm, first choose appropriate area, select qualified patch material, tested material is put into speckle examination device, uses
Amount is about 0.03g.Control wells is blank (not putting any material) (Fig. 1), gently presses with palm and is allowed to be pasted on equably skin
On skin, continue 24h (Fig. 2).
2) it is spaced 30min after removing tested material speckle examination device, after impression disappears, observes dermoreaction.
Patch test presses skin adverse reaction classification marking, and concrete grade scale is shown in Table 12.
Table 12
| Skin adverse reaction | Classification |
| Reactionless | 0 |
| Light red speckle | 1 |
| Erythema, pimple | 2 |
| Erythema, edema, pimple, vesicle | 3 |
| Erythema, edema, bulla | 4 |
Result: through 24 hours patch tests, 40 study subjects to two tested material all without occurring that erythema etc. is bad instead
Should, the food grade compositions with antiseptic activity of the present invention is applied in cosmetics without any zest.Partial test result
As shown in Figure 3, Figure 4.
Performance test:
A kind of food grade compositions with antiseptic activity of the present invention not only has antiseptic property, also has antiinflammatory, dispels
Pox, moisturizing, the effect of slow down aging.
Table 13
The Application Example 13 of compositions adding the present invention is carried out with the blank sample of the compositions being not added with the present invention
Clinical experiment evaluate, experiment condition is the volunteer 50 (each 25 of men and women) all having long pox phenomenon, the age be 18-35 year, its
In 50 volunteers long pox situations during on probation belong to 38 people of slight small pox, 8 people that small pox is more serious, 4 serious people.
Volunteer uses once every day, and left face tested material is the example 4 of the compositions adding the present invention, and right face tested material is for being not added with this
The blank sample of the compositions of invention.After using continuously 28 days, 28 days, the using effect to product is evaluated.Anti-acne effect is very
Being well 5 points, anti-acne effect preferably 4 points, anti-acne effect is generally 3 points, and anti-acne effect difference is 2 points.Moistening effect is 5 very well
Point, moistening effect preferably 4 points, moistening effect is generally 3 points, and moistening effect difference is 2 points.Experimental result is as shown in table 14 below:
Table 14
From upper table 14, the compositions of the present invention has good anti-acne and becomes reconciled moistening effect.
In sum, a kind of glycerol that food grade compositions is proper proportion octanoic acid with antiseptic activity of the present invention
Ester, p-anisic acid, Cortex Magnoliae Officinalis tree extract.Natural plant food preservative, in cosmetics application can not only effectively suppress antibacterial,
Mycete, yeast, protect product, extends life of product, the anti-acne also having had, moistening effect.
For a person skilled in the art, can technical scheme as described above and design, make other each
Plant corresponding change and deformation, and all these changes and deforms the protection model that all should belong to the claims in the present invention
Within enclosing.
Claims (10)
1. a food grade compositions with antiseptic activity, it is characterised in that include following group of weight percentage
Point:
Glycerol caprylate 10-80%
P-anisic acid 10-60%
Cortex Magnoliae Officinalis tree extract 5-60%；
The weight percentage sum of said components is 100%, and wherein, described Cortex Magnoliae Officinalis tree extract is with effective solid content component
Meter.
The food grade compositions with antiseptic activity the most according to claim 1, it is characterised in that include percentage by weight
The following component of content meter:
Glycerol caprylate 15-80%
P-anisic acid 15-55%
Cortex Magnoliae Officinalis tree extract 5-56%；
The weight percentage sum of said components is 100%.
The food grade compositions with antiseptic activity the most according to claim 2, it is characterised in that there is antiseptic activity
Food grade compositions, including the following component of weight percentage:
Glycerol caprylate 30-60%
P-anisic acid 30%
Cortex Magnoliae Officinalis tree extract 10-40%；
The weight percentage sum of said components is 100%.
The food grade compositions with antiseptic activity the most according to claim 3, it is characterised in that there is antiseptic activity
Food grade compositions, including the following component of weight percentage:
Glycerol caprylate 30%
P-anisic acid 30%
Cortex Magnoliae Officinalis tree extract 40%.
The food grade compositions with antiseptic activity the most according to claim 3, it is characterised in that there is antiseptic activity
Food grade compositions, including the following component of weight percentage:
Glycerol caprylate 60%
P-anisic acid 30%
Cortex Magnoliae Officinalis tree extract 10%.
6. according to claim 1-5 any one, there is the application in cosmetics of the food grade compositions of antiseptic activity,
Said composition addition in cosmetics is the 0.01%-5.00% of cosmetics gross weight.
The food grade compositions with antiseptic activity the most according to claim 6 application in cosmetics, its feature exists
In: said composition addition in cosmetics is the 0.3%-2.0% of cosmetics gross weight.
The food grade compositions with antiseptic activity the most according to claim 7 application in cosmetics, its feature exists
In: said composition addition in cosmetics is the 0.5-1.5% of cosmetics gross weight.
The food grade compositions with antiseptic activity the most according to claim 8 application in cosmetics, its feature exists
In: said composition addition in cosmetics is the 0.6-1.2% of cosmetics gross weight.
The food grade compositions with antiseptic activity the most according to claim 5 application in cosmetics, its feature exists
In: described cosmetics are facial film class cosmetics, water preparation class cosmetics, cleaning class cosmetics, type of latex type cosmetics or cream kind
Cosmetic.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610778566.6A CN106176480A (en) | 2016-08-30 | 2016-08-30 | A kind of food grade compositions with antiseptic activity and the application in cosmetics thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610778566.6A CN106176480A (en) | 2016-08-30 | 2016-08-30 | A kind of food grade compositions with antiseptic activity and the application in cosmetics thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106580795A (en) * | 2016-12-28 | 2017-04-26 | 中山市荼薇化妆品有限公司 | Extraction method of Tuwei flower extract having effects of moisture retention and whitening |
| CN112156050A (en) * | 2020-11-13 | 2021-01-01 | 东晟源研究院(广州)有限公司 | Plant preservative composition suitable for cosmetics and preparation method thereof |
| CN112438915A (en) * | 2019-08-28 | 2021-03-05 | 广州市南方医康生物科技有限公司 | Skin care composition, cosmetic and preparation method thereof |
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| CN102641225A (en) * | 2012-04-26 | 2012-08-22 | 天津郁美净集团有限公司 | Cosmetic containing plant bacteriostatic composition |
| CN104546522A (en) * | 2014-12-18 | 2015-04-29 | 广东雅威生物科技有限公司 | Composition with high-efficiency broad-spectrum antibacterial capacity and application of composition in cosmetics |
| CN104840399A (en) * | 2015-05-18 | 2015-08-19 | 中山安理汇日用品有限公司 | Firming cream formula with self corrosion-resistant property |
| CN107106434A (en) * | 2014-12-26 | 2017-08-29 | 莱雅公司 | Cosmetic composition comprising paraanisic acid and hydroxyacetophenone, its purposes and its cosmetic method |
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2016
- 2016-08-30 CN CN201610778566.6A patent/CN106176480A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102641225A (en) * | 2012-04-26 | 2012-08-22 | 天津郁美净集团有限公司 | Cosmetic containing plant bacteriostatic composition |
| CN104546522A (en) * | 2014-12-18 | 2015-04-29 | 广东雅威生物科技有限公司 | Composition with high-efficiency broad-spectrum antibacterial capacity and application of composition in cosmetics |
| CN107106434A (en) * | 2014-12-26 | 2017-08-29 | 莱雅公司 | Cosmetic composition comprising paraanisic acid and hydroxyacetophenone, its purposes and its cosmetic method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106580795A (en) * | 2016-12-28 | 2017-04-26 | 中山市荼薇化妆品有限公司 | Extraction method of Tuwei flower extract having effects of moisture retention and whitening |
| CN112438915A (en) * | 2019-08-28 | 2021-03-05 | 广州市南方医康生物科技有限公司 | Skin care composition, cosmetic and preparation method thereof |
| CN112438915B (en) * | 2019-08-28 | 2023-05-05 | 广州市南方医康生物科技有限公司 | Skin care composition, cosmetic and method for producing same |
| CN112156050A (en) * | 2020-11-13 | 2021-01-01 | 东晟源研究院(广州)有限公司 | Plant preservative composition suitable for cosmetics and preparation method thereof |
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