CN106491455B - Composition containing buddleia davidii extract and application thereof - Google Patents
Composition containing buddleia davidii extract and application thereof Download PDFInfo
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- CN106491455B CN106491455B CN201611168359.5A CN201611168359A CN106491455B CN 106491455 B CN106491455 B CN 106491455B CN 201611168359 A CN201611168359 A CN 201611168359A CN 106491455 B CN106491455 B CN 106491455B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention discloses a composition containing buddleja davidii extract and application thereof, aiming at providing a composition which has remarkable moistening and moisturizing performances, can stably lock the moisture content of skin, strengthen the self-moisturizing function of cells, effectively improve the moisture content of stratum corneum cells, effectively improve the barrier function of skin, prevent moisture loss and reduce skin irritation, and the composition is mainly prepared from the following components in parts by weight: 20-70 parts of buddleia davidii extract; 10-30 parts of algae composite extract; the algae composite extract is prepared from the following raw materials in parts by weight: 12-30 parts of undaria pinnatifida; 10-20 parts of Ascophyllum nodosum; 30-40 parts of Fucus vesiculosus; 30-40 parts of Arthodium hirsutum; 10-16 parts of Kappaphycus alvarezii; belongs to the field of cosmetics.
Description
Technical Field
The invention relates to a composition, in particular to a composition containing buddleia davidii extract, and also relates to application of the composition as a skin care product additive, belonging to the field of cosmetics.
Background
In recent years, natural and efficient skin care products are more and more accepted by consumers, wherein the effectiveness of marine biological components on human skin is accepted by the world authorities, and a plurality of scientific research results are widely applied to the field of cosmetics. Compared with traditional plant or artificial biochemical cosmetic components, the marine biological components are natural and efficient, and are more suitable for skin absorption.
Currently, the most widely used non-algal genus is the genus morus in marine biological compositions. Algae have evolved advanced defense mechanisms in the face of ocean extreme environments (e.g., high salt, high pressure, sunlight, etc.). And different algae extracts can bring different skin beautifying effects such as moisturizing, skin tendering, whitening, purifying, sun protection, ageing resistance and the like to the skin.
The skin-beautifying efficacy of the algae extract is undoubted, but the proper algae is selected, the proper active ingredients are separated from the algae, the algae is prepared into the efficient and safe composition, and the composition is finally added into the skin care product to obtain the corresponding skin-beautifying efficacy, so that the algae extract is a hotspot in industrial development and a difficulty to be solved in the industrial development.
Disclosure of Invention
In view of the above problems, a first object of the present invention is to provide a composition containing buddleja davidii extract, which has significant moisturizing and moisturizing properties, can stably lock the moisture content of skin, enhance the self-moisturizing function of cells, effectively increase the moisture content of stratum corneum cells, effectively improve the barrier function of skin, prevent moisture loss, and reduce skin irritation. The second purpose of the invention is to provide the application of the composition containing the buddleia davidii extract as a skin care product additive.
In order to solve the first technical problem, the first technical solution provided by the present invention is as follows:
a composition containing buddleia davidii extract is mainly prepared from the following components in parts by weight: 20-70 parts of buddleia davidii extract; 10-30 parts of algae composite extract;
the algae composite extract is prepared from the following raw materials in parts by weight: 12-30 parts of undaria pinnatifida; 10-20 parts of Ascophyllum nodosum; 30-40 parts of Fucus vesiculosus; 30-40 parts of Arthodium hirsutum; 10-16 parts of Kappaphycus alvarezii.
Further, the composition containing the buddleia davidii extract comprises the following raw materials in parts by weight: 10-20 parts of gulfweed; 15-40 parts of ulva lactuca.
Further, the composition containing the buddleia davidii extract also comprises the following components in parts by weight: 5-50 parts of a grass cotton extract; 20-30 parts of laminaria cuneata extract.
Further, the composition containing the buddleia davidii extract is prepared from the following components in parts by weight: 30-60 parts of buddleia davidii extract; 10-40 parts of a grass cotton extract; 20-30 parts of laminaria cuneata extract; 20-30 parts of algae composite extract;
the algae composite extract is prepared from the following raw materials in parts by weight: 15-20 parts of undaria pinnatifida; 10-20 parts of Ascophyllum nodosum; 30-40 parts of Fucus vesiculosus; 30-40 parts of Arthodium hirsutum; 10-15 parts of Kappaphycus alvarezii; 10-20 parts of gulfweed; 30-40 parts of ulva lactuca.
Further, the composition containing the buddleia extract is prepared by the following steps:
1) cleaning the algae raw material with the formula dosage by using clear water, airing, crushing, uniformly mixing with distilled water according to the solid-to-liquid ratio of 1g/30ml-5g/30ml, transferring to an ultrahigh pressure extraction tank, pressurizing to 300MPa at normal temperature, maintaining the pressure for 5-10min, releasing the pressure within 2-3s after reaching the pressure maintaining time, and taking out the extracting solution;
2) centrifuging the extracting solution obtained in the step 1) at the rotating speed of 5000-;
3) uniformly mixing the buddleia davidii extract and the algae composite extract according to the formula dosage, and spray-drying to obtain the buddleia davidii algae composite extract.
Preferably, the step 3) further comprises mixing 5-50 parts of the extract of gossypium herbaceum and 20-30 parts of the extract of laminaria cuneata with the formulated amount of the extract of buddleia davidii and the algae complex extract.
Preferably, the air inlet temperature of the spray drying in the step 3) is 180-.
The second technical scheme provided by the invention is the application of the composition containing the buddleia davidii extract as a skin care product additive.
Compared with the prior art, the technical scheme provided by the invention has the following beneficial effects:
1. the algae composite extract provided by the invention can help to moisten skin and bring a lasting moisturizing effect to the skin by the synergistic effect of the extracts of the undaria pinnatifida, the ascophyllum nodosum, the fucus vesiculosus, the pinus tomentosus and the kappaphycus alvarezii.
On the basis, the skin moisturizing cream is compounded with the gulfweed and the ulva, so that the moisture content of the skin can be further stably locked, the moisture loss is prevented, and the self-moisturizing function of cells is enhanced.
2. The buddleja davidii extract, the gossypium herbaceum extract and the laminaria cuneata extract provided by the invention cooperate with one another, so that the water content of stratum corneum cells is effectively improved, the barrier function of skin is improved, and the skin irritation is reduced.
Detailed Description
The following claims are hereby incorporated into the detailed description of the present invention, with the understanding that the present disclosure is not to be considered as limiting, and that modifications made by anyone within the scope of the present invention may be made without departing from the scope of the present invention.
It should be noted that the raw materials used in the technical scheme provided by the present invention, except for the specific description, are prepared by conventional means or purchased through commercial channels.
Buddleja davidii extract was purchased from Impermann (China) Co., Ltd; the grass cotton extract is purchased from Guangzhou Rongdao chemical company Limited; laminaria angustata extract was purchased from Baihabo Co., Guangzhou, Inc.
Example 1
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 20g of buddleia davidii extract; 30g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 12g of undaria pinnatifida; 20g of Ascophyllum nodosum; 30g of Fucus vesiculosus; 40g of Arthodium hirsutum; kappaphycus alvarezii 10 g.
Example 2
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 70g of buddleia davidii extract; 10g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 30g of undaria pinnatifida; 10g of Ascophyllum nodosum; 40g of Fucus vesiculosus; 30g of Arthodium hirsutum; kappaphycus alvarezii 16 g.
Example 3
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 50g of buddleia davidii extract; 20g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 20g of undaria pinnatifida; 15g of Ascophyllum nodosum; 35g of Fucus vesiculosus; 35g of Arthodium hirsutum; kappaphycus alvarezii 13 g.
Example 4
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 30g of buddleia davidii extract; 25g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 15g of undaria pinnatifida; 18g of Ascophyllum nodosum; 36g of Fucus vesiculosus; 32g of Arthodium hirsutum; 15g of Kappaphycus alvarezii; 10g of gulfweed; 40g of ulva lactuca.
Example 5
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 25g of buddleia davidii extract; 25g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 13g of undaria pinnatifida; 16g of Ascophyllum nodosum; fucus vesiculosus 32 g; 36g of Arthodium hirsutum; kappaphycus alvarezii 11 g; 20g of gulfweed; ulva 15 g.
Example 6
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 35g of buddleia davidii extract; 15g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 25g of undaria pinnatifida; 12g of Ascophyllum nodosum; 30g of Fucus vesiculosus; 40g of Arthodium hirsutum; 15g of Kappaphycus alvarezii; 15g of gulfweed; ulva 25 g.
Example 7
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 40g of buddleia davidii extract; 30g of a grass cotton extract; 30g of kelp wedge extract; 18g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 14g of undaria pinnatifida; 13g of Ascophyllum nodosum; 39g of Fucus vesiculosus; 33g of Arthodium hirsutum; kappaphycus alvarezii 12 g.
Example 8
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 60g of buddleia davidii extract; 5g of a grass cotton extract; 20g of kelp wedge extract; 14g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 23g of undaria pinnatifida; 19g of Ascophyllum nodosum; 34g of Fucus vesiculosus; 31g of Arthodium hirsutum; kappaphycus alvarezii 10 g.
Example 9
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 55g of buddleia davidii extract; 50g of a grass cotton extract; 25g of kelp wedge extract; 22g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 28g of undaria pinnatifida; 14g of Ascophyllum nodosum; 38g of Fucus vesiculosus; 34g of Arthodium hirsutum; kappaphycus alvarezii 16 g.
Example 10
The invention provides a composition containing buddleia davidii extract, which is prepared from the following components in parts by mass: 45g of buddleia davidii extract; 40g of a grass cotton extract; 25g of kelp wedge extract; 16g of algae compound extract; the algae composite extract is prepared from the following raw materials in mass number: 14g of undaria pinnatifida; 11g of Ascophyllum nodosum; 31g of Fucus vesiculosus; 33g of Arthodium hirsutum; kappaphycus alvarezii 14 g; 15g of gulfweed; ulva 35 g.
A method for preparing a composition containing buddleia extract as provided in any one of examples 1 to 10, by sequentially performing the steps of:
1) cleaning the algae raw material with the formula dosage by using clear water, airing, crushing, uniformly mixing with distilled water according to the solid-to-liquid ratio of 1g/30ml-5g/30ml (preferably 3g/30ml), transferring to an ultrahigh pressure extraction tank, pressurizing to 300MPa (preferably 300MPa) at normal temperature, maintaining the pressure for 5-10min (preferably 10min), releasing the pressure within 2-3s after reaching the pressure maintaining time, and taking out the extracting solution;
2) centrifuging the extracting solution obtained in the step 1) at the rotation speed of 5000-;
3) and uniformly mixing the extract with the formula dosage and the algae composite extract, and spray-drying to obtain the algae composite extract. Wherein the inlet air temperature of the spray drying is 180-200 ℃ (preferably 200 ℃), the atomization pressure is 0.1-0.2Mpa (preferably 0.15Mpa), and the feeding speed is 600-800ml/h (preferably 700 ml/h).
To better illustrate the beneficial effects of the present invention, the following is a verification test of a composition containing buddleia extract provided by the present invention:
first, irritation test
To verify the irritation of the present invention, the test samples prepared in examples 1-10 of the present invention were sent to a third party for testing skin irritation, and 6 chick embryos were used for continuous skin irritation test for each test sample, and the bleeding, clotting and vessel thawing time of the chick embryos in the test group was higher than 300 minutes.
The results show that the calculated irritation scores for the test samples prepared in the above examples are all zero points, indicating that the test samples prepared in examples 1-10 of the present invention are non-irritating products.
Second, efficacy test
Comparative example for efficacy test
Comparative example 1
Only contains essence base.
Comparative example 2
A commercially available moisturizing essence was purchased.
Comparative example 3
The same as in example 10 was repeated except that the buddleia davidii extract was not contained.
Comparative example 4
The same as example 10 was repeated except that the algae-derived complex extract was not contained.
Comparative example 5
The algae complex extract raw material contained no Ascophyllum nodosum and Codium hirsutum, and the rest was the same as example 10.
(II) preparation of test sample
First, the compositions of examples 2, 4, 8, and 10 and comparative examples 3 to 5 were added to essence bases, respectively, to prepare essences.
Wherein: the mass ratio of the composition to the essence base is 4: 96.
The essence base is an essence base conventionally used by the essence in the field, and the components and the content thereof are shown in the table 1 according to the total mass of 100 g:
TABLE 1
The preparation method of the essence base comprises the following steps:
heating deionized water in phase A to 80-90 deg.C, adding the rest material in phase A, dispersing uniformly, homogenizing until no particles exist, cooling to 50-60 deg.C, adding phase B to adjust pH to 6-7, stirring, cooling to 45 deg.C, adding phase C, stirring uniformly, and cooling to 35 deg.C.
The preparation method of the essence comprises the following steps:
and adding the composition in any one of the groups 2, 4, 8 and 10 and comparative examples 3-5 and the phase C into the mixture prepared from the phase A and the phase B, uniformly stirring, and cooling to 35 ℃ to obtain the essence.
(III) test of moisture Retention Performance
1. The test population: 90 subjects with dry skin, age 20-60 years, were randomized sex and divided into 9 groups of 10 persons each.
2. The test method comprises the following steps:
1) the technician uses the skin moisture content test Corneometer CM825 to measure the test site of the subject, and the average is taken and recorded as a blank value.
2) Subjects measured 5 times using a Corneometer CM825, a skin moisture content test by a technician after 0.5h, 1h, 2h, 4h, 6h of continuous use of the test samples, averaged, and the values recorded, the results are shown in table 2; the hydration rate was calculated by the following formula, and the results are shown in Table 3.
Hydration { (test value-blank value)/blank value } × 100%
3) After the test samples were continuously used for one month by the subjects, the water dispersion loss of skin on the back of the hand [ TEWL, g/(h · m2) ] was measured using the epidermal water loss meter TM300, and the TEWL value reflected the effect of improving the skin barrier function, and the lower the TEWL value, the less the water loss, indicating the better the skin barrier function. The results are shown in Table 4.
Table 2 moisture content test results
Table 3 hydration test results
| Test sample | 0h | 0.5h | 1h | 2h | 4h | 6h |
| EXAMPLE 2 essence | 0 | 79.20 | 64.67 | 53.05 | 46.06 | 41.25 |
| EXAMPLE 4 essence | 0 | 81.60 | 65.67 | 54.26 | 48.12 | 44.39 |
| EXAMPLE 8 essence | 0 | 83.94 | 66.86 | 57.97 | 50.27 | 46.34 |
| EXAMPLE 10 essence | 0 | 87.18 | 69.40 | 60.26 | 52.59 | 48.43 |
| Comparative example 1 essence base | 0 | 30.08 | 24.54 | 20.77 | 13.27 | 6.12 |
| Comparative example 2 commercially available moisturizing essence | 0 | 46.25 | 37.49 | 30.88 | 23.38 | 15.32 |
| Comparative example 3 essence | 0 | 69.88 | 53.56 | 42.85 | 38.66 | 35.27 |
| Comparative example 4 essence | 0 | 47.36 | 38.02 | 31.24 | 24.37 | 16.78 |
| Comparative example 5 essence | 0 | 70.31 | 55.42 | 44.46 | 40.15 | 35.81 |
TABLE 4 skin Water Dispersion loss TEWL values
The above results show that the essence prepared by the compositions of examples 2, 4, 8 and 10 of the invention has good moisturizing performance, and can significantly improve the skin barrier function and reduce the water dispersion loss of the skin.
In particular, after the essence prepared by the composition of example 10 is added, the moisture content of the essence is obviously higher than that of the essences prepared by the compositions of examples 2, 4 and 8 and comparative examples 3 to 5, the essence base of comparative example 1 and the commercially available moisturizing essence of comparative example 2, and the TEWL value of the essence is obviously lower than that of the essences prepared by the compositions of examples 2, 4 and 8 and comparative examples 3 to 5, the essence base of comparative example 1 and the commercially available moisturizing essence of comparative example 2.
Therefore, on the basis of the synergistic effect of seven kinds of algae, namely undaria pinnatifida, Ascophyllum nodosum, Fucus vesiculosus, Ardisia tomentosa, Kappaphycus alvarezii, gulfweed and Ulva lactuca, the three kinds of extracts, namely the buddleia davidii extract, the gossypium herbaceum extract and the Laminaria angustata keystone extract, are compounded, so that the moisturizing performance and the skin barrier function improving performance are obviously synergistic, the moisturizing performance is best, the skin barrier function can be effectively improved, and the moisture loss is reduced.
And the moisture content of comparative example 3 is relatively lower than that of the essence prepared by the composition of example 10, which shows that the zostera marina and pinus tomentosa in the raw materials of the zostera marina extract, the algae compound extract and the algae compound extract are synergistic with other components, and play an important role in the moisturizing performance and the skin barrier function of the composition of the invention.
And after the test sample prepared by the invention is insisted on being used by the test subject for 3 months, no allergic symptoms such as face pain and itch, red swelling, edema, inflammation and the like appear.
(IV) sensory evaluation test
In order to evaluate the use effect of the composition of the present invention, the essences prepared from the compositions of examples 1, 5, 7 and 10 were used as test samples, and the control sample was the commercial moisturizing essence of comparative example 2. Randomly selecting 150 subjects of 20-50 years old, dividing the subjects into 5 groups of 30 persons, insisting on using the test samples every day, carrying out sensory evaluation on the test samples after 1 month, wherein the number represents the number of persons who approve the test samples according to the number of the persons, and the results are shown in Table 4.
TABLE 4 sensory evaluation test results
| Test sample | Mildness property | Long-acting moisture retention | Moistening property |
| EXAMPLE 1 essence | 30 persons | 22 persons | 23 persons |
| EXAMPLE 5 essence | 30 persons | 24 persons | 25 persons |
| EXAMPLE 7 essence | 30 persons | 25 persons | 26 persons |
| EXAMPLE 10 essence | 30 persons | 29 persons | 29 persons |
| Comparative example 2 commercially available moisturizing essence | 25 persons | 10 persons | 15 persons |
The result shows that the essence of the embodiment of the invention has better mildness, long-acting moisture retention and moistening property, and the overall use feeling is better than that of the commercially available moisture retention essence.
In conclusion, the buddleja davidii extract, the gossypium herbaceum extract, the laminaria cuneata extract and the algae composite extract are scientifically combined to achieve synergistic effect, the moisturizing and moisturizing performance is remarkable, the moisture content of skin can be stably locked, the self-moisturizing function of cells is enhanced, the moisture content of cells in stratum corneum is effectively improved, the barrier function of skin is effectively improved, the moisture loss is prevented, and the skin irritation is reduced.
Claims (5)
1. A composition containing buddleia davidii extract is characterized by being mainly prepared from the following components in parts by weight: 20-70 parts of buddleia davidii extract; 5-50 parts of a grass cotton extract; 20-30 parts of laminaria cuneata extract; 10-30 parts of algae composite extract;
the algae composite extract is prepared from the following raw materials in parts by weight: 12-30 parts of undaria pinnatifida; 10-20 parts of Ascophyllum nodosum; 30-40 parts of Fucus vesiculosus; 30-40 parts of Arthodium hirsutum; 10-16 parts of Kappaphycus alvarezii;
the preparation method of the composition comprises the following steps:
1) cleaning the algae raw material with the formula dosage by using clear water, airing, crushing, uniformly mixing with distilled water according to the solid-to-liquid ratio of 1g/30ml-5g/30ml, transferring to an ultrahigh pressure extraction tank, pressurizing to 300MPa at normal temperature, maintaining the pressure for 5-10min, releasing the pressure within 2-3s after reaching the pressure maintaining time, and taking out the extracting solution;
2) centrifuging the extracting solution obtained in the step 1) at the rotating speed of 5000-;
3) mixing 5-50 parts of grass cotton extract and 20-30 parts of laminaria cuneata extract with the formula amount of buddleia davidii extract and algae composite extract uniformly, and spray drying to obtain the final product.
2. The composition containing buddleia davidii extract as claimed in claim 1, wherein the composition is prepared from the following components in parts by weight: 30-60 parts of buddleia davidii extract; 10-40 parts of a grass cotton extract; 20-30 parts of laminaria cuneata extract; 20-30 parts of algae composite extract.
3. A composition containing buddleia davidii extract is characterized by being mainly prepared from the following components in parts by weight: 20-70 parts of buddleia davidii extract; 5-50 parts of a grass cotton extract; 20-30 parts of laminaria cuneata extract; 10-30 parts of algae composite extract;
the algae composite extract is prepared from the following raw materials in parts by weight: 15-20 parts of undaria pinnatifida; 10-20 parts of Ascophyllum nodosum; 30-40 parts of Fucus vesiculosus; 30-40 parts of Arthodium hirsutum; 10-15 parts of Kappaphycus alvarezii; 10-20 parts of gulfweed; 30-40 parts of ulva lactuca.
4. The composition as claimed in claim 1, wherein the inlet temperature of the spray drying in step 3) is 180-.
5. Use of a composition comprising an extract of buddleia in claim 1 as an additive in the preparation of a skin care product.
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| CN109498521A (en) * | 2018-12-23 | 2019-03-22 | 广州素颜皮肤管理科技有限公司 | It is a kind of to have effects that the plant extracts of antiallergy and its application |
| CN112057359B (en) * | 2020-10-22 | 2021-07-27 | 北京唯爱生物科技有限公司 | Deep-sea pinus hirsuta moisturizing composition and preparation method and application thereof |
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| CN101896159A (en) * | 2007-11-14 | 2010-11-24 | 科蒂德国股份有限公司 | Cosmetic product for protecting the skin from environmental influences |
| CN104906015A (en) * | 2015-05-13 | 2015-09-16 | 登封市科创商务咨询有限公司 | Cubilose whitening and beautifying mask |
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| CN101896159A (en) * | 2007-11-14 | 2010-11-24 | 科蒂德国股份有限公司 | Cosmetic product for protecting the skin from environmental influences |
| CN104906015A (en) * | 2015-05-13 | 2015-09-16 | 登封市科创商务咨询有限公司 | Cubilose whitening and beautifying mask |
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