CN1116923C - 低密度凝胶组合物的生产方法 - Google Patents
低密度凝胶组合物的生产方法 Download PDFInfo
- Publication number
- CN1116923C CN1116923C CN98806028A CN98806028A CN1116923C CN 1116923 C CN1116923 C CN 1116923C CN 98806028 A CN98806028 A CN 98806028A CN 98806028 A CN98806028 A CN 98806028A CN 1116923 C CN1116923 C CN 1116923C
- Authority
- CN
- China
- Prior art keywords
- gel
- equal
- gel composition
- esterification
- catalyst
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/0052—Preparation of gels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/0091—Preparation of aerogels, e.g. xerogels
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
- Colloid Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Silicon Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/826,982 US6172120B1 (en) | 1997-04-09 | 1997-04-09 | Process for producing low density gel compositions |
| US08/826,982 | 1997-04-09 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1259885A CN1259885A (zh) | 2000-07-12 |
| CN1116923C true CN1116923C (zh) | 2003-08-06 |
Family
ID=25248012
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN98806028A Expired - Fee Related CN1116923C (zh) | 1997-04-09 | 1998-04-09 | 低密度凝胶组合物的生产方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6172120B1 (enExample) |
| EP (1) | EP0973604A1 (enExample) |
| JP (1) | JP2001518835A (enExample) |
| KR (1) | KR20010006212A (enExample) |
| CN (1) | CN1116923C (enExample) |
| AU (1) | AU7112798A (enExample) |
| BR (1) | BR9814240A (enExample) |
| CA (1) | CA2286147A1 (enExample) |
| WO (1) | WO1998045035A1 (enExample) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8042771B2 (en) | 2007-05-25 | 2011-10-25 | Karl F. Milde, Jr. | Method and apparatus for treating fuel to temporarily reduce its combustibility |
| US7222821B2 (en) * | 2001-11-21 | 2007-05-29 | Matos Jeffrey A | Method and apparatus for treating fuel to temporarily reduce its combustibility |
| US20030203980A1 (en) * | 2002-04-30 | 2003-10-30 | Valdes Reynaldo A. | Sol-gel composition, methods for manufacturing sol-gels, and applications for sol-gels |
| US7118801B2 (en) | 2003-11-10 | 2006-10-10 | Gore Enterprise Holdings, Inc. | Aerogel/PTFE composite insulating material |
| US20050270746A1 (en) * | 2004-06-04 | 2005-12-08 | Reis Bradley E | Insulating structure having combined insulating and heat spreading capabilities |
| US7618608B1 (en) | 2005-12-13 | 2009-11-17 | Keller Companies, Inc. | Aerogel and method of manufacturing same |
| US7750056B1 (en) | 2006-10-03 | 2010-07-06 | Sami Daoud | Low-density, high r-value translucent nanocrystallites |
| US7794805B2 (en) * | 2007-06-29 | 2010-09-14 | Schlumberger Technology Corporation | Thermal insulation barriers |
| US8293178B2 (en) | 2007-11-06 | 2012-10-23 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | Chemochromic detector for sensing gas leakage and process for producing the same |
| DE102008046444A1 (de) | 2008-09-09 | 2010-03-11 | Evonik Röhm Gmbh | Fassadenplatte, System und Verfahren zur Energiegewinnung |
| WO2011020671A1 (de) | 2009-08-20 | 2011-02-24 | Evonik Röhm Gmbh | Dämmplatte aus kunststoff, system und verfahren zur wärmedämmung |
| CN102115088B (zh) * | 2010-01-04 | 2013-04-17 | 新疆大学 | 以醇胺为碱性催化剂制备二氧化硅气凝胶的方法 |
| MX337353B (es) * | 2010-06-24 | 2016-02-29 | Pq Corp | Soportes de catalizador, catalizadores y su manufactura y uso. |
| US8815603B2 (en) | 2011-07-11 | 2014-08-26 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | Incorporation of chemochromic pigment into a variety of articles as an indicator for the presence of hypergolic fuels |
| EP3083794A1 (en) | 2013-12-19 | 2016-10-26 | W. L. Gore & Associates, Inc. | Thermally insulative expanded polytetrafluoroethylene articles |
| CN110506073A (zh) | 2017-03-29 | 2019-11-26 | W.L.戈尔及同仁股份有限公司 | 热绝缘膨体聚四氟乙烯制品 |
| US10822807B2 (en) | 2019-02-18 | 2020-11-03 | Royal Building Products (Usa) Inc. | Assembly for improved insulation |
| CN112337032A (zh) * | 2020-10-30 | 2021-02-09 | 中北大学 | 一种超分子有机凝胶组合物及其在环己胺泄漏中的应用 |
| CA3219673A1 (en) | 2021-06-11 | 2022-12-15 | W. L. Gore & Associates, Inc. | High temperature insulative composites and articles thereof |
| WO2025071812A1 (en) | 2023-09-29 | 2025-04-03 | Dow Global Technologies Llc | Silicone - acrylic binder for liquid applied thermal insulation coating compositions to resist corrosion under insulation |
| WO2025071811A1 (en) | 2023-09-29 | 2025-04-03 | Dow Global Technologies Llc | Silicone – acrylic binder for thermal insulation coatings to provide resistance to corrosion under insulation |
Family Cites Families (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2269059A (en) | 1938-05-14 | 1942-01-06 | Corning Glass Works | Method of preparing finely comminuted oxides |
| US2765242A (en) * | 1952-02-29 | 1956-10-02 | Du Pont | Process of making reinforced silica gel and esterified silica gel |
| US2739075A (en) | 1952-03-06 | 1956-03-20 | Du Pont | Product and process |
| US2832794A (en) | 1952-11-05 | 1958-04-29 | Allied Chem & Dye Corp | Hydrolysis of organosilanes |
| US2901460A (en) | 1956-02-07 | 1959-08-25 | Gen Electric | Halosilane hydrolysis with tetrahydrofuran and water |
| FR1568817A (enExample) | 1967-11-30 | 1969-05-30 | ||
| US3652214A (en) | 1968-08-06 | 1972-03-28 | Nat Petro Chemicals Co Inc | Preparation of silica gels |
| DE2313073C2 (de) | 1973-03-16 | 1984-11-29 | Istvan Prof. Dr. 6600 Saarbruecken Halasz | Verfahren zur chemischen Modifizierung von Oberflächen anorganischer Festkörper und deren Verwendung |
| DE2414478C3 (de) | 1974-03-26 | 1978-07-13 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Aerogelartige strukturierte Kieselsäure und Verfahren zu ihrer Herstellung |
| DE3429671A1 (de) | 1984-08-11 | 1986-02-20 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von aerogelen |
| US4561872A (en) | 1984-10-22 | 1985-12-31 | Corning Glass Works | Method for making glass or ceramic article |
| FR2585973A1 (fr) | 1985-08-06 | 1987-02-13 | Centre Nat Rech Scient | Gel monolithique et poudre d'oxydes d'elements de transition, procede de fabrication du gel et procede de preparation de couches minces de ces oxydes |
| US4810415A (en) | 1985-09-24 | 1989-03-07 | Dresser Industries, Inc. | Process for manufacturing ultra pure silica and resulting encapsulated products |
| DE3616133A1 (de) | 1985-09-25 | 1987-11-19 | Merck Patent Gmbh | Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel |
| JPS6374911A (ja) | 1986-09-19 | 1988-04-05 | Shin Etsu Chem Co Ltd | 微細球状シリカの製造法 |
| ATE73423T1 (de) | 1988-11-22 | 1992-03-15 | Degussa | Verfahren zur herstellung von kieselsaeuren. |
| US5158758A (en) | 1989-04-24 | 1992-10-27 | International Minerals & Chemical Corp. | Production of silica having high specific surface area |
| US5017540A (en) | 1989-09-15 | 1991-05-21 | Sandoval Junior E | Silicon hydride surface intermediates for chemical separations apparatus |
| US4983369A (en) | 1989-11-22 | 1991-01-08 | Allied-Signal Inc. | Process for forming highly uniform silica spheres |
| IT1240673B (it) | 1990-04-24 | 1993-12-17 | Tenav | Microsfere di aerogels di ossidi inorganici a stretta distribuzione dei diametri dei pori e metodo per la loro preparazione |
| US5409683A (en) | 1990-08-23 | 1995-04-25 | Regents Of The University Of California | Method for producing metal oxide aerogels |
| DE69128073T2 (de) | 1990-08-23 | 1998-02-26 | Univ California As Represented | Verfahren zur herstellung von metalloxidaerogelen mit dichte weniger als 0,02 g/cm3 |
| US5106604A (en) | 1991-03-12 | 1992-04-21 | Pradyot Agaskar | Use of metal salts in the synthesis of oligomeric hydrogensilsesquioxanes via hydrolysis/condensation reactions |
| US5206189A (en) | 1991-10-25 | 1993-04-27 | Instituto Guido Donegani S.P.A. | Sol-gel method for the preparation of monolithic multicomponent oxide glasses |
| EP0585456B1 (en) * | 1992-02-18 | 1997-05-07 | Matsushita Electric Works Ltd | Process for producing hydrophobic aerogel |
| US5565142A (en) | 1992-04-01 | 1996-10-15 | Deshpande; Ravindra | Preparation of high porosity xerogels by chemical surface modification. |
| JP3314935B2 (ja) | 1992-05-20 | 2002-08-19 | イー・アイ・デユポン・ドウ・ヌムール・アンド・カンパニー | 無機ゲルを作るための方法 |
| US5395805A (en) | 1993-03-25 | 1995-03-07 | Regents Of The University Of California | Method for making monolithic metal oxide aerogels |
| US5420168A (en) | 1993-04-01 | 1995-05-30 | The Regents Of The University Of California | Method of low pressure and/or evaporative drying of aerogel |
| US5376449A (en) | 1993-07-09 | 1994-12-27 | Martin Marietta Energy Systems, Inc. | Silica powders for powder evacuated thermal insulating panel and method |
| WO1995017347A1 (en) | 1993-12-23 | 1995-06-29 | Ppg Industries, Inc. | Silica aerogel produced under subcritical conditions |
| US5470802A (en) * | 1994-05-20 | 1995-11-28 | Texas Instruments Incorporated | Method of making a semiconductor device using a low dielectric constant material |
| DE4422912A1 (de) * | 1994-06-30 | 1996-01-11 | Hoechst Ag | Xerogele, Verfahren zu ihrer Herstellung, sowie ihre Verwendung |
| US5473826A (en) | 1994-08-19 | 1995-12-12 | Yazaki Corporation | Process for drying sol-gel derived porous bodies at elevated subcritical temperatures and pressures |
| DE4437424A1 (de) | 1994-10-20 | 1996-04-25 | Hoechst Ag | Aerogelhaltige Zusammensetzung, Verfahren zu ihrer Herstellung sowie ihre Verwendung |
| US5807494A (en) | 1994-12-15 | 1998-09-15 | Boes; Ralph Ulrich | Gel compositions comprising silica and functionalized carbon products |
| US5876686A (en) | 1995-06-28 | 1999-03-02 | E. I. Du Pont De Nemours And Company | Process for making inorganic oxide gels in fluorocarbon solvents |
| AU1421597A (en) | 1995-12-20 | 1997-07-14 | E.I. Du Pont De Nemours And Company | Rapid process for making silica gel and silicate polymer and low density gels made thereby |
| US5928723A (en) * | 1997-04-09 | 1999-07-27 | Cabot Corporation | Progress for producing surface modified metal oxide compositions |
-
1997
- 1997-04-09 US US08/826,982 patent/US6172120B1/en not_active Expired - Lifetime
-
1998
- 1998-04-09 EP EP98918149A patent/EP0973604A1/en not_active Withdrawn
- 1998-04-09 KR KR1019997009292A patent/KR20010006212A/ko not_active Ceased
- 1998-04-09 CA CA002286147A patent/CA2286147A1/en not_active Abandoned
- 1998-04-09 WO PCT/US1998/007374 patent/WO1998045035A1/en not_active Ceased
- 1998-04-09 BR BR9814240-2A patent/BR9814240A/pt not_active IP Right Cessation
- 1998-04-09 JP JP54319398A patent/JP2001518835A/ja not_active Ceased
- 1998-04-09 AU AU71127/98A patent/AU7112798A/en not_active Abandoned
- 1998-04-09 CN CN98806028A patent/CN1116923C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| US6172120B1 (en) | 2001-01-09 |
| WO1998045035A1 (en) | 1998-10-15 |
| BR9814240A (pt) | 2002-02-05 |
| AU7112798A (en) | 1998-10-30 |
| CA2286147A1 (en) | 1998-10-15 |
| KR20010006212A (ko) | 2001-01-26 |
| EP0973604A1 (en) | 2000-01-26 |
| CN1259885A (zh) | 2000-07-12 |
| JP2001518835A (ja) | 2001-10-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20030806 Termination date: 20160409 |