CN1116266C - 酰化的环状,1,3－二羰基化合物的制备方法 - Google Patents

酰化的环状,1,3－二羰基化合物的制备方法 Download PDF

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Publication number
CN1116266C
CN1116266C CN98809707A CN98809707A CN1116266C CN 1116266 C CN1116266 C CN 1116266C CN 98809707 A CN98809707 A CN 98809707A CN 98809707 A CN98809707 A CN 98809707A CN 1116266 C CN1116266 C CN 1116266C
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CN
China
Prior art keywords
alkyl
haloalkyl
hydrogen
formula
group
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Expired - Fee Related
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CN98809707A
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English (en)
Chinese (zh)
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CN1272837A (zh
Inventor
S·M·布朗
T·W·本特莱
R·O·琼斯
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SINZETA Ltd
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Zeneca Ltd
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Publication of CN1116266C publication Critical patent/CN1116266C/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/12—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C315/00—Preparation of sulfones; Preparation of sulfoxides
    • C07C315/04—Preparation of sulfones; Preparation of sulfoxides by reactions not involving the formation of sulfone or sulfoxide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
    • C07C45/46—Friedel-Crafts reactions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/54—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of compounds containing doubly bound oxygen atoms, e.g. esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
    • C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
    • C07D233/56—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
    • C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
CN98809707A 1997-11-27 1998-11-17 酰化的环状,1,3－二羰基化合物的制备方法 Expired - Fee Related CN1116266C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GBGB9725135.9A GB9725135D0 (en) 1997-11-27 1997-11-27 Chemical process
GB9725135.9 1997-11-27

Publications (2)

Publication Number Publication Date
CN1272837A CN1272837A (zh) 2000-11-08
CN1116266C true CN1116266C (zh) 2003-07-30

Family

ID=10822758

Family Applications (1)

Application Number Title Priority Date Filing Date
CN98809707A Expired - Fee Related CN1116266C (zh) 1997-11-27 1998-11-17 酰化的环状,1,3－二羰基化合物的制备方法

Country Status (19)

Country Link
US (1) US6218579B1 (enExample)
EP (1) EP1034159B1 (enExample)
JP (1) JP4384353B2 (enExample)
KR (1) KR100558626B1 (enExample)
CN (1) CN1116266C (enExample)
AT (1) ATE231483T1 (enExample)
AU (1) AU1167199A (enExample)
BR (1) BR9815026B1 (enExample)
CA (1) CA2295892C (enExample)
DE (1) DE69810962T2 (enExample)
DK (1) DK1034159T3 (enExample)
ES (1) ES2187073T3 (enExample)
GB (1) GB9725135D0 (enExample)
HU (1) HUP0004664A3 (enExample)
IL (1) IL134635A (enExample)
IN (1) IN191500B (enExample)
PT (1) PT1034159E (enExample)
TW (1) TW528747B (enExample)
WO (1) WO1999028282A1 (enExample)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106565560A (zh) * 2016-11-11 2017-04-19 湖北广富林生物制剂有限公司 一种硝磺草酮的合成工艺
CN106565557A (zh) * 2016-11-11 2017-04-19 湖北广富林生物制剂有限公司 一种2‑硝基‑4‑甲磺酰基苯甲酰氯的合成工艺
CN106565558A (zh) * 2016-11-11 2017-04-19 湖北广富林生物制剂有限公司 一种2‑硝基‑4‑甲磺酰基苯甲酰氯的合成工艺
CN106565561A (zh) * 2016-11-11 2017-04-19 湖北广富林生物制剂有限公司 一种2‑硝基‑4‑甲磺酰基苯甲酰氯的合成工艺
CN106748919A (zh) * 2016-11-11 2017-05-31 湖北广富林生物制剂有限公司 一种硝磺草酮的合成工艺

Families Citing this family (20)

* Cited by examiner, † Cited by third party
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US6809206B2 (en) 1999-02-12 2004-10-26 E. I. Du Pont De Nemours And Company Method for acylating cyclic compounds
AU9409101A (en) * 2000-09-08 2002-03-22 Syngenta Participations Ag Mesotrione formulations
BR0207414A (pt) * 2001-03-26 2004-08-10 Syngenta Ltd Método para remover impurezas de ácido 2-nitro-4-metil-sulfonilbenzóico, ácido 2-nitro-4-metilsulfonilbenzóico purificado, processo para fabricação de mesotriona, e, mesotriona ames-negativo
AUPR484201A0 (en) * 2001-05-08 2001-05-31 Bioprospect Limited Pesticidal compositions
DE10209645A1 (de) * 2002-03-05 2003-09-18 Bayer Cropscience Ag Substituierte Arylketone
TWI348999B (en) * 2003-10-02 2011-09-21 Syngenta Participations Ag Process
GB0323090D0 (en) * 2003-10-02 2003-11-05 Syngenta Participations Ag Novel process
GB0406894D0 (en) * 2004-03-26 2004-04-28 Syngenta Participations Ag Process
GB0419075D0 (en) 2004-08-26 2004-09-29 Syngenta Participations Ag Process
EP1795674A1 (en) * 2004-12-08 2007-06-13 Matsushita Electric Industrial Co., Ltd. Door handle device, door member with the door handle device, and smart entry system with the door member
US7856033B2 (en) * 2006-11-14 2010-12-21 Lantiq Deutschland Gmbh Methods and systems for adaptive communication
CN100537530C (zh) * 2007-06-08 2009-09-09 浙江工业大学 一种磺草酮的合成方法
CN103965084A (zh) * 2014-05-14 2014-08-06 江苏常隆农化有限公司 硝草酮的生产方法
JP5944597B2 (ja) * 2014-06-16 2016-07-05 イハラケミカル工業株式会社 トリケトン化合物の製造方法
GB2530838B (en) 2015-06-08 2020-01-22 Rotam Agrochem Int Co Ltd Process for purifying mesotrione
US20170327454A1 (en) * 2016-05-13 2017-11-16 Sirrus, Inc. High purity 1,1-dicarbonyl substituted-1-alkenes and methods for their preparation
CN108440352B (zh) * 2018-03-30 2020-04-14 江苏丰山集团股份有限公司 一种硝磺草酮的制备方法
CN113845450B (zh) * 2020-06-28 2024-12-13 沈阳中化农药化工研发有限公司 一种硝磺草酮及其同系物的合成方法
CN113943235B (zh) * 2020-07-17 2022-06-14 沈阳中化农药化工研发有限公司 一种制备硝磺草酮除草剂的方法
CN115784949A (zh) * 2022-12-08 2023-03-14 江苏扬农化工股份有限公司 一种三酮类化合物的制备方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3025219A1 (de) * 1980-07-03 1982-01-28 Bayer Ag, 5090 Leverkusen Benzoyl-azole, verfahren zu ihrer herstellung sowie ihre verwendung als fungizide
US4780127A (en) * 1982-03-25 1988-10-25 Stauffer Chemical Company Certain 2-(substituted benzoyl)-1,3-cyclohexanediones and their use as herbicides
US4806146A (en) * 1984-12-20 1989-02-21 Stauffer Chemical Company Certain 2-(2-substituted benzoyl)-1,3-cyclohexanediones
US4695673A (en) * 1985-11-20 1987-09-22 Stauffer Chemical Company Process for the production of acylated 1,3-dicarbonyl compounds
JPS62185034A (ja) * 1986-02-12 1987-08-13 Nippon Soda Co Ltd 固定化触媒によるシクロヘキサンジオン誘導体の製造方法
DE3604871A1 (de) * 1986-02-15 1987-08-20 Basf Ag Cyclohexenonderivate, verfahren zu ihrer herstellung und ihre verwendung als mittel zur regulierung des pflanzenwachstums
US6096930A (en) * 1994-08-18 2000-08-01 Korea Research Institute Of Chemical Technology Herbicidal cyclohexane-1,3-dione derivatives and their preparation process
GB9501433D0 (en) * 1995-01-25 1995-03-15 Zeneca Ltd Chemical process
GB9501434D0 (en) * 1995-01-25 1995-03-15 Zeneca Ltd Chemical process

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106565560A (zh) * 2016-11-11 2017-04-19 湖北广富林生物制剂有限公司 一种硝磺草酮的合成工艺
CN106565557A (zh) * 2016-11-11 2017-04-19 湖北广富林生物制剂有限公司 一种2‑硝基‑4‑甲磺酰基苯甲酰氯的合成工艺
CN106565558A (zh) * 2016-11-11 2017-04-19 湖北广富林生物制剂有限公司 一种2‑硝基‑4‑甲磺酰基苯甲酰氯的合成工艺
CN106565561A (zh) * 2016-11-11 2017-04-19 湖北广富林生物制剂有限公司 一种2‑硝基‑4‑甲磺酰基苯甲酰氯的合成工艺
CN106748919A (zh) * 2016-11-11 2017-05-31 湖北广富林生物制剂有限公司 一种硝磺草酮的合成工艺

Also Published As

Publication number Publication date
JP4384353B2 (ja) 2009-12-16
DK1034159T3 (da) 2003-05-05
PT1034159E (pt) 2003-06-30
CA2295892A1 (en) 1999-06-10
AU1167199A (en) 1999-06-16
TW528747B (en) 2003-04-21
IL134635A0 (en) 2001-04-30
EP1034159B1 (en) 2003-01-22
HUP0004664A3 (en) 2002-02-28
US6218579B1 (en) 2001-04-17
KR100558626B1 (ko) 2006-03-13
DE69810962T2 (de) 2004-01-08
CN1272837A (zh) 2000-11-08
EP1034159A1 (en) 2000-09-13
CA2295892C (en) 2008-02-05
BR9815026A (pt) 2000-10-03
IL134635A (en) 2005-08-31
GB9725135D0 (en) 1998-01-28
KR20010032495A (ko) 2001-04-25
ES2187073T3 (es) 2003-05-16
JP2001524539A (ja) 2001-12-04
HUP0004664A2 (hu) 2001-05-28
IN191500B (enExample) 2003-12-06
DE69810962D1 (de) 2003-02-27
WO1999028282A1 (en) 1999-06-10
ATE231483T1 (de) 2003-02-15
BR9815026B1 (pt) 2009-12-01

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C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: SIGENTIS CO., LTD.

Free format text: FORMER NAME OR ADDRESS: ZENECA LTD

CP03 Change of name, title or address

Address after: surrey

Patentee after: Sinzeta Ltd.

Address before: London, England, England

Patentee before: Zeneca Limited

C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20030730

Termination date: 20131117