CN110897984B - Repair ice crystal and preparation method thereof - Google Patents
Repair ice crystal and preparation method thereof Download PDFInfo
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- CN110897984B CN110897984B CN201911237975.5A CN201911237975A CN110897984B CN 110897984 B CN110897984 B CN 110897984B CN 201911237975 A CN201911237975 A CN 201911237975A CN 110897984 B CN110897984 B CN 110897984B
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention belongs to the technical field of cosmetics, and provides a repair ice crystal which comprises the following components in parts by weight: 10-23 parts of cogongrass rhizome extract, 8-15 parts of eclipta alba extract, 7-13 parts of centella asiatica extract, 5-12 parts of oriental wormwood extract, 2-7 parts of tremella fuciformis extract, 1-3 parts of honey, 0.5-2 parts of carbomer, 0.5-2 parts of glycerol, 0.3-0.8 part of triethanolamine, 0.1-0.5 part of glycerol monostearate and 35-50 parts of cucumber water, wherein in the preparation method, 10 parts of cucumber water are added after the cogongrass rhizome extract, the yerbadetajo herba extract, the centella asiatica extract, the oriental wormwood extract and the tremella fuciformis extract are mixed, and the mixture is uniformly stirred to obtain a first mixed solution; adding triethanolamine into 5 parts of cucumber water, adding glycerol and carbomer, stirring uniformly to obtain a second mixed solution, adding the second mixed solution into the first mixed solution, adding monostearin, mixing, adding honey and the rest cucumber water, and mixing uniformly to obtain the repair ice crystal. Through the technical scheme, the problem that the repair effect of the after-sun repair product in the prior art is not good is solved.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and relates to a repaired ice crystal and a preparation method thereof.
Background
The skin of a human body is seriously killed by ultraviolet rays and air pollution, and the skin is red and swollen, generates heat, is allergic and the like due to long-term pollution of the ultraviolet rays and the environment, so special care is needed, the ice crystals are repaired, the red, itching, scalding and other symptoms caused by sunshine and the environment can be relieved, and the moisture required by the skin is supplemented; the comfort and the freshness of the skin are improved; stabilize and prolong the natural skin color after sun exposure; protecting skin against free radical damage.
In the prior art, the product for repairing after sun is poor in repairing effect on the skin after sun, and the conditions of skin dryness, desquamation, skin erythema and skin swelling after sun exposure are not well improved by consumers. Therefore, research on a repair product with good repair effect is urgently needed to meet the needs of consumers.
Disclosure of Invention
The invention provides a repair ice crystal and a preparation method thereof, which solve the problem of poor repair effect of a repair product after solarization in the prior art.
The technical scheme of the invention is realized as follows:
the ice crystal repairing agent comprises the following components in parts by weight:
10-23 parts of cogongrass rhizome extract, 8-15 parts of eclipta alba extract, 7-13 parts of centella asiatica extract, 5-12 parts of oriental wormwood extract, 2-7 parts of tremella fuciformis extract, 1-3 parts of honey, 0.5-2 parts of carbomer, 0.5-2 parts of glycerol, 0.3-0.8 part of triethanolamine, 0.1-0.5 part of glycerol monostearate and 35-50 parts of cucumber water.
As a further technical scheme, the paint comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 8 parts of oriental wormwood extract, 5 parts of tremella fuciformis extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
As a further technical scheme, the preparation method of the cogongrass rhizome extract comprises the following steps: adding the lalang grass rhizome dry powder into 10 times of water, steaming and decocting for 40min, filtering to obtain filtrate, concentrating the filtrate, and drying to obtain lalang grass rhizome extract.
As a further technical scheme, the preparation method of the eclipta alba extract comprises the following steps: soaking eclipta alba dry powder in 80% ethanol by mass, wherein the material-liquid ratio is 15: 1, ultrasonic extracting at 40 ℃ for 20min, filtering to obtain filtrate, concentrating the filtrate, and drying to obtain the eclipta alba extract.
As a further technical scheme, the preparation method of the centella asiatica extract comprises the following steps: adding the dry centella asiatica powder into water with the mass of 10 times of the dry centella asiatica powder, cooking for 40min, filtering to obtain filtrate, eluting the filtrate with 80% ethanol by mass, concentrating, and drying to obtain the centella asiatica extract.
As a further technical scheme, the preparation method of the oriental wormwood extract comprises the following steps: adding herba Artemisiae Scopariae dry powder into 10 times of water, decocting for 80min, filtering to obtain filtrate, purifying with XDA-7 type macroporous adsorbent resin, eluting with 80% ethanol, concentrating, and drying to obtain herba Artemisiae Scopariae extract.
As a further technical scheme, the preparation method of the tremella extract comprises the following steps: adding the dried tremella powder into water with the mass of 10 times of that of the tremella powder, cooking for 5 hours, carrying out ultrasonic treatment on the cooking liquor for 20 minutes, filtering to obtain filtrate, eluting the filtrate with 80% ethanol by mass, concentrating and drying to obtain the tremella extract.
As a further technical scheme, the preparation method of the cucumber water comprises the following steps: peeling fructus Cucumidis Sativi, slicing, mashing, adding into 20 times of water, steaming for 30min, filtering the decoction, adding the residue into 20 times of water, steaming for 30min, filtering, mixing the filtrates, and ultraviolet sterilizing to obtain fructus Cucumidis Sativi water.
The invention also provides a preparation method for repairing the ice crystal, which comprises the following steps:
s1, weighing each component for later use according to the formula for repairing the ice crystals;
s2, mixing the lalang grass rhizome extract, the eclipta alba extract, the centella asiatica extract, the oriental wormwood extract and the tremella fuciformis extract, adding 10 parts of cucumber water, and uniformly stirring to obtain a first mixed solution;
s3, adding triethanolamine into 5 parts of cucumber water, adding glycerol and carbomer, and uniformly stirring to obtain a second mixed solution;
s4, adding the second mixed solution obtained in the step S3 into the first mixed solution obtained in the step S2, stirring while adding, adding monostearin, uniformly mixing, adding honey and the residual cucumber water, and stirring for 20min at the speed of 600-800 r/min to obtain the repair ice crystal.
The working principle and the beneficial effects of the invention are as follows:
1. according to the invention, the prepared repairing ice crystals have a good repairing effect on the skin after being dried, and after the repairing ice crystals act on the skin after being dried, the ice crystals are cool and moisturized, the drying and desquamation condition of the skin after being dried can be effectively improved, the comfort and freshness of the skin can be improved, the ice crystals can clear away heat and toxic materials, inhibit bacteria and kill viruses, the swelling of the skin after being dried can be eliminated, meanwhile, the damage of ultraviolet radiation on the skin can be reduced, and the erythema condition of the skin can be improved. Therefore, the repair ice crystal is suitable for repairing and nursing the skin after being dried, can be used for replenishing water and moisturizing, can be used for improving the skin conditions such as dryness, desquamation, erythema and swelling of the skin caused by the sun, has good repairing effect, meets the use requirements of consumers, has good using effect, and solves the problem of poor repairing effect of the repair product after being dried in the sun in the prior art.
2. According to the invention, the components of the ice crystal repairing raw material are mutually compatible and have a synergistic effect, so that the effect of repairing the skin after solarization is achieved, and the components are one by one. The cogongrass rhizome extract and the tremella extract are matched, so that the effects of cooling, moisturizing, permeating into skin, improving the dryness degree of the skin, reducing the desquamation phenomenon of the skin and achieving a good repairing effect are achieved; the cogongrass rhizome extract, the eclipta alba extract and the asiatic centella extract have synergistic effect, clear away heat and toxic materials, and have antibacterial and anti-inflammatory effects, so that the skin swelling after solarization is eliminated; the yerbadetajo herba ecliptae extract and the tremella extract have synergistic effect, oxygen free radicals are removed, and damage of ultraviolet radiation to the skin is relieved, so that the skin is relieved, and erythema of the skin after sunburn is eliminated; the cucumber water contains rich vitamin E, and effectively promotes the metabolism of the skin, so that the repair of the skin after the sun is effectively improved; the prepared repairing ice crystals have good skin-friendly property, and are compatible with cucumber water, so that the infiltration and absorption of the cogongrass rhizome extract, the eclipta alba extract, the snow cover extract and the white fungus extract in the skin are promoted, the performance of the after-sun skin repairing efficacy of the cogongrass rhizome extract, the eclipta alba extract, the snow cover extract and the white fungus extract is promoted, and the honey also has the water locking and moisturizing efficacy, so that the elasticity and the water moisture of the after-sun skin are recovered, and the drying and desquamation condition of the after-sun skin is improved.
3. According to the invention, the honey, the tremella extract and the cucumber water are added into the repairing ice crystal raw material, and the honey, the tremella extract and the cucumber water are compatible with each other, so that the effects of well supplementing water and moisture are achieved, the moisture required by the skin is supplemented, the skin is tender and glossy, and the problem of dry skin and desquamation caused by drying in the sun is effectively solved.
4. In the preparation method, a step-by-step mixing preparation method is adopted, and the cogongrass rhizome extract, the eclipta alba extract, the centella asiatica extract, the oriental wormwood extract and the tremella extract are mixed and then added with 10 parts of cucumber water, and the mixture is uniformly stirred to obtain a first mixed solution; and adding triethanolamine into 5 parts of cucumber water, adding glycerol and carbomer, uniformly stirring to obtain a second mixed solution, adding the second mixed solution into the first mixed solution, adding monostearin, mixing, adding honey and the rest cucumber water, and uniformly mixing.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The ice crystal repairing agent comprises the following components in parts by weight:
10 parts of cogongrass rhizome extract, 8 parts of eclipta alba extract, 7 parts of centella asiatica extract, 5 parts of oriental wormwood extract, 2 parts of tremella fuciformis extract, 1 part of honey, 0.5 part of carbomer, 0.5 part of glycerol, 0.3 part of triethanolamine, 0.1 part of glycerol monostearate and 35 parts of cucumber water;
the preparation method comprises the following steps:
s1, firstly, preparing a cogongrass rhizome extract, an eclipta alba extract, a centella asiatica extract, an oriental wormwood extract, a tremella extract and cucumber water respectively according to the following methods: adding the lalang grass rhizome dry powder into 10 times of water, steaming and decocting for 40min, filtering to obtain filtrate, concentrating the filtrate, and drying to obtain lalang grass rhizome extract; soaking eclipta alba dry powder in 80% ethanol by mass, wherein the material-liquid ratio is 15: 1, performing ultrasonic extraction at 40 ℃ for 20min, filtering to obtain filtrate, concentrating the filtrate, and drying to obtain an eclipta alba extract; adding the dry centella asiatica powder into water with the mass of 10 times of the dry centella asiatica powder, steaming and boiling for 40min, filtering to obtain filtrate, eluting the filtrate with 80% ethanol by mass, concentrating, and drying to obtain a centella asiatica extract; adding herba Artemisiae Scopariae dry powder into 10 times of water, decocting for 80min, filtering to obtain filtrate, purifying the filtrate with XDA-7 type macroporous adsorbent resin, eluting with 80% ethanol, concentrating, and drying to obtain herba Artemisiae Scopariae extract; adding the dried tremella powder into water with the mass of 10 times of that of the tremella powder, cooking for 5 hours, carrying out ultrasonic treatment on the cooking liquor for 20 minutes, filtering to obtain filtrate, eluting the filtrate with 80% ethanol by mass, concentrating and drying to obtain a tremella extract; peeling fructus Cucumidis Sativi, slicing, mashing, adding into 20 times of water, steaming for 30min, filtering the decoction, adding the residue into 20 times of water, steaming for 30min, filtering, mixing the filtrates, and ultraviolet sterilizing to obtain fructus Cucumidis Sativi water; then, weighing each component for later use according to the formula for repairing the ice crystal;
s2, mixing the lalang grass rhizome extract, the eclipta alba extract, the centella asiatica extract, the oriental wormwood extract and the tremella fuciformis extract, adding 10 parts of cucumber water, and uniformly stirring to obtain a first mixed solution;
s3, adding triethanolamine into 5 parts of cucumber water, adding glycerol and carbomer, and uniformly stirring to obtain a second mixed solution;
s4, adding the second mixed solution obtained in the step S3 into the first mixed solution obtained in the step S2, stirring while adding, adding monostearin, uniformly mixing, adding honey and the residual cucumber water, and stirring for 20min at the speed of 600-800 r/min to obtain the repair ice crystal.
Example 2
The ice crystal repairing agent comprises the following components in parts by weight:
23 parts of cogongrass rhizome extract, 15 parts of eclipta alba extract, 13 parts of centella asiatica extract, 12 parts of oriental wormwood extract, 7 parts of tremella fuciformis extract, 3 parts of honey, 2 parts of carbomer, 2 parts of glycerol, 0.8 part of triethanolamine, 0.5 part of glycerol monostearate and 50 parts of cucumber water;
the preparation method is the same as that of example 1.
Example 3
The ice crystal repairing agent comprises the following components in parts by weight:
12 parts of cogongrass rhizome extract, 13 parts of eclipta alba extract, 13 parts of centella asiatica extract, 12 parts of oriental wormwood extract, 3 parts of tremella fuciformis extract, 3 parts of honey, 0.5 part of carbomer, 1 part of glycerol, 0.8 part of triethanolamine, 0.1 part of glycerol monostearate and 45 parts of cucumber water.
The preparation method is the same as that of example 1.
Example 4
The ice crystal repairing agent comprises the following components in parts by weight:
20 parts of cogongrass rhizome extract, 10 parts of eclipta alba extract, 8 parts of centella asiatica extract, 7 parts of oriental wormwood extract, 3 parts of tremella fuciformis extract, 3 parts of honey, 1.5 parts of carbomer, 1.5 parts of glycerol, 0.5 part of triethanolamine, 0.2 part of glycerol monostearate and 38 parts of cucumber water.
The preparation method is the same as that of example 1.
Example 5
The ice crystal repairing agent comprises the following components in parts by weight:
18 parts of cogongrass rhizome extract, 9 parts of eclipta alba extract, 9 parts of centella asiatica extract, 10 parts of oriental wormwood extract, 6 parts of tremella extract, 1 part of honey, 1 part of carbomer, 1.6 parts of glycerol, 0.3 part of triethanolamine, 0.4 part of glycerol monostearate and 46 parts of cucumber water.
The preparation method is the same as that of example 1.
Example 6
The ice crystal repairing agent comprises the following components in parts by weight:
15 parts of cogongrass rhizome extract, 12 parts of eclipta alba extract, 11 parts of centella asiatica extract, 9 parts of oriental wormwood extract, 4 parts of tremella fuciformis extract, 2 parts of honey, 0.8 part of carbomer, 1.2 parts of glycerol, 0.7 part of triethanolamine, 0.2 part of glycerol monostearate and 40 parts of cucumber water.
The preparation method is the same as that of example 1.
Example 7
The ice crystal repairing agent comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 8 parts of oriental wormwood extract, 5 parts of tremella fuciformis extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
The preparation method is the same as that of example 1.
Comparative example 1
The ice crystal repairing agent comprises the following components in parts by weight:
11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 8 parts of oriental wormwood extract, 5 parts of tremella fuciformis extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
The preparation method is the same as example 1 except that no lalang grass rhizome extract is added in steps S1 and S2.
Comparative example 2
The ice crystal repairing agent comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 10 parts of asiatic centella extract, 8 parts of oriental wormwood extract, 5 parts of tremella extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of monostearyl fatty acid glyceride and 42 parts of cucumber water.
The preparation method is the same as that of example 1 except that no yerbadetajo herba ecliptae extract is added in steps S1 and S2.
Comparative example 3
The ice crystal repairing agent comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 8 parts of oriental wormwood extract, 5 parts of tremella extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
The preparation method is the same as that of example 1 except that no snowflake extract is added in steps S1 and S2.
Comparative example 4
The ice crystal repairing agent comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 5 parts of tremella fuciformis extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
The preparation method is the same as example 1 except that the herba Artemisiae Scopariae extract is not added in steps S1 and S2.
Comparative example 5
The ice crystal repairing agent comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 8 parts of oriental wormwood extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
The preparation method is the same as that of example 1 except that no Tremella extract is added in steps S1 and S2.
Comparative example 6
The ice crystal repairing agent comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 8 parts of oriental wormwood extract, 5 parts of tremella fuciformis extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of distilled water.
The preparation method is the same as that of example 1 except that cucumber water is not added in steps S1, S2, S3 and S4 and is replaced by distilled water.
Comparative example 7
The ice crystal repairing agent comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 8 parts of oriental wormwood extract, 5 parts of tremella fuciformis extract, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
The preparation method is the same as example 1 except that honey is not added in step S4.
Comparative example 8
The ice crystal repairing agent comprises the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 8 parts of oriental wormwood extract, 5 parts of tremella fuciformis extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
The preparation method comprises the step of directly and uniformly mixing the components in the formula to obtain the repaired ice crystal.
The following efficacy tests were performed on the repaired ice crystals prepared in examples 1 to 7 and comparative examples 1 to 8:
1. post-sun skin repair efficacy testing: 170 white mice were selected and randomly divided into 17 groups of 10 mice each, namely a normal group, a model group, an example 1-example 7 group, and a comparative example 1-comparative example 8 group. The mice were depilated 24 hours before the experiment and had their backs depilated and had an area of about 3cm by 3 cm. The skin of the back of rats was molded with 2, 4-Dinitrochlorobenzene (DNCB) in each group except the normal group and irradiated with ultraviolet rays for 12 hours, after the molding was successful (the skin showed symptoms of dry desquamation, burning, stabbing pain, swelling, erythema, etc.). The normal and model groups were each coated with 0.5mL of deionized water on the back at the depilated area over a range of about 2.5cm by 2.5cm, and the remaining groups were each coated with 0.5mL of test samples from the different groups once a day for 9 consecutive days. On day 10, the skin condition of the right back of each group of rats was visually observed and recorded according to the test evaluation criteria of table 1, and the results are shown in table 2:
TABLE 1 test and evaluation criteria for skin repair efficacy after sun exposure
Table 2 test results of skin repair efficacy after ice crystal solarization repair of examples 1 to 7 and comparative examples 1 to 8
The data in the table 2 show that compared with the repair ice crystals of comparative examples 1 to 8, the repair ice crystals of examples 1 to 7 have a good repair effect on the skin after sun exposure, and after the repair ice crystals of examples 1 to 7 are continuously used for 9 days by a white rat, the conditions of the skin after sun exposure, such as dry desquamation, skin swelling, skin erythema and the like, are remarkably improved, so that the repair ice crystals prepared in examples 1 to 7 are suitable for repairing and nursing the skin after sun exposure, can improve the skin conditions of the skin, such as dry desquamation, erythema, swelling and the like, caused by sun exposure, and have a good repair and maintenance effect. The formula and the preparation method of the embodiment 7 are relatively excellent embodiments of the invention, and the prepared repair ice crystals have better repair effect on the skin after sunburn.
Compared with the repair ice crystal of the example 7, the swelling condition of the skin after sunburn of the white rat after the repair ice crystal of the comparative example 1 is obviously improved, but the skin has severe dryness and desquamation and moderate erythema; after sunburn with the repair ice crystals of comparative example 2, the skin appeared slightly dry, desquamating, moderate edema and severe erythema; after sunburn with the repair ice crystals of comparative example 3, the skin appeared to be slightly dry, desquamated, moderately edematous and slightly erythematous; after sunburn, the skin developed slight dryness, desquamation, slight edema and severe erythema after the repair of ice crystals using comparative example 4; after sunburn with the repair of ice crystals of comparative example 5, the skin appeared moderately dry, slightly desquamating, slightly edematous and slightly erythematous; after sunburn, the skin developed slight dryness, desquamation, slight edema and slight erythema after the repair of ice crystals using comparative example 6; after sunburn with the repair of ice crystals of comparative example 7, the skin appeared moderately dry, slightly desquamating, slightly edematous and slightly erythematous; after the ice crystal repairing materials of the invention are used, the sun-cured skin has slight dryness, desquamation, slight edema and slight erythema, because the cogongrass rhizome extract is not added in the formula of the ice crystal repairing material of the comparative example 1, the yerbadetajo herba extract is not added in the formula of the ice crystal repairing material of the comparative example 2, the centella asiatica extract is not added in the formula of the ice crystal repairing material of the comparative example 3, the oriental wormwood extract is not added in the formula of the ice crystal repairing material of the comparative example 4, the tremella fuciformis extract is not added in the formula of the ice crystal repairing material of the comparative example 5, the cucumber water is not added in the formula of the ice repairing material of the comparative example 6, the honey is not added in the formula of the ice repairing material of the comparative example 7, and the preparation method of the ice crystal repairing material of the comparative example 8 is direct mixing, which shows that the cogongrass rhizome extract and the tremella fuciformis extract are matched to cool, moisturize, permeate into the skin, improve the dryness degree of the skin and reduce the desquamation phenomenon of the skin, the repair effect is good; the cogongrass rhizome extract, the eclipta alba extract and the asiatic centella extract have synergistic effect, clear away heat and toxic materials, and have antibacterial and anti-inflammatory effects, so that the skin swelling after solarization is eliminated; the yerbadetajo herba ecliptae extract and the tremella extract have synergistic effect, oxygen free radicals are removed, and damage of ultraviolet radiation to the skin is relieved, so that the skin is relieved, and erythema of the skin after sunburn is eliminated; the cucumber water contains rich vitamin E, and effectively promotes the metabolism of the skin, so that the repair of the skin after the sun is effectively improved; the prepared repairing ice crystals have good skin-friendly property, and are compatible with cucumber water, so that the infiltration and absorption of the cogongrass rhizome extract, the eclipta alba extract, the snow cover extract and the white fungus extract in the skin are promoted, the performance of the after-sun skin repairing efficacy of the cogongrass rhizome extract, the eclipta alba extract, the snow cover extract and the white fungus extract is promoted, and the honey also has the water locking and moisturizing efficacy, so that the elasticity and the water moisture of the after-sun skin are recovered, and the drying and desquamation condition of the after-sun skin is improved. Therefore, the components in the formula are mutually compatible and have a synergistic effect to play a role in repairing the skin after the sun is cured, the components are not indispensable, and the preparation method of mixing the components step by step enables the effects of the components in the formula to be better played, so that the repairing effect of repairing ice crystals on the skin after the sun is cured is better.
2. Testing the moisturizing effect: the moisture content of the skin stratum corneum is measured according to a capacitance method specified in QB/T4256-2011 'guidelines for evaluating moisturizing effects of cosmetics'. During testing, 30 female volunteers are selected, the average age is 30 years old, the test subjects are in the positions of the test subjects, the inner sides of the forearms of the two hands of the test subjects are divided into a use area and a blank control area before use, the repair ice crystals prepared in the embodiments 1-7 and the comparative examples 1-8 are respectively used in the use area, the blank control group is not treated, the moisture content of the stratum corneum of the skin is respectively tested on the use area and the blank control area by using a skin moisture tester before use and after 4 hours of use, and the test results are shown in a table 3:
TABLE 3 moisture retention test results for repairing ice crystals of examples 1 to 7 and comparative examples 1 to 8
As can be seen from the data in Table 3, the repair ice crystals of examples 1 to 7 have very good moisturizing efficacy compared with the repair ice crystals of comparative examples 1 to 8. In comparative examples 1 to 8, the water replenishing and moisturizing effects of the repair ice crystals of comparative examples 5 to 7 are relatively poor, and the honey, the tremella extract and the cucumber water added in the invention are mutually compatible, so that the water replenishing and moisturizing effects are good, and the problem of dry and desquamation of skin caused by sun drying is effectively solved.
As the test results of the skin repair effect after sun exposure and the moisturizing effect show that the repair ice crystals of the embodiments 1 to 7 can repair the skin after sun exposure well, the following human body effect evaluations are carried out on the repair ice crystals of the embodiments 1 to 7:
selecting 70 foreign tourists as volunteers in a white cloud mountain scenic spot in Guangzhou city, wherein the female visitors are 22-35 years old and randomly divided into 7 groups, 10 persons in each group, and 1-7 groups of volunteers respectively use the repair ice crystals of the embodiments 1-7 of the invention at the evening after sun exposure, if 1 group of volunteers use the repair ice crystals of the embodiment 1 and 2 groups of volunteers use the repair ice crystals … … of the embodiment 2, after the continuous use for 7 days, the user scores the skin repair function of the used repair ice crystals after sun exposure according to the skin condition, the scoring interval is 0-10, the better the function is, the higher the score is, otherwise, the score is lower, and the comprehensive scoring condition is shown in the following table:
TABLE 4 evaluation results of ice crystal repair in human body of examples 1 to 7
As can be seen from the data in table 4, after 7 days, the skin repair function of the repair ice crystals used in embodiments 1 to 7 of the present invention after sun exposure is scored very high according to the skin conditions of the volunteers, and the scores of the skin dryness, desquamation, skin swelling, skin erythema, pigmentation and water replenishing and moisturizing effects of the repair ice crystals are all above 9 minutes, which indicates that the repair ice crystals in embodiments 1 to 7 of the present invention have a good repair effect on the skin after sun exposure, effectively improve the skin conditions after sun exposure, replenish water and moisturize, satisfy the use requirements of consumers, and have a good use effect.
The present invention is not limited to the above preferred embodiments, and any modifications, equivalent substitutions, improvements, etc. within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (3)
1. The repair ice crystal is characterized by comprising the following components in parts by weight:
10-23 parts of cogongrass rhizome extract, 8-15 parts of eclipta alba extract, 7-13 parts of centella asiatica extract, 5-12 parts of oriental wormwood extract, 2-7 parts of tremella fuciformis extract, 1-3 parts of honey, 0.5-2 parts of carbomer, 0.5-2 parts of glycerol, 0.3-0.8 part of triethanolamine, 0.1-0.5 part of glycerol monostearate and 35-50 parts of cucumber water;
the preparation method of the cogongrass rhizome extract comprises the following steps: adding the lalang grass rhizome dry powder into 10 times of water, steaming and decocting for 40min, filtering to obtain filtrate, concentrating the filtrate, and drying to obtain lalang grass rhizome extract;
the preparation method of the eclipta alba extract comprises the following steps: soaking eclipta alba dry powder in 80% ethanol by mass, wherein the material-liquid ratio is 15: 1, performing ultrasonic extraction at 40 ℃ for 20min, filtering to obtain filtrate, concentrating the filtrate, and drying to obtain an eclipta alba extract;
the preparation method of the centella asiatica extract comprises the following steps: adding the dry centella asiatica powder into water with the mass of 10 times of the dry centella asiatica powder, steaming and boiling for 40min, filtering to obtain filtrate, eluting the filtrate with 80% ethanol by mass, concentrating, and drying to obtain a centella asiatica extract;
the preparation method of the herba artemisiae capillaris extract comprises the following steps: adding herba Artemisiae Scopariae dry powder into 10 times of water, decocting for 80min, filtering to obtain filtrate, purifying the filtrate with XDA-7 type macroporous adsorbent resin, eluting with 80% ethanol, concentrating, and drying to obtain herba Artemisiae Scopariae extract;
the preparation method of the tremella extract comprises the following steps: adding the dried tremella powder into water with the mass of 10 times of that of the tremella powder, cooking for 5 hours, carrying out ultrasonic treatment on the cooking liquor for 20 minutes, filtering to obtain filtrate, eluting the filtrate with 80% ethanol by mass, concentrating and drying to obtain a tremella extract;
the preparation method of the cucumber water comprises the following steps: peeling fructus Cucumidis Sativi, slicing, mashing, adding into 20 times of water, steaming for 30min, filtering the decoction, adding the residue into 20 times of water, steaming for 30min, filtering, mixing the filtrates, and ultraviolet sterilizing to obtain fructus Cucumidis Sativi.
2. The repair ice crystal of claim 1, which is prepared from the following components in parts by weight:
16 parts of cogongrass rhizome extract, 11 parts of eclipta alba extract, 10 parts of centella asiatica extract, 8 parts of oriental wormwood extract, 5 parts of tremella fuciformis extract, 2 parts of honey, 1.3 parts of carbomer, 1.3 parts of glycerol, 0.5 part of triethanolamine, 0.3 part of glycerol monostearate and 42 parts of cucumber water.
3. A preparation method for repairing ice crystals is characterized by comprising the following steps:
s1, weighing the components according to the formula for repairing the ice crystal as claimed in any one of claims 1-2 for later use;
s2, mixing the cogongrass rhizome extract, the yerbadetajo herba ecliptae extract, the centella asiatica extract, the oriental wormwood extract and the tremella fuciformis extract, adding 10 parts of cucumber water, and uniformly stirring to obtain a first mixed solution;
s3, adding triethanolamine into 5 parts of cucumber water, adding glycerol and carbomer, and uniformly stirring to obtain a second mixed solution;
s4, adding the second mixed solution obtained in the step S3 into the first mixed solution obtained in the step S2, stirring while adding, adding the monostearyl fatty acid glyceride, uniformly mixing, adding the honey and the residual cucumber water, and stirring at the speed of 600-800 r/min for 20min to obtain the repair ice crystal.
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