CN110772435A - Anti-dandruff shampoo and preparation method thereof - Google Patents
Anti-dandruff shampoo and preparation method thereof Download PDFInfo
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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Abstract
The invention belongs to the field of daily chemicals. An anti-dandruff shampoo comprises the following components: phase A: ethylene diamine tetraacetic acid, fatty alcohol-polyoxyethylene ether sodium sulfate, ammonium lauryl sulfate, acrylic acid (ester)/C10-30 alcohol acrylate crosslinked polymer sodium, pyridone ethanolamine salt, pepper extract and alligator oil; phase B: 1, 3-dimethylmethyloldimethylhydantoin; and C phase: sodium lauroyl sarcosinate, selenium sulfide; and the balance water. The shampoo has good antibacterial, anti-inflammatory, dandruff-removing and itching-relieving effects, is capable of keeping moisture for a long time, nourishing scalp, growing hair and nourishing hair, is mild in formula and low in irritation, and can effectively relieve the problems of dandruff, itching, dry scalp, scalp inflammation and the like.
Description
Technical Field
The invention belongs to the field of daily chemicals, and relates to an anti-dandruff shampoo and a preparation method thereof.
Background
In daily life, under the influence of pressure and environmental pollution, more and more people are troubled by the problems of scurf, scalp itch, scalp inflammation and the like, most of the existing scurf removing products on the market adopt pyridine sulfate as the scurf removing agent, but the existing scurf removing agent has the defects that the pyridine sulfate is strong in irritation, insoluble in water and organic solvent, and is easy to appear poor in compatibility with other components, difficult to disperse, easy to precipitate and agglomerate when being applied to shampoo, so that the scurf removing effect is unstable. In the prior art, the plant extract is used as the anti-dandruff agent, and the anti-dandruff agent has the characteristics of mildness and no stimulation, but the plant extract has complex components, unclear effective components and beneficial effects, unobvious effects or even no claimed effect of a product, the effective components of the plant extract are easily influenced by an extraction process, and other components and shelf life in a system also easily influence the stability of the plant extract and the high activity of active substances, so that the anti-dandruff effect is unstable.
Disclosure of Invention
The anti-dandruff shampoo has good effects of inhibiting bacteria, resisting inflammation, removing dandruff and relieving itching, can keep moisture for a long time, nourish scalp, grow hair and nourish hair, has a mild formula and small irritation, and can effectively relieve the problems of dandruff, scalp dryness, scalp inflammation and the like.
The technical scheme of the invention is as follows:
an anti-dandruff shampoo comprises the following components in percentage by weight:
phase A: 0.01-0.1% of ethylenediamine tetraacetic acid, 10-20% of fatty alcohol-polyoxyethylene ether sodium sulfate, 0.01-5% of ammonium lauryl sulfate, 0.1-10% of acrylic acid (ester)/C10-30 alcohol acrylate cross-linked polymer sodium, 0.01-0.5% of pyridone ethanol amine salt, 0.1-1% of pepper extract and 0.1-1% of alligator oil;
phase B: 0.2 to 0.5 percent of 1, 3-dimethylol dimethyl hydantoin;
and C phase: 2-5% of sodium lauroyl sarcosinate and 1-2% of selenium sulfide;
and the balance water.
Further, the phase A also comprises 0.1-2.5% of first conditioning agent, 0.1-6% of surfactant and 0.1-0.5% of thickening agent.
Further, the first conditioning agent is at least one of the following components: polyquaternium-10, cetearyl alcohol, salicylic acid, allantoin and DL-panthenol.
Further, the surfactant is at least one of sodium lauroamphoacetate and coconut oil fatty acid monoethanolamide.
Further, the thickening agent is carbomer.
Furthermore, the phase B also comprises 0.1-4.5% of a second conditioner, 0.1-1% of a softener and 0.1-0.5% of essence.
Further, the second conditioning agent is at least one of the following components: arginine, menthol, emulsified silicone oil, guar hydroxypropyl trimethyl ammonium chloride, monoglyceride citrate and PEG-7 glyceryl cocoate.
Further, the softener is at least one of the following components: polydimethylsiloxane, C12-15 alkanol polyether-3, and triethanolamine dodecylbenzene sulfonate.
The preparation method of the anti-dandruff shampoo comprises the following steps:
a. mixing the components in the phase C, and stirring until the components are completely dissolved to obtain a phase C mixture;
b. heating water to 50-55 deg.C, adding the components of phase A, stirring and heating to 80-85 deg.C, stirring at 35-40r/min, dissolving completely, and keeping the temperature for 30-35 min;
c. cooling to 45-50 deg.C, adding the components of phase B, stirring at constant temperature for 30-35min at 20-25 r/min;
cooling to 38-40 ℃, adding the C phase mixture, stirring until the C phase mixture is completely dissolved, and vacuumizing for 10-15min to obtain the anti-dandruff shampoo.
The invention has the following beneficial effects:
the selected pepper extract has the effects of inhibiting bacteria, resisting bacteria, diminishing inflammation and relieving itching, can effectively kill fungi on the scalp, and fundamentally inhibits the generation of dandruff; the selected alligator oil is rich in unsaturated fatty acid natural oil, has good permeability, moisturizing and repairing effects, can soften and dissolve cutin, improves the moisture content of the scalp, and avoids the problem of dandruff and itching caused by dryness of the scalp; the alligator oil and the pepper extract have the effects of promoting blood circulation and accelerating metabolism, and the alligator oil and the pepper extract synergistically activate the cell regeneration function, repair damaged hair follicles and promote hair growth; the selected conditioning agents such as allantoin and salicylic acid are matched, so that the antibacterial, anti-inflammatory and lasting moisturizing effects of the shampoo are further improved, the problems of dandruff, scalp inflammation and the like are effectively relieved, the irritation of pyridone ethanolamine salt and selenium sulfide to the scalp is reduced, and the problem of alopecia, dandruff and scalp itching caused by the irritation of the dandruff remover is avoided.
The preparation method ensures that the components insoluble in water in the composition can be completely dissolved and uniformly mixed with other components by limiting the adding sequence and the preparation temperature of the components, avoids the failure of selenium sulfide due to poor control of the preparation temperature, and simultaneously ensures the stability and high activity of active substances such as pepper extract, crocodile oil and the like in the composition.
Detailed Description
The present invention will be described in detail with reference to examples, which are only preferred embodiments of the present invention and are not intended to limit the present invention.
Examples
The following table shows the formulation of 3 examples of the anti-dandruff shampoo of the present invention (unit:%).
The preparation method of the anti-dandruff shampoo comprises the following steps:
a. mixing the components in the phase C, and stirring until the components are completely dissolved to obtain a phase C mixture;
b. heating water to 50-55 deg.C, adding the components of phase A, stirring and heating to 80-85 deg.C, stirring at 35-40r/min, dissolving completely, and keeping the temperature for 30-35 min;
c. cooling to 45-50 deg.C, adding the components of phase B, stirring at constant temperature for 30-35min at 20-25 r/min;
cooling to 38-40 ℃, adding the C phase mixture, stirring until the C phase mixture is completely dissolved, and vacuumizing for 10-15min to obtain the anti-dandruff shampoo.
Comparative example
The following table shows the formulation of 3 comparative examples of anti-dandruff shampoos according to the invention (unit:%), prepared by mixing with stirring, as is conventional in the art.
300 subjects with close scalp health were selected and divided into 6 groups of 50 persons, and the performance of each group was measured using an equal amount of each of examples 1 to 3 and comparative examples 1 to 3, and the results are shown in the following table.
| Sample (I) | Example 1 | Example 2 | Example 3 | Comparative example 1 | Comparative example 2 | Comparison ofExample 3 |
| Instant percutaneous water loss rate% | 4.1 | 3.6 | 2.5 | 7.9 | 5.6 | 4.8 |
| Instant water content reduction rate% | 5.4 | 4.3 | 3.2 | 7.7 | 6.3 | 5.5 |
| Malassezia bacteria inhibition rate% | 76 | 89 | 96 | 70 | 75 | 82 |
| The ratio of scalp tension% | 12 | 8 | 8 | 34 | 24 | 22 |
| The inflammatory reaction crowd accounts for | 12 | 10 | 8 | 28 | 36 | 42 |
| The scurf and the head itch account for the whole | 14 | 8 | 6 | 30 | 44 | 48。 |
Therefore, the anti-dandruff shampoo disclosed by the invention can supplement water, preserve moisture, diminish inflammation and inhibit bacteria, and can effectively relieve dandruff, scalp itching and scalp inflammation.
The anti-dandruff shampoo disclosed by the invention has good antibacterial, anti-inflammatory, anti-dandruff and itching relieving effects, is capable of keeping moisture for a long time, nourishing scalp, growing hair and nourishing hair, is mild in formula and small in irritation, and can effectively relieve the problems of dandruff, itching of head, dry scalp, scalp inflammation and the like.
Claims (9)
1. The anti-dandruff shampoo is characterized by comprising the following components in percentage by weight:
phase A: 0.01-0.1% of ethylenediamine tetraacetic acid, 10-20% of fatty alcohol-polyoxyethylene ether sodium sulfate, 0.01-5% of ammonium lauryl sulfate, 0.1-10% of acrylic acid (ester)/C10-30 alcohol acrylate cross-linked polymer sodium, 0.01-0.5% of pyridone ethanol amine salt, 0.1-1% of pepper extract and 0.1-1% of alligator oil;
phase B: 0.2 to 0.5 percent of 1, 3-dimethylol dimethyl hydantoin;
and C phase: 2-5% of sodium lauroyl sarcosinate and 1-2% of selenium sulfide;
and the balance water.
2. The anti-dandruff shampoo of claim 1, further comprising 0.1 to 2.5% of a first conditioner, 0.1 to 6% of a surfactant, and 0.1 to 0.5% of a thickener in the phase A.
3. The anti-dandruff shampoo according to claim 2, wherein the first conditioning agent is at least one of the following components: polyquaternium-10, cetearyl alcohol, salicylic acid, allantoin and DL-panthenol.
4. The anti-dandruff shampoo of claim 2, wherein the surfactant is at least one of sodium lauroamphoacetate and coconut oil fatty acid monoethanolamide.
5. The anti-dandruff shampoo of claim 2, wherein the thickener is carbomer.
6. The anti-dandruff shampoo according to claim 1, wherein the phase B further comprises 0.1-4.5% of a second conditioner, 0.1-1% of a softener and 0.1-0.5% of essence.
7. The anti-dandruff shampoo according to claim 6, wherein the second conditioning agent is at least one of the following components: arginine, menthol, emulsified silicone oil, guar hydroxypropyl trimethyl ammonium chloride, monoglyceride citrate and PEG-7 glyceryl cocoate.
8. The anti-dandruff shampoo according to claim 6, wherein the softener is at least one of the following components: polydimethylsiloxane, C12-15 alkanol polyether-3, and triethanolamine dodecylbenzene sulfonate.
9. A method for preparing an anti-dandruff shampoo as claimed in claim 1, characterized by comprising the following steps:
mixing the components in the phase C, and stirring until the components are completely dissolved to obtain a phase C mixture;
heating water to 50-55 deg.C, adding the components of phase A, stirring and heating to 80-85 deg.C, stirring at 35-40r/min, dissolving completely, and keeping the temperature for 30-35 min;
cooling to 45-50 deg.C, adding the components of phase B, stirring at constant temperature for 30-35min at 20-25 r/min;
cooling to 38-40 ℃, adding the C phase mixture, stirring until the C phase mixture is completely dissolved, and vacuumizing for 10-15min to obtain the anti-dandruff shampoo.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111888286A (en) * | 2020-07-21 | 2020-11-06 | 集思美创(广州)科技有限公司 | Compound plant dandruff-removing and itching-relieving shampoo and preparation method thereof |
| CN112691055A (en) * | 2021-02-09 | 2021-04-23 | 惠州市光大化妆品有限公司 | Anti-dandruff shampoo and preparation method thereof |
| CN112812906A (en) * | 2021-01-22 | 2021-05-18 | 王建功 | Shampoo soap containing selenium sulfide plant extract and preparation method and application thereof |
| CN112891285A (en) * | 2021-02-09 | 2021-06-04 | 惠州市光大化妆品有限公司 | Mite removing composition, shower gel containing mite removing composition and preparation method of shower gel |
| CN113509424A (en) * | 2021-04-28 | 2021-10-19 | 惠州市肌缘生物科技股份有限公司 | Selenium sulfide dandruff-removing itching-relieving plant mite-removing shampoo and preparation process thereof |
| CN114748373A (en) * | 2022-05-30 | 2022-07-15 | 澳思美科技(广州)有限公司 | Low-irritation amino acid anti-dandruff mutual ligand and preparation method and application thereof |
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