CN117159403A - Oil-control fluffy composition and preparation method and application thereof - Google Patents

Oil-control fluffy composition and preparation method and application thereof Download PDF

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CN117159403A
CN117159403A CN202311246452.3A CN202311246452A CN117159403A CN 117159403 A CN117159403 A CN 117159403A CN 202311246452 A CN202311246452 A CN 202311246452A CN 117159403 A CN117159403 A CN 117159403A
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oil
fluffy
control
composition
oil control
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韩婕珺
招嘉斯
龚天贵
王斌
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Meichulai Hangzhou Cosmetics Co ltd
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Meichulai Hangzhou Cosmetics Co ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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Abstract

The invention relates to an oil-control fluffy composition, and a preparation method and application thereof, and belongs to the technical field of cosmetics. The invention provides an oil control fluffy composition, which comprises hydrolyzed ginsenoside, magnolia bark extract, peony fermentation liquor and hydroxypropyl starch, wherein the mass ratio of the hydrolyzed ginsenoside, magnolia bark extract, peony fermentation liquor and hydroxypropyl starch is as follows: (0.01-1): (0.01-0.5): (0.1-5): (0.1-1). The oil-control fluffy composition disclosed by the invention can effectively and mildly control abnormal secretion of scalp grease, strengthen scalp skin barrier, promote scalp moisturizing ability and regulate scalp microecological balance through reasonable combination and proportion of components; meanwhile, the fluffing effect of the hairline can be enhanced, and the long-acting oil control is fluffy.

Description

Oil-control fluffy composition and preparation method and application thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to an oil-control fluffy composition, and a preparation method and application thereof.
Background
Oily scalp is characterized by overactive sebaceous glands and excessive sebum secretion, which can lead to greasy and heavy hair, less hair appearance, easy collapse, and cause pathological manifestations such as dandruff, irritation, itching, and the like. Thus, consumers of oily scalp would prefer to increase the frequency of hair washing, use targeted oil control hair washes, help slow sebum secretion, and reduce hair greasy feel.
Most of the existing oil control shampoos adopt a strategy of strengthening the cleaning force to strongly remove grease, but the irritation to scalp is high, excessive cleaning can be caused by long-term use, the skin barrier of the scalp is damaged, more grease can be secreted by the scalp rather quickly, the long-term oil control effect cannot be achieved, only the oil is controlled immediately, and the fluffy effect is poor. Patent CN113425624a discloses a composition for removing dandruff and controlling oil, a preparation method and application thereof, wherein the composition can cause excessive cleaning to scalp, damage the ecological environment of scalp, cause scalp dryness, cause abnormal grease secretion and damage the health of scalp. Patent CN 115737487A provides a shampoo composition for controlling scalp grease secretion, which can effectively clean scalp and hair and simultaneously relieve the irritation to the scalp, maintain the water-oil balance of the scalp and achieve the effect of durable oil control through the cooperation of components such as functional grease, oily hair conditioner, keratin, amino acid surfactant, humectant and the like, but the bulking effect of the composition is poor.
Based on the problems, the oil control product for oily scalp is subjected to a mild cleaning strategy, so that the stimulation to the scalp is reduced while the superfluous grease is removed, the micro-ecological environment of the scalp is maintained, the skin barrier of the scalp is enhanced, the fluffy effect of hairlines is improved, and healthy scalp hair is manufactured.
Therefore, the oil control fluffy product capable of effectively controlling excessive secretion of scalp grease, improving the micro-ecological environment and the health state of the scalp and improving the fluffy degree of hairline has important significance.
Disclosure of Invention
The invention aims to overcome the problems in the prior art and provide an oil control fluffy composition and a preparation method and application thereof.
The invention is realized by the following technical scheme:
in a first aspect, the invention provides an oil control fluffy composition, which comprises hydrolyzed ginsenoside, magnolia bark extract, peony fermentation liquor and hydroxypropyl starch, wherein the mass ratio of the hydrolyzed ginsenoside, magnolia bark extract, peony fermentation liquor and hydroxypropyl starch is as follows: (0.01-1): (0.01-0.5): (0.1-5): (0.1-1).
The hydrolysis ginsenoside in the oil-control fluffy composition can effectively inhibit the activity of 5 alpha-reductase, slow down the speed of secreting grease from skin and effectively control oil; can also effectively resist free radicals and oxidation pressure. Cortex Magnolia officinalis bark extract has broad-spectrum antibacterial effect, and can inhibit flora by inhibiting synthesis of DNA and RNA. For oily scalp people, excessive sebum secretion can cause the abnormal proliferation of the lipotrope microorganisms, destroy the microecological balance of the scalp, and the magnolia bark extract can inhibit the abnormal proliferation of the malassezia, regulate unbalanced microorganism composition and restore the healthy state of the scalp. The peony fermentation liquor contains rich substances such as flavone, polyphenol and the like, has the effects of resisting oxidation, moisturizing, relieving and repairing, can enhance the moisturizing capability of the scalp, and promote the barrier function of the scalp, thereby relieving the abnormal secretion of scalp grease. The high molecular polymer hydroxypropyl starch can be deposited on the surface of hair to form a film in a small amount, so that the bulkiness of the hair is improved. The oil-control fluffy composition provided by the invention can be used for effectively and mildly controlling abnormal secretion of scalp grease, enhancing scalp skin barrier, improving scalp moisturizing ability and regulating scalp microecological balance through reasonable component combination and proportioning adjustment. Meanwhile, the fluffy effect of the hair can be enhanced, so that the scalp and hair can be recovered to a healthy state.
Preferably, the hydrolyzed ginsenoside is prepared from ginseng by a specific enzyme conversion technology; the hydrolyzed ginsenoside includes rare ginsenoside F2, ginsenoside Rh1 and ginsenoside Rg2. The preparation yield of the hydrolyzed ginsenoside is ten thousand times higher than that of the common extraction process, and the obtained hydrolyzed ginsenoside has core component of rare ginsenoside F2 and ginsenoside with Rg2, rh1 and other configurations. The structural formula of rare ginsenoside F2 is shown in formula I, the structural formula of ginsenoside Rh1 is shown in formula II, and the structural formula of ginsenoside Rg2 is shown in formula III:
preferably, the preparation method of the peony fermentation broth comprises the following steps: at least one of branches, flowers and leaves of peony is used as a raw material, lactobacillus is used as a fermentation strain, and the peony is prepared by a supermolecular biological catalysis technology.
The supermolecular biocatalysis technology refers to the technology that under the supermolecular solvent system, the enzyme shows higher activity, selectivity and stability, so as to obtain higher active matter content; and the additive does not need to be added with solubilizer, emulsifier and the like, so that adverse reaction of the additive to the skin can be reduced. Compared with the common peony extract, the peony fermentation liquor prepared by the supermolecular biocatalysis technology is lower in sensitivity and purer, fully releases active ingredients in peony, greatly improves water solubility and biological activity, and is rich in substances such as flavone, polyphenol and the like.
As a preferred embodiment of the oil control fluffy composition, the mass ratio of the hydrolyzed ginsenoside, the magnolia bark extract, the peony fermentation liquor and the hydroxypropyl starch is as follows: (0.1-0.5): (0.02-0.2): (0.5-2): (0.2-1). The oil-control fluffy composition has better oil-control fluffy effect.
Preferably, the mass ratio of the hydrolyzed ginsenoside, magnolia bark extract, peony fermentation liquor and hydroxypropyl starch is as follows: 0.3:0.1:2:0.3.
in a second aspect, the present invention provides a method for preparing the oil control fluff composition, comprising the steps of:
(1) Heating hydrolyzed ginsenoside in acidic solution, and adding alkali for neutralization to obtain precipitate;
(2) Dissolving the precipitate obtained in the step (1) in an alcohol solvent, adding peony fermentation liquor, stirring and standing to obtain self-assembled ginsenoside-peony nano micelle solution;
(3) Mixing the ginsenoside-peony nano micelle solution obtained in the step (2) with magnolia bark extract and hydroxypropyl starch to obtain the oil-control fluffy composition.
In the invention, hydrolyzed ginsenoside is taken as natural amphiphilic glycoside, and can self-assemble to form ginsenoside nano micelle through the interaction of alkyl-alkyl and hydrogen bond under the conditions of acid hydrolysis and alkali neutralization. The peony fermentation liquor adopted by the invention has the advantages that the high-activity flavone and polyphenol contain rich hydroxyl groups, and the high-activity flavone and polyphenol can form the ginsenoside-peony nano micelle solution with ginsenoside under specific conditions through hydrogen bond and electrostatic action, so that the biocompatibility is effectively improved, and the penetration of active substances to skin is promoted. The preparation method provided by the invention can fully exert the effects of all components in the composition, improves the bioavailability of the oil-control fluffy composition, and ensures that the composition has an excellent oil-control fluffy effect.
Preferably, in the step (1), the acidic solution is an acetic acid solution, and the base is sodium carbonate; the heating temperature is 75-85 ℃ and the heating time is 3-5 h. More preferably, the heating is at a temperature of 80 ℃ for a period of 4 hours.
Preferably, in the step (2), the alcohol solvent comprises at least one of butanediol, 1, 3-propanediol and ethanol; the dissolution temperature is 60-65 ℃; the temperature of stirring is 3-5 ℃ and the time is 20-40 min; the temperature is 3-5 ℃ and the time is 3-5 h when the mixture is kept stand. More preferably, the temperature of the stirring is 4 ℃ and the time is 30min; the temperature during standing is 4 ℃ and the time is 4 hours.
In a third aspect, the present invention provides the use of said oil control fluff composition or said oil control fluff composition prepared by a process for the preparation of said oil control fluff composition in cosmetics.
The composition has excellent oil control and fluffiness effects, and can be widely applied to cosmetics, preferably shampoo.
In a fourth aspect, the invention provides an oil control and fluffy shampoo, which comprises the oil control and fluffy composition, wherein the mass percentage of the oil control and fluffy composition in the oil control and fluffy shampoo is 0.05-3%.
Preferably, the mass percentage of the oil control fluffy composition in the oil control fluffy shampoo is 0.5-2%.
As a preferred embodiment of the oil control and fluffing shampoo of the present invention, the oil control and fluffing shampoo comprises, in mass percent: 5 to 30 percent of surfactant, 0.1 to 5 percent of hair conditioner, 0.05 to 3 percent of oil control fluffy composition, 0.2 to 4 percent of excipient, 0.1 to 2 percent of preservative, 0.1 to 2 percent of essence, 0.01 to 1 percent of pH regulator and the balance of water.
Preferably, the surfactant comprises: at least one of sodium lauroyl sarcosinate, sodium cocoyl amidopropionate, sodium cocoyl methyl taurate, sodium methyl cocoyl taurate, decyl glucoside, lauryl glucoside, cocoamidopropyl betaine, cocamidopropyl hydroxysulfobetaine, lauramidopropyl hydroxysulfobetaine, sodium lauroyl amphoacetate, sodium C14-16 olefin sulfonate, sodium laurylglycol carboxylate, cocoamidomethyl MEA, cocoamidoMEA.
Preferably, the hair conditioner comprises: at least one of polyquaternium 67, polyquaternium 10, polyquaternium 11, polyquaternium 7, polyquaternium 52, guar hydroxypropyl trimethylammonium chloride, hydroxypropyl guar hydroxypropyl trimethylammonium chloride, behenyl trimethylammonium methylsulfate and western Qu An methylsulfate.
Preferably, the ester forming agent comprises: at least one of propylene glycol laurate, lauric acid, PPG-5-cetyl polyether-20, PPG-3 octyl ether, C12-13 alcohol lactate, peony seed oil and glycerol caprylate.
Preferably, the preservative comprises: at least one of sodium benzoate, potassium sorbate, chlorphenesin, phenoxyethanol, colloidal silver, and piroctone olamine salt.
Preferably, the pH adjuster comprises: at least one of arginine, citric acid, lactic acid, lactobionic acid, sodium hydroxide, potassium hydroxide, aminomethylpropanol, and tromethamine.
In a fifth aspect, the invention provides a preparation method of the oil-control fluffy shampoo, which comprises the following steps:
s1, dispersing a hair conditioner in water, heating to 70-80 ℃ while stirring, and stirring until the hair conditioner is completely dissolved to obtain a phase A;
s2, adding a surfactant and an ester forming agent into the phase A, and stirring for 0.5-2 hours at a constant temperature to obtain a phase B;
s3, cooling to 50-60 ℃, adding the oil-control fluffy composition into the phase B, and stirring until the oil-control fluffy composition is completely dissolved to obtain a phase C;
s4, cooling to 40-50 ℃, adding a pH regulator to adjust the pH to 5.5-6.5, and adding a preservative and essence to prepare the oil-control fluffy shampoo.
The preparation method of the oil-control fluffy shampoo is simple, and the prepared shampoo has remarkable oil-control, moisturizing and fluffy effects, is long-acting in oil control and fluffy, and can regulate scalp and hair health.
The invention has the following beneficial effects:
1. the oil control fluffy composition adopts the thought of mildness and oil control, does not excessively remove grease, protects scalp barriers and realizes the sustainability of oil control effect.
2. The grease secretion of the scalp is vigorous, which inevitably leads to the abnormal proliferation of the malassezia with the fat, and damages the micro-ecological balance of the scalp; the oil-control fluffy composition is matched with magnolia bark extract with inhibition effect on malassezia, so that the composition is mild and antibacterial, and can maintain scalp steady state.
3. The preparation process of the oil-control fluffy composition is different from the common process, so that the affinity of the oil-control fluffy composition with scalp is improved, and the utilization efficiency of the oil-control fluffy composition in a flushing type product is higher.
4. The oil control and fluffing composition provided by the invention contains both an oil control component aiming at scalp and a fluffing component aiming at hair, and achieves the effects of refreshing scalp and fluffing hair under the combined action.
Detailed Description
For a better description of the objects, technical solutions and advantages of the present invention, the present invention will be further described with reference to the following specific examples. It will be appreciated by persons skilled in the art that the specific embodiments described herein are for purposes of illustration only and are not intended to be limiting.
The test methods used in the examples are conventional methods unless otherwise specified; the materials, reagents and the like used, unless otherwise specified, are all commercially available.
The component content ratios of the oil control and fluffy shampoos of examples and comparative examples are shown in tables 1 and 2 below, wherein the hydrolyzed ginsenoside compounds described in examples and comparative examples are available from Suni Jinsenoside PLF of three ant technologies (guangzhou) inc; the peony fermentation broth is purchased from SHINE+peony fermentation filtrate of Shenzhen Hemerocallis, biotechnology Co.
The component content ratio (mass percent) of the oil-control fluffy shampoo of the embodiment of table 1
Table 2 comparative examples of the component content ratios (mass percent) of the oil-controlling and fluffy shampoos
The preparation method of the oil control fluffy compositions of the other examples and comparative examples, except comparative example 6, comprises the following steps:
(1) Dissolving the hydrolyzed ginsenoside powder in acetic acid solution according to the mass percentage, carrying out heat preservation and reflux for 4 hours at 80 ℃, and then adding Na 2 CO 3 Neutralizing to obtain a precipitate;
(2) Dissolving the precipitate obtained in the step (1) in ethanol at 65 ℃, adding the peony fermentation liquor with the mass percentage, stirring the solution at the constant temperature of 4 ℃ for 0.5h, and standing at the constant temperature of 4 ℃ for 4h to obtain a self-assembled ginsenoside-peony nano micelle solution;
(3) Mixing the ginsenoside-peony nano micelle solution obtained in the step (2) with magnolia bark extract and hydroxypropyl starch according to the mass percentage to obtain the oil-control fluffy composition.
The preparation method of the oil control fluffy composition of comparative example 6 comprises the following steps: according to the mass percentage, dissolving the hydrolyzed ginsenoside powder and the magnolia bark extract in ethanol at 65 ℃, then adding the peony fermentation liquor and the hydroxypropyl starch, and uniformly mixing to obtain the oil-control fluffy composition.
The preparation method of the oil-control fluffy shampoo of the embodiment and the comparative example comprises the following steps:
s1, dispersing a hair conditioner in water, heating to 75 ℃ while stirring, and stirring until the hair conditioner is completely dissolved to obtain a phase A;
s2, adding a surfactant and an ester forming agent into the phase A, and carrying out heat preservation and stirring for 2 hours to obtain a phase B;
s3, cooling to 60 ℃, adding the oil control fluffy composition into the phase B, and stirring until the oil control fluffy composition is completely dissolved to obtain a phase C;
s4, cooling to 50 ℃, adding a pH regulator to adjust the pH to 5.5-6.5, and adding a preservative and essence to prepare the oil-control fluffy shampoo.
Effect example 15 alpha-reductase inhibition test
The oil control fluffy compositions in the examples and the comparative examples are respectively prepared into samples with the mass concentration of 20%, testosterone is selected as a substrate, finasteride is selected as a positive control, the results are analyzed by high performance liquid chromatography, the change of the testosterone concentration before and after the reaction is measured, and the inhibition rate of the oil control fluffy composition to 5 alpha-reductase is calculated, and the results are shown in table 3.
TABLE 3 inhibition of 5 alpha-reductase by the oil control fluff composition of examples and comparative examples
Group of 5 alpha-reductase inhibition/%
Blank group 0
Positive group 80.21
Example 1 64.83
Example 2 62.41
Example 3 62.57
Example 4 51.46
Example 5 59.82
Example 6 57.26
Comparative example 1 0
Comparative example 2 21.05
Comparative example 3 30.21
Comparative example 4 26.51
Comparative example 5 23.54
Comparative example 6 24.53
Comparative example 7 3.64
Comparative example 8 5.41
Comparative example 9 63.54
Comparative example 10 62.71
Comparative example 11 52.46
Comparative example 12 58.64
As can be seen from table 3, the oil control fluffy composition of the embodiment of the invention has a good 5 alpha-reductase inhibition effect, has obvious 5 alpha-reductase inhibition activity improvement compared with comparative examples 1-8, can effectively slow down the speed of secreting grease from skin, resists free radicals, and realizes the oil control effect.
Effect example 2 human body Patch test
30 volunteers are recruited, 15 volunteers are used for men and women, the ages are 20-50 years, an equal amount (0.020 mL-0.025 mL) of oil control fluffy shampoo (with the mass fraction of 20%) of the example and the comparative example is placed in a specific patch tester, the shampoo is applied to the arms of the volunteers by using hyposensitization adhesive tapes, and the shampoo is uniformly applied to the skin by light pressure and stays for 24 hours; the blank group was volunteer without product. After 24h, the patch tester was removed, and after 0.5h, 24h, 48h, the skin reaction was observed and the results recorded. The adverse reaction grade of the skin is shown in Table 4, and the test results of the patch test on the human body are shown in Table 5.
TABLE 4 adverse reaction grade of skin
Table 5 results of body patch test of the oil control and conditioning shampoo of examples and comparative examples
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As can be seen from the above table 5, the oil control and fluffy composition of the present invention does not have skin adverse reaction when applied to shampoo, but comparative example 2, comparative example 4, comparative example 10 and comparative example 12 have 1-grade adverse reaction, respectively; therefore, under reasonable combination of the combination and the proportion, the oil-control fluffy composition is safe and has no stimulation to human skin.
Effect example 3 human efficacy test
180 volunteers with scalp easy to get oil and fine and soft hair are recruited, the age is 18-45 years, 10 people are randomly grouped, each group of volunteers respectively use 1 group of shampoo, wash hair once every two days, and the use lasts for 14 days.
(3.1) scalp oil secretion amount, scalp moisture content, scalp percutaneous moisture loss Rate
A region (1 cm) was shaved on the volunteer's head 2 ) Measuring scalp fat amount by professional using fat testing instrument Sebumeter before use (D0) and after use (D14), measuring 3 times of data, and taking average value; scalp moisture content was measured using a Derma Lab, 5 times of data were measured, and an average value was taken; measuring the TEWL value by using a percutaneous moisture loss instrument Tewameter, measuring 3 times of data, and taking an average value; from the addition amount of the oil control fluffy composition, comparative example 1 was a blank, and the test results are shown in table 6.
Table 6 results of scalp fat secretion, scalp moisture content, scalp percutaneous moisture loss test of examples and comparative examples
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As can be seen from table 6, the oil-control and fluffy shampoo of the invention can effectively reduce the secretion of scalp grease, improve the moisture content of the scalp, reduce the percutaneous moisture loss of the scalp, realize the purposes of controlling oil and regulating scalp health, and the shampoos of comparative example 9 and comparative example 10 can not realize the water-oil balance, degrade the moisture content of the scalp and ensure scalp health although the shampoo can effectively control oil.
(3.2) Malachillea number
The scalp fixation area (1 cm) 2 ) The results of staining and counting the number of malassezia were shown in table 7.
Table 7 results of the test for the number of Malachillea bacteria in examples and comparative examples
From Table 7, it can be seen that the oil-control fluffy shampoo of the invention can effectively inhibit the propagation of malassezia, regulate and control the microecological balance of scalp and restore the scalp health.
(3.3) questionnaire: the volunteers were subjected to a questionnaire investigation, and feedback of the oil control fluffy effect was collected, wherein there was 5 scores with very obvious effect, 4 scores with more obvious effect, 3 scores with general effect, 2 scores with slight improvement, 1 score without improvement, and the average score of each item was counted, and the results are shown in table 8.
Table 8 results of the oil control and conditioning hair conditioner questionnaire of examples and comparative examples
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The results in Table 8 show that the oil-control fluffy composition provided by the invention has good use effect, can effectively regulate scalp state while controlling oil and fluffy, and can control oil and fluffy for a long time.
According to the test results of the effect examples, the oil-control fluffy composition disclosed by the invention can be used for effectively solving the greasy problem of scalp and hair through reasonable collocation of the oil-control moisturizing antibacterial component and the fluffy component and a unique preparation process, and improving the health state of the scalp at the same time, so that the long-acting oil-control fluffy effect is achieved.
Finally, it should be noted that the above embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solution of the present invention may be modified or substituted equally without departing from the spirit and scope of the technical solution of the present invention.

Claims (10)

1. The oil-control fluffy composition is characterized by comprising hydrolyzed ginsenoside, magnolia bark extract, peony fermentation liquor and hydroxypropyl starch, wherein the mass ratio of the hydrolyzed ginsenoside to the magnolia bark extract to the peony fermentation liquor to the hydroxypropyl starch is as follows: (0.01-1): (0.01-0.5): (0.1-5): (0.1-1).
2. The oil control fluffy composition according to claim 1, wherein the mass ratio of the hydrolyzed ginsenoside, the magnolia bark extract, the peony fermentation broth and the hydroxypropyl starch is as follows: (0.1-0.5): (0.02-0.2): (0.5-2): (0.2-1).
3. A process for preparing the oil control fluff composition of claim 1 or 2 comprising the steps of:
(1) Heating hydrolyzed ginsenoside in acidic solution, and adding alkali for neutralization to obtain precipitate;
(2) Dissolving the precipitate obtained in the step (1) in an alcohol solvent, adding peony fermentation liquor, stirring and standing to obtain self-assembled ginsenoside-peony nano micelle solution;
(3) Mixing the ginsenoside-peony nano micelle solution obtained in the step (2) with magnolia bark extract and hydroxypropyl starch to obtain the oil-control fluffy composition.
4. A process for the preparation of an oil control fluff composition according to claim 3, wherein in step (2), the temperature of the stirring is 3 ℃ to 5 ℃ for 20min to 40min; the temperature is 3-5 ℃ and the time is 3-5 h when the mixture is kept stand.
5. Use of the oil control fluff composition of claim 1 or 2 or the oil control fluff composition prepared by the method of preparing the oil control fluff composition of claim 3 or 4 in cosmetics.
6. An oil control and fluffy shampoo is characterized by comprising the oil control and fluffy composition as claimed in claim 1 or 2, wherein the mass percentage of the oil control and fluffy composition in the oil control and fluffy shampoo is 0.05-3%.
7. The oil control and fluffy shampoo of claim 6 wherein the oil control and fluffy composition comprises 0.5-2% by mass of the oil control and fluffy shampoo.
8. The oil control and conditioning shampoo of claim 6, further comprising, in mass percent: 5 to 30 percent of surfactant, 0.1 to 5 percent of hair conditioner, 0.2 to 4 percent of ester forming agent, 0.1 to 2 percent of preservative, 0.1 to 2 percent of essence, 0.01 to 1 percent of pH regulator and the balance of water.
9. The oil control and conditioning shampoo of claim 8, wherein at least one of:
(1) The surfactant comprises: at least one of sodium lauroyl sarcosinate, sodium cocoyl amidopropionate, sodium cocoyl methyl taurate, sodium methyl cocoyl taurate, decyl glucoside, lauryl glucoside, cocoamidopropyl betaine, cocamidopropyl hydroxysulfobetaine, lauramidopropyl hydroxysulfobetaine, sodium lauroyl amphoacetate, sodium C14-16 olefin sulfonate, sodium lauryl glycolate, cocoamidomethyl MEA, cocoamidomea;
(2) The hair conditioner comprises: at least one of polyquaternium 67, polyquaternium 10, polyquaternium 11, polyquaternium 7, polyquaternium 52, guar hydroxypropyl trimethylammonium chloride, hydroxypropyl guar hydroxypropyl trimethylammonium chloride, behenyl trimethylammonium methylsulfate and western Qu An methylsulfate;
(3) The ester forming agent comprises: at least one of propylene glycol laurate, lauric acid, PPG-5-cetyl polyether-20, PPG-3 octyl ether, C12-13 alcohol lactate, peony seed oil and glycerol caprylate;
(4) The preservative comprises: at least one of sodium benzoate, potassium sorbate, chlorphenesin, phenoxyethanol, colloidal silver, piroctone olamine salt;
(5) The pH regulator comprises: at least one of arginine, citric acid, lactic acid, lactobionic acid, sodium hydroxide, potassium hydroxide, aminomethylpropanol, and tromethamine.
10. A method for preparing the oil-control fluffy shampoo according to claim 8, which is characterized by comprising the following steps:
s1, dispersing a hair conditioner in water, heating to 70-80 ℃ while stirring, and stirring until the hair conditioner is completely dissolved to obtain a phase A;
s2, adding a surfactant and an ester forming agent into the phase A, and stirring for 0.5-2 hours at a constant temperature to obtain a phase B;
s3, cooling to 50-60 ℃, adding the oil-control fluffy composition into the phase B, and stirring until the oil-control fluffy composition is completely dissolved to obtain a phase C;
s4, cooling to 40-50 ℃, adding a pH regulator to adjust the pH to 5.5-6.5, and adding a preservative and essence to prepare the oil-control fluffy shampoo.
CN202311246452.3A 2023-09-26 2023-09-26 Oil-control fluffy composition and preparation method and application thereof Pending CN117159403A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118141736A (en) * 2024-05-11 2024-06-07 威莱(广州)日用品有限公司 Scalp oil control maintenance composition and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118141736A (en) * 2024-05-11 2024-06-07 威莱(广州)日用品有限公司 Scalp oil control maintenance composition and preparation method thereof

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