CN110693755A - Novel safe and environment-friendly optically variable nail polish - Google Patents

Novel safe and environment-friendly optically variable nail polish Download PDF

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Publication number
CN110693755A
CN110693755A CN201911163108.1A CN201911163108A CN110693755A CN 110693755 A CN110693755 A CN 110693755A CN 201911163108 A CN201911163108 A CN 201911163108A CN 110693755 A CN110693755 A CN 110693755A
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nail polish
optically variable
finished
essence
semi
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金继月
戴永求
叶志勇
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Jinhua City Keweisi Chemical Co Ltd
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Jinhua City Keweisi Chemical Co Ltd
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Priority to CN201911163108.1A priority Critical patent/CN110693755A/en
Publication of CN110693755A publication Critical patent/CN110693755A/en
Priority to PCT/CN2020/106188 priority patent/WO2021103632A1/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q3/00Manicure or pedicure preparations
    • A61Q3/02Nail coatings
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42Colour properties
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42Colour properties
    • A61K2800/43Pigments; Dyes
    • A61K2800/438Thermochromatic; Photochromic; Phototropic
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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Abstract

The invention provides a novel safe and environment-friendly optically variable nail polish, which comprises the following components: butyl acetate, ethyl acetate, a film forming agent, denatured ethanol, a plasticizer, a thickening suspending agent, an optically variable material, a pigment and essence. The safe and environment-friendly naphthopyran optically variable materials are used in the optically variable nail polish, and different colors and bright colors can be changed under the irradiation of sunlight; the photochromic nail polish uses one of watermelon essence, rose essence, grapefruit essence, chocolate essence and strawberry essence, and has fragrance similar to perfume; ethyl acetate, butyl acetate and denatured ethanol which have less irritation to human bodies and skins are used as solvents, and toluene and acetone which have great harm to human bodies are abandoned; the other materials are benzene-free, toluene-free, DBP-free and formaldehyde-free materials, so that the nail and skin of a human body are less damaged, the color can be changed according to illumination, and the nail polish has the characteristics of bright color, strong adhesive force, high storage stability and the like.

Description

Novel safe and environment-friendly optically variable nail polish
Technical Field
The invention relates to the technical field of cosmetics, in particular to novel safe and environment-friendly optically variable nail polish.
Background
The nail polish belongs to a color cosmetic product in cosmetics, is widely used for beautifying and decorating fingernails or toenails, has rich and gorgeous color and both attractive appearance and protective effect, and is a cosmetic which can not be replaced by beauty-loving women. The existing nail polish only has a fixed color, is monotonous and cannot meet the requirement of women on the diversity of the nail polish. There are also patents reporting optically variable nail polish products.
CN201310746497.7 discloses a novel photochromic nail polish, which has the characteristics of changing into different colors under the irradiation of sunlight, uniform color and high firmness. But it uses camphor, which is not safe and environmentally friendly, as a plasticizer. CN201410582427.7 discloses a long-acting color-changing nail polish which has the characteristics of bright color, color changing, good economy, easy drying and the like. But the acetone which is forbidden in the cosmetic industry is used as a solvent, so that the harm to the health of the human body is large. CN201110391738.1 and
cn201710179691.x discloses a composition of a color-changing nail polish and a color-changing nail polish, respectively, both of which change color with light to produce different decorative aspects. But the solvent is toluene which is feared by people, so the method is not suitable for market popularization. In addition, optically variable materials or color-changing materials used in the commercially available optically variable nail polish are not good for human health, and can cause environmental pollution; meanwhile, the method forms a technical barrier for export trade due to the fact that the method does not conform to the law of the European Union, American cosmetic law.
Disclosure of Invention
The invention aims to provide a novel safe and environment-friendly optically variable nail polish to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a novel safe environmental protection's light becomes nail polish, includes base stock raw materials and mixing of colors raw materials, the base stock raw materials include butyl acetate, ethyl acetate, film-forming agent, denatured ethanol, plasticizer and thickening suspending agent, the mixing of colors raw materials includes light becomes material, pigment and essence:
the concrete weight components are as follows: butyl acetate: 26-36 parts by weight of ethyl acetate: 20-28 parts by weight of film forming agent: 18-23 parts by weight of denatured ethanol: 3-5 parts by weight of plasticizer: 2-5 parts by weight of thickening suspending agent: 0-3 parts by weight of optically variable material: 5-10 parts of pigment: 0-5 parts by weight of essence: 0 to 3 parts by weight.
Preferably, the film forming agent is one or more of nitrocellulose, acrylic resin, alkyd resin and polyester resin.
Preferably, the plasticizer is one or more of acetyl tributyl citrate, tributyl citrate and tricresyl phosphate.
Preferably, the thickening suspending agent is one or more of selectrium chloride hectorite and silica.
Preferably, the optically variable material is a photochromic material containing a naphthopyran organic substance.
Preferably, the pigment is one or more of an inorganic pigment, an organic pigment, pearlescent mica and colored PET spangles.
Preferably, the essence can be set to be one of watermelon essence, rose essence, grapefruit essence, chocolate essence and strawberry essence.
The invention also provides a preparation method of the novel safe and environment-friendly optically variable nail polish, which comprises the following specific steps:
the method comprises the following steps: mixing base materials: adding butyl acetate, ethyl acetate, a film forming agent, denatured ethanol, a plasticizer and a thickening suspending agent which form the base material raw materials into a stirring barrel, starting a stirrer to stir at a high speed, ensuring that the base material raw materials are uniformly stirred to form a semi-finished product, and standing for later use after the uniformly stirred semi-finished product is discharged;
step two: mixing the base material and the color matching raw material: adding the semi-finished product prepared in the step one into a stirring barrel, sequentially adding the optically variable material, the pigment and the essence which form the color matching raw material into the stirring barrel for mixing and stirring, ensuring that the base material raw material and the color matching raw material are uniformly mixed to form a nail polish semi-finished product, ensuring that the color meets the standard requirement, and standing the nail polish semi-finished product after the uniformly mixed nail polish semi-finished product is discharged for later use;
step three: and (3) inspecting the semi-finished nail polish product: detecting the appearance, color and drying time items of the semi-finished nail polish product according to the quality requirement of the nail polish, entering the next procedure after the semi-finished nail polish product is qualified, and if the semi-finished nail polish product is unqualified, conveying the unqualified semi-finished nail polish product to a waste product centralized recycling pool for concentration;
step four: safe filling: slowly adding the qualified semi-finished nail polish product prepared in the step three into a filling machine, covering a cover on an inserted air pipe, filling the semi-finished nail polish product into a nail polish bottle through the filling machine, and packaging to form a finished nail polish product, wherein the filling operation must pay strict attention to production safety and fire safety;
step five: inspecting a nail polish finished product: installing the packaged finished nail polish products with the execution standard of nail polish QB/T2287-2011 for sampling inspection, warehousing after the finished nail polish products are qualified, and conveying the unqualified finished nail polish products to a waste centralized recovery pool for concentration if the finished nail polish products are unqualified;
step six: and after the production in the steps is finished, cleaning the stirrer, the filling machine and the filling machine table by using ethyl acetate, and airing.
The preparation method of the novel safe and environment-friendly optically variable nail polish as claimed in claim 8, wherein the preparation method comprises the following steps: and C, inspecting the materials consisting of the nail polish bottles selected in the step four, wherein the inspected materials consisting of the nail polish bottles do not react with the base material raw materials and the color mixing raw materials, if the inspected materials do not react, the materials are discarded, and then the inspected qualified nail polish bottles are unpacked and sterilized to be filled with the semi-finished nail polish.
Preferably, the materials of the nail polish bottles selected in the fourth step need to be inspected, the materials of the inspected nail polish bottles do not react with the base material raw materials and the color matching raw materials, if the materials of the inspected nail polish bottles do not react with the base material raw materials and the color matching raw materials, the materials of the inspected nail polish bottles are discarded, and then the qualified nail polish bottles are subjected to unpacking sterilization and then filled with semi-finished nail polish.
The invention has the technical effects and advantages that:
by adopting the technical scheme, the safe and environment-friendly naphthopyran type optically variable material is used in the novel safe and environment-friendly optically variable nail polish, so that the nail polish can change different colors and bright colors under the irradiation of sunlight; the photochromic nail polish uses one of watermelon essence, rose essence, grapefruit essence, chocolate essence and strawberry essence, so that the photochromic nail polish has fragrance similar to perfume; ethyl acetate, butyl acetate and denatured ethanol which have small stimulation to human bodies and skin are used as solvents in the optically variable nail polish, and toluene and acetone which have great harm to human bodies are abandoned; the other materials in the optically variable nail polish are benzene-free, toluene-free, DBP-free and formaldehyde-free materials. The optically variable nail polish has the characteristics of less damage to human nails and skin, capability of achieving the purpose of changing color according to illumination, bright color, strong adhesive force, high storage stability and the like.
Drawings
Fig. 1 is a schematic view of a preparation method of the novel safe and environment-friendly optically-variable nail polish.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention discloses a novel safe and environment-friendly optically variable nail polish, which comprises base material raw materials and color matching raw materials, wherein the base material raw materials comprise butyl acetate, ethyl acetate, a film forming agent, denatured ethanol, a plasticizer and a thickening suspending agent, and the color matching raw materials comprise optically variable materials, pigments and essence;
the concrete weight components are as follows: butyl acetate: 26-36 parts by weight of ethyl acetate: 20-28 parts by weight of film forming agent: 18-23 parts by weight of denatured ethanol: 3-5 parts by weight of plasticizer: 2-5 parts by weight of thickening suspending agent: 0-3 parts by weight of optically variable material: 5-10 parts of pigment: 0-5 parts by weight of essence: 0 to 3 parts by weight.
More specifically:
the film forming agent is one or more of nitrocellulose, acrylic resin, alkyd resin and polyester resin.
The plasticizer is one or more of acetyl tributyl citrate, tributyl citrate and tricresyl phosphate.
The thickening suspending agent is one or more of selectrium chloride hectorite and silica.
The photochromic material is photochromic material containing NAPHTHOPYRAN organics (diphenyl methyl ester ACETOXY NAPHTHOPYRAN/diphenyl methyl ester methoxy NAPHTHOPYRAN), and is in accordance with the cosmetic law of European Union, U.S. export country. The naphthopyran compound has three-dimensional structure change in the photochromic process, the absorption wavelength of the naphthopyran compound is usually in an ultraviolet absorption region and does not show color when the naphthopyran compound is in a solution, C-O bonds in molecules are subjected to heterolysis after the naphthopyran compound is excited by ultraviolet light, the conformation and electronic arrangement of the molecules are greatly changed, and colorful color is shown after red shift of absorption. The molecule after bond breaking is generally called as "ring-opening body" or "color-changing body", and under the action of light with longer wavelength, the ring-opening body can produce ring-closing reaction and can be recovered into starting compound.
The pigment is one or more of inorganic pigment, organic pigment, pearl mica and colorful PET bright flake.
The essence can be one of watermelon essence, rose essence, grapefruit essence, chocolate essence and strawberry essence.
The concrete proportioning mode is as follows:
example 1: the invention relates to a novel safe and environment-friendly optically variable nail polish, which comprises the following components in parts by weight:
components Parts by weight Function(s)
Acetic acid butyl ester 36 Solvent(s)
Ethyl acetate 28 Solvent(s)
Nitrocellulose 10 Film forming agent
Acrylic resin 8 Film forming agent
Alkyd resin 3 Film forming agent
Polyester resin 2 Film forming agent
Denatured ethanol 3 Solvent(s)
Citric acid tributyl ester 5 Plasticizer
Optically variable material 5 Optically variable material
The components are weighed and then dispersed and stirred uniformly at 1200r/min to prepare the novel safe colorless optically variable nail polish.
Example 2: the invention relates to a novel safe and environment-friendly optically variable nail polish, which comprises the following components in parts by weight:
components Parts by weight Function(s)
Acetic acid butyl ester 34 Solvent(s)
Ethyl acetate 20 Solvent(s)
Acrylic resin 18 Film forming agent
Denatured ethanol 5 Solvent(s)
Acetyl tributyl citrate 1 Plasticizer
Triphenol phosphate 1 Plasticizer
Selea-ammonium chloride hectorite 3 Thickening suspension agent
Optically variable material 10 Optically variable material
Titanium dioxide 5 Pigment (I)
Watermelon essence 3 Essence
The components are weighed and then dispersed and stirred uniformly at 1000r/min to prepare the novel safe watermelon-flavor white photochromic nail polish.
Example 3: the invention relates to a novel safe and environment-friendly optically variable nail polish, which comprises the following components in parts by weight:
Figure BDA0002286679810000061
Figure BDA0002286679810000071
the components are weighed and then dispersed and stirred uniformly at 1500r/min to prepare the novel safe rose-flavored color paillette optically variable nail polish.
Example 4: the invention relates to a novel safe and environment-friendly optically variable nail polish, which comprises the following components in parts by weight:
components Parts by weight Function(s)
Acetic acid butyl ester 30 Solvent(s)
Ethyl acetate 24 Solvent(s)
Acrylic resin 15 Film forming agent
Alkyd resin 5 Film forming agent
Denatured ethanol 5 Solvent(s)
Acetyl tributyl citrate 2 Plasticizer
Citric acid tributyl ester 3 Plasticizer
Silica 2 Thickening suspension agent
Optically variable material 9 Optically variable material
Pearl mica 4 Pigment (I)
Grapefruit essence 1 Essence
The components are weighed and then dispersed and stirred uniformly at 1400r/min to prepare the novel safe grapefruit-flavor pearlescent mica light-variable nail polish.
Example 5: the invention relates to a novel safe and environment-friendly optically variable nail polish, which comprises the following components in parts by weight:
components Parts by weight Function(s)
Acetic acid butyl ester 32 Solvent(s)
Ethyl acetate 27 Solvent(s)
Nitrocellulose 6 Film forming agent
Acrylic resin 12 Film forming agent
Alkyd resin 2 Film forming agent
Denatured ethanol 4 Solvent(s)
Triphenol phosphate 4 Plasticizer
Selea-ammonium chloride hectorite 3 Thickening suspension agent
Optically variable material 6 Optically variable material
Red No. 6 2 Pigment (I)
Chocolate essence 2 Essence
The components are weighed and then dispersed and stirred uniformly at 1300r/min to prepare the novel safe chocolate-flavored red light-variable nail polish.
Example 6: the invention relates to a novel safe and environment-friendly optically variable nail polish, which comprises the following components in parts by weight:
Figure BDA0002286679810000081
Figure BDA0002286679810000091
the components are weighed and then dispersed and stirred uniformly at 1400r/min to prepare the novel safe strawberry-flavored blue light-variable nail polish.
Example 7: the invention relates to a novel safe and environment-friendly optically variable nail polish, which comprises the following components in parts by weight:
Figure BDA0002286679810000092
Figure BDA0002286679810000101
the components are weighed and then dispersed and stirred uniformly at 1350r/min to prepare the novel safe watermelon-flavor red pearlescent mica color PET bright flake optically-variable nail polish.
Test example 1
The performance evaluation of the safe and environment-friendly optically-variable nail polish prepared in the embodiments 1 to 7 of the invention is carried out to detect the drying time and the firmness according to the technical requirements of type I in QB/T2287-2011 nail polish; detecting the storage stability of the product according to a T/ZZB0623-2018 heat-resistant and cold-resistant detection method; the photochromic performance is detected by observing the color change condition of the fingernail sheet which is uniformly coated with the photochromic nail polish under illumination; odor and irritation were tested by applying nail polish to the nails and skin of volunteers. The results are shown in Table 1.
TABLE 1
Figure BDA0002286679810000102
The test results all meet the relevant standards. From the test results, it was found that: the optically variable nail polish has the advantages of less damage to human nails and skin, capability of achieving the purpose of changing color according to illumination, bright color, strong adhesive force, high storage stability and the like.
In addition, as shown in fig. 1, the invention also discloses a preparation method of the novel safe and environment-friendly optically variable nail polish, which comprises the following specific steps:
the method comprises the following steps: mixing base materials: adding butyl acetate, ethyl acetate, a film forming agent, denatured ethanol, a plasticizer and a thickening suspending agent which form the base material raw materials into a stirring barrel, starting a stirrer to stir at a high speed, ensuring that the base material raw materials are uniformly stirred to form a semi-finished product, and standing for later use after the uniformly stirred semi-finished product is discharged;
step two: mixing the base material and the color matching raw material: adding the semi-finished product prepared in the step one into a stirring barrel, sequentially adding the optically variable material, the pigment and the essence which form the color matching raw material into the stirring barrel for mixing and stirring, ensuring that the base material raw material and the color matching raw material are uniformly mixed to form a nail polish semi-finished product, ensuring that the color meets the standard requirement, and standing the nail polish semi-finished product after the uniformly mixed nail polish semi-finished product is discharged for later use;
step three: and (3) inspecting the semi-finished nail polish product: detecting the appearance, color and drying time items of the nail polish semi-finished product body according to the nail polish quality requirement (refer to a nail polish execution standard: QB/T2287-2011), entering the next procedure after the nail polish semi-finished product body is detected to be qualified, and if the nail polish semi-finished product body is detected to be unqualified, conveying the unqualified nail polish semi-finished product body to a waste product centralized recycling pool for concentration;
step four: safe filling: slowly adding the qualified semi-finished nail polish product prepared in the step three into a filling machine, covering a cover on an inserted air pipe tightly to prevent volatilization from affecting quality, and filling the semi-finished nail polish product into nail polish bottles through the filling machine for packaging to form a finished nail polish product, wherein the filling operation must pay strict attention to production safety and fire safety;
step five: inspecting a nail polish finished product: installing the packaged nail polish finished product with an execution standard of nail polish QB/T2287-2011 for sampling inspection, warehousing after the nail polish finished product is qualified, and conveying the unqualified nail polish finished product to a waste centralized recovery pool for concentration if the nail polish finished product is unqualified;
step six: and after the production in the steps is finished, cleaning the stirrer, the filling machine and the filling machine table by using ethyl acetate, and airing.
And further, the materials consisting of the nail polish bottles selected in the step four need to be inspected, the inspected materials consisting of the nail polish bottles do not react with the base material raw materials and the color matching raw materials, if the inspected materials do not react, the materials are discarded, and then the qualified nail polish bottles are subjected to unpacking sterilization and then filled with semi-finished nail polish.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention.

Claims (9)

1. The utility model provides a novel safe environmental protection's light becomes nail polish, includes base stock raw materials and mixing of colors raw materials, its characterized in that: the base material comprises butyl acetate, ethyl acetate, a film forming agent, denatured ethanol, a plasticizer and a thickening suspending agent, and the toning raw material comprises an optically variable material, a pigment and essence;
the concrete weight components are as follows: butyl acetate: 26-36 parts by weight of ethyl acetate: 20-28 parts by weight of film forming agent: 18-23 parts by weight of denatured ethanol: 3-5 parts by weight of plasticizer: 2-5 parts by weight of thickening suspending agent: 0-3 parts by weight of optically variable material: 5-10 parts of pigment: 0-5 parts by weight of essence: 0 to 3 parts by weight.
2. The novel safe and environment-friendly optically variable nail polish as claimed in claim 1, wherein: the film forming agent is one or more of nitrocellulose, acrylic resin, alkyd resin and polyester resin.
3. The novel safe and environment-friendly optically variable nail polish as claimed in claim 1, wherein: the plasticizer is one or more of acetyl tributyl citrate, tributyl citrate and tricresyl phosphate.
4. The novel safe and environment-friendly optically variable nail polish as claimed in claim 1, wherein: the thickening suspending agent is one or more of selectrium chloride hectorite and silica.
5. The novel safe and environment-friendly optically variable nail polish as claimed in claim 1, wherein: the photochromic material is a photochromic material containing naphthopyran organics.
6. The novel safe and environment-friendly optically variable nail polish as claimed in claim 1, wherein: the pigment is one or more of inorganic pigment, organic pigment, pearlescent mica and colorful PET bright flake.
7. The novel safe and environment-friendly optically variable nail polish as claimed in claim 1, wherein: the essence can be one of watermelon essence, rose essence, grapefruit essence, chocolate essence and strawberry essence.
8. The preparation method of the novel safe and environment-friendly optically variable nail polish is characterized by comprising the following specific steps of:
the method comprises the following steps: mixing base materials: adding butyl acetate, ethyl acetate, a film forming agent, denatured ethanol, a plasticizer and a thickening suspending agent which form the base material raw materials into a stirring barrel, starting a stirrer to stir at a high speed, ensuring that the base material raw materials are uniformly stirred to form a semi-finished product, and standing for later use after the uniformly stirred semi-finished product is discharged;
step two: mixing the base material and the color matching raw material: adding the semi-finished product prepared in the step one into a stirring barrel, sequentially adding the optically variable material, the pigment and the essence which form the color matching raw material into the stirring barrel for mixing and stirring, ensuring that the base material raw material and the color matching raw material are uniformly mixed to form a nail polish semi-finished product, ensuring that the color meets the standard requirement, and standing the nail polish semi-finished product after the uniformly mixed nail polish semi-finished product is discharged for later use;
step three: and (3) inspecting the semi-finished nail polish product: detecting the appearance, color and drying time items of the semi-finished nail polish product according to the quality requirement of the nail polish, entering the next procedure after the semi-finished nail polish product is qualified, and if the semi-finished nail polish product is unqualified, conveying the unqualified semi-finished nail polish product to a waste product centralized recycling pool for concentration;
step four: safe filling: slowly adding the qualified semi-finished nail polish product prepared in the step three into a filling machine, covering a cover on an inserted air pipe, filling the semi-finished nail polish product into a nail polish bottle through the filling machine, and packaging to form a finished nail polish product, wherein the filling operation must pay strict attention to production safety and fire safety;
step five: inspecting a nail polish finished product: installing the packaged finished nail polish products with the execution standard of nail polish QB/T2287-2011 for sampling inspection, warehousing after the finished nail polish products are qualified, and conveying the unqualified finished nail polish products to a waste centralized recovery pool for concentration if the finished nail polish products are unqualified;
step six: and after the production in the steps is finished, cleaning the stirrer, the filling machine and the filling machine table by using ethyl acetate, and airing.
9. The preparation method of the novel safe and environment-friendly optically variable nail polish as claimed in claim 8, wherein the preparation method comprises the following steps: and C, inspecting the materials consisting of the nail polish bottles selected in the step four, wherein the inspected materials consisting of the nail polish bottles do not react with the base material raw materials and the color mixing raw materials, if the inspected materials do not react, the materials are discarded, and then the inspected qualified nail polish bottles are unpacked and sterilized to be filled with the semi-finished nail polish.
CN201911163108.1A 2019-11-25 2019-11-25 Novel safe and environment-friendly optically variable nail polish Pending CN110693755A (en)

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PCT/CN2020/106188 WO2021103632A1 (en) 2019-11-25 2020-07-31 Safe and environmentally friendly iridescent nail polish

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WO2021103632A1 (en) * 2019-11-25 2021-06-03 金华市科维思日化有限公司 Safe and environmentally friendly iridescent nail polish

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