CN110403883A - A kind of long anti-ageing smoothing toner of pubescence Chinese yam and preparation method thereof - Google Patents

A kind of long anti-ageing smoothing toner of pubescence Chinese yam and preparation method thereof Download PDF

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CN110403883A
CN110403883A CN201910828179.2A CN201910828179A CN110403883A CN 110403883 A CN110403883 A CN 110403883A CN 201910828179 A CN201910828179 A CN 201910828179A CN 110403883 A CN110403883 A CN 110403883A
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extract
long
chinese yam
water
smoothing toner
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庄培民
冯中军
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Hangzhou Qiandao Lake Blue Angel Industrial Co Ltd
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Hangzhou Qiandao Lake Blue Angel Industrial Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706—Algae
    • A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74—Biological properties of particular ingredients
    • A61K2800/75—Anti-irritant

Abstract

The present invention relates to a kind of long anti-ageing smoothing toners of pubescence Chinese yam and preparation method thereof.The skin softening water component includes: glycerol, glycine betaine, carbomer, xanthan gum, butanediol, Sodium Hyaluronate, avenabeta glucosan, rice chaff extract, oat kernel extract, Apple cell culture extract, collagen, natto gum, long pubescence Chinese yam root extract, bladder-wrack extract, arginine, camellia flower extract.The smoothing toner has preferable anti-aging and whitening, moisture-keeping efficacy.

Description

A kind of long anti-ageing smoothing toner of pubescence Chinese yam and preparation method thereof
Technical field
The invention belongs to smoothing toner and its preparation field, in particular to the anti-ageing smoothing toner of a kind of long pubescence Chinese yam and its preparation Method.
Background technique
With the high speed development of China's economic, the operating pressure and life stress of people is increasing, and people are to skin care item Pursuit it is also higher and higher, it is desirable that skin care item not only moisturizing, and maintain skin elasticity goes to wrinkle, and highlights with smooth skin etc.. Such as smoothing toner is used after face cleaning, has a moisturizing, the effect of cutin-softening, be a kind of moisturizing, whitening, Firm, oil-control, Wrinkle resistant skin-protection product can be controlled cortex secretion, skin can be allowed clearly clean, be after face cleaning using smoothing toner with pore refining Skin increases nutrition, has delaying skin aging, enables the more flexible effect of skin.There are many existing skin care item type, still Using effect is bad.Such as Chinese patent CN106265330A disclose it is a kind of go anti-ageing cream of wrinkling, which includes Long pubescence Chinese yam root extract etc., the cream use the efficient combination of a variety of active ingredients, effectively increase anti-ageing effect of wrinkling Fruit, but the effect of wrinkle anti-aging, whitening are gone in the combination of these active constituents, is inadequate.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of long anti-ageing smoothing toner of pubescence Chinese yam and preparation method thereof, with The defects of overcoming the anti-ageing and whitening effect that goes to wrinkle of anti-ageing cosmetics in the prior art bad.
The present invention provides a kind of long anti-ageing smoothing toner of pubescence Chinese yam, and the skin softening water component includes: according to weight percent Glycerol 2~4%, glycine betaine 1~3%, carbomer 0.06~0.12%, xanthan gum 0.08~0.12%, butanediol 3~5%, thoroughly Bright matter acid sodium 0.08~0.12%, avenabeta glucosan 0.5~1.0%, rice chaff extract 2~3%, oat kernel extract 1.5 ~2.5%, Apple cell culture extract 0.2~0.3%, collagen 1~3%, natto gum 0.9~1.8%, long pubescence Chinese yam root extract 4~5%, bladder-wrack extract 0.5~1%, arginine 0.08~0.12%, camellia flower extract 0.5~ 0.8%, pasque flower extract 0.3~0.4%, long and thin hot pepper berry extract 0.3~0.4%, palpus extractive of usnea 0.3~ 0.4%, the water of surplus.
The skin softening water component includes: glycerol 2%, glycine betaine 1%, carbomer 0.06%, xanthan according to weight percent Glue 0.08%, butanediol 3%, Sodium Hyaluronate 0.08%, avenabeta glucosan 0.5%, rice chaff extract 2%, oat kernel mentions Take object 1.5%, Apple cell culture extract 0.2%, collagen 1%, natto gum 0.9%, long pubescence Chinese yam root extraction Object 4%, bladder-wrack extract 0.5%, arginine 0.08%, camellia flower extract 0.5%, pasque flower extract 0.3%, Long and thin hot pepper berry extract 0.3%, palpus extractive of usnea 0.3%, the water of surplus.
The skin softening water component includes: glycerol 3%, glycine betaine 2%, carbomer 0.1%, xanthan gum according to weight percent 0.1%, butanediol 4%, Sodium Hyaluronate 0.1%, avenabeta glucosan 0.8%, rice chaff extract 2%, oat kernel extract 2%, Apple cell culture extract 0.25%, collagen 1%, natto gum 1%, long pubescence Chinese yam root extract 4.5%, Bladder-wrack extract 0.8%, arginine 0.1%, camellia flower extract 0.7%, pasque flower extract 0.35%, prickly ash berries Extract 0.35%, palpus extractive of usnea 0.35%, the water of surplus.
The skin softening water component includes: glycerol 4%, glycine betaine 3%, carbomer 0.12%, xanthan according to weight percent Glue 0.12%, butanediol 5%, Sodium Hyaluronate 0.12%, avenabeta glucosan 1.0%, rice chaff extract 3%, oat kernel mentions Take object 2.5%, Apple cell culture extract 0.3%, collagen 3%, natto gum 1.8%, long pubescence Chinese yam root extraction Object 5%, bladder-wrack extract 1%, arginine 0.12%, camellia flower extract 0.8%, pasque flower extract 0.4%, the Qin Green pepper berry extract 0.4%, palpus extractive of usnea 0.4%, the water of surplus.
The present invention also provides a kind of preparation methods of long anti-ageing smoothing toner of pubescence Chinese yam, comprising the following steps:
(1) by glycerol 2~4%, glycine betaine 1~3%, carbomer 0.06~0.12%, 0.08~0.12% and of xanthan gum Water 47.92~71.7% mixes, and is preheating to 85 ° -90 °, and insulated sterilizing cools down；
(2) butanediol 3~5% is dispersed by Sodium Hyaluronate 0.08~0.12% and avenabeta glucosan 0.5~1.0% In, the dilution dissolution of water 10~20% is added；
(3) be cooled to 40-45 ° in step (1), sequentially add dissolved solution, rice chaff extract 2 in step (2)~ 3%, oat kernel extract 1.5~2.5%, Apple cell culture extract 0.2~0.3%, collagen 1~3%, Na Tuo Glue 0.9~1.8%, long pubescence Chinese yam root extract 4~5%, bladder-wrack extract 0.5~1%, arginine 0.08~ 0.12%, camellia flower extract 0.5~0.8%, pasque flower extract 0.3~0.4%, long and thin hot pepper berry extract 0.3~ 0.4%, palpus extractive of usnea 0.3~0.4%, discharges after stirring；
Material content is weight percentage in step (1)-(3).
Soaking time is 20~40min in the step (1).
Mixing time is 15~25min in the step (3).
Beneficial effect
The present invention extracts long pubescence Chinese yam (DIOSCOREA VILLOSA) root extract, rice chaff extract, oat kernel Object, natto gum, bladder-wrack (FUCUS VESICULOSUS) extract, camellia (CAMELLIA JAPONICA) flower extract knot Altogether, have effects that anti-aging, whitening and moisturizing, and add apple (MALUS DOMESTICA) fruit cell culture Extract and oat (AVENA SATIVA) beta glucan, can increase senile-resistant efficacy.Camellia (CAMELLIA simultaneously JAPONICA) flower extract makes skin not allergy as anti-sensitizer.
Specific embodiment
Present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate the present invention Rather than it limits the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, those skilled in the art Member can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited Range.
Embodiment 1
A kind of long anti-ageing smoothing toner of pubescence Chinese yam is present embodiments provided, the skin softening water component is according to weight percent are as follows: Glycerol 2%, glycine betaine 1%, carbomer 0.06%, xanthan gum 0.08%, butanediol 3%, Sodium Hyaluronate (200,000 molecular weight) 0.08%, avenabeta glucosan 0.5%, rice chaff extract 2%, oat kernel extract 1.5%, Apple cell culture mentions Take object 0.2%, collagen 1%, natto gum 0.9%, long pubescence Chinese yam root extract 4%, bladder-wrack extract 0.5%, arginine 0.08%, camellia flower extract 0.5%, pasque flower extract 0.3%, long and thin hot pepper berry extract 0.3% must extractive of usnea 0.3%, the water of surplus.
The present embodiment also provides a kind of preparation method of long anti-ageing smoothing toner of pubescence Chinese yam, specifically:
(1) glycerol 2%, glycine betaine 1%, carbomer 0.06%, xanthan gum 0.08% and water 61.7% are put into water phase pot Mixing is preheating to 85 °, is pumped into main cooker and carries out heat preservation 20min sterilizing, cooling；
(2) butanediol 3% is dispersed by Sodium Hyaluronate (200,000 molecular weight) 0.08% and avenabeta glucosan 0.5% In, the dilution dissolution of water 20% is added；
(3) 40 ° are cooled in step (1), sequentially add dissolved solution, rice chaff extract in step (2) to main cooker 2%, oat kernel extract 1.5%, Apple cell culture extract 0.2%, collagen 1%, natto gum 0.9%, length are soft Hair Chinese yam root extract 4%, bladder-wrack extract 0.5%, arginine 0.08%, camellia flower extract 0.5%, pasque flower Extract 0.3%, long and thin hot pepper berry extract 0.3%, palpus extractive of usnea 0.3%, 30 turns/min discharge after stirring 15min；
Material content is weight percentage in step (1)-(3).
Embodiment 2
A kind of long anti-ageing smoothing toner of pubescence Chinese yam is present embodiments provided, the skin softening water component is according to weight percent are as follows: Glycerol 3%, glycine betaine 2%, carbomer 0.1%, xanthan gum 0.1%, butanediol 4%, Sodium Hyaluronate (200,000 molecular weight) 0.1%, avenabeta glucosan 0.8%, rice chaff extract 2%, oat kernel extract 2%, the extraction of Apple cell culture Object 0.25%, collagen 1%, natto gum 1%, long pubescence Chinese yam root extract 4.5%, bladder-wrack extract 0.8%, arginine 0.1%, camellia flower extract 0.7%, pasque flower extract 0.35%, long and thin hot pepper berry extract 0.35% must sunglo extraction Object 0.35%, the water of surplus.
The present embodiment also provides a kind of preparation method of long anti-ageing smoothing toner of pubescence Chinese yam, specifically:
(1) glycerol 3%, glycine betaine 2%, carbomer 0.1%, xanthan gum 0.1% and water 66.5% investment water phase pot are mixed It closes, is preheating to 90 °, heat preservation 30min sterilizing cools down；
(2) it disperses Sodium Hyaluronate (200,000 molecular weight) 0.1% and avenabeta glucosan 0.8% in butanediol 4%, The dilution dissolution of water 10% is added；
(3) 42 ° are cooled in step (1), sequentially add dissolved solution, rice chaff extract in step (2) to main cooker 2%, oat kernel extract 2%, Apple cell culture extract 0.25%, collagen 1%, natto gum 1%, long pubescence potato Chinese yam root extract 4.5%, bladder-wrack extract 0.8%, arginine 0.1%, camellia flower extract 0.7%, pasque flower mention Object 0.35%, long and thin hot pepper berry extract 0.35%, palpus extractive of usnea 0.35% are taken, is discharged after 25 turns/min stirring 20min；
Material content is weight percentage in step (1)-(3).
Embodiment 3
A kind of long anti-ageing smoothing toner of pubescence Chinese yam is present embodiments provided, the skin softening water component is according to weight percent are as follows: Glycerol 4%, glycine betaine 3%, carbomer 0.12%, xanthan gum 0.12%, butanediol 5%, Sodium Hyaluronate 0.12%, oat β- Glucan 1.0%, rice chaff extract 3%, oat kernel extract 2.5%, Apple cell culture extract 0.3%, glue Original 3%, natto gum 1.8%, long pubescence Chinese yam root extract 5%, bladder-wrack extract 1%, arginine 0.12%, camellia mentions Take object 0.8%, pasque flower extract 0.4%, long and thin hot pepper berry extract 0.4%, palpus extractive of usnea 0.4%, the water of surplus.
The present embodiment also provides a kind of preparation method of long anti-ageing smoothing toner of pubescence Chinese yam, specifically:
(1) glycerol 4%, glycine betaine 3%, carbomer 0.12%, xanthan gum 0.12% and water 57.92% are put into water phase pot Mixing, is preheating to 90 °, and heat preservation 40min sterilizing cools down；
(2) it disperses Sodium Hyaluronate 0.12% and avenabeta glucosan 1.0% in butanediol 5%, water 10% is added Dilution dissolution；
(3) 45 ° are cooled in step (1), sequentially add dissolved solution, rice chaff extract in step (2) to main cooker 3%, oat kernel extract 2.5%, Apple cell culture extract 0.3%, collagen 3%, natto gum 1.8%, length are soft Hair Chinese yam root extract 5%, bladder-wrack extract 1%, arginine 0.12%, camellia flower extract 0.8%, pasque flower mention Object 0.4%, long and thin hot pepper berry extract 0.4%, palpus extractive of usnea 0.4% are taken, is discharged after 40 turns/min stirring 25min；
Material content is weight percentage in step (1)-(3).
Comparative example 1
According to embodiment 1, skin softening water component does not add long pubescence Chinese yam root extract, and the weight percent of water is changed to 85.7%, remaining is same as Example 1.
The preparation method of smoothing toner, which is removed, does not add that long pubescence Chinese yam root extract, the weight percent of water changes in step (1) It is 65.7%, remaining is same as Example 1.
Comparative example 2
According to embodiment 1, skin softening water component does not add bladder-wrack extract, and the weight percent of water is changed to 82.2%, Yu Jun is same as Example 1.
The preparation method of smoothing toner, which is removed, does not add that bladder-wrack extract, the weight percent of water is changed in step (1) 62.2%, remaining is same as Example 1.
Comparative example 3
According to embodiment 1, skin softening water component does not add camellia flower extract, and the weight percent of water is changed to 82.2%, Yu Jun is same as Example 1.
The preparation method of smoothing toner, which is removed, does not add that camellia flower extract, the weight percent of water is changed in step (1) 62.2%, remaining is same as Example 1.
Comparative example 4
According to embodiment 1, skin softening water component does not add rice chaff extract, and the weight percent of water is changed to 83.7%, remaining It is same as Example 1.
The preparation method of smoothing toner, which is removed, does not add that rice chaff extract, the weight percent of water is changed to 63.7% in step (1), Remaining is same as Example 1.
Comparative example 5
According to embodiment 1, skin softening water component does not add oat kernel extract, and the weight percent of water is changed to 83.2%, Yu Jun is same as Example 1.
The preparation method of smoothing toner, which is removed, does not add that oat kernel extract, the weight percent of water is changed in step (1) 63.2%, remaining is same as Example 1.
Comparative example 6
According to embodiment 1, skin softening water component does not add Apple cell culture extract, and the weight percent of water changes It is 81.9%, remaining is same as Example 1.
The preparation method of smoothing toner remove do not add Apple cell culture extract, in step (1) water weight hundred Ratio is divided to be changed to 61.9%, remaining is same as Example 1.
Comparative example 7
According to embodiment 1, skin softening water component does not add natto gum, and the weight percent of water is changed to 82.6%, remaining with Embodiment 1 is identical.
The preparation method of smoothing toner, which is removed, does not add that natto gum, the weight percent of water is changed to 62.6% in step (1), remaining It is same as Example 1.
Comparative example 8
According to Chinese patent CN106265330A, this comparative example provides anti-ageing cream of wrinkling, and goes anti-ageing cream of wrinkling Each ingredient by weight percentage are as follows: methyl glucoside sesquistearate 4%, isononyl isononanoate 1.0%, cetearyl alcohol Alcohol ethylhexoate 3%, 16-18 alcohol 4.0%, ring five dimethyl silicone polymer 3%, dimethicone 2.4%, glycerol 2%, fourth Glycol 3%, Sodium Hyaluronate (200,000 molecular weight) 0.08%, carbomer 0.04%, triethanolamine 1%, EDTA 1.2%, allantois Element 0.1%, green tea 0.84%, Punica granatum L. extract 1%, golden button extract 1%, long and thin hot pepper berry extract 0.3% must sunglo extraction Object 0.3%, Radix Pulsatillae extract 0.3%, dipotassium glycyrrhizinate 0.2%, watermiscible vitamin E 1.2%, snake venom peptide 0.9%, length are soft Hair Chinese yam root extract 4%, surplus is water.
Anti-aging, whitening, moisture-keeping efficacy are carried out to cream in smoothing toner in embodiment 1-3 and comparative example 1-7, comparative example 8 Test.
1. whitening spot-removing and other effects is tested
Looking for face of 330 ages between 20-55 years old to have the female volunteers of color spot, (wherein 165 volunteers belong to Easy allergic constitution), give cream in smoothing toner in embodiment 1-3 and comparative example 1-7, comparative example 8 to 330 volunteers' tests respectively It uses (corresponding 30 people of each product), is respectively smeared once, gently after study subject every morning and evening clear water face cleaning in face Flicking is depressed into absorption, and the results are shown in Table 1 after 30 days for continuous use, other any products, wherein moisturizing are not used during test Effect is given a mark, and best result 5 divides, and minimum point 1 point, each sample is averaged.
Table 1
As shown in Table 1, the freckle removing and whitening of smoothing toner in embodiment 1-3, go to wrinkle that anti-ageing, moistening effect is all preferable.Work as skin softening Water component does not add long pubescence Chinese yam root extract, bladder-wrack extract, rice chaff extract, oat kernel extract or natto gum, It goes the effect of wrinkle to be substantially reduced, and illustrates that the addition of these substances can increase the effect of wrinkle.When smoothing toner not Long pubescence Chinese yam root extract or rice chaff extract are added, freckle removing and whitening effect is substantially reduced, and illustrates that both substances can be with Increase freckle removing and whitening effect.And camellia flower extract and natto gum also have a certain impact to the freckle removing and whitening effect of smoothing toner. Although cream and embodiment 1 contain same amount of long pubescence Chinese yam root extract in comparative example 8, its freckle removing and whitening effect, Wrinkle effect and moistening effect is gone to be not so good as the embodiment of the present invention 1.
2. senile-resistant efficacy is tested
Detect oxidation resistance, be investigate skin aging important indicator, it is anti-oxidant be cause skin aging it is main because One of element, the variation of characteristic absorption after being captured according to DPPH free radical by antioxidant deduce antioxidant to DPPH freedom The Scavenging activity of base whereby characterizes the senile-resistant efficacy of cosmetics.
In organic solvent, DPPH free radical is relatively stable, and solution shows purple, and characteristic absorption peak is in 517nm.The lonely electricity of DPPH Son is reacted with free radical scavenger, enables color take off shallowly, light absorption value becomes smaller.The variation of absorbance can reflect that radicals scavenging is imitated Fruit embodies the antioxidant activity of essence cream of the present invention by free radical scavenging activity.
Sample to be tested prepares: cream in smoothing toner and comparative example 8 is taken in 10mg embodiment 1-3 and comparative example 1-7 respectively, It is dissolved with dehydrated alcohol and is settled to 200mL.
The preparation of DPPH solution: DPPH 10mg is weighed, is dissolved with dehydrated alcohol and is settled to 200mL.
Method: 2mL sample to be tested and 2mL DPPH solution are put into the test tube of tool plug, are subsequently placed in insulating box 37 DEG C Constant temperature 1h measures the absorbance A of sample using dehydrated alcohol as blank control at 517nmi, and clearance rate is calculated as follows:
Clearance rate=[1- (Ai-Aj)/Ac] × 100%；
Wherein, Ac: 2mL dehydrated alcohol adds the absorbance of 2mL DPPH solution；
Ai: 2mL sample to be tested adds the absorbance of 2mL DPPH solution；
Aj: 2mL sample to be tested adds the absorbance of 2mL ethanol solution；
Each sample to be tested surveys three groups of Duplicate Samples, averages, as a result as shown in table 2 below.
Table 2
Sample to be tested Free radical scavenging activity
Embodiment 1 94.3%
Embodiment 2 95.8%
Embodiment 3 97.8%
Comparative example 1 61.2%
Comparative example 2 75.5%
Comparative example 3 80.6%
Comparative example 4 70.4%
Comparative example 5 69.3%
Comparative example 6 85.6%
Comparative example 7 72.1%
Comparative example 8 66.3%
As shown in Table 2, the free radical scavenging activity of smoothing toner is higher in embodiment 1-3, illustrates smoothing toner in embodiment 1-3 Senile-resistant efficacy is preferable.The free radical scavenging activity of smoothing toner is substantially reduced in comparative example 1-7, illustrates that long pubescence Chinese yam root extracts Object, bladder-wrack extract, camellia flower extract, rice chaff extract, oat kernel extract, Apple cell culture extract Object and natto gum have an impact to free radical scavenging activity.Cream free radical scavenging activity is lower in comparative example 8, illustrates that its is anti-ageing Old effect is bad.
3. storage stability test
Smoothing toner in embodiment 1-3 and comparative example 1-7, in comparative example 8 cream respectively 30 days at -15 DEG C, 5 DEG C, 30 DEG C It is without exception, in addition white fluorescent lamp 3000Lux illumination, room temperature lower 10 days, smoothing toner, comparative example in embodiment 1-3 and comparative example 1-7 Cream has preferable storage stability without discoloration in 8.

Claims (7)

1. a kind of long anti-ageing smoothing toner of pubescence Chinese yam, which is characterized in that the skin softening water component includes: sweet according to weight percent Oil 2~4%, glycine betaine 1~3%, carbomer 0.06~0.12%, xanthan gum 0.08~0.12%, butanediol 3~5% are transparent Matter acid sodium 0.08~0.12%, avenabeta glucosan 0.5~1.0%, rice chaff extract 2~3%, oat kernel extract 1.5~ 2.5%, Apple cell culture extract 0.2~0.3%, collagen 1~3%, natto gum 0.9~1.8%, long pubescence potato Chinese yam root extract 4~5%, bladder-wrack extract 0.5~1%, arginine 0.08~0.12%, camellia flower extract 0.5~ 0.8%, pasque flower extract 0.3~0.4%, long and thin hot pepper berry extract 0.3~0.4%, palpus extractive of usnea 0.3~ 0.4%, the water of surplus.
2. smoothing toner according to claim 1, which is characterized in that the skin softening water component includes: sweet according to weight percent Oil 2%, glycine betaine 1%, carbomer 0.06%, xanthan gum 0.08%, butanediol 3%, Sodium Hyaluronate 0.08%, oat β-Portugal Glycan 0.5%, rice chaff extract 2%, oat kernel extract 1.5%, Apple cell culture extract 0.2%, collagen 1%, natto gum 0.9%, long pubescence Chinese yam root extract 4%, bladder-wrack extract 0.5%, arginine 0.08%, camellia mentions Take object 0.5%, pasque flower extract 0.3%, long and thin hot pepper berry extract 0.3%, palpus extractive of usnea 0.3%, the water of surplus.
3. smoothing toner according to claim 1, which is characterized in that the skin softening water component includes: sweet according to weight percent Oil 3%, glycine betaine 2%, carbomer 0.1%, xanthan gum 0.1%, butanediol 4%, Sodium Hyaluronate 0.1%, oat β-Portugal are poly- Sugar 0.8%, rice chaff extract 2%, oat kernel extract 2%, Apple cell culture extract 0.25%, collagen 1%, Natto gum 1%, long pubescence Chinese yam root extract 4.5%, bladder-wrack extract 0.8%, arginine 0.1%, camellia flower extract 0.7%, pasque flower extract 0.35%, long and thin hot pepper berry extract 0.35%, palpus extractive of usnea 0.35%, the water of surplus.
4. smoothing toner according to claim 1, which is characterized in that the skin softening water component includes: sweet according to weight percent Oil 4%, glycine betaine 3%, carbomer 0.12%, xanthan gum 0.12%, butanediol 5%, Sodium Hyaluronate 0.12%, oat β-Portugal Glycan 1.0%, rice chaff extract 3%, oat kernel extract 2.5%, Apple cell culture extract 0.3%, collagen 3%, natto gum 1.8%, long pubescence Chinese yam root extract 5%, bladder-wrack extract 1%, arginine 0.12%, camellia extraction Object 0.8%, pasque flower extract 0.4%, long and thin hot pepper berry extract 0.4%, palpus extractive of usnea 0.4%, the water of surplus.
5. a kind of preparation method of the long anti-ageing smoothing toner of pubescence Chinese yam, comprising the following steps:
(1) by glycerol 2~4%, glycine betaine 1~3%, carbomer 0.06~0.12%, xanthan gum 0.08~0.12% and water 47.92~71.7% mixing, are preheating to 85 ° -90 °, and insulated sterilizing cools down；
(2) it disperses Sodium Hyaluronate 0.08~0.12% and avenabeta glucosan 0.5~1.0% in butanediol 3~5%, The dilution dissolution of water 10~20% is added；
(3) be cooled to 40-45 ° in step (1), sequentially add dissolved solution in step (2), rice chaff extract 2~3%, Oat kernel extract 1.5~2.5%, Apple cell culture extract 0.2~0.3%, collagen 1~3%, natto gum 0.9~1.8%, long pubescence Chinese yam root extract 4~5%, bladder-wrack extract 0.5~1%, arginine 0.08~0.12%, Camellia flower extract 0.5~0.8%, pasque flower extract 0.3~0.4%, long and thin hot pepper berry extract 0.3~0.4%, palpus pine Trailing plants extract 0.3~0.4% discharges after stirring；
Material content is weight percentage in step (1)-(3).
6. method according to claim 5, which is characterized in that soaking time is 20~40min in the step (1).
7. method according to claim 5, which is characterized in that mixing time is 15~25min in the step (3).
CN201910828179.2A 2019-09-03 2019-09-03 A kind of long anti-ageing smoothing toner of pubescence Chinese yam and preparation method thereof Pending CN110403883A (en)

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Application publication date: 20191105