CN106389195A - Blueberry moisturizing and hydrating facial mask and preparation method thereof - Google Patents

Blueberry moisturizing and hydrating facial mask and preparation method thereof Download PDF

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Publication number
CN106389195A
CN106389195A CN201610816446.0A CN201610816446A CN106389195A CN 106389195 A CN106389195 A CN 106389195A CN 201610816446 A CN201610816446 A CN 201610816446A CN 106389195 A CN106389195 A CN 106389195A
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blueberry
preparation
moisturizing
masque apaisant
apaisant hydratant
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徐青
黄筑
周元敬
贾强
聂飞
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Guizhou Institute of Biology
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Guizhou Institute of Biology
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/731Cellulose; Quaternized cellulose derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The invention relates to the field of daily cosmetics, and in particular relates to a blueberry moisturizing and hydrating facial mask and a preparation method thereof. The blueberry moisturizing and hydrating facial mask is prepared from the following raw materials: hydroxyethyl cellulose, trehalose, butanediol, hyaluronic acid, a blueberry extract, a preservative and water. The preparation method comprises the following steps: adding the hydroxyethyl cellulose into deionized water, and heating and stirring to be 58 to 65DEG C; then stirring at constant temperature until a solution is transparent, adding the trehalose and uniformly stirring; cooling a mixture to be below 40DEG C, adding the butanediol, the hyaluronic acid, the blueberry extract and the preservative, uniformly stirring, and cooling to normal temperature, thus obtaining a finished product. The facial mask disclosed by the invention has the efficacy of brightening skin tone, preserving moisture, increasing skin nutrition, improving skin elasticity and conditioning the skin, and is safe and irritation-free.

Description

A kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof
Technical field
The present invention relates to daily cosmetics field, more particularly, to a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof.
Background technology
Blueberry enjoys " one of big healthy food of the mankind five " and the good reputation of " one of big best nutritional food in the world ten ", fruit For blue berry, in addition to containing conventional sugared, sour and vitamin C, also it is rich in vitamin E, vitamin A, B family vitamin, super oxygen Thing mutase, ursin, protein, anthocyanidin, dietary fibre and various mineral matter element, its vitamin and anthocyanidin content It it is several times even tens times of general fruit, anthocyanidin is as a kind of nutritious supplementary pharmaceutical of pure natural anti-aging, studied card Bright is that mankind nowadays find maximally effective natural, is referred to as " oral cosmetics for skin ", can excite skin itself Nutrition regenerates, and becomes smooth and high resilience by the suppression of elastoser and Collagenase is made with skin, promotes skin Smoothness, strengthen the effect of cutaneous immunisation power and anti-aging, accelerate skin absorption, prevent by over-drying led to skin Skin damages.
With overtime work of staying up late, or Long-Time Service electronic product, or long-time exposure is outdoor, skin is day by day dried, and with The increase at age, skin metabolism slows down, and cutaneous immunisation power and anti-aging ability are also gradually reduced, and therefore, skin is carried out Nursing is most important.
As one of the series of skin care item, its principle is using covering in the of short duration time of face, be temporarily isolating outer to facial mask The air on boundary and pollution, promote sweat gland secretion and metabolism, and make moisture in facial mask penetrate into the cuticula of epidermis, so that skin is become Softness, even so, the function of facial mask still cannot meet people for beautiful, healthy and young pursuit.
With the mankind, the pursuit of pure natural skin care item is also gradually risen, such as the patent No. 201310521959.5《A kind of blue Certain kind of berries wine mud nourishing pack and preparation method thereof》, disclose using facial mask base fluid, pretreatment blueberry wine mud, NMF, preservative, Antioxidant, pearl powder, natural aromatic oil, vitamin E are made;The and for example patent No. 201210155179.9《One kind has The rhodiola facial mask of skin nursing effect》, disclose using rhodiola root extract, black tea extract, blueberries Extract, hydrolysis silk, 1,2- hexylene glycol, Carbomer, xanthan gum, glycerine, butanediol, Sodium Hyaluronate, propane diols, nicotinoyl Amine, triethanolamine, water are made;But facial mask still suffers from some shortcomings in the prior art, such as containing harmful change Learn material so that the easy allergy of skin, human organ and function caused damage, and for example composition proportion unreasonable so that skin not Can fully absorb, function is limited to so that the scope of application is narrow for another example.
Content of the invention
For solving above-mentioned technical problem, the invention provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof.
The present invention is achieved by the following technical programs.
A kind of blueberry moisturizing MASQUE APAISANT HYDRATANT, is made up of following percentage by weight raw material:Hydroxyethyl cellulose 0.2-0.5%, Trehalose 1-3%, butanediol 1-3%, hyaluronic acid 3-6%, blueberry extract 0.1-0.3%, preservative 0.02-0.2%, remaining Measure as deionized water.
Further, it is made up of following percentage by weight raw material:Hydroxyethyl cellulose 0.2-0.4%, trehalose 1.3- 2.8%th, butanediol 1.3-2.8%, hyaluronic acid 4-6%, blueberry extract 0.15-0.3%, preservative 0.02-0.15%, remaining Measure as deionized water.
Further, it is made up of following percentage by weight raw material:Hydroxyethyl cellulose 0.3%, trehalose 2%, fourth two Alcohol 2%, hyaluronic acid 5%, blueberry extract 0.24%, preservative 0.1%, balance of deionized water.
Present invention also offers the preparation method of blueberry moisturizing MASQUE APAISANT HYDRATANT, comprise the following steps:
1) hydroxyethyl cellulose is added to deionized water, to 58-65 DEG C, then constant temperature stirs to solution heating stirring Transparent shape, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, stirs evenly, and is cooled to normal temperature, obtains final product.
Further, described preservative is OIT (LH-1), imidazolidinyl urea (Germall115) or 1,2- penta Any one or more composition in glycol (PTD).
Further, described blueberry extract is to extract the vitamin C in blueberry, anthocyanidin and superoxide dismutase Out.
Further, described blueberry extract is to be obtained through enzymolysis, alcohol extracting.
Further, the making step of described blueberry extract is:Add its weight 0.005-0.5% in blueberries Biology enzyme, after shading standing 1-5h, adds alcoholic solution, 3-8h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry Extract.
Further, described biology enzyme be cellulase, appointing in pectase, fruit juice enzyme, compound pulp enzyme, dextranase One or more of composition.
Further, described alcoholic solution, its volumetric concentration is 40-95%.
Further, the consumption of described alcoholic solution is 2-20 times of blueberry weight.
Further, described alcoholic solution is any one in methyl alcohol, ethanol, propyl alcohol or butanol.
The present invention also provides a kind of blueberry moisturizing moisturizing using method slowly, comprises the following steps:
1), after warm water clean skin, appropriate blueberry moisturizing MASQUE APAISANT HYDRATANT is equably applied in face;
2) quiet deposited 15-20min, clear water is cleaned or cotton pads removes facial mask;
The usage cycles of the blueberry moisturizing MASQUE APAISANT HYDRATANT of the present invention are:2-3 times/week.
The beneficial effects of the present invention is:
Using the blueberry moisturizing MASQUE APAISANT HYDRATANT that proportioning and the method for the present invention are made, there is bright color, moisturizing, increasing Plus skin-nourishing, improve skin elasticity and effect of conditioning skin, and safe and non-stimulating.
The present invention, by rational proportion design, can supplement the nutrients for skin, using raw material interphase interaction, makes Obtain hyaluronic acid to act synergistically with trehalose, and then enhance reparation and the water lock ability of skin, carried by adding blueberry Take thing so that anthocyanidin occurs cooperative effect with vitamin C in the environment of common presence, improve the antioxygenic property of skin, With this understanding so that superoxide dismutase and hyaluronic acid there is synergy so that facial mask composition can effectively by Skin absorption, enhances the immunity of skin, improves the activity of skin.
The present invention combines the restriction of the technological parameter in step of preparation process so that it can form protection in skin surface Film, reaches the ability removing grease and dirt, coordinates appropriate raw material proportioning, protects the immunocompetence of epidermal cell, promotes The metabolism of superficial cell, by rational using method, further improves skin water lock ability and removes free radical Ability.
Specific embodiment
Technical scheme be described further below, but claimed scope be not limited to described.
Embodiment 1
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.3%, trehalose 2%, butanediol 2%, hyaluronic acid 5%, blueberry extract 0.24%, anti- Rotten agent 0.1%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries Middle add its weight 0.1% cellulase, shading standing 3h after, add volumetric concentration be 90% ethanol solution, blueberry with The solid-liquid ratio of ethanol solution is 1:10,5h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 65 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is OIT, stirs evenly, is cooled to normal temperature, obtains final product.
Embodiment 2
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.3%, trehalose 2%, butanediol 2%, hyaluronic acid 5%, blueberry extract 0.24%, anti- Rotten agent 0.1%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries The middle compound pulp enzyme adding its weight 0.005%, after shading standing 5h, adds the methanol solution that volumetric concentration is 80%, blue The certain kind of berries is 1 with the solid-liquid ratio of methanol solution:20,7h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 60 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is imidazolidinyl urea, stirs evenly, is cooled to normal temperature, obtains final product.
Embodiment 3
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.2%, trehalose 3%, butanediol 3%, hyaluronic acid 3%, blueberry extract 0.1%, anti- Rotten agent 0.2%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries The middle biology enzyme adding its weight 0.3%, biology enzyme is by cellulase, pectase and dextranase in mass ratio 1:1:1 composition, After shading standing 4h, add the butanol solution that volumetric concentration is 45%, blueberry is 1 with the solid-liquid ratio of butanol solution:2, shading is stirred Mix 3h, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 55 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is 1,2- pentanediol, stirs evenly, is cooled to normal temperature, obtains final product.
Embodiment 4
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.5%, trehalose 3%, butanediol 3%, hyaluronic acid 6%, blueberry extract 0.3%, anti- Rotten agent 0.2%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries The middle pectase adding its weight 0.5%, after shading standing 1h, adds the propanol solution that volumetric concentration is 85%, blueberry and third The solid-liquid ratio of alcoholic solution is 1:5,4h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 66 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is the composition of OIT, imidazolidinyl urea and 1,2- pentanediol, stirs evenly, is cooled to Normal temperature, obtains final product.
Embodiment 5
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.2%, trehalose 1%, butanediol 1%, hyaluronic acid 3%, blueberry extract 0.1%, anti- Rotten agent 0.02%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries The middle fruit juice enzyme adding its weight 0.08%, after shading standing 5h, adds butanol solution, blueberry and the fourth that volumetric concentration is 70% The solid-liquid ratio of alcoholic solution is 1:10,6h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 65 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is the composition of OIT and imidazolidinyl urea, stirs evenly, is cooled to normal temperature, obtains final product.
Embodiment 6
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.25%, trehalose 1.5%, butanediol 1.5%, hyaluronic acid 6%, blueberry extract 0.25%th, preservative 0.05%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries Middle add its weight 0.01% dextranase, shading standing 2h after, add volumetric concentration be 95% propanol solution, blueberry with The solid-liquid ratio of propanol solution is 1:15,8h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 58 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is the composition of OIT, imidazolidinyl urea and 1,2- pentanediol, stirs evenly, is cooled to Normal temperature, obtains final product.
Embodiment 7
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.4%, trehalose 1.3%, butanediol 1.3%, hyaluronic acid 5%, blueberry extract 0.15%th, preservative 0.15%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries The middle biology enzyme adding its weight 0.008%, biology enzyme is 2 by pectase, fruit juice enzyme in mass ratio:1 composition, shading stands 4h Afterwards, add the ethanol solution that volumetric concentration is 60%, blueberry is 1 with the solid-liquid ratio of ethanol solution:2,7h is stirred in shading, passes through Filter, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 63 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is the composition of OIT and 1,2- pentanediol, stirs evenly, is cooled to normal temperature, obtains final product.
Embodiment 8
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.3%, trehalose 2.8%, butanediol 2.8%, hyaluronic acid 4%, blueberry extract 0.15%th, preservative 0.12%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries The middle biology enzyme adding its weight 0.008%, biology enzyme by the cellulase of equivalent, pectase, fruit juice enzyme, compound pulp enzyme, Dextranase forms, and after shading standing 4h, adds the solid-liquid ratio of the ethanol solution that volumetric concentration is 50%, blueberry and ethanol solution For 1:5,3h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 60 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is OIT, stirs evenly, is cooled to normal temperature, obtains final product.
Embodiment 9
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.18%, trehalose 0.9%, butanediol 0.9%, hyaluronic acid 2.95%, blueberry extract 0.06%th, preservative 0.01%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries The middle biology enzyme adding its weight 0.05, biology enzyme is 1 by fruit juice enzyme, compound pulp enzyme in mass ratio:3 compositions, shading stands After 3h, add the methanol solution that volumetric concentration is 80%, blueberry is 1 with the solid-liquid ratio of methanol solution:10,5h, warp are stirred in shading Filter, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 55 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is the composition of imidazolidinyl urea and 1,2- pentanediol, stirs evenly, is cooled to normal temperature, obtains final product.
Embodiment 10
The present embodiment provides a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT and preparation method thereof, comprises the following steps:
1st, raw material prepares:
Hydroxyethyl cellulose 0.6%, trehalose 4%, butanediol 4%, hyaluronic acid 7%, blueberry extract 0.5%, anti- Rotten agent 0.3%, balance of deionized water;
2nd, the extraction of blueberry:
Adopt and with the following method the vitamin C in blueberry, anthocyanidin and superoxide dismutase are extracted:To blueberries The middle biology enzyme adding its weight 0.2%, biology enzyme is by the cellulase of equivalent, pectase, compound pulp enzyme and dextranase Composition, after shading standing 5h, adds the butanol solution that volumetric concentration is 40%, blueberry is 1 with the solid-liquid ratio of butanol solution:15, 8h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract;
3rd, making face mask:
1) hydroxyethyl cellulose is added to deionized water, to 68 DEG C, then constant temperature stirs and to solution is in heating stirring Transparence, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, add butanediol, hyaluronic acid, blueberry extract and anti-corrosion Agent, preservative used by the present embodiment is 1,2- pentanediol, stirs evenly, is cooled to normal temperature, obtains final product.
Test example 1
Given the test agent title:Blueberry moisturizing MASQUE APAISANT HYDRATANT;
Test purpose:Detection sample effect and the possibility causing human body skin bad reaction;
Method of testing:Select 60 skin of face health, clean, no acne women, be divided into 5 groups, every group gives respectively The blueberry moisturizing MASQUE APAISANT HYDRATANT of embodiment 1,6,10 preparation, after daily warm water clean skin, takes blueberry moisturizing MASQUE APAISANT HYDRATANT 12mL uniform Be applied in facial (avoiding eyes and face), quiet deposited 15min, clear water is cleaned, and continuous examination applies 1 month, observes facial bad feelings Condition, result is as shown in table 1:
Table 1:

Claims (10)

1. a kind of blueberry moisturizing MASQUE APAISANT HYDRATANT is it is characterised in that be made up of following percentage by weight raw material:Hydroxyethyl cellulose 0.2-0.5%, trehalose 1-3%, butanediol 1-3%, hyaluronic acid 3-6%, blueberry extract 0.1-0.3%, preservative 0.02-0.2%, balance of deionized water.
2. blueberry moisturizing MASQUE APAISANT HYDRATANT as claimed in claim 1 is it is characterised in that be made up of following percentage by weight raw material: Hydroxyethyl cellulose 0.2-0.4%, trehalose 1.3-2.8%, butanediol 1.3-2.8%, hyaluronic acid 4-6%, blueberry extract Thing 0.15-0.3%, preservative 0.02-0.15%, balance of deionized water.
3. blueberry moisturizing MASQUE APAISANT HYDRATANT as claimed in claim 1 or 2 is it is characterised in that by following percentage by weight raw material group Become:Hydroxyethyl cellulose 0.3%, trehalose 2%, butanediol 2%, hyaluronic acid 5%, blueberry extract 0.24%, preservative 0.1%, balance of deionized water.
4. a kind of preparation method of the blueberry moisturizing MASQUE APAISANT HYDRATANT as described in any one as claim 1-3 is it is characterised in that include Following steps:
1) hydroxyethyl cellulose is added to deionized water, to 58-65 DEG C, then constant temperature stirs to solution is in thoroughly to heating stirring Bright shape, adds trehalose and stirs evenly;
2) by step 1) gains are cooled to less than 40 DEG C, and add butanediol, hyaluronic acid, blueberry extract and preservative, stir Even, it is cooled to normal temperature, obtain final product.
5. the preparation method of blueberry moisturizing MASQUE APAISANT HYDRATANT as claimed in claim 4 is it is characterised in that described preservative is different thiophene Any one or more composition in oxazoline ketone (LH-1), imidazolidinyl urea (Germall115) or 1,2- pentanediol (PTD).
6. the preparation method of blueberry moisturizing MASQUE APAISANT HYDRATANT as claimed in claim 4 is it is characterised in that described blueberry extract is It is obtained through enzymolysis, alcohol extracting.
7. the preparation method of blueberry moisturizing MASQUE APAISANT HYDRATANT as claimed in claim 6 is it is characterised in that described blueberry extract Making step is:Add the biology enzyme of its weight 0.005-0.5% in blueberries, after shading standing 1-5h, add alcoholic solution, 3-8h is stirred in shading, through filtering, filtrate decompression is reclaimed, obtains final product blueberry extract.
8. the preparation method of blueberry moisturizing MASQUE APAISANT HYDRATANT as claimed in claim 7 is it is characterised in that described biology enzyme is fiber The composition of any one or more in plain enzyme, pectase, fruit juice enzyme, compound pulp enzyme, dextranase.
9. the preparation method of blueberry moisturizing MASQUE APAISANT HYDRATANT as claimed in claim 7 is it is characterised in that described alcoholic solution, its body Long-pending concentration is 40-95%.
10. the preparation method of blueberry moisturizing MASQUE APAISANT HYDRATANT as claimed in claim 7 is it is characterised in that the use of described alcoholic solution Measure 2-20 times for blueberry weight.
CN201610816446.0A 2016-09-12 2016-09-12 Blueberry moisturizing and hydrating facial mask and preparation method thereof Pending CN106389195A (en)

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CN107456423A (en) * 2017-07-04 2017-12-12 贵州省生物研究所 A kind of blueberry freckle-removing beauty cream and preparation method thereof
CN107485587A (en) * 2017-07-04 2017-12-19 贵州省生物研究所 A kind of crease-resistant beauty treatment honey of blueberry and preparation method thereof
CN108261379A (en) * 2018-04-26 2018-07-10 张建华 A kind of facial mask and preparation method thereof
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CN111053704A (en) * 2018-10-17 2020-04-24 东莞市维康医疗投资有限公司 Earthworm protein and anthocyanin repair beauty mask and preparation method thereof
CN109394641A (en) * 2018-11-13 2019-03-01 贵州省生物研究所 A kind of rose blueberry cosmetics and the preparation method and application thereof

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