CN111297737A - A Chinese medicinal facial mask containing Sargassum extract for promoting blood circulation and resisting aging, and its preparation method - Google Patents
A Chinese medicinal facial mask containing Sargassum extract for promoting blood circulation and resisting aging, and its preparation method Download PDFInfo
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- CN111297737A CN111297737A CN202010347718.3A CN202010347718A CN111297737A CN 111297737 A CN111297737 A CN 111297737A CN 202010347718 A CN202010347718 A CN 202010347718A CN 111297737 A CN111297737 A CN 111297737A
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Abstract
The invention discloses a blood-activating and anti-aging traditional Chinese medicine mask containing seaweed extracts, which comprises 60-85% of lily water, 3-10% of glycerol, 3-10% of seaweed extracts, 5-15% of efficacy traditional Chinese medicine extracts, 0.1-2% of micromolecule sodium hyaluronate, 0.1-3% of cold-extracted snake oil, 0.05-2% of xanthan gum, 0.5-2% of 1, 2-hexanediol and 0.1-1% of p-hydroxyacetophenone, wherein the efficacy traditional Chinese medicine extracts comprise extracts of dendrobium huoshanense, caulis spatholobi, leonurus, salvia miltiorrhiza, ganoderma lucidum, wild chrysanthemum, radix puerariae, honeysuckle, folium mori, cortex albiziae, folium artemisiae argyi and rhizoma smilacis glabrae. According to the invention, the active ingredient natural seaweed extract is obtained by adopting algae with wide resources in deep sea through an enzymolysis method, the principle of local material taking is fully utilized, the genuine Chinese medicinal materials in Dabie mountain areas of Anhui are selected, the seaweed extract with high moisture retention and rich nutrition is combined with the Chinese medicinal material extracts for promoting blood circulation, resisting aging, whitening, resisting inflammation and the like, so that the traditional Chinese medicine mask with the effects of obvious moisture retention, resisting aging, brightening skin, nature, safety, no toxic or side effect and the like is prepared.
Description
Technical Field
The invention relates to the technical field of traditional Chinese medicine cosmetics, in particular to a traditional Chinese medicine mask containing seaweed extract for promoting blood circulation and resisting aging and a preparation method thereof.
Background
With the increasing environmental pollution and the increasing working pressure of people, the skin problems which become more serious are widely existed. Meanwhile, with the continuous improvement of modern living standard, more consumers pay attention to skin care, and especially natural skin care cosmetics are favored. Chinese herbal medicine resources are rich, the theory of traditional Chinese medicine is profound and has a long history, and the application of the Chinese herbal medicine extract to skin care products by virtue of natural characteristics becomes a hotspot of research of people at present.
The wild medicinal animal and plant species and the cultured and cultivated species in the Dabie mountain area of Anhui province are rich, and the application and popularization of the Dabie mountain Chinese medicinal materials are facilitated by selecting the medicinal materials with the functions of promoting blood circulation, removing blood stasis and resisting aging in the Dabie mountain area to the cosmetic series. The action mechanism of the blood-activating Chinese medicinal material extract is to increase the metabolism of skin in a blood-activating and stasis-removing way, discharge precipitated melanin and aged cutin out of body, maintain beauty and keep young and brighten skin color.
In the beauty skin care products, the facial mask belongs to a skin care mode for rapidly supplying moisture and nutrient substances to skin. However, the traditional Chinese medicine facial mask in the market is mixed with fish, some facial mask liquids contain excessive essence, chemical preservatives, bactericides and the like, and the problems of irritation, allergy, ineffectiveness, toxic and side effects, disease induction and the like are caused, so that the design of the natural, effective, safe and non-irritant traditional Chinese medicine facial mask has important practical value.
Disclosure of Invention
In order to solve the problems, the invention provides a blood-activating and anti-aging traditional Chinese medicine mask containing seaweed extracts and a preparation method thereof, and designs a safe and effective blood-activating and anti-aging traditional Chinese medicine mask.
The invention provides a blood-activating and anti-aging traditional Chinese medicine mask containing seaweed extract, which comprises the following components, by percentage, 60-85% of lily water, 3-10% of glycerol, 3-10% of seaweed extract, 5-15% of efficacy type traditional Chinese medicine extract, 0.1-2% of micromolecule sodium hyaluronate, 0.1-3% of cold-extracted snake oil, 0.05-2% of xanthan gum, 0.5-2% of 1, 2-hexanediol and 0.1-1% of p-hydroxyacetophenone.
The preparation method of the traditional Chinese medicine mask for promoting blood circulation and resisting aging comprises the following steps: dispersing xanthan gum into glycerol according to the formula amount, uniformly stirring, sequentially adding lily flower water, seaweed extract, micromolecular sodium hyaluronate and cold-extracted snake oil, heating to 80 ℃, fully dissolving, cooling to 50 ℃, adding functional traditional Chinese medicine extract, 1, 2-hexanediol and p-hydroxyacetophenone, uniformly stirring, filtering with 400 meshes, discharging, completely immersing a mask cloth into the mask liquid, and forming to obtain the traditional Chinese medicine mask for activating blood circulation and resisting aging.
An extraction process of a seaweed extract comprises the steps of cleaning 200g of seaweed with clear water to remove impurities, drying in a constant-temperature oven at 45 ℃ for 12h, crushing with a crusher, sieving with a 100-mesh sieve, adding 3L of distilled water, adjusting the pH to =5.0, adding cellulase with the dosage of 2%, carrying out enzymolysis at constant temperature for 3h, inactivating enzyme at 90 ℃ for 10min, centrifuging in a centrifuge at the rotating speed of 3000r/min for 10min, extracting supernatant, adding activated carbon for decolorization, filtering, carrying out rotary evaporation concentration at 50 ℃, and carrying out freeze drying to obtain the seaweed extract.
Wherein the seaweed comprises one or more of Zostera Marinae, red algae, Spirulina, Chlorella, Macrocystis, Chlorella, Brown algae, blue algae, Fucus vesiculosus, Corallium japonicum Kishinouye, Chlorella, and Nemacystus Decipiens.
The functional traditional Chinese medicine extract is prepared from the following traditional Chinese medicine raw materials in parts by weight: the functional traditional Chinese medicine extract is prepared from the following traditional Chinese medicine raw materials in parts by weight: 5-20 parts of dendrobium huoshanense, 5-18 parts of caulis spatholobi, 5-15 parts of motherwort, 5-13 parts of salvia miltiorrhiza, 5-10 parts of lucid ganoderma, 5-10 parts of wild chrysanthemum, 5-10 parts of kudzu root, 2-8 parts of honeysuckle, 1-8 parts of mulberry leaf, 1-6 parts of cortex albiziae, 1-6 parts of folium artemisiae argyi and 1-5 parts of rhizoma smilacis glabrae.
The invention also introduces a preparation process of the functional traditional Chinese medicine extract, which comprises the following steps: quickly washing the traditional Chinese medicine raw materials in parts by weight for 3 times, removing floating impurities and sinking residues, drying, carrying out superfine grinding, sieving to obtain mixed medicinal powder, adding distilled water, decocting and extracting at 85 ℃ for 3 times, combining the extracting solutions for 3 times, concentrating under reduced pressure, and standing to room temperature to obtain the functional traditional Chinese medicine extract.
The functional traditional Chinese medicine extract comprises:
1. the Chinese medicinal materials with the effects of activating blood circulation and resisting oxidation: the action mechanisms of the dendrobium huoshanense, the caulis spatholobi and the motherwort are to increase the metabolism of skin in a blood circulation promoting and stasis removing mode, improve the blood circulation of a human body, discharge precipitated melanin and aged cutin out of the body and fundamentally solve the skin problem.
2. The Chinese medicinal materials with the functions of resisting senility and whitening: the anti-aging traditional Chinese medicinal materials mainly comprise traditional Chinese medicinal flavonoid and polysaccharide compounds, have the effects of resisting oxidation, removing free radicals, inhibiting bacteria and the like, and the whitening traditional Chinese medicinal components mainly have the activity of inhibiting tyrosinase.
3. The traditional Chinese medicinal materials with anti-inflammatory effects: honeysuckle and mulberry leaves, the traditional Chinese medicine extract has the functions of resisting fungi and bacteria, the microorganisms causing putrefaction are various at present, and the commonly used preservatives comprise nipagin, isothiazolinone, adamantane chloride, imidazolidinyl urea, benzoic acid and derivatives thereof, alcohols and derivatives thereof and the like.
4. The traditional Chinese medicinal materials with the anti-allergic effect: the effective components of the cortex albiziae, the folium artemisiae argyi and the folium artemisiae argyi are not only release retardants of allergic mediators but also antagonists of the allergic mediators, and the cortex albiziae extract is a very efficient histamine inhibitor and has an antiallergic effect.
5. The Chinese medicinal materials with the skin firming effect: poria cocos, which can reduce the diameter and volume of collagen encapsulated by fibroblasts, has a shrinking effect, and thus the extract of Poria cocos can be used in skin-tightening cosmetics.
6. The traditional Chinese medicinal materials with moisturizing effect: extracts of flos Lilii Viriduli and Sargassum. The lily is rich in protein, sugar, phosphorus, iron and various trace elements, and has high medical value. The macromolecular seaweed extract contains various nutrient substances such as seaweed gel, vitamins, amino acids and the like, has good moisturizing and film-forming properties, forms a layer of natural protective film on the surface of skin, and has the effects of protecting and providing moisturizing, nourishing and conditioning.
Compared with the prior art, the invention has the beneficial effects that:
1. the components of the mask liquid are matched by applying the medication principle of 'syndrome differentiation and treatment, assistant and guide' in traditional Chinese medicine, so that the components can exert respective action advantages and have synergistic effect, and the safe and effective blood-activating anti-aging traditional Chinese medicine mask is obtained;
2. according to the invention, the active ingredient natural seaweed extract is obtained by adopting algae with wide resources in deep sea through an enzymolysis method, the principle of local material taking is fully utilized, and genuine Chinese medicinal materials in Dabie mountain areas of Anhui are selected, so that the seaweed extract with high moisture retention and rich nutrition and the Chinese medicinal material extracts for promoting blood circulation, resisting aging, whitening, resisting inflammation and the like are combined for use, and the synergistic effect is achieved, and the traditional Chinese medicine mask with the effects of obvious moisture retention, resisting aging, skin color brightening, nature, safety, no toxic or side effect and the like is prepared.
Drawings
FIG. 1 is a flow diagram of a manufacturing process of the present invention;
FIG. 2 is a graph of the change in moisture content of the skin of a test subject over time during a course of treatment according to the present invention;
figure 3 is a graph of the change in skin elasticity of a test subject over time during a course of treatment according to the present invention.
Detailed Description
Example 1
The formula design of the mask liquid comprises: 60-85% of lily water, 3-10% of glycerol, 3-10% of seaweed extract, 5-15% of efficacy type traditional Chinese medicine extract, 0.1-2% of small molecular sodium hyaluronate, 0.1-3% of cold-extracted snake oil, 0.05-2% of xanthan gum, 0.5-2% of 1, 2-hexanediol and 0.1-1% of p-hydroxyacetophenone.
The extraction process of the seaweed extract comprises the following steps: cleaning 200g of seaweed with clear water to remove impurities, drying in a constant-temperature oven at 45 ℃ for about 12h, crushing by a crusher, sieving by a 100-mesh sieve, adding 3L of distilled water, wherein the dosage of the cellulase is 2%, adjusting the pH to =5.0, adding the cellulase, performing constant-temperature enzymolysis for 3h, inactivating the enzyme at 90 ℃ for 10min, centrifuging (3000r/min, 10min), extracting supernatant, adding activated carbon for decoloring, filtering, performing rotary evaporation and concentration at 50 ℃ to a certain volume, and performing freeze drying to obtain a seaweed extract, wherein the seaweed comprises one or a combination of more of zostera marina, rhodophyta, spirulina, chlorella, kelp, green algae, brown algae, blue algae, fucus, coral algae, chlorella and nemacystus.
The functional traditional Chinese medicine extract is prepared from the following traditional Chinese medicines in parts by weight: 20 parts of dendrobium huoshanense, 18 parts of caulis spatholobi, 15 parts of motherwort, 13 parts of salvia miltiorrhiza, 10 parts of lucid ganoderma, 10 parts of wild chrysanthemum flower, 10 parts of kudzu root, 8 parts of honeysuckle, 8 parts of mulberry leaf, 6 parts of cortex albiziae, 6 parts of folium artemisiae argyi and 5 parts of rhizoma smilacis glabrae, the raw materials are quickly washed for 3 times, floating impurities and sinking residues are removed, drying and superfine grinding are carried out, mixed medicinal powder is obtained through sieving, distilled water is added, decocting extraction is carried out for 3 times at 85 ℃, all extracting solutions are combined, concentration is carried out under reduced pressure, and the mixture is placed to room temperature, so that the.
The mask making process comprises the following steps: dispersing xanthan gum in glycerol according to the formula amount, uniformly stirring, sequentially adding lily flower water, a seaweed extract, micromolecular sodium hyaluronate and cold-extracted snake oil, heating to 80 ℃, fully dissolving, cooling to 50 ℃, adding an efficacy type traditional Chinese medicine extract a, 1, 2-hexanediol and p-hydroxyacetophenone, uniformly stirring, filtering with a 400-mesh sieve, discharging, completely immersing a mask cloth in mask liquid, and forming to obtain the traditional Chinese medicine mask 1.
Example 2
Example 2 differs from example 1 in that: the functional traditional Chinese medicine extract is prepared from the following raw material medicines in parts by weight: 5 parts of dendrobium huoshanense, 5 parts of caulis spatholobi, 5 parts of motherwort, 13 parts of salvia miltiorrhiza, 10 parts of lucid ganoderma, 10 parts of wild chrysanthemum flower, 10 parts of kudzu root, 8 parts of honeysuckle, 8 parts of mulberry leaf, 6 parts of cortex albiziae, 6 parts of folium artemisiae argyi and 5 parts of rhizoma smilacis glabrae, the raw materials are quickly washed for 3 times, floating impurities and sinking residues are removed, drying and superfine grinding are carried out, mixed medicinal powder is obtained through sieving, distilled water is added, the decoction is carried out for 3 times at 85 ℃, all extracting solutions are combined, the pressure reduction concentration is carried out, the mixture is placed to the room temperature, the functional traditional Chinese medicine extract b is obtained, and the functional traditional Chinese.
Example 3
Example 3 differs from example 1 in that: the functional traditional Chinese medicine extract is prepared from the following traditional Chinese medicines, by weight, 20 parts of dendrobium huoshanense, 18 parts of caulis polygoni multiflori, 15 parts of leonurus, 5 parts of salvia miltiorrhiza, 5 parts of lucid ganoderma, 5 parts of wild chrysanthemum, 5 parts of kudzuvine root, 5 parts of honeysuckle, 4 parts of mulberry leaf, 6 parts of cortex albiziae, 6 parts of folium artemisiae argyi and 5 parts of rhizoma smilacis glabrae, the raw materials are quickly washed for 3 times, floating impurities and sinking residues are removed, the raw materials are dried, superfine crushed and sieved to obtain mixed medicinal powder, distilled water is added, the mixed medicinal powder is decocted and extracted for 3 times at 85 ℃, all extracting solutions are combined, the pressure reduction concentration is carried out, the mixed medicinal powder is placed to room temperature, the functional.
Example 4
Example 4 differs from example 1 in that: the formula adopts the functional traditional Chinese medicine extract a, but the seaweed extract is removed, and other raw materials are unchanged, and the traditional Chinese medicine mask 4 is prepared according to the mask preparation process of the embodiment 1.
Example 5
Example 5 differs from example 1 in that: the functional traditional Chinese medicine extract is removed from the formula, and other raw materials are unchanged, so that the traditional Chinese medicine mask 5 is prepared according to the mask preparation process of the embodiment 1.
Example 6
Example 6 differs from example 1 in that: the functional traditional Chinese medicine extract is prepared from the following traditional Chinese medicines, by weight, 20 parts of dendrobium huoshanense, 18 parts of caulis polygoni multiflori, 15 parts of leonurus, 13 parts of salvia miltiorrhiza, 10 parts of lucid ganoderma, 10 parts of wild chrysanthemum flower, 10 parts of kudzuvine root, 2 parts of honeysuckle flower, 1 part of mulberry leaf, 1 part of cortex albiziae, 1 part of folium artemisiae argyi and 1 part of glabrous greenbrier rhizome, the raw materials are quickly washed for 3 times, floating impurities and sinking residues are removed, the raw materials are dried, superfine crushed and sieved to obtain mixed medicinal powder, distilled water is added, the mixed medicinal powder is decocted and extracted for 3 times at 85 ℃, all extracting solutions are combined, the pressure reduction concentration is carried out, the mixed medicinal powder is placed to room temperature.
The following performance tests were performed on examples 1-6:
1. determination method of tyrosinase inhibition:
accurately sucking 0.5mL of traditional Chinese medicine mask liquid sample, 2.0mL of phosphate buffer solution with pH =6.81, 0.5mL of L-tyrosine solution (weight concentration of 0.8 mg/mL) and Folin reagent to start reaction, continuously reacting for 20min in a constant-temperature water bath at 37 ℃, and measuring absorbance at 520 nm.
Calculated according to the following formula: tyrosinase inhibition rate P (%)
（1）
In the formula, A1-represents the absorbance measured by a sample mixed solution only added with tyrosinase and without added with mask liquid;
a01-represents the absorbance measured for a blank control without addition of facial mask fluid and enzyme;
a2-represents the absorbance measured by the mixture of facial mask solution and enzyme;
a3-represents the absorbance measured for the sample mixture with the addition of facial mask solution only and no enzyme.
2、•O2Determination of the radical clearance:
adding 2mL of Tris-HCl buffer solution with pH =8.3 into a stoppered test tube, standing in a water bath at about 25 ℃ for 15min, then adding 1mL of facial mask solution and 0.1mL of 3mmol/L pyrogallol solution (10mmol/L HC1 solution is used as a solvent), shaking up, placing in a water bath at about 25 ℃ for reaction for 4min, and selecting the wavelength of 360nm to determine the absorbance A4; replacing pyrogallol solution with 0.1mL HC1 solution, and measuring absorbance A5; the mask solution was replaced with 1mL of distilled water and the absorbance A02 was measured. The inhibition rate Q (%) was calculated according to formula (4).
O2 radical clearance Q (%) =
（2）
3. Method for determining the radical clearance:
adding 2mL of facial mask solution and 2mL of DPPH and ethanol solution (concentration is 0.2 mmol/L) into the same test tube with a plug, shaking up, standing in the dark for 40min, and measuring the absorbance A6 of the mixed solution at 520nm by using an ultraviolet-visible spectrophotometer; measuring the absorbance A03 of 2mL of pure water mixed with 2mL of DPPH/ethanol solution (concentration is 0.2 mmol/L); the absorbance a7 after mixing 2mL of the mask solution with 2mL of absolute ethanol was taken, and dpph. radical clearance R (%) was calculated according to formula (2).
DPPH radical clearance R (%) =
（3）
4. Method for determination of OH radical clearance:
2mL each of salicylic acid-ethanol solution (5mmol/L), FeSO4 solution (5mmol/L), and facial mask solution were added to the same stoppered tube, followed by 2mL of H2O2Shaking the solution (5mmol/L), placing in water bath at 37 deg.C for reaction for 40min, and selecting wavelength of 512nm to determine absorbance A8; 2mL of distilled water was used instead of H2O2Measuring the absorbance A9 of the solution; the mask solution was replaced with 2mL of distilled water and the absorbance A04 was measured. The inhibition rate S (%) was calculated according to formula (3).
OH radical clearance S (%) =
（4）
Determining the inhibition rate of the traditional Chinese medicine facial mask 1-5 on tyrosinase and the inhibition rate on O according to the 4 methods2The results of the removal rates of OH free radicals are shown in table 1, and the results show that the formula of the facial mask 1 has the best efficacy and the best antioxidant and anti-aging effects; the results of the mask 2 show that the blood-activating medicinal materials such as dendrobium huoshanense, sargentgloryvine stem, motherwort herb and the like have good antioxidant activity on superoxide radical and hydroxyl radical; the result of the mask 3 shows that the salvia miltiorrhiza, the lucid ganoderma, the wild chrysanthemum and the kudzuvine root have better effects on the inhibition of tyrosinase and the elimination of three free radicals; the results of the mask 4 show that the seaweed extract has the effect of resisting the bacteria in the formulaOxidation, and the traditional Chinese medicine extract is compatible to play a synergistic effect; the result of the mask 5 shows that the traditional Chinese medicine extract is the main functional raw material in the formula and is indispensable.
Table 1 inhibition ratio P (%) of tyrosinase,. O of five formula masks2Radical inhibition rate Q (%), seedingoh radical inhibition rate R (%), dpph
And (3) testing antibacterial performance: and selecting the mask 1 and the mask 6 with the optimal formula according to the verification to perform an antibacterial property detection test, and dividing 10 brown glass bottles into two groups of 5 bottles, wherein one group is the mask 1, the other group is the mask 6, and each glass bottle is used for containing one mask. The method comprises the steps of opening a bottle cap, placing the bottle cap in a room with the environment of 35 ℃ and the relative humidity of 85% and containing various mixed bacteria, continuously observing and testing, recording the occurrence time of mildew stains, taking two groups of average values, and obtaining test results shown in table 2.
TABLE 2 mildew appearance time of mask 1 and mask 6
| Face pack 1 | Face pack 6 | |
| Mildew spot appearing time (sky) | 70 | 52 |
Method for stability testing:
1. and (3) performing heat resistance test, namely adjusting the constant-temperature incubator to 50 +/-1 ℃, placing 1-6 parts of the facial mask in the constant-temperature incubator for 24 hours, taking out, recovering the room temperature, and observing whether phenomena such as thinning, discoloration, layering, hardness change and the like exist, wherein the method is repeated for 3 times with the same facial mask to judge the heat resistance of the product, and the specific results are shown in table 3.
2. And (3) cold resistance testing, namely adjusting the refrigerator to minus 20 +/-1 ℃, placing 1-6 parts of the facial mask in the refrigerator for 24 hours, taking out, recovering the room temperature, and observing whether the phenomena of thinning, discoloration, layering, hardness change and the like exist, wherein the method is repeated for 3 times with the same facial mask to judge the cold resistance of the product, and the specific result is shown in table 3.
As can be seen from Table 3, the facial masks 1-4 had good stability; the mask 5 and the mask 6 lack all traditional Chinese medicine extracts and the antibacterial traditional Chinese medicinal materials are reduced, so that the oxidation resistance, the color and the antibacterial rate are changed, and the stability is reduced.
TABLE 3 changes of color, viscosity, antibacterial rate and antioxidant property of facial masks 1-6 after heat and cold resistance test
| Face pack 1 | Face pack 2 | Face pack 3 | Face pack 4 | |
Face pack 6 | |
| Color and luster | Is not changed | Is not changed | Is not changed | Is not changed | Slight yellowing | Is not changed |
| Viscosity of the oil | Is not changed | Is not changed | Is not changed | Is not changed | Is not changed | Slight thinning |
| Rate of inhibition of bacteria | Is not changed | Is not changed | Is not changed | Is not changed | Is not changed | Slightly lower |
| Oxidation resistance | Is not changed | Is not changed | Is not changed | Is not changed | Slightly lower | Is not changed |
Randomly extracting 300 tested persons, namely mixed skin aged 30-50 years, and allowing the tested persons to continuously try the mask for 1 month, applying the mixed skin for 1 time every night, testing the changes of moisture, elasticity, collagen fibers and pigment content in the skin of the tested persons before and after use, investigating whether allergy exists or not and whether irritation exists, testing the skin elasticity change of the tested persons after the tested persons use for 1 month by adopting a skin elasticity tester MPA580 of German CK company, and specifically, as shown in a table 4, the result shows that the moisturizing, anti-aging and whitening effects of the mask 1 are the best; the result of the mask 2 shows that the blood-activating medicinal materials such as dendrobium huoshanense, sargentgloryvine stem, motherwort herb and the like can increase the metabolism of skin, discharge precipitated melanin and aged cutin out of the body, brighten the skin color and ensure that the beautifying effect is durable and stable; the results of the mask 3 show that the salvia miltiorrhiza, the lucid ganoderma, the wild chrysanthemum and the kudzuvine root have better effects on moisture preservation, oxidation resistance and wrinkle removal; the result of the mask 4 shows that the macromolecular seaweed extract has a relatively good moisturizing effect in the formula, forms a layer of natural protective film on the surface of the skin, has the effects of moisturizing, nourishing and conditioning, and has a synergistic effect on the effects of the traditional Chinese medicine extract on the premise of resisting aging and whitening; the result of the facial mask 5 shows that the traditional Chinese medicine extract is the main functional raw material in the formula, and the characteristics of moisture retention, aging resistance, oxidation resistance and the like of the facial mask are greatly reduced after the traditional Chinese medicine extract is lacked; the results of the facial mask 6 show that the honeysuckle, the mulberry leaves, the silktree albizzia bark, the Chinese mugwort leaves and the glabrous greenbrier rhizome have the effects of bacteriostasis and anti-allergy, and the facial mask has a certain sensitization rate after the weight is greatly reduced.
TABLE 4 moisture increment, elasticity increment, collagen fiber increment, pigment decrement, allergic condition, and irritant condition of subjects who used masks 1-6
| Water content increase amount | Increase in elasticity | Collagen fiber increment | Pigment reduction amount | Allergic conditions | Irritative conditions | |
| Face pack 1 | 26.5% | 17.8% | 16.3% | 13.3% | Is free of | Is free of |
| Face pack 2 | 25.8% | 13.7% | 12.8% | 10.1% | Is free of | Is free of |
| Face pack 3 | 26.3% | 12.6% | 11.5% | 9.2% | Is free of | Is free of |
| Face pack 4 | 15.6% | 11.5% | 10.3% | 8.7% | Is free of | Is free of |
| |
17.4% | 7.2% | 5.8% | 4.9% | Is free of | Is free of |
| Face pack 6 | 24.5% | 12.1% | 11.2% | 8.9% | Minor amount of allergy | Is free of |
Determining the mask treatment course: by combining the test results in tables 1,2, 3 and 4, selecting the mask 1 as a traditional Chinese medicine mask with an optimal formula, testing the determination of the treatment course of the mask 1, randomly extracting 100 tested persons, and testing the skin of the tested persons with the age of 30-50 years for 42 days, applying 1 time every night, testing the moisture and elasticity of the skin of the tested persons for 0 day, 7 days, 14 days, 28 days, 35 days and 42 days, and determining the result as shown in fig. 2 and 3, wherein the result shows that the moisture content and the elasticity are obviously increased after 1 week of use, the effects of moisturizing and anti-aging are gradually increased after 2 weeks, and the effect reaches the optimal value until 4-5 weeks, so that the treatment course of the mask 1 is determined to be 4-5 weeks.
Claims (7)
1. A traditional Chinese medicine mask containing seaweed extracts for promoting blood circulation and resisting aging is characterized in that the mask liquid comprises the following formula in percentage by mass: 60-85% of lily water, 3-10% of glycerol, 3-10% of seaweed extract, 5-15% of efficacy type traditional Chinese medicine extract, 0.1-2% of small molecular sodium hyaluronate, 0.1-3% of cold-extracted snake oil, 0.05-2% of xanthan gum, 0.5-2% of 1, 2-hexanediol and 0.1-1% of p-hydroxyacetophenone.
2. The preparation method of the blood-activating and anti-aging traditional Chinese medicine facial mask containing the seaweed extract as claimed in claim 1, is characterized in that xanthan gum is dispersed in glycerol according to the formula amount, the mixture is uniformly stirred, lily flower water, the seaweed extract, small-molecule sodium hyaluronate and cold-extracted snake oil are sequentially added, the mixture is heated to 80 ℃ and fully dissolved, then cooled, the mixture is cooled to 50 ℃, the functional traditional Chinese medicine extract, 1, 2-hexanediol and p-hydroxyacetophenone are added, the mixture is uniformly stirred, filtered by a 400-mesh sieve and discharged, a facial mask cloth is completely immersed in the facial mask liquid, and the blood-activating and anti-aging traditional Chinese medicine facial mask is obtained through molding.
3. The preparation method of the blood circulation-promoting and anti-aging traditional Chinese medicine facial mask containing the seaweed extract as claimed in claim 2 is characterized in that the extraction process of the seaweed extract comprises the steps of cleaning 200g of seaweed with clear water to remove impurities, drying the seaweed in a constant-temperature oven at 45 ℃ for 12 hours, crushing the seaweed with a crusher, sieving the seaweed with a 100-mesh sieve, adding 3L of distilled water, adjusting the pH to be =5.0, adding cellulase with the dosage of 2%, performing enzymolysis at constant temperature for 3 hours, inactivating the enzyme at 90 ℃ for 10 minutes, centrifuging the seaweed in a centrifuge, extracting supernatant, adding activated carbon to decolor, filtering, performing rotary evaporation concentration at 50 ℃, and freeze-drying to obtain the seaweed extract.
4. The method for preparing the blood circulation-promoting and anti-aging traditional Chinese medicine mask containing the seaweed extract as claimed in claim 3, wherein the seaweed comprises one or more of the combination of macroalgae, red algae, spirulina, chlorella, kelp, green algae, brown algae, blue algae, fucus, coral algae, chlorella and nemacystus.
5. The preparation method of the blood-activating and anti-aging traditional Chinese medicine mask containing the seaweed extract as claimed in claim 3 is characterized in that: the rotating speed of the centrifugal machine is 3000r/min, and the centrifugal time is 10 min.
6. The preparation method of the blood-activating and anti-aging traditional Chinese medicine mask containing the seaweed extract as claimed in claim 2, wherein the functional traditional Chinese medicine extract is prepared from the following traditional Chinese medicine raw materials in parts by weight: 5-20 parts of dendrobium huoshanense, 5-18 parts of caulis spatholobi, 5-15 parts of motherwort, 5-13 parts of salvia miltiorrhiza, 5-10 parts of lucid ganoderma, 5-10 parts of wild chrysanthemum, 5-10 parts of kudzu root, 2-8 parts of honeysuckle, 1-8 parts of mulberry leaf, 1-6 parts of cortex albiziae, 1-6 parts of folium artemisiae argyi and 1-5 parts of rhizoma smilacis glabrae.
7. The preparation method of the blood-activating and anti-aging traditional Chinese medicine mask containing the seaweed extract as claimed in claim 6, is characterized in that the preparation process of the functional traditional Chinese medicine extract comprises the following steps: quickly washing the traditional Chinese medicine raw materials in parts by weight for 3 times, removing floating impurities and sinking residues, drying, carrying out superfine grinding, sieving to obtain mixed medicinal powder, adding distilled water, decocting and extracting at 85 ℃ for 3 times, combining the extracting solutions for 3 times, concentrating under reduced pressure, and standing to room temperature to obtain the functional traditional Chinese medicine extract.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109700733A (en) * | 2017-10-26 | 2019-05-03 | 张家界茶坤缘生物科技开发有限公司 | Plant mask and preparation method thereof |
| CN109998937A (en) * | 2019-03-22 | 2019-07-12 | 南京工业大学 | Serial cosmetics and preparation method thereof containing glycosylglycerol (α GG) |
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| CN109700733A (en) * | 2017-10-26 | 2019-05-03 | 张家界茶坤缘生物科技开发有限公司 | Plant mask and preparation method thereof |
| CN109998937A (en) * | 2019-03-22 | 2019-07-12 | 南京工业大学 | Serial cosmetics and preparation method thereof containing glycosylglycerol (α GG) |
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| CN113288846A (en) * | 2021-04-27 | 2021-08-24 | 杜莲 | Traditional Chinese medicine seaweed mask and preparation method thereof |
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Application publication date: 20200619 |