CN110339083A - A kind of oligopeptides repairs Essence and its application method - Google Patents
A kind of oligopeptides repairs Essence and its application method Download PDFInfo
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- CN110339083A CN110339083A CN201910774415.7A CN201910774415A CN110339083A CN 110339083 A CN110339083 A CN 110339083A CN 201910774415 A CN201910774415 A CN 201910774415A CN 110339083 A CN110339083 A CN 110339083A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/88—Two- or multipart kits
- A61K2800/882—Mixing prior to application
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Abstract
The invention discloses a kind of oligopeptides to repair Essence and its application method, it is related to technical field of skin care, it is made of reparation freeze-dried powder and reparation solvent liquid, the reparation freeze-dried powder includes mannitol, glutathione, oligopeptides -1, oligopeptides -2, the reparation solvent liquid includes water, glycerol, propylene glycol, HERBA DENDROBII stem extraction, kuh-seng root extract, aloe barbadensis Miller leaf extract, Echinacea angustifolia extract, lycium barbarum berry extract, parahydroxyacet-ophenone, 1,2- hexylene glycol;The made Essence of the present invention is suitable for the deep layer maintenance after various skin injuries, improves skin quality;It is particularly suitable for the reparation of skin after shining, skin rapid sedation is made to get off, mitigates the degree of injury of skin after shining, shortens the maintenance time of skin after shining.
Description
Technical field:
The present invention relates to technical field of skin care, and in particular to a kind of oligopeptides repairs Essence and its application method.
Background technique:
Essence belongs to one kind of facial skin care product, containing more precious effect ingredient, such as plant extracts, neural acyl
Amine, saualane etc., its effect have anti-aging, crease-resistant, moisturizing, whitening, despeckle etc..Due in Essence be rich in multiple efficacies at
Divide and concentration is higher, therefore price is compared with other skin care item valuableness.
Currently, Essence generallys use bottled mode, and it is filling in bottle after multiple efficacies ingredient is mixed, in use process
In can make internal functional component ingress of air because being repeatedly opened Packaging Bottle, and long-time ingress of air will affect partial efficacy at
The using effect divided.For this problem, people start to pack using ampoule bottle, and an ampoule once can be used.
Through researching and developing with great concentration for many years, repair Essence the present invention provides a kind of oligopeptides, the Essence by reparation freeze-dried powder and
Solvent liquid composition is repaired, optimizes the using effect of Essence by addition various plants extract and functional component.
Summary of the invention:
Technical problem to be solved by the present invention lies in a kind of oligopeptides reparation Essence is provided, which is suitable for a variety of
Deep layer maintenance after skin injury improves skin quality;It is particularly suitable for the reparation of skin after shining, so that skin rapid sedation is got off, subtracts
The degree of injury of skin, shortens the maintenance time of skin after shining after light solarization.
The following technical solution is employed for the technical problems to be solved by the invention to realize:
A kind of oligopeptides reparation Essence, is made of, the reparation freeze-dried powder is by sweet dew reparation freeze-dried powder and reparation solvent liquid
Sugar alcohol, glutathione, oligopeptides -1, oligopeptides -2 are made, and the reparation solvent liquid is extracted by water, glycerol, propylene glycol, HERBA DENDROBII stem
Object, kuh-seng root extract, aloe barbadensis Miller leaf extract, Echinacea angustifolia extract, lycium barbarum berry extract, para hydroxybenzene second
Ketone, 1,2- hexylene glycol are made.
The reparation freeze-dried powder and reparation solvent liquid are filling in ampoule respectively.
Each raw material weight number for repairing freeze-dried powder are as follows: 5-15 parts of mannitol, 0.5-5 parts of glutathione, widow
- 1 0.1-3 parts of peptide, -2 0.1-3 parts of oligopeptides;
It is described repair solvent liquid each raw material weight number are as follows: 50-200 parts of water, 5-20 parts of glycerol, 0.5-5 parts of propylene glycol,
0.5-5 parts of HERBA DENDROBII stem extraction, 0.5-5 parts of kuh-seng root extract, 0.5-5 parts of aloe barbadensis Miller leaf extract, purple pine nut
0.05-3 parts of chrysanthemum extract, 0.05-3 parts of lycium barbarum berry extract, 0.01-0.5 parts of parahydroxyacet-ophenone, 1,2- hexylene glycol
0.01-0.5 parts.
Above-mentioned HERBA DENDROBII stem extraction, kuh-seng root extract, aloe barbadensis Miller leaf extract, Echinacea angustifolia extract,
Lycium barbarum berry extract is purchased from market.
Above-mentioned oligopeptides repairs the application method of Essence are as follows: in use, opening ampoule, will repair solvent liquid and pour into reparation jelly
It in dry powder, can be applied on skin after being sufficiently mixed, without washing.
In order to further increase the cosmetic result that above-mentioned oligopeptides repairs Essence, the present invention is also added in repairing freeze-dried powder
Raspberry extract, it may be assumed that
Each raw material weight number for repairing freeze-dried powder are as follows: 5-15 parts of mannitol, 0.5-5 parts of glutathione, widow
- 1 0.1-3 parts of peptide, -2 0.1-3 parts of oligopeptides, 0.05-1 parts of raspberry extract.
The raspberry extract is made of raspberry through alcohol extracting rear decoloring, specifically the preparation method comprises the following steps: fresh raspberry is utilized
Slurry is made in fiberizer, and dehydrated alcohol is added as Extraction solvent, and dilute hydrochloric acid is added dropwise and adjusts pH value to 2-3, is heated to 50-
60 DEG C of heat preservations are extracted, and are centrifuged, are filtered after extraction, decolorising agent is added into filtrate, stands after stirring, filters again, filtrate
Thick paste is made after being concentrated under reduced pressure, is freeze-dried after thick paste natural cooling to get raspberry extract.
The decolorising agent is active carbon.
Good decolorizing effect can be obtained using active carbon as decolorising agent, but can adsorb a certain amount of tree while decoloration
Certain kind of berries extract, to cause the loss of this part raspberry extract after decolorising agent filtering, therefore the present invention also provides one kind
The preparation method of decoloring agent, it is specific the preparation method is as follows:
The decolorising agent is made of aluminium-magnesium silicate through N hydroxymethyl acrylamide modification, preparation method are as follows: by magnesium silicate
Aluminium is dispersed in water, and adds N hydroxymethyl acrylamide and ammonium persulfate, and it is anti-to be heated to 75-85 DEG C of heat preservation under stiring
It answers, stands after reaction, filter, obtained solid is ground into powder after drying.
The mass ratio of the aluminium-magnesium silicate, N hydroxymethyl acrylamide and ammonium persulfate is 5-10:0.5-5:0.05-
0.25。
N hydroxymethyl acrylamide generates polyacrylamide, polypropylene through self-polymerization under initiator ammonium persulfate effect
Amide incorporates in the distinctive three-D space structure of aluminium-magnesium silicate the physical modification realized to aluminium-magnesium silicate, silicon after modified
Sour magnalium has good decolorizing effect, and raspberry extract caused by decolorization operations can be reduced for active carbon
Loss amount.
The beneficial effects of the present invention are:
(1) the made Essence of the present invention avoids storing by repairing freeze-dried powder and repairing the independent packaging of solvent liquid
In journey because Multiple components it is miscible due to influence using effect, and this independent packaging mode is also avoided that the excess of preservative adds
Add;
(2) the made Essence of the present invention is easy to use, can disposably be made after ampoule opening by quantitative filling mode
It is finished, avoiding conventional skin care product, ingress of air influences asking for subsequent using effect in turn due to repeatedly opening in use
Topic;
(3) the made Essence of the present invention is suitable for the deep layer maintenance after various skin injuries, improves skin quality;It is particularly suitable for
The reparation of skin after solarization, makes skin rapid sedation get off, and mitigates the degree of injury of skin after shining, when shortening the maintenance of skin after shining
Between.
Specific embodiment:
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
HERBA DENDROBII stem extraction is purchased from Ningxia vanilla Bioisystech Co., Ltd, and kuh-seng root extract is purchased from the green day in Xi'an
Bioisystech Co., Ltd, aloe barbadensis Miller leaf extract are purchased from Xi'an Xu Huang Bioisystech Co., Ltd, and purple coneflower is extracted
Object is purchased from Xi'an Bioisystech Co., Ltd, Tianrui, and lycium barbarum berry extract is purchased from Xi'an Tian Bao Biotechnology Co., Ltd,
Active carbon is purchased from Liyang City Tian Sheng active carbon Co., Ltd.
Embodiment 1
Repair the preparation of freeze-dried powder: 0.2g mannitol, 0.075g glutathione, 0.05g oligopeptides -1 and 0.025g is few
Peptide -2 is dissolved in 2g parts of water, filling to be lyophilized after ampoule.
Repair solvent liquid preparation: by 1g water, 0.08g glycerol, 0.02g propylene glycol, 0.02g HERBA DENDROBII stem extraction,
0.01g kuh-seng root extract, 0.01g aloe barbadensis Miller leaf extract, 0.01g Echinacea angustifolia extract, 0.005g lycium barbarum
Berry extract, 0.001g parahydroxyacet-ophenone, 0.001g 1,2- hexylene glycol are filling in ampoule after mixing.
Embodiment 2
Repair the preparation of freeze-dried powder: 0.2g mannitol, 0.075g glutathione, 0.05g oligopeptides -1 and 0.05g is few
Peptide -2 is dissolved in 2g parts of water, filling to be lyophilized after ampoule.
Repair solvent liquid preparation: by 1g water, 0.08g glycerol, 0.02g propylene glycol, 0.02g HERBA DENDROBII stem extraction,
0.01g kuh-seng root extract, 0.01g aloe barbadensis Miller leaf extract, 0.01g Echinacea angustifolia extract, 0.005g lycium barbarum
Berry extract, 0.001g parahydroxyacet-ophenone, 0.001g 1,2- hexylene glycol are filling in ampoule after mixing.
Embodiment 3
It is control with embodiment 2, the embodiment 3 repaired and add raspberry extract in freeze-dried powder is set, remaining operation is same
Embodiment 2, raspberry extract dosage are 0.005g.
The preparation of raspberry extract: slurry is made using fiberizer in the fresh raspberry of 5g, and 200mL dehydrated alcohol is added
As Extraction solvent, dropwise addition dilute hydrochloric acid adjusting pH value to 2 is heated to 60 DEG C of heat preservations and extracts 3h, is centrifuged, filters after extraction,
1g bleaching agent activated carbon is added into filtrate, stands after stirring, filters again, thick paste, thick paste is made in filtrate after being concentrated under reduced pressure
It is freeze-dried after natural cooling to get raspberry extract.
Embodiment 4
It is control with embodiment 3, setting is with the embodiment 4 of equivalent self-control decolorising agent substitution active carbon, remaining operation is the same as real
Apply example 3.
The preparation of decolorising agent: 10g aluminium-magnesium silicate is dispersed in water, add 2.5g N hydroxymethyl acrylamide and
0.125g ammonium persulfate, and it is heated to 75 DEG C of insulation reaction 3h under stiring, it stands, filters after reaction, obtained solid warp
Powder is ground into after drying.
Comparative example
It is control with embodiment 3, with the comparative example of equivalent aluminium-magnesium silicate substitution active carbon, remaining operates same embodiment for setting
3。
It is utilized respectively embodiment 1-4 and comparative example prepares Essence, and according to " cosmetics safety technical specification " (2015
Year version) made Essence is detected, it is the testing result that Li Chuan detection technique Services Co., Ltd, Zhongshan city provides below,
As shown in table 1, table 2 and table 3.
1 appearance of table, fragrance, pH, heat-resisting, resist cold testing result
2 Micro biological Tests result of table
Inspection project | Inspection result | Limit value |
Total plate count (CFU/g) | < 10 | ≤1000 |
Yeast and mold sum (CFU/g) | < 10 | ≤100 |
Heat-resisting coliform (/g) | It is not detected | It must not detect |
Staphylococcus aureus (/g) | It is not detected | It must not detect |
Pseudomonas aeruginosa (/g) | It is not detected | It must not detect |
3 health chemical testing result of table
It is detected according to skin irritation of the GB/T 16886.10-2005 to made Essence, observation uses respectively
1h, for 24 hours, the skin condition of 48h, 72h.The results show that having no that erythema, oedema or other irritative responses occurs in skin.
After-sun recovery test: 100 20-40 years old women are randomly selected and carry out after-sun recovery test, test equipment is moral
CK company, state skin analyzer measures embodiment 1-4 and the made Essence of comparative example respectively and uses haematochrome at cheek after 4 weeks
It is worth and using red pigment value at the cheek of preceding same area, calculates red pigment value reduced rate and be simultaneously averaged, as a result such as 4 institute of table
Show.
Red pigment value reduced rate=[(red pigment value after red pigment value-reparation before repairing)/red pigment value before repairing] ×
100%.
The after-sun recovery effect of 4 Essence of table
Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Comparative example |
Red pigment value reduced rate/% | 18.2 | 19.7 | 24.1 | 26.6 | 24.8 |
As shown in Table 4, the addition of raspberry extract can enhance the after-sun recovery ability of Essence, and to make decolorising agent by oneself
Substitution active carbon can improve after-sun recovery effect by reducing the loss amount of raspberry extract, directly using aluminium-magnesium silicate as taking off
Although toner not will cause the excessive loss of raspberry extract, decolorizing effect is very weak, is unable to reach desired decolorizing effect.
In order to test the decolorizing effect of decolorising agent, embodiment is measured using U.S.'s Hash LICO690 liquid coloration analyzer
3, embodiment 4, in comparative example in raspberry extract preparation process before and after decolorization operations filtrate chromatic value, calculate coloration reduced rate
And be averaged, the results are shown in Table 5.
Coloration reduced rate=[(chromatic value after chromatic value-decoloration before decolourizing)/chromatic value before decolourizing] × 100%.
The decolorizing effect of 5 decolorising agent of table
Test item | Embodiment 3 | Embodiment 4 | Comparative example |
Coloration reduced rate/% | 98.75 | 98.12 | 36.94 |
As shown in Table 5, embodiment 4, which makes decolorising agent by oneself, can obtain the decolorizing effect close to active carbon, and directly with silicic acid
Magnalium is very poor as the comparative example decolorizing effect of decolorising agent.
Therefore, the present invention, which makes decolorising agent by oneself, can obtain the decolorizing effect close to active carbon, while be able to solve active carbon
Excessive adsorption raspberry extract in turn results in the problem of raspberry extract loss when decoloration.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (9)
1. a kind of oligopeptides repairs Essence, it is characterised in that: be made of reparation freeze-dried powder and reparation solvent liquid, the reparation freeze-drying
Powder includes mannitol, glutathione, oligopeptides -1, oligopeptides -2, and the reparation solvent liquid includes water, glycerol, propylene glycol, golden hairpin stone
It is dry measure used in former times stem extraction, kuh-seng root extract, aloe barbadensis Miller leaf extract, Echinacea angustifolia extract, lycium barbarum berry extract, right
Hydroxy acetophenone, 1,2- hexylene glycol.
2. oligopeptides according to claim 1 repairs Essence, it is characterised in that: the reparation freeze-dried powder and reparation solvent liquid
It is filling in ampoule respectively.
3. oligopeptides according to claim 1 repairs Essence, it is characterised in that: each raw material weight for repairing freeze-dried powder
Number are as follows: 5-15 parts of mannitol, 0.5-5 parts of glutathione, -1 0.1-3 parts of oligopeptides, -2 0.1-3 parts of oligopeptides.
4. oligopeptides according to claim 1 repairs Essence, it is characterised in that: each raw material weight for repairing solvent liquid
Number are as follows: 50-200 parts of water, 5-20 parts of glycerol, 0.5-5 parts of propylene glycol, 0.5-5 parts of HERBA DENDROBII stem extraction, radix sophorae extract
0.5-5 parts of object, 0.5-5 parts of aloe barbadensis Miller leaf extract, 0.05-3 parts of Echinacea angustifolia extract, lycium barbarum berry extract
0.05-3 parts, 0.01-0.5 parts of parahydroxyacet-ophenone, 0.01-0.5 parts of 1,2- hexylene glycol.
5. the application method that oligopeptides described in claim 1 repairs Essence, it is characterised in that: in use, opening ampoule, will repair
It redissolves matchmaker's liquid to pour into reparation freeze-dried powder, can be applied on skin after being sufficiently mixed, without washing.
6. oligopeptides according to claim 1 repairs Essence, it is characterised in that: the reparation freeze-dried powder is also mentioned comprising raspberry
Take object.
7. oligopeptides according to claim 6 repairs Essence, it is characterised in that: each raw material weight for repairing freeze-dried powder
Number are as follows: 5-15 parts of mannitol, 0.5-5 parts of glutathione, -1 0.1-3 parts of oligopeptides, -2 0.1-3 parts of oligopeptides, raspberry are extracted
0.05-1 parts of object.
8. oligopeptides according to claim 7 repairs Essence, it is characterised in that: the raspberry extract is by raspberry through alcohol extracting
Rear decoloring is made, and specifically the preparation method comprises the following steps: slurry is made using fiberizer in fresh raspberry, and dehydrated alcohol conduct is added and mentions
Solvent is taken, dilute hydrochloric acid is added dropwise and adjusts pH value to 2-3, is heated to 50-60 DEG C of heat preservation and extracts, be centrifuged, filter after extraction, to filter
Decolorising agent is added in liquid, stands after stirring, filters again, thick paste is made in filtrate after being concentrated under reduced pressure, and thick paste natural cooling is laggard
Row freeze-drying is to get raspberry extract.
9. oligopeptides according to claim 8 repairs Essence, it is characterised in that: the decolorising agent is active carbon.
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CN110604718A (en) * | 2019-11-11 | 2019-12-24 | 奢脉国际化妆品(北京)有限公司 | Full-effect polypeptide eye essence and preparation method thereof |
CN110840808A (en) * | 2019-12-15 | 2020-02-28 | 宁波德沃生物科技有限公司 | Plant spot-removing skin care product |
CN111067852A (en) * | 2020-01-16 | 2020-04-28 | 猫头鹰(福州)日用品有限公司 | Essence containing polypeptide and preparation method thereof |
CN111265430A (en) * | 2020-02-19 | 2020-06-12 | 中国热带农业科学院海口实验站 | Camellia oleifera facial mask essence and camellia oleifera facial mask thereof |
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