CN110331388A - 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 - Google Patents
一种基于水热法快速生长ZnO纳米多孔薄膜的方法 Download PDFInfo
- Publication number
- CN110331388A CN110331388A CN201910560268.3A CN201910560268A CN110331388A CN 110331388 A CN110331388 A CN 110331388A CN 201910560268 A CN201910560268 A CN 201910560268A CN 110331388 A CN110331388 A CN 110331388A
- Authority
- CN
- China
- Prior art keywords
- thin film
- zno nano
- porous thin
- growth
- hydro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000010409 thin film Substances 0.000 title claims abstract description 55
- 238000000034 method Methods 0.000 title claims abstract description 20
- 238000001027 hydrothermal synthesis Methods 0.000 title claims abstract description 17
- 239000000758 substrate Substances 0.000 claims abstract description 32
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000008367 deionised water Substances 0.000 claims abstract description 15
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims abstract description 14
- 235000019441 ethanol Nutrition 0.000 claims abstract description 13
- AGGKEGLBGGJEBZ-UHFFFAOYSA-N tetramethylenedisulfotetramine Chemical compound C1N(S2(=O)=O)CN3S(=O)(=O)N1CN2C3 AGGKEGLBGGJEBZ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000004506 ultrasonic cleaning Methods 0.000 claims abstract description 7
- 235000005074 zinc chloride Nutrition 0.000 claims abstract description 7
- 239000011592 zinc chloride Substances 0.000 claims abstract description 7
- 239000000243 solution Substances 0.000 claims description 25
- 239000011259 mixed solution Substances 0.000 claims description 24
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 22
- 238000013019 agitation Methods 0.000 claims description 12
- FMRLDPWIRHBCCC-UHFFFAOYSA-L Zinc carbonate Chemical compound [Zn+2].[O-]C([O-])=O FMRLDPWIRHBCCC-UHFFFAOYSA-L 0.000 claims description 6
- 238000005352 clarification Methods 0.000 claims description 6
- 238000004321 preservation Methods 0.000 claims description 6
- 235000004416 zinc carbonate Nutrition 0.000 claims description 6
- 239000011667 zinc carbonate Substances 0.000 claims description 6
- 229910000010 zinc carbonate Inorganic materials 0.000 claims description 6
- -1 and dry Substances 0.000 claims description 5
- 239000002184 metal Substances 0.000 claims description 5
- 229910052751 metal Inorganic materials 0.000 claims description 5
- 239000011521 glass Substances 0.000 claims description 2
- 229910052594 sapphire Inorganic materials 0.000 claims description 2
- 239000010980 sapphire Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 7
- 239000010408 film Substances 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000007789 sealing Methods 0.000 abstract 1
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 107
- 239000011787 zinc oxide Substances 0.000 description 54
- 229960001296 zinc oxide Drugs 0.000 description 7
- 239000012528 membrane Substances 0.000 description 5
- 238000013033 photocatalytic degradation reaction Methods 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- RBTBFTRPCNLSDE-UHFFFAOYSA-N 3,7-bis(dimethylamino)phenothiazin-5-ium Chemical compound C1=CC(N(C)C)=CC2=[S+]C3=CC(N(C)C)=CC=C3N=C21 RBTBFTRPCNLSDE-UHFFFAOYSA-N 0.000 description 3
- 229960000907 methylthioninium chloride Drugs 0.000 description 3
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- 239000002086 nanomaterial Substances 0.000 description 2
- 239000004793 Polystyrene Substances 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000004005 microsphere Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001699 photocatalysis Effects 0.000 description 1
- 238000007146 photocatalysis Methods 0.000 description 1
- 230000005622 photoelectricity Effects 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000011896 sensitive detection Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 230000005476 size effect Effects 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/23—Oxides
- C03C17/25—Oxides by deposition from the liquid phase
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
- C23C18/1208—Oxides, e.g. ceramics
- C23C18/1216—Metal oxides
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/21—Oxides
- C03C2217/216—ZnO
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/11—Deposition methods from solutions or suspensions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Thermal Sciences (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Composite Materials (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
Abstract
Description
Claims (7)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910560268.3A CN110331388B (zh) | 2019-06-26 | 2019-06-26 | 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 |
PCT/CN2020/081900 WO2020258960A1 (zh) | 2019-06-26 | 2020-03-28 | 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201910560268.3A CN110331388B (zh) | 2019-06-26 | 2019-06-26 | 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN110331388A true CN110331388A (zh) | 2019-10-15 |
CN110331388B CN110331388B (zh) | 2021-05-28 |
Family
ID=68142844
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201910560268.3A Active CN110331388B (zh) | 2019-06-26 | 2019-06-26 | 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 |
Country Status (2)
Country | Link |
---|---|
CN (1) | CN110331388B (zh) |
WO (1) | WO2020258960A1 (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2020258960A1 (zh) * | 2019-06-26 | 2020-12-30 | 五邑大学 | 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101823759A (zh) * | 2010-04-01 | 2010-09-08 | 江苏工业学院 | 连续大面积氧化锌纳米薄片及其制备方法 |
CN101844876A (zh) * | 2010-05-14 | 2010-09-29 | 北京科技大学 | 一种大面积高取向性的氧化锌纳米薄片阵列的制备方法 |
CN107887592A (zh) * | 2017-11-17 | 2018-04-06 | 武汉理工大学 | 碳包覆ZnO纳米线及其制备方法和应用 |
CN108411614A (zh) * | 2018-03-02 | 2018-08-17 | 华南理工大学 | 一种基于氧化锌/银纳米线杂化网络的柔性多功能传感纤维及其制备方法 |
EP3508622A1 (en) * | 2016-08-30 | 2019-07-10 | Korea University Research and Business Foundation | Nanofiber-nanowire composite and preparation method therefor |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP5339372B2 (ja) * | 2009-11-25 | 2013-11-13 | 独立行政法人産業技術総合研究所 | Zn(OH)2ナノシートとZnOナノウィスカー膜によるハイブリッドフィルム、ZnOナノシートとZnOナノウィスカー膜によるハイブリッドフィルム、およびそれらの作製方法 |
CN102693844B (zh) * | 2012-05-30 | 2014-12-03 | 辽宁工业大学 | 采用脉冲电磁场制备Al掺杂ZnO纳米片阵列的方法 |
ES2597983B1 (es) * | 2015-06-24 | 2017-12-12 | Consejo Superior De Investigaciones Cientificas (Csic) | Sistema y dispositivo de recolección de energía piezoeléctrico |
CN110331388B (zh) * | 2019-06-26 | 2021-05-28 | 五邑大学 | 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 |
-
2019
- 2019-06-26 CN CN201910560268.3A patent/CN110331388B/zh active Active
-
2020
- 2020-03-28 WO PCT/CN2020/081900 patent/WO2020258960A1/zh active Application Filing
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101823759A (zh) * | 2010-04-01 | 2010-09-08 | 江苏工业学院 | 连续大面积氧化锌纳米薄片及其制备方法 |
CN101844876A (zh) * | 2010-05-14 | 2010-09-29 | 北京科技大学 | 一种大面积高取向性的氧化锌纳米薄片阵列的制备方法 |
EP3508622A1 (en) * | 2016-08-30 | 2019-07-10 | Korea University Research and Business Foundation | Nanofiber-nanowire composite and preparation method therefor |
CN107887592A (zh) * | 2017-11-17 | 2018-04-06 | 武汉理工大学 | 碳包覆ZnO纳米线及其制备方法和应用 |
CN108411614A (zh) * | 2018-03-02 | 2018-08-17 | 华南理工大学 | 一种基于氧化锌/银纳米线杂化网络的柔性多功能传感纤维及其制备方法 |
Non-Patent Citations (1)
Title |
---|
黄开金等: "水热法制备纳米ZnO的研究现状", 《材料导报:综述篇》 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2020258960A1 (zh) * | 2019-06-26 | 2020-12-30 | 五邑大学 | 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 |
Also Published As
Publication number | Publication date |
---|---|
CN110331388B (zh) | 2021-05-28 |
WO2020258960A1 (zh) | 2020-12-30 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN106970117B (zh) | 一种基于电极表面原位生长纳米ZnO的NO2传感器 | |
CN108560035A (zh) | 一种低成本制备ZnO&TiO2异质结薄膜的方法 | |
CN104965008A (zh) | 一种丙酮气体传感器及其制备方法 | |
CN109052453A (zh) | 一种ZnCo2O4/ZnO异质结构复合气敏材料及制备方法 | |
CN105489694A (zh) | 氧化锌/硅p-n异质结紫外光探测器及其制备方法 | |
CN104264131A (zh) | 一种在ZnO纳米线阵列上生长的纤维状ZnO纳米线及其制备方法 | |
CN104475116A (zh) | 二氧化锡纳米线修饰的三氧化二铁纳米棒阵列的制备方法 | |
CN110241439A (zh) | 一种等离子体处理制备表面羟基化wo3薄膜光电极材料的方法 | |
CN110331388A (zh) | 一种基于水热法快速生长ZnO纳米多孔薄膜的方法 | |
CN108893728A (zh) | 具有高比表面积的超薄ZnO纳米片阵列的制备方法 | |
CN103265067B (zh) | 一种增强TiO2电极电化学性能的处理方法 | |
CN103135224A (zh) | 一种光控可逆润湿涂层的制备方法 | |
CN104628263A (zh) | 一种制备氧化铟八面体纳米晶薄膜的方法 | |
CN104071833A (zh) | 一种锐钛矿型TiO2纳米片的制备方法及应用 | |
CN111215044A (zh) | 一种基于柔性衬底的Ga2O3纳米柱光催化材料及制备方法 | |
CN110165142A (zh) | 一种原位制备纳米复合电极材料的方法 | |
CN105702472A (zh) | 一种太阳能电池电极及其制备方法、太阳能电池 | |
CN103334141B (zh) | 一种双稀土掺杂TiO2纳米管有序阵列的制备方法 | |
CN108179455A (zh) | 一种Cu2O纳米颗粒/TiO2纳米管阵列复合异质结薄膜的制备方法 | |
CN104399503A (zh) | 铁、氮、氟共掺杂二氧化钛纳米管阵列光催化剂及其制备方法和应用 | |
CN104947043A (zh) | 一种Si-ITO复合纳米线有序阵列的制备方法 | |
CN104096557B (zh) | 异质结型MVO4与TiO2复合光催化纤维的制备方法 | |
CN106830072B (zh) | 一种二氧化钛纳米线阵列的制备方法 | |
CN109837516A (zh) | 一种磁控溅射制备ZnFe2O4/Fe2O3三维异质结纳米材料的方法 | |
CN105990030A (zh) | 具有[10-10]取向及高比表面积的ZnO纳米线阵列及其制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20240218 Address after: 1003, Building A, Zhiyun Industrial Park, No. 13 Huaxing Road, Tongsheng Community, Dalang Street, Longhua District, Shenzhen City, Guangdong Province, 518000 Patentee after: Shenzhen Wanzhida Enterprise Management Co.,Ltd. Country or region after: China Address before: 529020, No. 22, Dongcheng village, Pengjiang District, Guangdong, Jiangmen Patentee before: WUYI University Country or region before: China |
|
TR01 | Transfer of patent right |