CN109806218A - A kind of Goat Placenta polypeptide women facial mask liquid and preparation method thereof - Google Patents
A kind of Goat Placenta polypeptide women facial mask liquid and preparation method thereof Download PDFInfo
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Abstract
A kind of Goat Placenta polypeptide women facial mask liquid and preparation method thereof, is related to skin care industry.The facial mask is mainly prepared from the following raw materials: glycerol, soy bean edible fiber powder, propylene glycol, glycine betaine, Goat Placenta anti-oxidation peptide, methylparaben etc. are at being grouped as.Facial mask provided by the invention not only has excellent moisture retention, oil absorption, moreover it is possible to can play the role of improving skin elasticity, oxidation resistant, while the licorice extract and papaya extractives that contain in facial mask also make it have white-skinned face function.
Description
Technical field
The present invention relates to cosmetic skin fields, and in particular to a kind of Goat Placenta polypeptide women facial mask liquid and its preparation side
Method.
Background technique
Polypeptide is a kind of compound of the molecular structure between amino acid and protein, and protein is made to have certain life
Manage function.In the vital movement of the mankind, the digestion and absorption of peptide in vivo is different from amino better than free amino acid
The internal delivery system of acid.Certain small peptides are while providing nutriment necessary to growth in humans, development, additionally it is possible to prevent
Or treatment disease, adjust function of human body.
Goat Placenta polypeptide is that biologically active small-molecular peptides are extracted from Goat Placenta.Goat Placenta, which is rich in, breeds life institute
Required all primitive life substances.Modern medical research has found that protein rich in Goat Placenta, 17 kinds of amino acid,
14 kinds of microelements, phosphatide, lipopolysaccharides, vitamins, there are also more to immune function and the relevant various active of body normal operation
Peptide has and adjusts immunity of organisms, improve microcirculation, the cholesterol in reduction blood, adjust organism endocrine and other effects.Science
Family confirms that the ratio that nutritional ingredient is naturally arranged in pairs or groups is the nourishing reinforced vital energy closest to the demand of human body by many experiments
Antasthenic.
Facial mask is a kind of numerous women commonly skin care item, with the development of society, the destruction of environment, ultraviolet light, air-conditioning,
Dust storm, excessive bathing etc. can all cause to have dry skin；In addition the age increase of itself, hyposteatosis, the big, fatigue of pressure etc.
It will also result in dry skin.Existing nourishing pack, face mask of traditional Chinese medicine are varied, Various Functions, but these facial masks or add
Added with various chemicals, although quick, dependence is strong, and skin becomes more even worse than in the past after deactivating, and skin self is repaired
Multiple function reduction.
Summary of the invention
The purpose of the present invention is: Goat Placenta polypeptide is applied in cosmetics, a kind of Ms's skin whitening, moisturizing is provided, improves skin
Skin elasticity, while there is the facial mask liquid of antioxidation.
To achieve the above object, the present invention adopts the following technical scheme:
A kind of Goat Placenta polypeptide women facial mask liquid, it is characterised in that: the ingredient comprising following parts by weight:
A kind of preparation method of Goat Placenta polypeptide women facial mask liquid, comprises the following steps:
S1, it prepares Goat Placenta anti-oxidation peptide liquid: fresh Goat Placenta being thawed, is rinsed with physiological saline, is shredded, remove fascia
And blood vessel, by high-shearing dispersion emulsifying machine homogenate, multigelation 3 times, refrigerated centrifuge.It collects to precipitate to be freezed and do
Dry, the sample after freeze-drying is rubbed with pulverizer, is crossed 60 meshes, is collected the powder of filtration；Weigh 30~40g Goat Placenta leftover bits and pieces feed powder
End adds distilled water to be made into the substrate solution of 30~40g/L, is adjusted to pH=6.0~7.0, and Mixed enzyme for animal proteolysis is added
1~4h is digested, enzyme additive amount is 4000~5000U/g；It is warming up to 90~100 DEG C after enzymatic hydrolysis, 10min is kept to carry out enzyme deactivation
Processing is cooled to 25 DEG C, adjusts pH=6.0~7.5, is centrifuged 20min under the conditions of 1~10 DEG C and 3500~4000rpm, collects
Supernatant；Under the conditions of 20-30 DEG C, pH=7,0.9~0.8MPa of inlet pressure, 0.6~0.5MPa of outlet pressure, ultrafiltration membrane is used
Supernatant is collected by filtration, the Goat Placenta anti-oxidation peptide liquid rich in function factors such as various amino acid is made.
S2, it prepares licorice extract: Radix Glycyrrhizae is crushed, cross 80 meshes, at 60 DEG C, feed liquid mass ratio is the condition of 1:10
Under, 90min, four layers of filtered through gauze are extracted with the hydrochloric acid solution that concentration is 1mol/L, liquid to be filtered is cooled to room temperature, and 1mol/L is added
Sodium hydroxide solution be adjusted to neutrality, obtain licorice extract.
S3, papaya extractives are prepared: pawpaw is removed the peel into deseeding, cleaned, the water of 5 times of weight is added, is smashed to pieces with blender；It presses
750u/g ratio crushes in liquid to pawpaw and pectase is added, and then 45 DEG C of condition digests 5h, heat temperature raising after enzymatic hydrolysis again
To 90~100 DEG C, 15min is kept the temperature, enzyme deactivation is living, is separated by solid-liquid separation after being cooled to room temperature, and filtrate is collected, and centrifugation takes supernatant,
It adjusts pH value to 6.0, is concentrated, is drying to obtain papaya extractives.
S4, preparation water phase: precise half is formulated the deionized water of deal in beaker, is added into beaker and matches square gauge
Glycerol, propylene glycol, glycine betaine, EDTA-2 sodium, trehalose, the emulsifier, allantoin for determining deal, beaker is put into water-bath,
Under the conditions of 85 DEG C of bath temperature, mixing speed 150rpm, 10min is mixed, water phase is made.
S5, prepare oily phase: precise formula provides xanthan gum, carragheen, licorice extract, the papaya extractives of deal
With citric acid in beaker, it is 80 DEG C in bath temperature, under the conditions of mixing speed 150rpm, stirs 10min, 80 DEG C of heat preservation 5h,
Oily phase is made.
S6, preparation function phase: Goat Placenta anti-oxidation peptide battalion is added in beaker in the deionized water of precise half deal
Nutrient solution and soy bean edible fiber powder are 50 DEG C in bath temperature, under the conditions of mixing speed 150rpm, stir 15min, standing 2h,
Function phase is made.
S7, prepare asperities film liquid: oil phase made from step S5 is heated to 80 DEG C under 150rpm mixing speed, to oily phase
In water phase made from step S4 is slowly at the uniform velocity added, continue to stir 10min under the conditions of revolving speed 150rpm, be then cooled to 30~
40 DEG C, it is added step S6 obtained function phase, methylparaben and essence, under the conditions of low whipping speed 150rpm, stirring
10min obtains asperities film liquid.
S8, preparation facial mask liquid: at 30~50 DEG C, under the conditions of 10000~15000rpm, 5~15min of homogeneous both obtains facial mask
Liquid.
A kind of Goat Placenta polypeptide women facial mask liquid, it is characterised in that: emulsifier be Tween 80 or rilanit special RH40 or
The two quality is the mixture that 1:2 is mixed to get.
A kind of preparation method of Goat Placenta polypeptide women facial mask liquid, it is characterised in that: ultrafiltration membrane aperture described in step S1 is
0.45μm。
A kind of preparation method of Goat Placenta polypeptide women facial mask liquid, it is characterised in that: soybean dietary fiber described in step S6
Powder Particle Size is 45~48 μm.
Technical effect and advantage of the invention:
Licorice extract contains a large amount of licoflavone, has anti-inflammatory, antiviral, heart tonifying, calmness and analgesia and antioxygen
Change, anti-aging, it is antitumor the effects of.
The ferment that papaya extractives contain plays the role of except cutin, the tartaric acid contained in pawpaw there are also removing pore rubbish,
Play the role of moisturizing, Fructus Chaenomelis ferment contained by pawpaw can promote skin to be metabolized, and the sebum accumulated in pore is dissolved in help
And aging cutin, allow skin to seem brighter, more pure and fresh.
The present invention has multi-functional moisturizer using new food preservative Sensiva SC50, can play suppression in formula
The effect of bacterium, it can not only be added to water phase, but also may be added to oily phase.When being added to water phase, it can form an antibacterial environment, to whole
A formula plays antisepsis；Sensiva SC50 can repeat challenge it is demonstrated experimentally that in a water with synergy alcohols and glycols
In the lotion for wrapping oil, the antibacterial action of glycols such as pentanediol or ethohexadiol can be improved；Sensiva SC50 deodorizing effect, energy
Effectively inhibit the growth and breeding for causing the bacterium of peculiar smell, while not influencing the beneficial skin flora of human body.
The soybean dietary fiber micro mist that the present invention adds has good retentiveness, moreover it is possible to the grease of skin surface is adsorbed,
Soybean dietary fiber micro mist also can increase the package protection to Goat Placenta polypeptide liquid.
Goat Placenta anti-oxidation peptide liquid (containing nucleotide, peptides, various amino acid, epidermal growth factor, microelement etc.) tool
There is good nutritive value, the present invention adds Goat Placenta anti-oxidation peptide in facial treatment mask using Goat Placenta polypeptide as functional component
In, the facial treatment mask physical stability of the anti-oxidation peptide containing Goat Placenta is good, and the facial treatment mask of addition anti-oxidation peptide containing Goat Placenta can
Increase skin of face water content, reduce skin fluid loss, increase skin elasticity, there is excellent moisture retention, improvement skin can be played
The effect of skin elasticity.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that described herein, specific examples are only used to explain the present invention, and does not have to
It is of the invention in limiting.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creative work premise
Under every other embodiment obtained, shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of Goat Placenta polypeptide women facial mask liquid includes the ingredient of following parts by weight: 0.1 part of glycerol, soy bean edible fiber powder
3 parts, 3 parts of propylene glycol, 5 parts of glycine betaine, 0.05 portion of EDTA-2 sodium, 3 parts of trehalose, 3.6 parts of Tween 80,3 parts of allantoin, xanthan gum
1.5 parts, 0.2 part of carragheen, 5 parts of papaya extractives of 5 parts of licorice extract, 2 parts of citric acid, 1 part of Goat Placenta anti-oxidation peptide, Ni Bo
0.02 part of tortoise beetle ester, 0.1 part of essence, 10 parts of deionized water.
A kind of preparation method of Goat Placenta polypeptide women facial mask liquid, comprises the following steps:
S1, fresh Goat Placenta is thawed, is rinsed, is shredded with physiological saline, removed fascia and blood vessel, pass through high shear dispersion
Mulser prepares homogenate, and multigelation 3 times, refrigerated centrifuge.It collects precipitating to be freeze-dried, the sample after freeze-drying crushes
Machine rubs, and crosses 60 meshes, collects the powder of filtration；300g Goat Placenta leftover bits and pieces powder is weighed, distilled water is added to be made into 300g/L's
Substrate solution is adjusted to pH=7.0, and Mixed enzyme for animal proteolysis is added and digests 1h, enzyme additive amount is 4600U/g；Enzymatic hydrolysis knot
It is warming up to 100 DEG C after beam, 10min is kept to carry out destroy the enzyme treatment, is cooled to 25 DEG C, pH=7.5 is adjusted, in 6 DEG C and 3500rpm item
It is centrifuged 20min under part, collects supernatant；Under the conditions of 30 DEG C, pH=7, inlet pressure 0.8MPa, outlet pressure 0.5MPa, use
The ultrafiltration membrance filter that 0.45 μm of aperture collects supernatant, spare.
S2, it prepares licorice extract: 10g Radix Glycyrrhizae is crushed, cross 80 meshes, as in 500mL beaker, it is dense that 100mL is added
The hydrochloric acid solution for spending 1mol/L extracts 90min, then four layers of filtered through gauze at 60 DEG C, collects filtrate, and liquid to be filtered is cooled to room
Temperature, the sodium hydroxide solution that 1mol/L is added are adjusted to neutrality, obtain licorice extract, spare.
S3, papaya extractives are prepared: pawpaw is removed the peel into deseeding, cleaned, the water of 5 times of weight is added, is smashed to pieces with blender；It presses
750u/g ratio crushes in liquid to pawpaw and pectase is added, and then 45 DEG C of condition digests 5h, heat temperature raising after enzymatic hydrolysis again
To 90 DEG C, 15min is kept the temperature, enzyme deactivation is living, is separated by solid-liquid separation after being cooled to room temperature, and filtrate is collected, and centrifugation takes supernatant, adjusts pH
Value is concentrated to 6.0, is drying to obtain papaya extractives.
S4, preparation water phase: precise 50g deionized water in beaker, into beaker addition glycerol 1g, propylene glycol 30g,
Glycine betaine 50g, EDTA-2 sodium 0.5g, trehalose 30g, Tween 80 36g, allantoin 30g, beaker are put into water-bath, in water
85 DEG C of bath temperature, under the conditions of mixing speed 150rpm, 10min is mixed, water phase is made.
S5, prepare oily phase: precise formula provides the xanthan gum 15, carragheen 2, licorice extract 50g, pawpaw of deal
Extract 50g and citric acid 20g are 80 DEG C in bath temperature, under the conditions of mixing speed 150rpm, stir 10min in beaker,
80 DEG C of heat preservation 5h, are made oily phase.
S6, preparation function phase: 10g Goat Placenta anti-oxidation peptide nutrient solution is added in beaker in precise 50g deionized water
It is 45~48 μm of DE soy bean edible fiber powders with 30g granularity, is 50 DEG C in bath temperature, under the conditions of mixing speed 150rpm, stirs
15min is mixed, 2h is stood, function phase is made.
S7, prepare asperities film liquid: oil phase made from step S5 is heated to 80 DEG C under 150rpm mixing speed, to oily phase
In slowly at the uniform velocity be added step S4 made from water phase, continue under the conditions of revolving speed 150rpm stir 10min, be then cooled to 30
DEG C, it is added step S6 obtained function phase, 0.2g methylparaben and 1g essence, under the conditions of low whipping speed 150rpm, stirring
10min obtains asperities film liquid.
S8, preparation facial mask liquid: at 30 DEG C, under the conditions of 10000rpm, homogeneous 15min both obtains facial mask liquid.
Embodiment 2:
A kind of Goat Placenta polypeptide women facial mask liquid includes the ingredient of following parts by weight: 0.5 part of glycerol, soy bean edible fiber powder
8 parts, 10 parts of propylene glycol, 1 part of glycine betaine, 0.01 portion of EDTA-2 sodium, 0.2 part of trehalose, 3.6 parts of rilanit special RH40, allantois
1 part of element, 1 part of xanthan gum, 0.2 part of carragheen, 10 parts of licorice extract, 5 parts of papaya extractives, 2 parts of citric acid, Goat Placenta antioxygen
1 part of peptide of change, 0.1 part of methylparaben, 0.1 part of essence, 20 parts of deionized water.
A kind of preparation method of Goat Placenta polypeptide women facial mask liquid, comprises the following steps:
S1, fresh Goat Placenta is thawed, is rinsed, is shredded with physiological saline, removed fascia and blood vessel, pass through high shear dispersion
Mulser prepares homogenate, and multigelation 3 times, refrigerated centrifuge.It collects precipitating to be freeze-dried, the sample after freeze-drying crushes
Machine rubs, and crosses 60 meshes, collects the powder of filtration；400g Goat Placenta leftover bits and pieces powder is weighed, distilled water is added to be made into 300g/L's
Substrate solution is adjusted to pH=6.5, and Mixed enzyme for animal proteolysis is added and digests 4h, enzyme additive amount is 5000U/g；Enzymatic hydrolysis knot
It is warming up to 90 DEG C after beam, 10min is kept to carry out destroy the enzyme treatment, is cooled to 25 DEG C, adjusts pH=6.0, at 1 DEG C, 4000rpm item
It is centrifuged 20min under part, collects supernatant；Under the conditions of 20 DEG C, pH=7, inlet pressure 0.9MPa, outlet pressure 0.55MPa, use
The ultrafiltration membrance filter that 0.45 μm of aperture collects supernatant, spare.
S2, it prepares licorice extract: 10g Radix Glycyrrhizae is crushed, cross 80 meshes, as in 500mL beaker, it is dense that 100mL is added
The hydrochloric acid solution for spending 1mol/L extracts 90min, then four layers of filtered through gauze at 60 DEG C, collects filtrate, and liquid to be filtered is cooled to room
Temperature, the sodium hydroxide solution that 1mol/L is added are adjusted to neutrality, obtain licorice extract, spare.
S3, papaya extractives are prepared: pawpaw is removed the peel into deseeding, cleaned, the water of 5 times of weight is added, is smashed to pieces with blender；It presses
750u/g ratio crushes in liquid to pawpaw and pectase is added, and then 45 DEG C of condition digests 5h, heat temperature raising after enzymatic hydrolysis again
To 100 DEG C, 15min is kept the temperature, enzyme deactivation is living, is separated by solid-liquid separation after being cooled to room temperature, and filtrate is collected, and centrifugation takes supernatant, adjusts pH
Value is concentrated to 6.0, is drying to obtain papaya extractives.
S4, preparation water phase: glycerol 5g, propylene glycol are added into beaker in beaker for precise 100g deionized water
100g, glycine betaine 10g, EDTA-2 sodium 0.1g, trehalose 2g, rilanit special RH40 36g, allantoin 10g, beaker is put into
In water-bath, under the conditions of 85 DEG C of bath temperature, mixing speed 150rpm, 10min is mixed, water phase is made.
S5, prepare oily phase: precise formula provide the xanthan gum 10g of deal, carragheen 2g, licorice extract 100g,
Papaya extractives 50g and citric acid 20g are 80 DEG C in bath temperature in beaker, under the conditions of mixing speed 150rpm, stirring
10min, 80 DEG C of heat preservation 5h, is made oily phase.
S6, preparation function phase: the anti-oxidation peptide nutrition of 10g Goat Placenta is added in beaker in precise 100g deionized water
Liquid and 80g granularity are 45~48 μm of DE soy bean edible fiber powders, are 50 DEG C in bath temperature, under the conditions of mixing speed 150rpm,
15min is stirred, 2h is stood, function phase is made.
S7, prepare asperities film liquid: oil phase made from step S5 is heated to 80 DEG C under 150rpm mixing speed, to oily phase
In slowly at the uniform velocity be added step S4 made from water phase, continue under the conditions of revolving speed 150rpm stir 10min, be then cooled to 40
DEG C, it is added step S6 obtained function phase, 1g methylparaben and 1g essence, under the conditions of low whipping speed 150rpm, stirring
10min obtains asperities film liquid.
S8, preparation facial mask liquid: at 50 DEG C, under the conditions of 15000rpm, homogeneous 5min both obtains facial mask liquid.
Embodiment 3:
A kind of Goat Placenta polypeptide women facial mask liquid includes the ingredient of following parts by weight: 10 parts of glycerol, soy bean edible fiber powder
10 parts, 1 part of propylene glycol, 10 parts of glycine betaine, 0.01 portion of EDTA-2 sodium, 5 parts of trehalose, 1.8 parts of rilanit special RH40, Tween 80
1.8 parts, 5 parts of allantoin, 5 parts of xanthan gum, 0.2 part of carragheen, 5 parts of licorice extract, 10 parts of papaya extractives, 2 parts of citric acid,
1 part of Goat Placenta anti-oxidation peptide, 0.02 part of methylparaben, 0.05 part of essence, 30 parts of deionized water.
A kind of preparation method of Goat Placenta polypeptide women facial mask liquid, comprises the following steps:
S1, fresh Goat Placenta is thawed, is rinsed, is shredded with physiological saline, removed fascia and blood vessel, pass through high shear dispersion
Mulser prepares homogenate, and multigelation 3 times, refrigerated centrifuge.It collects precipitating to be freeze-dried, the sample after freeze-drying crushes
Machine rubs, and crosses 60 meshes, collects the powder of filtration；400g Goat Placenta leftover bits and pieces powder is weighed, distilled water is added to be made into 400g/L's
Substrate solution is adjusted to pH=6.0, and Mixed enzyme for animal proteolysis is added and digests 2h, enzyme additive amount is 4000U/g；Enzymatic hydrolysis knot
It is warming up to 100 DEG C after beam, 10min is kept to carry out destroy the enzyme treatment, be cooled to 25 DEG C, adjust pH=7.0, at 10 DEG C, 4000rpm item
It is centrifuged 20min under part, collects supernatant；Under the conditions of 20 DEG C, pH=7, inlet pressure 0.9MPa, outlet pressure 0.6MPa, use
The ultrafiltration membrance filter that 0.45 μm of aperture collects supernatant, spare.
S2, it prepares licorice extract: 10g Radix Glycyrrhizae is crushed, cross 80 meshes, as in 500mL beaker, it is dense that 100mL is added
The hydrochloric acid solution for spending 1mol/L extracts 90min, then four layers of filtered through gauze at 60 DEG C, collects filtrate, and liquid to be filtered is cooled to room
Temperature, the sodium hydroxide solution that 1mol/L is added are adjusted to neutrality, obtain licorice extract, spare.
S3, papaya extractives are prepared: pawpaw is removed the peel into deseeding, cleaned, the water of 5 times of weight is added, is smashed to pieces with blender；It presses
750u/g ratio crushes in liquid to pawpaw and pectase is added, and then 45 DEG C of condition digests 5h, heat temperature raising after enzymatic hydrolysis again
To 100 DEG C, 15min is kept the temperature, enzyme deactivation is living, is separated by solid-liquid separation after being cooled to room temperature, and filtrate is collected, and centrifugation takes supernatant, adjusts pH
Value is concentrated to 6.0, is drying to obtain papaya extractives.
S4, preparation water phase: glycerol 100g, propylene glycol are added into beaker in beaker for precise 150g deionized water
10g, glycine betaine 100g, EDTA-2 sodium 0.1g, trehalose 50g, rilanit special RH40 18g, Tween 80 18g, allantoin
Beaker is put into water-bath by 50g, under the conditions of 85 DEG C of bath temperature, mixing speed 150rpm, mixes 10min, water is made
Phase.
S5, prepare oily phase: precise formula provides the xanthan gum 50g, carragheen 2g, licorice extract 50g, wood of deal
Melon extract 100g and citric acid 20g are 80 DEG C in bath temperature in beaker, under the conditions of mixing speed 150rpm, stirring
10min, 80 DEG C of heat preservation 5h, is made oily phase.
S6, preparation function phase: the anti-oxidation peptide nutrition of 10g Goat Placenta is added in beaker in precise 150g deionized water
Liquid and 100g granularity are 45~48 μm of DE soy bean edible fiber powders, are 50 DEG C in bath temperature, under the conditions of mixing speed 150rpm,
15min is stirred, 2h is stood, function phase is made.
S7, prepare asperities film liquid: oil phase made from step S5 is heated to 80 DEG C under 150rpm mixing speed, to oily phase
In slowly at the uniform velocity be added step S4 made from water phase, continue under the conditions of revolving speed 150rpm stir 10min, be then cooled to 40
DEG C, it is added step S6 obtained function phase, 0.2g methylparaben and 0.5g essence, under the conditions of low whipping speed 150rpm, stirs
10min is mixed, asperities film liquid is obtained.
S8, preparation facial mask liquid: at 35 DEG C, under the conditions of 12000rpm, homogeneous 5min both obtains facial mask liquid.Randomly select above-mentioned reality
The sample in example is applied, product quality analysis is carried out:
Physicochemical property detection: it is detected according to QB/T 2872-2017 " facial mask " regulation, testing result is shown in Table 1.
Moisturizing, moistening effect evaluation: taking the facial mask liquid of above-mentioned preparation to carry out the measurement of the water content and elasticity of skin of face,
This experiment has randomly selected 30 healthy student enrollment and has tested, and 10 people/group are randomly assigned, and is divided into tri- groups of A, B, C, point
Do not determine their face before non-face mask film, rigid face mask film and after face mask film 1 day, 3 days, 7 days skin it is aqueous
Amount, test result are as shown in Table 2,3.
Facial mask liquid removes DPPH determining free radicals: taking 2m L facial mask liquid that 1mL distilled water and 3mL 0.1mmol/L is added
The ethanol solution of DPPH, solution is mixed, and is protected from light 30min under room temperature, is centrifuged 20min in 4 000rpm after being protected from light
The absorbance A at 517nm is measured afterwardsS；DPPH ethanol solution is replaced to measure absorbance A with dehydrated alcoholX；Use distilled water
Absorbance A is measured instead of enzymolysis liquidC.Measurement result is shown in Table 4.
Facial mask liquid DPPH clearance rate
The physicochemical property of 1 facial mask of table
2 moisture content of skin test result of table
3 skin elasticity test result of table
| Volunteer | Non- face mask film | 1 day after applying | 3 days after applying | 7 days after applying |
| A group | It is general | It is partially soft and fine | It is soft and fine | It is soft and fine |
| B group | It is general | It is general | It is partially soft and fine | It is soft and fine |
| C group | It is general | It is partially soft and fine | It is soft and fine | It is soft and fine |
4 embodiment facial mask liquid of table removes DPPH determining free radicals result
| Embodiment | As | Ax | Ac | SA |
| 1 | 0.195 | 0.001 | 0.357 | 45.63% |
| 2 | 0.199 | 0.001 | 0.356 | 44.25% |
| 3 | 0.198 | 0.002 | 0.357 | 44.93% |
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and the above embodiments and description only describe originals of the invention
Reason, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes and improvements
It all fall within the protetion scope of the claimed invention.The claimed scope of the invention is by appending claims and equivalents circle
It is fixed.
Claims (6)
1. a kind of Goat Placenta polypeptide women facial mask liquid, it is characterised in that: the ingredient comprising following parts by weight:
。
2. a kind of preparation method of Goat Placenta polypeptide women facial mask liquid, which is characterized in that comprise the following steps:
S1, it prepares Goat Placenta anti-oxidation peptide liquid: fresh Goat Placenta being thawed, is rinsed with physiological saline, is shredded, remove fascia and blood
Pipe, by high-shearing dispersion emulsifying machine homogenate, multigelation 3 times, refrigerated centrifuge.Precipitating is collected to be freeze-dried,
Sample after freeze-drying is rubbed with pulverizer, is crossed 60 meshes, is collected the powder of filtration；30~40g Goat Placenta leftover bits and pieces powder is weighed,
Add distilled water to be made into the substrate solution of 30~40g/L, be adjusted to pH=6.0~7.0, Mixed enzyme for animal proteolysis enzymatic hydrolysis is added
1~4h, enzyme additive amount are 4000~5000U/g；It is warming up to 90~100 DEG C after enzymatic hydrolysis, 10min is kept to carry out at enzyme deactivation
Reason, is cooled to 25 DEG C, adjusts pH=6.0~7.5, is centrifuged 20min under the conditions of 1~10 DEG C and 3500~4000rpm, in collection
Clear liquid；Under the conditions of 20-30 DEG C, pH=7,0.9~0.8MPa of inlet pressure, 0.6~0.5MPa of outlet pressure, with ultrafiltration membrane mistake
Supernatant is collected in filter, and the Goat Placenta anti-oxidation peptide liquid rich in function factors such as various amino acid is made.
S2, it prepares licorice extract: Radix Glycyrrhizae is crushed, cross 80 meshes, at 60 DEG C, under conditions of feed liquid mass ratio is 1:10, use
The hydrochloric acid solution that concentration is 1mol/L extracts 90min, four layers of filtered through gauze, and liquid to be filtered is cooled to room temperature, and the hydrogen of 1mol/L is added
Sodium hydroxide solution is adjusted to neutrality, obtains licorice extract.
S3, papaya extractives are prepared: pawpaw is removed the peel into deseeding, cleaned, the water of 5 times of weight is added, is smashed to pieces with blender；It presses
750u/g ratio crushes in liquid to pawpaw and pectase is added, and then 45 DEG C of condition digests 5h, heat temperature raising after enzymatic hydrolysis again
To 90~100 DEG C, 15min is kept the temperature, enzyme deactivation is living, is separated by solid-liquid separation after being cooled to room temperature, and filtrate is collected, and centrifugation takes supernatant,
It adjusts pH value to 6.0, is concentrated, is drying to obtain papaya extractives.
S4, preparation water phase: precise half is formulated the deionized water of deal in beaker, and formula regulation part is added into beaker
Glycerol, propylene glycol, glycine betaine, EDTA-2 sodium, trehalose, the emulsifier, allantoin of amount, beaker are put into water-bath, in water
85 DEG C of bath temperature, under the conditions of mixing speed 150rpm, 10min is mixed, water phase is made.
S5, prepare oily phase: precise formula provides xanthan gum, carragheen, licorice extract, papaya extractives and the lemon of deal
Lemon acid is 80 DEG C in bath temperature, under the conditions of mixing speed 150rpm, stirs 10min, 80 DEG C of heat preservation 5h are made in beaker
Oily phase.
S6, preparation function phase: Goat Placenta anti-oxidation peptide nutrient solution is added in beaker in the deionized water of precise half deal
And soy bean edible fiber powder, it is 50 DEG C in bath temperature, under the conditions of mixing speed 150rpm, stirs 15min, stand 2h, be made
Function phase.
S7, prepare asperities film liquid: oil phase made from step S5 is heated to 80 DEG C under 150rpm mixing speed, to oily Xiang Zhonghuan
Slowly water phase made from step S4 is at the uniform velocity added, continues to stir 10min under the conditions of revolving speed 150rpm, is then cooled to 30~40
DEG C, it is added step S6 obtained function phase, methylparaben and essence, under the conditions of low whipping speed 150rpm, stirs 10min,
Obtain asperities film liquid.
S8, preparation facial mask liquid: at 30~50 DEG C, under the conditions of 10000~15000rpm, 5~15min of homogeneous both obtains facial mask liquid.
3. a kind of Goat Placenta polypeptide women facial mask liquid described in claim 1, it is characterised in that: emulsifier is Tween 80 or hydrogenation
The mixture of castor oil RH40 or both.
4. a kind of Goat Placenta polypeptide women facial mask liquid as claimed in claim 3, it is characterised in that: the mass ratio of two kinds of emulsifiers is
1:2。
5. a kind of preparation method of Goat Placenta polypeptide women facial mask liquid as claimed in claim 2, it is characterised in that: described in step S1
Ultrafiltration membrane aperture is 0.45 μm.
6. a kind of preparation method of Goat Placenta polypeptide women facial mask liquid as claimed in claim 2, it is characterised in that: described in step S6
Soy bean edible fiber powder granularity is 45~48 μm.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110292554A (en) * | 2019-06-17 | 2019-10-01 | 海南新生命干细胞医疗有限公司 | A kind of cosmetics and preparation method thereof containing placenta tissue extract |
| CN114886790A (en) * | 2022-04-20 | 2022-08-12 | 叶春兰 | Anti-wrinkle and anti-aging essence emulsion |
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| CN108096113A (en) * | 2018-01-17 | 2018-06-01 | 王清秀 | Goat Placenta-peptide composition, the facial mask liquid containing the Goat Placenta-peptide composition |
| CN108653136A (en) * | 2018-06-26 | 2018-10-16 | 戴伟 | A kind of Chinese medicine composition and its mixed extract being used for cosmetics frost breast and facial mask |
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| CN107308090A (en) * | 2017-06-15 | 2017-11-03 | 安徽吉乃尔电器科技有限公司 | A kind of preparation method of the anti-oxidant emulsion of Goat Placenta |
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| CN108653136A (en) * | 2018-06-26 | 2018-10-16 | 戴伟 | A kind of Chinese medicine composition and its mixed extract being used for cosmetics frost breast and facial mask |
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Application publication date: 20190528 |