CN105832648A - Skin-nourishing anti-aging peony seed oil face mask and manufacturing method thereof - Google Patents

Skin-nourishing anti-aging peony seed oil face mask and manufacturing method thereof Download PDF

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Publication number
CN105832648A
CN105832648A CN201610234516.1A CN201610234516A CN105832648A CN 105832648 A CN105832648 A CN 105832648A CN 201610234516 A CN201610234516 A CN 201610234516A CN 105832648 A CN105832648 A CN 105832648A
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China
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seed oil
peony seed
skin
aging
extract
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CN105832648B (en
Inventor
李秀丽
陈法志
戢小梅
陈镇
杨阳
戴志刚
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Wuhan Academy of Agricultural Sciences
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Fruit Tree Research Institute Of Forestry Science Wuhan Academy Of Agricultural Science & Technology
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations

Abstract

The invention discloses a skin-nourishing anti-aging peony seed oil face mask and a manufacturing method thereof. The face mask is manufactured by using silk face mask paper to fully absorb a face masking liquid and sterilizing the obtained face mask. The face masking liquid is prepared from the following components: peony seed oil, sweet almond oil, an emulsifier, cananga odorata hydrosol, a chamomile extract, a yeast extract, an epidermis deep-penetration water-locking factor, an antiseptic and deionized water. The peony seed oil, sweet almond oil, chamomile extract, epidermis deep-penetration water-locking factor, and the like are mixed to form the face masking liquid having the function of locking water, moistening the skin and resisting oxidation. The face masking liquid containing peony seed oil and sweet almond oil matches the face mask paper for usage. The face mask paper tightly cover the skin to isolate the skin from the outside air and to make water slowly penetrate through the cuticle of the epidermis, thereby promoting the skin to absorb the face masking liquid, quickening the blood microcirculation deep in the skin and improving the activity of cells in each layer of the epidermis. The face mask can prevent water in the face mask from being quickly lost, and has the function of increasing the elasticity of the skin, tightening and lifting the skin, resisting wrinkles and aging, and diminishing inflammation and expelling toxin.

Description

Anti-aging peony seed oil mask sheet of a kind of nourishing and preparation method thereof
Technical field
The invention belongs to daily cosmetics technical field, relate to a kind of nourishing anti-aging cosmetic composition, particularly relate to Anti-aging peony seed oil mask sheet of a kind of nourishing and preparation method thereof.
Background technology
Face is positioned at more than neck, head dead ahead, and face is made up of muscle skeleton and various tissue, be human body Important image embodiment, can be divided into oiliness, neutrality, dryness and anaphylaxis skin quality etc..Owing to skin of face is thin pliable, Springiness, containing more sebaceous glands, sweat gland and hair follicle, Blasius' duct and abundant vasomotor nerve, by outward When boundary stimulates, reaction is the sensitiveest.Society the most now, the time that many working womens works every day before computer is general All at about 10h, cause many skin problems, such as: the colour of skin is obscure, dry, easy produces microgroove etc., work in addition Making pressure big, not free and energy carries out skin care, accelerates the aging of skin.And facial mask is exactly each since ancient times Plant the face beautifying health keeping product that Mrs skin quality commonly uses, except providing the nutrition that skin care item are not provided of skin basis, it is also possible to Excite the maximum vigor of skin at short notice, thus be effectively improved the skin problem of face.
Presently commercially available facial mask is a feast for the eyes, according to different efficacies be divided into moisturizing, Sage Extract, whitening, clean, compact, Anti-aging, facial mask etc. of releiving, but in most products, not only mercury, lead, phenol content exceed standard, and can add a large amount of Thickener, such as materials such as triethanolamine, card ripple, PAA/sodium acryloyldimethyl taurate copolymers, and EDTA chelating agent and the preservative containing Form aldehyde release body, although can temporarily make skin present glossy soft state, but It is thinning that Long-Time Service can make cuticula come off, and causes red swelling of the skin, forms color spot, is unfavorable for skin health.And natural plant Species facial mask is because of its more and more welcomed by the people green, natural, safe, harmless.
CN103784381A discloses a kind of anti-inflammatory facial mask liquid, and described facial mask liquid is extracted by green tea powder, glycerine, cucumber The raw material such as liquid, fresh milk and dried peppermint leaf extract composition, the facial mask liquid prepared can effectively alleviate scytitis, right No skin irritation, it is adaptable to sensitiveness skin.But, this facial mask liquid function singleness, do not meet the requirement of modern.
CN104644510A discloses and a kind of promotes that skin regeneration resists quick facial mask liquid, described facial mask liquid by hyaluronic acid, Trenaxmine, hesperidin methyl, Sensor Chip CM 5, wheat gluten hydrolyzate, lophatherum gracile extract, root of large-flowered skullcap extract, Red sage root extract, ginger extract, extract solution from aloe, mother chrysanthemum extract, bighead atractylodes rhizome extract and 1,2-hexylene glycol Composition.The facial mask liquid prepared from endogenous regulation anti-inflammatory immune system, and can activate the repair ability of skin self, Use rear skin comfort, face's erythema can be improved, be suitable for various people and use.But, this facial mask liquid contains Trenaxmine, Easily there is the phenomenon of dermal toxicity in Long-Time Service, greatly limits the application of this facial mask liquid.
By retrieving domestic and international prior art, the most not yet find the literary composition utilizing peony seed oil and Sweet Almond Oil to prepare mask sheet Offer report, the more needleless efficacy detection technology to relevant mask sheet.
Summary of the invention
In view of the deficiencies in the prior art, it is an object of the invention to provide that a kind of to be available for the nourishing that various skin quality uses anti-aging Peony seed oil mask sheet and preparation method thereof, blank to fill up peony seed oil use in prepared by mask sheet, solution radiation, The various skin problems that the reason such as air pollution, fatigue causes.
In order to realize the purpose of the present invention, inventor, by lot of experiments research persistent exploration, is finally obtained such as next The preparation scheme of the kind anti-aging peony seed oil mask sheet of nourishing:
A kind of nourish anti-aging peony seed oil mask sheet, this mask sheet be silk mask paper is suctioned sterilization after facial mask liquid and , described facial mask liquid is prepared from by following component: peony seed oil, Sweet Almond Oil, emulsifying agent, Yilan hydrosol, ocean Flos Chrysanthemi extract, yeast extract, epidermis deep and thorough lock water fugacity, antiseptic, deionized water.
Preferably, the anti-aging peony seed oil mask sheet of a kind of nourishing as above, the matter of each component in facial mask liquid therein Amount percentage composition is: peony seed oil 0.3%-20%, Sweet Almond Oil 0.3%-20%, emulsifying agent 0.1%-5%, Yilan hydrosol 5%-70%, camomile extract 0.5%-30%, yeast extract 0.1%-10%, epidermis deep and thorough lock water fugacity 0.5%-5%, Antiseptic 0.05%-5%, surplus is deionized water.
Anti-aging peony seed oil mask sheet is nourished it is further preferred that as above a kind of, in facial mask liquid therein each group Point weight/mass percentage composition be: peony seed oil 2.5%, Sweet Almond Oil 2.5%, emulsifying agent 0.5%, Yilan hydrosol 30%, Camomile extract 2%, yeast extract 0.5%, epidermis deep and thorough lock water fugacity 1%, antiseptic 0.2%, surplus is for going Ionized water.
The most preferably, the anti-aging peony seed oil mask sheet of a kind of nourishing as above, emulsifying agent therein is selected from In cetostearyl alcohol, stearyl alcohol phosphate, C9-15 alcohol phosphate, laruyl alcohol phosphate and C20-22 alcohol phosphate extremely Few one.
The most preferably, the anti-aging peony seed oil mask sheet of nourishing as above, camomile extract therein is pressed Following method is prepared from: takes chamomile and adds in extraction kettle, is passed through carbon dioxide with 30-50L/h flow velocity, by 1-2L/h Speed add volumetric concentration be the ethanol of 75%-80%, temperature remain 40-60 DEG C, pressure be 10-15MPa's Under the conditions of extract 2-3h；Obtain chamomile ORGANIC SOLVENT MIXTURES；Put it in decompression low-temperature concentration equipment again, decompression To-0.05-0.05MPa, under the conditions of 45-55 DEG C, reclaim organic solvent, obtain camomile extract.
The most preferably, as above nourish anti-aging peony seed oil mask sheet, epidermis therein deep and thorough lock water because of Son is prepared as follows forming: is a kind of with kylin algae as raw material, utilizes supercritical CO2The red algae being obtained by extraction is oligomeric Sugar concentrates facial mask, and detailed process is that kylin algae adds in extraction kettle after pretreatment, is passed through dioxy with 20-60L/h flow velocity Changing carbon, adding volumetric concentration by the speed of 0.5-3L/h is the ethanol of 70%-90%, remains 30-60 DEG C, pressure in temperature Power is extraction 2-6h under conditions of 8-14MPa；Obtain kylin algae ethanol solvent mixture；Put it into decompression low temperature denseer In contracting equipment, it is depressurized to-0.05-0.05MPa, under the conditions of 40-60 DEG C, reclaims alcohol solvent, obtain kylin algae extract. Kylin algae extract is rich in galactolipin, Anhydrogalactose, multiple mineral element and abundant unrighted acid, especially ω-6 and ω-3 series.There is potent hygroscopicity, it is possible to catch outside moisture, and form water conservation film simultaneously, reduce water Shunting is lost；The synthesis of epidermis deep layer hyaluronic acid can be promoted, possess skin moisturizing and epidermal renewal effect；Can promote Silk polyprotein and the synthesis of tight junction protein 1, increase epidermis compactness, make skin compact dynamic.
The most preferably, the anti-aging peony seed oil mask sheet of nourishing as above, antiseptic therein is sorbic acid Potassium or pungent glycol press the Compositional antiseptic agent of 1:4 composition with pentanediol.
It addition, present invention also offers the preparation method of a kind of above-mentioned nourishing anti-aging peony seed oil mask sheet, the method bag Include following steps:
1) add the peony seed oil of recipe quantity, Sweet Almond Oil and emulsifying agent in a reservoir, stir, be denoted as solution I, Standby；
2) in another container, the deionized water of recipe quantity, Yilan hydrosol, camomile extract, yeast extract are added Lock water fugacity deep and thorough with epidermis, stirs, is denoted as solution II, standby；
3) solution II taking full dose 10%-15% adds in solution I, stirs 4-5min, after causing flocculence material occurs, Adding 20%-25% solution II, continue stirring 4-5min, facial mask liquid is molded, and adds remaining solution II, continues stirring Uniformly, standby；
4) in step 3) gained facial mask liquid adds antiseptic, i.e. obtain facial mask liquid after stirring；
5) take clean container again, add step 4) facial mask liquid prepared, silk mask paper is immersed, works as face paper After suctioning facial mask liquid, after being laid under uviol lamp sterilization, facial mask bag vacuum seal can be loaded.
It should be noted that the yeast extract that the present invention relates to is conventional commercial product, it is that yeast cells will after broken wall The wherein extracting such as amino acid, polypeptide, nucleic acid, vitamin, then through biological enzymolysis shear be refined into rich in amino acid, little Molecular peptide, the active skull cap components of nucleotides.Because the main component of yeast is protein, almost account for yeast dry matter Half content, and essential amino acid content is sufficient, especially more compared with the lysine content lacked in cereal. On the other hand, possibly together with substantial amounts of vitamin B1, vitamin B2 and niacin in yeast extract.Yeast is as high Eucaryote, has the gene of a large amount of coded protein to have homology highly with the gene of the coded protein of mammal, The product expressed also has the strongest homology, and therefore the nutritional labeling in yeast extract more can be conducive to human body the most effective Absorption.
It addition, find according to antioxygenic property experimental study, contain 2.5% peony seed oil and 2.5% dessert almond simultaneously The non-oxidizability of the sample 3 of oil is significantly higher than only adds 2.5% peony seed oil sample 2, Yi Jixian without Sweet Almond Oil Write higher than only add 2.5% Sweet Almond Oil without peony seed oil sample 1, peony seed oil and Sweet Almond Oil are added by this explanation When entering in skin care item, both have the collaborative effect removing skin histology excessive free radicals, make the non-oxidizability of product obtain Conspicuousness improves.The invention provides two kinds of specific components by a certain percentage associated with new opplication, it may be assumed that peony seed oil is with sweet Apricot kernel oil is the application in the skin care item of excessive free radicals in skin histology is removed in preparation；Or peony seed oil and Sweet Almond Oil Application in preparation non-oxidizability skin care item；Wherein peony seed oil is 0.5-15:1 with the weight ratio of Sweet Almond Oil, preferably For 0.8-5:1.It is further preferred that described skin care item are peony seed oil mask sheet.
Compared with prior art, the present invention by peony seed oil, Sweet Almond Oil, camomile extract, epidermis deep and thorough lock water because of The materials such as son are mixed to form a kind of lock oxidation resistant facial mask liquid of water moisturizing, and the facial mask liquid containing peony seed oil and Sweet Almond Oil is taken When joining face paper use, face paper wraps up skin tightly, allows skin open with extraneous air barrier, makes moisture content Gently infiltrate through the cuticula of epidermis, promote the skin absorption to facial mask liquid, accelerate the blood microcirculation of deep skin, Adding the vigor of each confluent monolayer cells of epidermis, the moisture content being simultaneously also prevented from film is quickly lost, and increases elasticity of skin, plays tight Cause lifting, wrinkle resistant anti-aging, the effect of anti-inflammatory toxin expelling.Therefore, the nourishing anti-aging peony seed oil facial mask that the present invention relates to Patch has the advantages that
1) it is a kind of mask sheet simply and easily being suitable for any skin quality, is especially suitable for being dried, having microgroove, the colour of skin obscure Skin person uses；
2) facial mask liquid carrier is silk mask, and quality property frivolous, docile is good, and softness, pure natural, water imbibition are strong, Good springiness, it is possible to import nutrient solution layer by layer, effectively facilitates the skin absorption to facial mask liquid, prevents the water in keratoderma Divide evaporation, reduce skin sense of discomfort；
3) facial mask liquid formula adds high-quality moisturizing ingredient, it is possible to intensive moisturizing, persistently moisten；
4) in two kinds of crude vegetals rich in multiple active skull cap components there is synergy, conspicuousness improves skin table Chrotoplast circulatory function, promotes the microcirculation of capillary of skin, the carrying out of anti-lipid peroxidation effect, improves Metabolism, delay skin aging process；
5) this product can improve skin problem by deep enough skin bottom, Long-Time Service, can not only bright color, moreover it is possible to makes Skin taking on a new look from inside to outside；
6) synergy of two kinds of crude vegetals, it is ensured that the moistness of product and non-oxidizability, and conspicuousness reduction oil The addition of phase raw material, thus purchasing of raw materials expense is greatly reduced, and the operability of this formula is extremely strong, and the suitableeest In factory's mass production.
Accompanying drawing explanation
Fig. 1 is the moisturizing rate curve map nourishing anti-aging peony seed oil facial mask liquid of embodiment 1 preparation；
Fig. 2 is the variable concentrations Vc curve map to DPPH clearance rate；
Fig. 3 is the DPPH clearance rate effect contrast figure of the facial mask liquid of different disposal.
Detailed description of the invention
Technical scheme and technique effect are only described further by the following examples, and limit never in any form The present invention processed.Yilan hydrosol used in the embodiment of the present invention is commercially available organic Yilan hydrosol, and Cananga odorata quintessence oil content is 0.05%；The technical indicator of yeast extract used is as follows: dry 5.33%, ash content 0.87%, albumen 3.4%, Amino acid 2.5%, nucleic acid 1.22%, mannosan 1777ppm, Dextran 8 13ppm, pH4.76, absorbance (410nm) 0.16, As < 0.01ppm, Pb < 0.092ppm, Hg < 0.00853ppm, total plate count < 10cfu/mL.In embodiment The part by weight of the raw material being previously mentioned can make the appropriate adjustments.
Embodiment 1: the preparation of camomile extract
Taking chamomile to add in extraction kettle, be passed through carbon dioxide with 30L/h flow velocity, adding volumetric concentration by 1L/h is 75% Ethanol, temperature remain 40 DEG C, pressure be 10MPa under conditions of extract 2h；Extract is put into pillar separate Still separates, obtains chamomile ORGANIC SOLVENT MIXTURES；Put it into again in decompression low-temperature concentration equipment, be depressurized to 0.01 MPa, reclaims organic solvent under the conditions of 50 DEG C, obtains camomile extract.
Embodiment 2: the preparation of epidermis deep and thorough lock water fugacity
With kylin algae as raw material, add in extraction kettle, be passed through carbon dioxide with 35L/h flow velocity, add by the speed of 1.2L/h Volumetric concentration is the ethanol of 80%, temperature remain 42 DEG C, pressure be 11MPa under conditions of extract 3h；By extract Put in pillar separating still and separate, obtain kylin algae ethanol solvent mixture；Put it in decompression low-temperature concentration equipment again, It is depressurized to 0.01MPa, under the conditions of 50 DEG C, reclaims alcohol solvent, obtain kylin algae extract.
Embodiment 3: nourish the preparation of anti-aging peony seed oil mask sheet
A kind of nourishing anti-aging peony seed oil mask sheet, its component and the weight percentage of each component thereof are shown in Table 1:
Table 1 nourishes anti-aging peony seed oil facial mask liquid formula 1
Preparation method is as follows:
1) carry out vessel sterilization with the alcohol of 75%, or carry out disinfection with ultraviolet irradiation 30min；
2) in the beaker of 100mL, add peony seed oil 2.5g, Sweet Almond Oil 2.5g, cetostearyl alcohol 0.5g, stir Mix uniformly, be denoted as solution I, standby；
3) in another beaker, add deionized water 60.8g, Yilan hydrosol 30g, camomile extract 2g, yeast extraction Liquid 0.5g, kylin algae extract 1g, stir, be denoted as solution II, standby；
4) take 10mL solution II and add in full dose solution I, stir 4-5min, after causing flocculence material occurs, add 20mL solution II, continues stirring 5min, facial mask liquid basic forming, adds remaining solution II, continue to stir, Standby；
5) in step 4) gained facial mask liquid adds antiseptic, i.e. obtain facial mask liquid after stirring.
6) take 1, clean beaker, add the above-mentioned facial mask liquid of 10-15mL, a piece of silk mask is immersed, works as facial mask After paper suctions facial mask liquid, after being laid under uviol lamp sterilization 30min, facial mask bag vacuum seal can be loaded.
Embodiment 4: nourish the preparation of anti-aging peony seed oil mask sheet
A kind of containing nourishing anti-aging peony seed oil mask sheet, its component and the weight percentage of each component thereof are shown in Table 2:
Table 2 nourishes anti-aging peony seed oil facial mask liquid formula 2
After the part by weight of raw material makes the appropriate adjustments, prepare facial mask according to embodiment 1 preparation method.
Embodiment 5: nourish the preparation of anti-aging peony seed oil mask sheet
The anti-aging peony seed oil mask sheet of a kind of nourishing, its component and the weight percentage such as table 3 below of each component thereof:
Table 3 nourishes anti-aging peony seed oil facial mask liquid formula 3
After the part by weight of raw material makes the appropriate adjustments, prepare facial mask according to embodiment 1 preparation method.
Embodiment 6: product apparent property is observed
Select the nourishing anti-aging peony seed oil mask sheet of embodiment 3 preparation, and observe its apparent index, result such as table 4, Result shows: product odour and stability are preferable, and pH value is 5.5, belongs to faintly acid, is especially suitable for Asians's skin (mean ph value is about 5.8), skin can be made to be in optimal nutrient absorption state.
The Apparent character nourishing anti-aging peony seed oil mask sheet of table 4 embodiment 3 preparation
Embodiment 7: product moisture retention determination test
Select the nourishing anti-aging peony seed oil mask sheet of embodiment 3 preparation, and test its moisture retention.According to Deng Yiqing " 4 Kind of marine shellfish polysaccharide extracts and moisture retention is studied " method in document, slightly modified, specific as follows: to use silica gel to do Dry device, environment temperature is 20 DEG C.Take facial mask liquid 1mL containing 2.5% peony seed oil and 2.5% Sweet Almond Oil and be placed in EP pipe In, its quality of accurate weighing is denoted as H0, be placed in drier, place 1,2,3,4,5,6,7, after 23h again Weigh, be denoted as Hn, moisturizing rate computing formula is as follows: moisturizing rate (%)=Hn/H0× 100%, in formula: H0Contain for sample Water quality, HnFor sample after placing n h containing water quality.
Experimental result is added up as shown in Figure 1.It will be seen from figure 1 that the moisture retention of this kind of facial mask liquid is after 7h, remain able to Reaching 99.1%, after 23h, moisturizing rate is also up to 97.7%, and moisture retention is far above " moisture-absorbing moisture-keepings of laminine such as Kong Hexin Property and dynamics research " NMF L lysine HCL (moisturizing rate: 87.6%) conventional in the skin care item mentioned in document With glycerine (moisturizing rate: 96%).
Embodiment 8: product non-oxidizability determination test
Select the nourishing anti-aging peony seed oil mask sheet of embodiment 3 preparation, and test its non-oxidizability.For more fully Whether assessment peony seed oil and Sweet Almond Oil exist synergy, introduce vitamin C (Vitamin c, Vc) conduct comparison, The research variable concentrations Vc impact on DPPH clearance rate；Design 3 process, only add 2.5% Sweet Almond Oil (processing 1) (use aliquots of deionized water replace peony seed oil), only add 2.5% peony seed oil (processing 2) (use equivalent go from Sub-water replaces Sweet Almond Oil) and add 2.5% peony seed oil and 2.5% Sweet Almond Oil (processing 3), research difference does not processes Between the otherness of DPPH clearance rate.With reference to " Antioxidative properties of xanthan on the such as Shimada Autoxidation of soybean oil in cyclodextrin " method mentioned in document, slightly modified, specific as follows: to take 2mL sample solution adds in EP pipe, adds people 2mL 0.5mmol L-1DPPH ethanol solution, lucifuge is black at room temperature Dark place reaction 30min, observes the change of its color, determines have the ascorbic of identical antioxidation according to this color Concentration.Take 2mL vitamin c solution to add in EP pipe, add people 2mL0.5mmol L-1DPPH ethanol solution；Take 2mL The ethanol solution of 70% adds in EP pipe, adds people 2mL 0.5mmol L-1DPPH ethanol solution, lucifuge exists at room temperature Reacting 30min at Hei An, the ethanol solution using 70%, as blank, measures absorbance (A at 525nm525), point It is not denoted as ASampleAnd AComparison.Each concentration is repeated 3 times tests to ensure the accuracy of experimental result, conduct of finally averaging Fitting data.DPPH clearance rate computing formula is as follows: DPPH clearance rate (%)=(1-ASample/AComparison)×100.Color is the most shallow, DPPH clearance rate is the highest, and non-oxidizability is the strongest.
Experimental result is as shown in Figures 2 and 3.Fig. 2 shows: when Vc concentration is less than 0.11mg/mL, DPPH removes With the increase of Vc concentration, conspicuousness strengthens rate, and linear relationship between the two can be come with y=25.764x+13.144 Represent, coefficient R2Can reach 0.9998；When Vc concentration is more than 0.11mg/mL, although DPPH clearance rate Also strengthen with the increase of Vc concentration, and significant difference occurs, but lie substantially in plateau, i.e. DPPH's Clearance rate is all more than 90%, and often increases one percentage point (such as: bring up to 92.3% from 90.6%), about needs to increase The Vc consumption adding 5 times can be only achieved this effect.The above results shows: the height of anti-oxidant degree be not anti-oxidant because of The simple addition of sub-pitch-based sphere, but there is increasingly complex relation, needs to carry out Comprehensive Assessment, and the most accurately Evaluate the standard of its non-oxidizability be DPPH clearance rate whether reach 90% or more than.In conjunction with information above, analyze 3 The difference (see Fig. 3) of DPPH clearance rate under the conditions of different disposal, result shows: process the non-oxidizability (76.3%) of 2 Conspicuousness is higher than the non-oxidizability of process 1 (48.8%), and the non-oxidizability of process 1 and 2 is below 80%, shows The non-oxidizability conspicuousness of peony seed oil is higher than the non-oxidizability of Sweet Almond Oil；The non-oxidizability (95.7%) of process 3 shows Work property, higher than processing 1 and processing the non-oxidizability of 2, reaches more than 95%, in conjunction with to variable concentrations Vc and non-oxidizability Between relationship analysis it can be seen that now the non-oxidizability of product reached plateau, if non-oxidizability reaches 95.7%, Being accomplished by the vegetable oil consumption at least increased by 500, this most fully shows that peony seed oil can effectively be assisted with Sweet Almond Oil Same-action, conspicuousness improves the facial mask clearance rate to free radical, thus effectively strengthens the non-oxidizability of product.
Embodiment 9: product beta test is tested
Select the nourishing anti-aging peony seed oil mask sheet of embodiment 3 preparation, test its trial effect.This mask sheet is divided Try out the Ms of 20 to 50 years old to 30 ages, it is stipulated that use 2 times weekly, after 4 weeks on probation, fill in trial effect feedback Table.Trial effect statistics is as shown in table 5:
The trial state nourishing anti-aging peony seed oil mask sheet of table 5 embodiment 3 preparation

Claims (10)

1. one kind is nourished anti-aging peony seed oil mask sheet, it is characterised in that this mask sheet is that silk mask paper is suctioned facial mask liquid Rear sterilization and obtain, described facial mask liquid is prepared from by following component: peony seed oil, Sweet Almond Oil, emulsifying agent, Yilan hydrosol, Camomile extract, yeast extract, epidermis deep and thorough lock water fugacity, antiseptic, deionized water.
Nourishing the most according to claim 1 anti-aging peony seed oil mask sheet, it is characterised in that in described facial mask liquid The weight/mass percentage composition of each component is: peony seed oil 0.3%-20%, Sweet Almond Oil 0.3%-20%, emulsifying agent 0.1%-5%, depend on Blue hydrosol 5%-70%, camomile extract 0.5%-30%, yeast extract 0.1%-10%, epidermis deep and thorough lock water fugacity 0.5%-5%, antiseptic 0.05%-5%, surplus is deionized water.
Nourishing the most according to claim 2 anti-aging peony seed oil mask sheet, it is characterised in that in described facial mask liquid The weight/mass percentage composition of each component is: peony seed oil 2.5%, Sweet Almond Oil 2.5%, emulsifying agent 0.5%, Yilan hydrosol 30%, Camomile extract 2%, yeast extract 0.5%, epidermis deep and thorough lock water fugacity 1%, antiseptic 0.2%, surplus is deionization Water.
4. according to the nourishing anti-aging peony seed oil mask sheet described in claim 1 or 2 or 3, it is characterised in that described Emulsifying agent is selected from cetostearyl alcohol, stearyl alcohol phosphate, C9-15 alcohol phosphate, laruyl alcohol phosphate and C20-22 alcohol phosphate In at least one.
5. according to the nourishing anti-aging peony seed oil mask sheet described in claim 1 or 2 or 3, it is characterised in that described Camomile extract is prepared as follows forming: takes chamomile and adds in extraction kettle, is passed through carbon dioxide with 30-50L/h flow velocity, By 1-2L/h speed add volumetric concentration be the ethanol of 75%-80%, temperature remain 40-60 DEG C, pressure be 10-15MPa Under conditions of extract 2-3h；Obtain chamomile ORGANIC SOLVENT MIXTURES；Put it into again in decompression low-temperature concentration equipment, be depressurized to -0.05-0.05MPa, reclaims organic solvent under the conditions of 45-55 DEG C, obtains camomile extract.
6. according to the nourishing anti-aging peony seed oil mask sheet described in claim 1 or 2 or 3, it is characterised in that described Epidermis deep and thorough lock water fugacity is prepared as follows forming: with kylin algae as raw material, adds in extraction kettle, with 20-60L/h flow velocity Be passed through carbon dioxide, by 0.5-3L/h speed add volumetric concentration be the ethanol of 70%-90%, temperature remain 30-60 DEG C, Pressure is extraction 2-6h under conditions of 8-14MPa；Obtain kylin algae ethanol solvent mixture；Put it into decompression low temperature again to concentrate In equipment, it is depressurized to-0.05-0.05MPa, under the conditions of 40-60 DEG C, reclaims alcohol solvent, obtain kylin algae extract, be table Skin deep and thorough lock water fugacity.
7. according to the nourishing anti-aging peony seed oil mask sheet described in claim 1 or 2 or 3, it is characterised in that described The Compositional antiseptic agent that antiseptic is potassium sorbate or pungent glycol and pentanediol is formed by 1:4.
8. according to claim 1 or 2 or 3, nourish a preparation method for anti-aging peony seed oil mask sheet, its feature Being, the method comprises the steps:
1) add the peony seed oil of recipe quantity, Sweet Almond Oil and emulsifying agent in a reservoir, stir, be denoted as solution I, standby；
2) in another container, the deionized water of recipe quantity, Yilan hydrosol, camomile extract, yeast extract and epidermis are added Deep and thorough lock water fugacity, stirs, and is denoted as solution II, standby；
3) solution II taking full dose 10%-15% adds in solution I, stirs 4-5min, after causing flocculence material occur, adds 20%-25% solution II, continues stirring 4-5min, and Essence is molded, adds remaining solution II, continue to stir, standby；
4) in step 3) gained Essence adds antiseptic, i.e. obtain facial mask liquid after stirring；
5) take clean container again, add step 4) facial mask liquid prepared, silk mask paper is immersed, when face paper suctions After facial mask liquid, after being laid under uviol lamp sterilization, facial mask bag vacuum seal can be loaded.
9. peony seed oil and the Sweet Almond Oil application in the mask sheet of excessive free radicals, wherein tree peony in skin histology is removed in preparation Seed oil is 0.5-15:1, preferably 0.8-5:1 with the weight ratio of Sweet Almond Oil.
10. peony seed oil and the Sweet Almond Oil application in preparation non-oxidizability mask sheet, wherein peony seed oil and Sweet Almond Oil Weight ratio is 0.5-15:1, preferably 0.8-5:1.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106727126A (en) * 2016-12-20 2017-05-31 铜陵凤丹种植科技开发有限责任公司 A kind of peony seed oil facial mask and preparation method thereof
CN109908035A (en) * 2019-04-25 2019-06-21 山西纳安生物科技有限公司 A kind of freckle-removing mask based on peony seed oil
CN112168743A (en) * 2019-07-01 2021-01-05 海南美肽生物科技有限公司 Anti-aging collagen peptide mask liquid and preparation method thereof

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CN103494747A (en) * 2013-10-11 2014-01-08 河南科技大学 Compound peony skin-caring essential oil and preparation method thereof
CN103705414A (en) * 2013-12-12 2014-04-09 诺斯贝尔(中山)无纺日化有限公司 Eye cream customized for Night Cats
CN104800146A (en) * 2015-05-13 2015-07-29 朱敏 Skin-whitening and spot-erasing mask solution, preparation method thereof and skin-whitening and spot-erasing mask

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CN103494747A (en) * 2013-10-11 2014-01-08 河南科技大学 Compound peony skin-caring essential oil and preparation method thereof
CN103705414A (en) * 2013-12-12 2014-04-09 诺斯贝尔(中山)无纺日化有限公司 Eye cream customized for Night Cats
CN104800146A (en) * 2015-05-13 2015-07-29 朱敏 Skin-whitening and spot-erasing mask solution, preparation method thereof and skin-whitening and spot-erasing mask

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106727126A (en) * 2016-12-20 2017-05-31 铜陵凤丹种植科技开发有限责任公司 A kind of peony seed oil facial mask and preparation method thereof
CN109908035A (en) * 2019-04-25 2019-06-21 山西纳安生物科技有限公司 A kind of freckle-removing mask based on peony seed oil
CN112168743A (en) * 2019-07-01 2021-01-05 海南美肽生物科技有限公司 Anti-aging collagen peptide mask liquid and preparation method thereof
CN112168743B (en) * 2019-07-01 2023-08-04 浙江宝韵生物科技有限公司 Anti-aging collagen peptide mask liquid and preparation method thereof

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