CN111374900A - Rose pigment glycoside skin-care fresh flower water and preparation method thereof - Google Patents

Abstract

The invention discloses rose pigment glycoside skin-care fresh flower water and a preparation method thereof. A rose pigment glycoside skin-care fresh flower water is prepared from the following raw materials in parts by weight: 90-92% (weight percentage) of rose pigment glycoside concentrated solution 5-10, aloe extract 2-5, tremella polysaccharide 0.5-3, honey 1-3, vitamin C0.5-1, vitamin E0.5-1, lemon juice 0.5-1, betaine 0.5-1, hyaluronic acid 0.1-0.5, phenoxyethanol/ethylhexyl glycerin 0.1-0.5, birch juice 2-5, xanthan gum 0.1-0.5, and rose flower solution 85-90. The anthocyanin in the rose is effectively protected and utilized, the effects of moisturizing, whitening, moistening, tendering and lightening the skin of people and enhancing the skin elasticity are achieved, and the quality and the skin-care using effect of the invention are improved.

Description

Rose pigment glycoside skin-care fresh flower water and preparation method thereof

Technical Field

The invention belongs to the technical field of cosmetics, and particularly belongs to rose pigment glycoside skin-care fresh flower water and a preparation method thereof.

Background

With the continuous improvement of living standard of people, the skin is sought by every women who love beauty because of the moistening, luster and youth activity, and the skin care is more and more paid more attention by people. At present, the skin of some people has sub-health states, such as dryness, color spots, black skin, wrinkles, allergy and the like, due to fast work rhythm, high living pressure, environmental pollution and abuse of various chemical cosmetics; in order to cope with these skin problems, various skin care products have been used to improve and maintain the skin. However, common skin care products in the market mostly take chemical components as main components, generally meaning skin brightening, skin tendering, skin moistening, moisture retention, water replenishing and melanocyte formation inhibition, but actually are only water infiltration and exudation processes, do not improve living environment of skin cells, do not improve life vitality of skin cells of people, and have poor skin brightening, skin tendering, skin moistening, moisture retention and skin nourishing effects; meanwhile, chemical components for inhibiting the formation of melanocytes added in the skin care product partially remain in skin cells and cause secondary damage to the skin; moreover, although the skin care products prepared by combining similar rose cell sap, rose hydrosol, rose extract and other raw materials have appeared, most of the liquids of the skin care products are products condensed during high-temperature distillation or drying of rose flowers, and the rose anthocyanin (also called anthocyanin) is seriously damaged in the processing process, so that the antioxidant property of the anthocyanin can not be utilized to remove free radicals so as to enhance the activity of skin cells and achieve the purpose of whitening and tendering skin. In addition, in the patent skin care product prepared by combining the rose with other raw materials, anthocyanin in the rose is not protected and utilized, so that the anthocyanin in the rose is oxidized too quickly, and the effects of oxidation resistance and free radical removal of the anthocyanin cannot be realized. Meanwhile, for the existing rose cell sap added when preparing the rose skin lotion, the existing rose cell sap is the liquid evaporated from the rose in the drying process and is the liquid obtained by collecting the rose by a physical method, and the rose flower cell sap belongs to a byproduct when the rose is dried. The setting of time, temperature, humidity and other parameters related to each step of the rose drying method mostly centers on how to shorten the rose drying time, improve the rose drying efficiency, keep the natural color and luster of the rose and enable the color of the dried rose buds and the rose crowns to be consistent inside and outside; the set method for preventing the loss of the nutrient components of energy, protein and carbohydrate contained in the roses and removing the rose wax causes the loss of a large amount of geraniol, citronellol and nerol in the fresh roses, so that the cell fluid of the fresh roses contains extremely small amount of geraniol, citronellol and nerol, and even the document material searched at present does not show the record of the cell fluid of the fresh roses containing geraniol, citronellol and nerol. In addition, the processing equipment and the process for drying the rose flower cause the overproof of microorganisms in the cell sap of the rose flower because the condensation and collection device of the cell sap of the rose flower is an open exhaust fan. Therefore, how to extract anthocyanin from the dried rose flower by taking the dried rose flower as a raw material; how to improve the quality of the fresh rose flower liquid by improving the extraction process of the fresh rose flower liquid, how to effectively protect and utilize anthocyanin in the rose to be compatible with other pure natural plant raw materials, how to prepare the fresh rose pigment glycoside skin-care flower water with the functions of moisturizing, moistening skin, brightening skin, cleaning skin, tendering skin, preventing sun, lightening spots, removing acnes and enhancing skin elasticity, how to keep the natural rose fragrance of the rose pigment glycoside skin-care water, how to improve the quality of the fresh rose pigment glycoside skin-care flower water and the skin-care use effect are the problems which need to be solved at present.

Disclosure of Invention

The invention aims to provide rose pigment glycoside skin-care fresh flower water, and the invention also aims to provide a preparation method of the rose pigment glycoside skin-care fresh flower water. The rose pigment glycoside skin-care fresh flower water prepared by the invention can effectively protect and utilize the anthocyanin in the rose, has the effects of moisturizing, whitening, moistening, tendering and lightening skin of people and enhancing the elasticity of facial skin, and can improve the quality and skin-care use effect of the rose pigment glycoside skin-care fresh flower water; the rose pigment glycoside skin-care fresh flower water prepared by the invention has no toxic or side effect on the skin of people, and is safe and reliable.

The technical scheme of the invention is that rose pigment glycoside skin-care fresh flower water is characterized in that: the composition is prepared from the following raw materials in parts by weight: 90-92% (weight percentage) of rose pigment glycoside concentrated solution 5-10, aloe extract 2-5, tremella polysaccharide 0.5-3, honey 1-3, vitamin C0.5-1, vitamin E0.5-1, lemon juice 0.5-1, betaine 0.5-1, hyaluronic acid 0.1-0.5, phenoxyethanol/ethylhexyl glycerin 0.1-0.5, birch juice 2-5, xanthan gum 0.1-0.5, and fresh rose flower solution 85-90;

the rose anthocyanin concentrated solution is prepared by the following steps: taking 60% (weight percentage) of acidic ethanol (pH value is 1) as an extracting agent, taking 1 part of dried rose flower under the condition that the material-liquid ratio is 1:10-12 (weight portion ratio), taking 10-12 parts of 60% (weight percentage) of acidic ethanol (pH value is 1) and heating to 50-52 ℃, adding 1 part of dried rose flower into 10-12 parts of 60% (weight percentage) of acidic ethanol (pH value is 1) with the temperature of 50-52 ℃, soaking, and leaching for 2-2.5 hours; repeatedly extracting for 3 times, filtering with microfiltration membrane, mixing filtrates, and vacuum concentrating to obtain 90-92% (by weight) rose pigment glycoside concentrated solution; the dry rose flower is a dry corolla of the double-petal rose;

the rose flower liquid is prepared by using rose flower liquid preparation equipment: the rose flower liquid preparation equipment comprises a drying box body and a movable trolley arranged in the drying box body, wherein the drying box body is provided with a sealing door, and further comprises a heat conduction oil furnace, a heat conduction oil output pipeline, a heat conduction oil return pipeline and at least 4 radiators arranged in the drying box body, wherein the heat conduction oil furnace is used for supplying heat to the drying box body; a thermometer and a hygrometer are also arranged on the drying box body; the rose flower liquid condensation and collection device is arranged at the top of the drying box body;

the rose flower liquid condensation collecting device comprises 2 condensers, a hot air circulation exhaust fan, an air exhaust pipeline section and an air supply pipeline section, wherein the hot air circulation exhaust fan is installed at the left position of a drying box body by using a hot air circulation exhaust fan installation seat, the 2 condensers are sequentially installed on a top plate of the drying box body, lower vertical pipeline sections are respectively installed at two sides of the axial lower bottom surface of the 2 condensers, and the other ends of the lower vertical pipeline sections respectively installed at two sides of the axial lower bottom surface of the 2 condensers respectively sequentially penetrate through the top plate of the drying box body and are longitudinally and fixedly installed on the top plate of the drying box body; the middle positions of the axial upper top surfaces of the 2 condensers are respectively provided with an upper vertical pipeline section, the other ends of the upper vertical pipeline sections which are respectively arranged at the middle positions of the axial upper top surfaces of the 2 condensers are respectively and fixedly connected with a horizontal pipeline section in a sealing way, one end of the air exhaust pipeline section is fixedly connected with an air inlet of a hot air circulation exhaust fan in a sealing way, and the other end of the air exhaust pipeline section is fixedly connected with the horizontal pipeline section which is respectively and fixedly connected with the other ends of the upper vertical pipeline sections which are respectively arranged at the middle positions of the axial upper top surfaces of the; one end of the air supply pipeline section is fixedly connected with an air outlet of the hot air circulation air extractor in a sealing way, and the other end of the air supply pipeline section is fixedly connected with an air inlet arranged at the lower part of the side wall of the right side of the drying box body in a sealing way; the rose flower liquid collecting device comprises a rose flower liquid discharging pipeline with a vertical section in an S-shaped bend and a rose flower liquid collecting tank, wherein the rose flower liquid discharging pipeline with the vertical section in the S-shaped bend is provided with a parallel pipeline section away from the vertical section in the S-shaped bend and a vertical pipeline section close to the vertical section in the S-shaped bend; the heat-conducting oil furnace, the installation of the heat-conducting oil furnace and the condenser are all completed by adopting the prior art;

the preparation process of the fresh rose flower liquid comprises the following steps:

step A: when the temperature in the drying box body is regulated and controlled to be increased to 35-40 ℃, a sealing door of the drying box body is opened, the movable trolley filled with fresh rose flowers is pushed in, and the sealing door of the drying box body is closed; a first working stage: the temperature of the drying box body is set to be 35-50 ℃, the humidity value is set to be 50% RH, the heat conduction oil furnace is started, the temperature in the drying box body rises, when the humidity value shows 50% RH, the hot air circulation exhaust fan is opened, the 2 condensers start to work, the gaseous rose flower liquid is condensed and gathered to form liquid through the 2 condensers, and the liquid enters the rose flower liquid collecting tank through the rose flower liquid discharge pipeline with the S-shaped vertical section; the air supply pipeline section fixedly connected with the air outlet of the hot air circulation exhaust fan in a sealing way circularly conveys the circulating air into the drying box body through an air inlet arranged at the lower part of the side wall at the right side of the drying box body; when humidity numerical value is less than 50% RH in the drying cabinet, the heated air circulation air exhauster is closed, 2 condensers stop working, first working phase circulation is reciprocal 10 hours, when humidity numerical value no longer reaches 50% RH in the drying cabinet, gets into the second working phase:

and a second working stage: the temperature in the drying box is set to be 50-60 ℃, the humidity value is set to be 45% RH, when the humidity value in the drying box shows 45% RH, the hot air circulation exhaust fan is opened, the 2 condensers start to work, the gaseous rose flower liquid is condensed and gathered into liquid through the 2 condensers, and the liquid enters the rose flower liquid collecting tank through a rose flower liquid discharge pipeline with an S-shaped vertical section; the air supply pipeline section fixedly connected with the air outlet of the hot air circulation exhaust fan in a sealing way circularly conveys the circulating air into the drying box body through an air inlet arranged at the lower part of the side wall at the right side of the drying box body; when the humidity value in the drying box body is lower than 45% RH, the hot air circulation exhaust fan is closed, and the 2 condensers stop working; the second working phase is circulated for 8 hours, and when the humidity does not reach 45% RH any more, the preparation process of the fresh rose flower liquid is finished;

and B, step: mixing the solutions, filtering with microfiltration membrane, sterilizing at ultrahigh temperature and ultraviolet ray, and storing in 316 stainless steel tank to obtain fresh rose solution;

the lemon juice is prepared by the following steps: taking 100-150 g of fresh lemon, peeling, putting into a juicer for juicing, filtering with a microfiltration membrane, heating to 100 ℃, sterilizing, and cooling to normal temperature for later use.

A preparation method of rose anthocyanin skin-care fresh flower water is characterized by comprising the following steps: the method comprises the following steps:

A. respectively weighing 90-92% (by weight) of rose pigment glycoside concentrated solution, aloe extract, tremella polysaccharide, honey, vitamin C, vitamin E, lemon juice, betaine, hyaluronic acid, phenoxyethanol/ethylhexyl glycerin, birch juice, xanthan gum and fresh rose flower solution according to the weight parts for later use;

B. sequentially adding 90-92% (by weight) of rose pigment glycoside concentrated solution prepared in the step A, honey, vitamin E, betaine, aloe extract, tremella polysaccharide, hyaluronic acid, white birch juice, xanthan gum and fresh rose flower solution into a stainless steel batching barrel, and stirring for 10-15 minutes clockwise and 10-15 minutes anticlockwise; adding vitamin C and lemon juice, and controlling the dosage of vitamin C and lemon juice to ensure that the pH value of the mixed solution added into the stainless steel batching barrel in the step B is between 4.5 and 5.5;

C. adding the phenoxyethanol/ethylhexyl glycerol prepared in the step A into the mixed solution prepared in the step B, and stirring for 10-15 minutes clockwise and anticlockwise respectively; and D, uniformly mixing the phenoxyethanol/ethylhexyl glycerin prepared in the step A and the mixed solution prepared in the step B, filtering by using a diaphragm pump, carrying out pasteurization in a sterile room, preparing the rose pigment glycoside skin moisturizer, and carrying out vacuum packaging, warehousing and normal-temperature storage.

When in use, the rose pigment glycoside skin-care fresh flower water is poured on the cosmetic cotton and is just soaked for later use; face care: washing the face with facial cleanser before sleeping/going out, applying the cosmetic cotton soaked with the rose pigment glycoside skin-care fresh flower water on the face, uniformly pressing or lightly beating for 3 times, and then nursing with essence, lotion, cream/sunscreen cream; nursing hands and feet and other skin parts, namely applying the compressed membrane paper soaked with the rose pigment glycoside skin-care fresh flower water to the hands and the feet and other parts of the skin, and slightly beating the hands and the feet and other parts of the skin after 5-10 minutes until the skin is completely absorbed.

The inventor thinks that:

rose pigment glycoside:

the rose anthocyanin is a natural pigment, is a flavonoid compound extracted from flos Rosae Rugosae, and contains cyanidin-3, 5-diglucoside (Cy-3,5-diglu) and cyanidin-3-glucoside (Cy-3-glu) as main ingredients. The rose pigment glycoside concentrated solution (anthocyanin content 90-92% (weight percentage)) used by the invention takes the dry flower of the double-petal rose as a raw material, adopts a direct extraction mode, and overcomes the technical problem that the existing technology for preparing skin care products by using the rose causes damage and loss of the rose anthocyanin; meanwhile, various components such as citronellol, geraniol and nerol are extracted in the process of extracting the rose anthocyanin, so that the natural fragrance of the rose is maintained; anthocyanins have strong effects of removing free radicals and resisting oxidation, and free radical reaction of oxygen and peroxidation of lipid substances can cause oxidative damage to proteins, fats, nucleic acids and the like in human cells, thereby causing skin cell aging; phenolic hydroxyl in molecular structure of anthocyanin, especially ortho phenolic hydroxyl of catechol and pyrogallol, not only can be combined with protein to prevent peroxidation, but also can provide proton to be combined with lipid free radical to cut off chain reaction of lipid oxidation, thus preventing lipid peroxidation and preventing and treating a plurality of skin diseases caused by free radical; the anthocyanin can inhibit the activity of tyrosinase participating in melanin formation, and prevent melanin and pigmentation caused by ultraviolet; the anthocyanin has effects of inhibiting variation activity of benzopyrene and amino fluorine, and repairing lymph ball in human blood. ("plant anthocyanin" Li Yingchang).

Aloe extract

The aloe extract contains abundant gel elements, and has good permeability to skin. And contains various moisture-retaining components and nutritional components beneficial to human body. Scientific research considers that: because the aloe contains glucose, mannose, uronic acid, calcium, hydrated protease,Biohormones、Hormone (hormone)Protein, protein,Amino acidsVitamins, minerals and other trace elements, thus having the efficacies of nourishing and moisturizing, sun screening, anti-inflammation, hairdressing and hair care and the like, and simultaneously having the remarkable efficacies of softening skin, astringing, preventing and treating acne, preventing pachylosis, diminishing inflammation and relieving itching, protecting hair, keeping skin fine, tender and white and the like. In addition, research has also shown that: the anthraquinone compounds contained in Aloe have skin astringing, softening, moisturizing, antiinflammatory, and bleaching effects. It also has effects in relieving sclerosis and keratinization, improving scar, preventing wrinkle, eye pouch, and cutis laxa, keeping skin moist and delicate, treating skin inflammation, and treating acne, freckle, acne, scald, knife wound, and insect bite. The aloe extract is matched with rose pigment glycoside, so that the permeability of anthocyanin is improved, the activity of skin cells is enhanced, the skin is richer in luster, and the skin brightening and moisturizing effects are more obvious; meanwhile, the rose anthocyanin has better effects of moisturizing, diminishing inflammation and tendering skin by being matched with the aloe extract.

Tremella polysaccharide

The tremella polysaccharide is an acidic heteropolysaccharide obtained from tremella sporophore, the main chain structure of the tremella polysaccharide is mannan connected by α - (1 → 3) glycosidic bonds, the branched chain is composed of glucuronic acid and xylose, and the acidic heteropolysaccharide exists in tremella submerged fermentation sporophytes.

Honey:

the honey contains fructose, glucose, enzyme, protein, vitamins and various minerals. The honey contains vitamin C, vitamin E, flavonoids, phenolic substances, superoxide dismutase and the like, has oxidation resistance, and can eliminate excessive free radicals accumulated in the metabolic process of a human body; the honey contains fructose, glucose, enzyme, protein, vitamins and various minerals, and can improve immunity. The honey and rose pigment glycoside enhance the glucoside environment required by anthocyanin stabilization, and have better effects of oxidation resistance and removal of excessive free radicals accumulated in the metabolic process of facial skin of people. The honey, the aloe extract and the tremella polysaccharide are combined to nourish the skin, moisturize the skin and enhance the effect of keeping the skin thin, tender and white.

Vitamin C

The vitamin C is used as an acidity regulator, provides a specific pH value of 4.5-5.5 for the stability of rose pigment glycoside; the vitamin C has strong oxidation resistance, can prevent dopa from being further oxidized into dopachrome in the reaction of tyrosine-tyrosinase, and can reduce synthesized dopachase into dopa to reduce the synthesis of melanin; the vitamin C can play a role in resisting oxidation and ageing, promote the proliferation of collagen and play a role in resisting wrinkles and ageing; the vitamin C can also help the rose anthocyanin to be free from the damage of ozone and ultraviolet rays, and delay the oxidative decomposition of the rose anthocyanin. The vitamin C is matched with the rose anthocyanin, so that the rose pigment glycoside is effectively protected, the oxidation resistance is enhanced, and the oxidation of the rose pigment glycoside is avoided; meanwhile, the vitamin C is combined with the aloe extract, so that the aloe extract has better effects of promoting skin astringency, moisturizing, preventing small wrinkles, eye bags and skin laxity, keeping the skin moist and delicate, and has enhanced curative effects on skin acnes, freckles and acnes.

Vitamin E:

vitamin E is a very powerful antioxidant, protects cells from free radical damage, and has anti-aging effect. Can effectively resist free radicals, inhibit lipid peroxide generation, and remove chloasma; inhibiting tyrosinase activity, thereby reducing melanin production. It can also eliminate excessive oxygen free radicals caused by ultraviolet rays, air pollution and other external factors, and has the effects of delaying skin aging, preventing sunburn, inhibiting generation of sunburn erythema and the like. Vitamin E is reinforced by the mutual reinforcement of rose anthocyanin, honey and vitamin C, and the effects of oxidation resistance and free radical removal are enhanced; the vitamin E is combined with the rose anthocyanin, the aloe extract and the tremella polysaccharide, has obvious effect of reducing the generation of skin melanin, and has positive effects of nourishing skin, moisturizing and keeping the skin fine, tender and white.

Fresh lemon

The lemon contains citric acid and vitamin C, the lemon juice is used as acidity regulator, and the use amount of the lemon juice and the vitamin C is controlled to provide a specific pH value of 4.5-5.5 for the stability of rose pigment glycoside. The citric acid can remove excessive oil and fat of the skin, has certain astringency to the skin, is rich in vitamin C, has strong oxidation resistance, can prevent dopa from being further oxidized into dopachrome in the reaction of tyrosine-tyrosinase, enables the synthesized dopachrome to be reduced into dopa, and reduces the synthesis of melanin. The vitamin C contained in fructus Citri Limoniae can also help the rose anthocyanin to prevent ozone and ultraviolet ray, and delay the oxidative decomposition of rose anthocyanin. The rose pigment glycoside is effectively protected by the compatibility of the citric acid and the rose pigment glycoside, the oxidation of the rose pigment glycoside is avoided, the oxidation resistance is enhanced, and the effect of reducing the synthesis of skin melanin of people is more obvious; the lemon is combined with the aloe extract and the vitamin C, so that the lemon has better effects of promoting skin astringency, moisturizing, keeping skin moist and tendering.

Betaine

Betaine is a unique moisturizing effect: betaine has the same moisturizing effect as glycerol, but different from the fixed water molecules of glycerol, the betaine allows the water molecules to be completely absorbed and utilized by the whole living cells, the moisturizing mechanism performance of the betaine is superior to that of other moisturizing agents, and the betaine can be used for lasting moisturizing even at low concentration. Secondly, the cell performance is protected: when the skin is subjected to high osmotic pressure of the external environment, a large amount of cell osmolytes are lost, so that the apoptosis is caused. Betaine osmolytes inhibit this process and penetrate through the stratum corneum of the skin to protect the cellular balance. The betaine is matched with the anthocyanin to enhance the stability (attached structure chart) of the anthocyanin through a conjugate effect, and the betaine is matched with the aloe extract, the tremella polysaccharide and the vitamin C to improve the water content of the skin epidermis, moisturize the skin, enable the skin to have good smooth and moist feeling, and have better effects of keeping the skin moist and tender.

Hyaluronic acid

Hyaluronic acid is an acidic mucopolysaccharide, has a special water-retaining effect, is the best natural moisture-retaining substance discovered at present, and is called as idealNatural moisturizing factor(Natural texturing factor, NMF), a 2% pure aqueous solution of hyaluronic acid strongly held 98% water. Hyaluronic acid can form a layer of breathable film on the surface of skin, is a good transdermal absorption enhancer while keeping moisture, makes the skin smooth and moist, can block the invasion of external bacteria, dust and ultraviolet rays, protects the skin from being damaged, and provides a stable environment for anthocyanin to resist oxidation and remove free radicals. The hyaluronic acid, the betaine, the aloe extract, the tremella polysaccharide and the vitamin C are combined to achieve better effects of moisturizing the skin, keeping the skin smooth and moist and tendering; meanwhile, the hyaluronic acid and the lemon can also enhance the rose anthocyanin from being damaged by ozone and ultraviolet rays, delay the oxidative decomposition of the rose pigment glycoside, effectively protect the rose pigment glycoside, avoid the oxidation of the rose anthocyanin, enhance the oxidation resistance and reduce the synthesis effect of skin melanin of people;

phenoxyethanol/ethylhexyl glycerin (PE9010)

The phenoxyethanol/ethylhexyl glycerin is a compound liquid preservative for cosmetics and an ideal humectant, and the surface tension on microbial cell membranes is influenced by the ethylhexyl glycerin, so that the preservative capability of the phenoxyethanol is improved. The phenoxyethanol/ethylhexyl glycerin has good inhibition effect on bacteria, yeasts and molds, is a typical antibacterial and antiseptic product, and also has certain bactericidal capacity. The phenoxyethanol/ethylhexyl glycerin can be combined with aloe extract to enhance the antibacterial, anti-inflammatory and antipruritic effects. Meanwhile, the addition of phenoxyethanol/ethylhexyl glycerin improves the moisturizing and anti-corrosion performance of the rose pigment glycoside skin moisturizer.

Birch sap

Birch sap is named as miraculous sap, is a physiological active water which is recognized in the world at present and is rich in nutrition, and is a source of birch life. Rich in various human body requirementsFructoseAmino acid, amino acid,Vitamin preparationBiotin, biotin,Mineral substanceAnd the like. Contains more than 20 amino acids, 24 kindsInorganic elementsVitamins B1, B2 and vitamin C,polysaccharidesAnd a reducing sugar. The birch sap has unique anti-inflammatory ability, and can isolate external bacterial infection, sterilize and promote cell growth; the birch sap also has antifatigue and antiaging effects; the birch sap also has skin whitening, moisturizing, acne removing, and speckle removing effects. The birch juice is compatible with anthocyanin, so that a needed glucoside environment is provided for anthocyanin stabilization, and the oxidation resistance of anthocyanin is enhanced; the birch juice is combined with the aloe extract and the phenoxyethanol/ethylhexyl glycerin, so that the effects of sterilization, anti-inflammation and itching relieving are better; the birch juice is combined with aloe extract and vitamin C to promote skin whitening, moisture retention, acne removal and freckle removal.

Xanthan gum

The xanthan gum contains a large amount of hydrophilic groups, is a good surface active substance, and has the effects of resisting oxidation, preventing skin aging and the like. The xanthan gum is combined with the aloe extract, the betaine, the tremella polysaccharide and the vitamin C, so that the water content of the skin epidermis is improved, the skin is moisturized, the skin has good smooth and moist feeling, and the skin is kept moist and tender; the xanthan gum and the tremella polysaccharide can promote the immune function of the organism and strengthen the anti-aging function; the xanthan gum is combined with anthocyanin, tremella polysaccharide, hyaluronic acid and betaine, so that the skin moisturizing effect is enhanced, the sustainability of anthocyanin penetration is improved, the oxidation resistance of anthocyanin is enhanced, the activity of skin cells is improved, and the skin wrinkle removing effect is better.

Rose flower liquid:

the fresh rose flower liquid is prepared by the preparation method. The setting of the parameters such as time, temperature, humidity and the like related to each step of preparing the rose flower liquid is set around how to realize the retention of natural aroma components and nutrient components such as geraniol, citronellol, nerol and the like in the rose flower liquid. The rose cell sap is liquid obtained by collecting the liquid evaporated from the petals of the rose or the rose buds in the low-temperature drying process by a physical method; the fresh rose flower cell sap belongs to a by-product when fresh rose flowers are dried at low temperature. The invention discloses equipment for drying roses in a low-temperature circulation manner and a method thereof, and relates to the equipment and the method for drying the roses in the low-temperature circulation manner, wherein the equipment is disclosed with the patent number of 201610783085.4 and the publication number of CN 106247776B, and the invention name is that how to realize the setting of time, temperature, humidity and other parameters related to each step of the method for drying the roses in the low-temperature circulation manner, the invention shortens the drying time of the roses, improves the drying efficiency of the roses, keeps the natural color and luster of the roses and enables the color of dried rosebuds and rosecrowns to be consistent inside and; but also can reduce the loss of energy, protein and carbohydrate nutrients contained in the rose and remove rose wax.

The fresh rose flower liquid is body fluid of fresh rose flowers, and through analysis, the fresh rose flower liquid contains natural aroma components such as geraniol, citronellol and nerol (the content of the natural aroma components such as geraniol, citronellol and nerol in the fresh rose flower liquid is shown in the attached figure 2 of the specification: research detection report of comprehensive inspection and detection center in Pingyin county); the fresh rose flower liquid can activate skin cells, has the effects of moisturizing, tendering and brightening skin, and also has the effects of inhibiting bacteria, resisting bacteria and enhancing human immunity. It is reported that: the fresh rose flower liquid has antiviral effect, can resist oxidation, and can remove DPPH free radical in human body; the fresh rose flower liquid is micromolecule water, is purely natural and easy to absorb, contains natural nutrient components and fragrance of fresh rose flowers, and is called as ' liquid fresh flowers ' and ' skin care products which can be eaten and drunk by people. The fresh rose flower liquid belongs to small molecular water, is beneficial to improving the permeability of the nutrient components of the rose flower liquid to the facial cells of people, and is beneficial to improving the effects of relaxing qi, activating blood, delaying the aging of the facial cells of people and enhancing the beauty maintaining and young keeping. The fresh rose flower liquid is matched with rose anthocyanin, aloe extract, honey, vitamin C and vitamin E, so that the stability and permeability of rose pigment glycoside are improved, the skin brightening and moisturizing effects are enhanced, and the activity of skin cells is improved; the rose flower liquid is matched with tremella polysaccharide and hyaluronic acid, so that the durability of the fragrance components of the rose pigment glycoside skin care water can be improved; the rose flower liquid is matched with the rose anthocyanin, the tremella polysaccharide and the hyaluronic acid, so that the effects of skin brightening, moisture preservation, skin tendering and skin fragrance are enhanced, and meanwhile, the natural fragrance of the rose anthocyanin concentrated solution is stronger; the rose pigment glycoside is added into the rose flower pigment glycoside so that the nutrient components of the rose in the rose pigment glycoside skin care water are more comprehensive; the fragrance of the rose pigment glycoside skin care lotion is improved and maintained, so that the natural fragrance of the rose pigment glycoside skin care lotion is stronger.

The invention has the beneficial effects that: the amount of melanin in skin cells, the activity of skin cells and the water content of stratum corneum of people determine the color, elasticity and smoothness of skin. The rose anthocyanin skin care lotion is prepared from rose pigment glycoside concentrated solution, aloe extract, tremella polysaccharide, honey, vitamin C, vitamin E, lemon juice, betaine, hyaluronic acid, phenoxyethanol/ethylhexyl glycerol, birch juice, xanthan gum and fresh rose flower solution according to the weight part ratio. The rose pigment glycoside is matched with aloe extract, tremella polysaccharide, honey, vitamin C, vitamin E, lemon juice, hyaluronic acid, rose pigment glycoside, aloe extract, tremella polysaccharide, honey, vitamin C, vitamin E, lemon juice and hyaluronic acid to interact, the effect of preventing the rose pigment glycoside from being damaged by ozone and ultraviolet rays is enhanced, the oxidation of the rose pigment glycoside is effectively prevented, the rose pigment glycoside is effectively protected, the sustainability of anthocyanin penetration is enhanced, the stability of the rose pigment glycoside is improved, the oxidation resistance of the rose pigment glycoside is enhanced, and the effect of removing excessive free radicals accumulated in the metabolic process of facial skin of people is better. The rose anthocyanin, the aloe extract, the honey, the vitamin C, the vitamin E and the fresh rose flower liquid are used together, so that the stability and the permeability of the rose anthocyanin are improved, the skin brightening and moisturizing effects of skin are enhanced, the activity of skin cells is improved, the skin is richer in luster, and the skin brightening and moisturizing effects are more obvious; rose pigment glycoside, tremella polysaccharide, honey, hyaluronic acid and xanthan gum are mutually reinforced, so that the effects of skin brightening, moisturizing, oxidation resistance and free radical removal are better; the birch juice is combined with the aloe extract and the phenoxyethanol/ethylhexyl glycerin, so that the effects of sterilization, anti-inflammation and itching relieving are better; the birch juice is combined with the aloe extract and the vitamin C to promote the skin whitening, moisturizing, acne removing and freckle removing effects to be enhanced; the betaine is combined with the aloe extract, the tremella polysaccharide and the vitamin C, so that the moisture content of the skin epidermis is improved, the skin is moisturized, the skin has good smooth and moist feeling, and the skin is kept moist and tender; the rose flower liquid is matched with tremella polysaccharide and hyaluronic acid, so that the durability of the fragrance components of the rose pigment glycoside skin care water can be improved; the fresh rose flower liquid is matched with rose anthocyanin, tremella polysaccharide and hyaluronic acid, so that the effects of brightening, moisturizing, tendering and perfuming the skin are enhanced.

When people use the rose pigment glycoside skin-care fresh flower water to replenish water for skin, active nutritional ingredients such as rose anthocyanin and the like permeate into epidermal cells of a human body along with water, the anthocyanin removes superoxide radical under specific environment, the living environment of skin cells is purified, the life activity of the skin cells is improved, the formation of melanocytes is inhibited, and meanwhile, the rose pigment glycoside skin-care fresh flower water also contains aromatic ingredients such as geraniol, citronellol and nerol; thereby achieving the effects of skin brightening, skin moistening, skin tendering, moisture retention, speckle lightening, acne removing and the like. The rose pigment glycoside skin-care fresh flower water is high in DPPH free radical scavenging capacity, high in anthocyanin content, rich in citronellol, nerol, geraniol and phenethyl alcohol, good in moisture-keeping effect and obvious in whitening effect. The rose pigment glycoside skin-care fresh flower water (DPPH free radical scavenging capacity, anthocyanin content, citronellol, nerol, geraniol and phenethyl alcohol content, a test method of moisturizing effect and whitening effect and data are shown in detection reports of Shandong province analysis test center, and the description is shown in attached figures 3-7); the fresh rose flower liquid is small molecular water extracted from fresh rose flowers at low temperature in a closed circulating state, contains a certain amount of rose essential oil, and is more comprehensive in nutrient components and rich in rose fragrance compared with the fresh rose flower liquid prepared by the existing process. Meanwhile, other raw material components of the rose anthocyanin skin lotion play roles respectively and promote each other, so that the activity of skin cells is enhanced, the moisture of the skin of people is supplemented, the melanin is reduced, the life activity of the skin cells is revived, the effects of lightening spots, preserving moisture, brightening skin and tendering skin are achieved, the elasticity of the skin is enhanced, the effects of resisting wrinkles and delaying skin aging are achieved, and the quality of the rose anthocyanin skin-care fresh flower lotion and the using effects of moisturizing, preserving moisture, brightening skin, moistening skin, tendering skin, lightening spots and removing acnes of the skin are improved; the rose pigment glycoside skin-care fresh flower water prepared by the invention has no toxic or side effect on the skin of people, and is safe and reliable.

Attached: the rose pigment glycoside skin-care fresh flower water detection and test effects of the invention are as follows:

first, description attached figures 3-7: detection report of Shandong province analysis and test center: (I) antioxidant experiment; (II) component content determination: comprises measuring anthocyanin content, and measuring the contents of aroma components citronellol, nerol, geraniol and phenethyl alcohol; (III) measuring the moisturizing effect; (IV) measurement of whitening effect).

Second, 20 volunteers used the rose pigment glycoside skin-care fresh flower water skin complexion, glossiness and color spot test effect

20 test volunteers;

white collar as occupation, female as gender, 20-40 years old;

test part, face, test period, 20 days, test time/frequency: before sleeping at night, the sleep time is once a day;

the trial method comprises the following steps: after cleaning the face, applying the makeup cotton soaked with the rose pigment glycoside skin-care fresh flower water on the face, and gently flapping for 3-5 minutes;

testing an instrument: skin analyzer (the larger the spot test data, the better the spot removing effect)

Statistical table of skin test effect of rose anthocyanin skin-care fresh flower water of 20 volunteers

In summary, the analysis: after the rose anthocyanin skin-care fresh flower lotion is used, the face skin color effect is increased by 6.8 percent (79.35-72.55), the glossiness is increased by 6.85 percent (79.15-72.3), and the color spot effect is increased by 5.4 percent (77.35-71.95).

Drawings

The invention is further explained below with reference to the figures and examples;

FIG. 1 is a schematic view showing the construction of an apparatus for preparing fresh rose liquid according to the present invention;

in the drawings: 1. the flower-like rose flower liquid drying device comprises a drying box body, 2. a movable trolley, 3. a heat conduction oil furnace, 4. a heat conduction oil output pipeline, 5. a heat conduction oil return pipeline, 6. a radiator, 7. a condenser, 8. a hot air circulation exhaust fan, 9. an air exhaust pipeline section, 10. an air supply pipeline section, 11. a rose flower liquid discharge pipeline with an S-shaped vertical section, and 12. a rose flower liquid collecting tank;

FIG. 2 is a research report of the content of natural fragrance components of geraniol, citronellol and nerol in fresh rose liquid detected by the Pingyin county comprehensive testing and detecting center;

FIGS. 3-7 are the skin-care fresh flower water (I) antioxidant test of rose pigment glycoside of the present invention, detected by the Shandong province analysis and test center; (II) component content determination: comprises measuring anthocyanin content, and measuring the contents of aroma components citronellol, nerol, geraniol and phenethyl alcohol; (III) measuring the moisturizing effect; (IV) a report on the measurement of whitening effect.

Detailed Description

The specific implementation mode of the invention is as follows:

in the case of the example 1, the following examples are given,

a rose pigment glycoside skin-care fresh flower water is characterized in that: the composition is prepared from the following raw materials in parts by weight: 90% (weight percentage) of rose pigment glycoside concentrated solution 5, aloe extract 2, tremella polysaccharide 0.5, honey 1, vitamin C0.5, vitamin E0.5, lemon juice 0.5, betaine 0.5, hyaluronic acid 0.1, phenoxyethanol/ethylhexyl glycerin 0.1, birch juice 2, xanthan gum 0.1, and fresh rose flower solution 85;

the rose anthocyanin concentrated solution is prepared by the following steps: taking 60% (weight percentage) of acidic ethanol (pH value is 1) as an extracting agent, taking 1 part of dried rose flower under the condition that the material-liquid ratio is 1:10 (weight portion ratio), taking 10 parts of 60% (weight percentage) of acidic ethanol (pH value is 1) and heating to 50 ℃, adding 1 part of dried rose flower into 10 parts of 60% (weight percentage) of acidic ethanol (pH value is 1) with the temperature of 50 ℃, soaking, and leaching for 2 hours; repeatedly extracting for 3 times, filtering with microfiltration membrane, mixing filtrates, and vacuum concentrating to obtain 90% (by weight) rose pigment glycoside concentrated solution; the dry rose flower is a dry corolla of the double-petal rose;

as shown in fig. 1: the rose flower liquid is prepared by using rose flower liquid preparation equipment: the rose flower liquid preparation equipment comprises a drying box body 1 and a movable trolley 2 arranged in the drying box body 1, wherein the drying box body 1 is provided with a sealing door, and the rose flower liquid preparation equipment also comprises a heat conduction oil furnace 3 for supplying heat to the drying box body, a heat conduction oil output pipeline 4, a heat conduction oil return pipeline 5 and at least 4 radiators 6 arranged in the drying box body 1, one end of the heat conduction oil output pipeline 4 is connected with a heat conduction oil output pipe of the heat conduction oil furnace 3, the other end of the heat conduction oil output pipeline is sequentially connected with the radiators 6 in series, one end of the heat conduction oil return pipeline 5 is connected with an oil outlet of the radiator 6 arranged at the tail end, and the other end of the; a thermometer (not shown in the attached drawings of the specification) and a hygrometer (not shown in the attached drawings of the specification) are also arranged on the drying box body 1; the rose flower liquid condensation and collection device is arranged at the top of the drying box body;

the rose flower liquid condensation collecting device comprises 2 condensers 7, a hot air circulation exhaust fan 8, an air exhaust pipeline section 9 and an air supply pipeline section 10, wherein the hot air circulation exhaust fan 8 is installed at the left side of a drying box body 1 by using a hot air circulation exhaust fan installation seat, the 2 condensers 7 are sequentially installed on a top plate of the drying box body 1, lower vertical pipeline sections are respectively installed at two sides of the axial lower bottom surface of the 2 condensers 7, and the other ends of the lower vertical pipeline sections respectively installed at two sides of the axial lower bottom surface of the 2 condensers 7 respectively sequentially penetrate through the top plate of the drying box body 1 and are longitudinally and fixedly installed on the top plate of the drying box body 1; the middle positions of the axial upper top surfaces of the 2 condensers 7 are respectively provided with an upper vertical pipeline section, the other ends of the upper vertical pipeline sections respectively arranged at the middle positions of the axial upper top surfaces of the 2 condensers 7 are respectively and fixedly connected with a horizontal pipeline section in a sealing way, one end of the air exhaust pipeline section 9 is fixedly connected with an air inlet of a hot air circulation exhaust fan 8 in a sealing way, and the other end of the air exhaust pipeline section is fixedly connected with the horizontal pipeline section respectively arranged at the middle positions of the axial upper top surfaces of the 2 condensers 7 in a sealing way; one end of the air supply pipeline section 10 is fixedly connected with an air outlet of the hot air circulation exhaust fan 8 in a sealing way, and the other end of the air supply pipeline section is fixedly connected with an air inlet arranged at the lower part of the side wall of the right side of the drying box body 1 in a sealing way; the rose flower liquid collecting device comprises a rose flower liquid discharging pipeline 11 with a vertical section in an S-shaped curve, a rose flower liquid collecting tank 12, a rose flower liquid discharging pipeline 11 with a vertical section in an S-shaped curve, a parallel pipeline section far away from the vertical section in an S-shaped curve and a vertical pipeline section close to the vertical section in an S-shaped curve, a parallel pipeline section far away from the vertical section in an S-shaped curve and a pipeline section close to the vertical section in an S-shaped curve, wherein the rose flower liquid discharging pipeline 11 with a vertical section in an S-shaped curve is fixedly connected with pipeline sections which are respectively arranged at the middle positions of the axial lower bottom surfaces of the 2 condensers 7 in a sealing manner, the end part of a section of vertical pipeline section with a vertical section which is S-shaped and is close to the vertical section, which is arranged on the rose flower liquid discharge pipeline 11 with the vertical section which is S-shaped, is inserted into a pot opening of a rose flower liquid collecting pot 12 which is arranged on one side of the drying box body 1 by using a supporting seat; the heat-conducting oil furnace, the installation of the heat-conducting oil furnace and the condenser are all completed by adopting the prior art;

the preparation process of the fresh rose flower liquid comprises the following steps:

step A: when the temperature in the drying box body 1 is regulated and controlled to be raised to 35 ℃, a sealing door of the drying box body 1 is opened, the movable trolley 2 filled with fresh rose flowers is pushed in, and the sealing door of the drying box body 1 is closed; a first working stage: the temperature of the drying box body 1 is set to be 35 ℃, the humidity value is set to be 50% RH, the heat conduction oil furnace 3 is started, the temperature in the drying box body 1 is increased, when the humidity value shows 50% RH, the hot air circulation exhaust fan 8 is opened, the 2 condensers 7 start to work, gaseous rose flower liquid is condensed and gathered to form liquid through the 2 condensers 7, and the liquid enters the rose flower liquid collecting tank 12 through the rose flower liquid discharge pipeline 11 with the S-shaped vertical section; a gas supply pipeline section 10 fixedly connected with a gas outlet of the hot air circulation exhaust fan 8 in a sealing way circularly conveys circulating gas into the drying box body 1 through a gas inlet arranged at the lower part of the side wall at the right side of the drying box body 1; when humidity value is less than 50% RH in the stoving box 1, heated air circulation air exhauster 8 closes, 2 condensers 7 stop working, and first working phase circulation is reciprocal 10 hours, when humidity value no longer reaches 50% RH in the stoving box 1, gets into the second working phase:

and a second working stage: the temperature in the drying box body 1 is set to be 50 ℃, the humidity value is set to be 45% RH, when the humidity value in the drying box body 1 shows 45% RH, the hot air circulation exhaust fan 8 is opened, the 2 condensers 7 start to work, the gaseous rose flower liquid is condensed and gathered by the 2 condensers 7 to form liquid, and the liquid enters the rose flower liquid collecting tank 12 through the rose flower liquid discharge pipeline 11 with the vertical section being S-shaped; a gas supply pipeline section 10 fixedly connected with a gas outlet of the hot air circulation exhaust fan 8 in a sealing way circularly conveys circulating gas into the drying box body 1 through a gas inlet arranged at the lower part of the side wall at the right side of the drying box body 1; when the humidity value in the drying box body 1 is lower than 45% RH, the hot air circulation exhaust fan 8 is closed, and the 2 condensers 7 stop working; the second working phase is circulated for 8 hours, and when the humidity does not reach 45% RH any more, the preparation process of the fresh rose flower liquid is finished;

and B, step: mixing the solutions, filtering with microfiltration membrane, sterilizing at ultrahigh temperature and ultraviolet ray, and storing in 316 stainless steel tank to obtain fresh rose solution;

the lemon juice is prepared by the following steps: peeling 100 g of fresh lemon, juicing in a juicer, filtering with a microfiltration membrane, heating to 100 ℃, sterilizing, and cooling to normal temperature for later use.

A preparation method of rose anthocyanin skin-care fresh flower water is characterized by comprising the following steps: the method comprises the following steps:

A. respectively weighing 90% (by weight) of rose pigment glycoside concentrated solution, aloe extract, tremella polysaccharide, honey, vitamin C, vitamin E, lemon juice, betaine, hyaluronic acid, phenoxyethanol/ethylhexyl glycerol, birch juice, xanthan gum and fresh rose flower solution according to the weight part ratio for later use;

B. sequentially adding 90 percent (weight percentage) of rose pigment glycoside concentrated solution prepared in the step A, honey, vitamin E, betaine, aloe extract, tremella polysaccharide, hyaluronic acid, birch juice, xanthan gum and fresh rose flower solution into a stainless steel batching barrel, and stirring for 10 minutes clockwise and 10 minutes anticlockwise; adding vitamin C and lemon juice, and controlling the dosage of the vitamin C and the lemon juice to ensure that the pH value of the mixed solution added into the stainless steel batching barrel in the step B is between 4.5;

C. adding the phenoxyethanol/ethylhexyl glycerol prepared in the step A into the mixed solution prepared in the step B, and stirring for 10 minutes clockwise and anticlockwise respectively; and D, uniformly mixing the phenoxyethanol/ethylhexyl glycerin prepared in the step A and the mixed solution prepared in the step B, filtering by using a diaphragm pump, carrying out pasteurization in a sterile room, preparing the rose pigment glycoside skin moisturizer, and carrying out vacuum packaging, warehousing and normal-temperature storage.

In the case of the example 2, the following examples are given,

a rose pigment glycoside skin-care fresh flower water is characterized in that: the composition is prepared from the following raw materials in parts by weight: 92% (weight percentage) of rose anthocyanin concentrated solution 10, aloe extract 5, tremella polysaccharide 3, honey 3, vitamin C1, vitamin E1, lemon juice 1, betaine 1, hyaluronic acid 0.5, phenoxyethanol/ethylhexyl glycerin 0.5, birch juice 5, xanthan gum 0.5 and fresh rose flower solution 90;

the rose anthocyanin concentrated solution is prepared by the following steps: taking 60% (weight percentage) of acidic ethanol (pH value is 1) as an extracting agent, taking 1 part of dried rose flower under the condition that the material-liquid ratio is 1:12 (weight portion ratio), taking 60% (weight percentage) of acidic ethanol (pH value is 1)12 parts, heating to 52 ℃, adding 1 part of dried rose flower into 12 parts of 60% (weight percentage) of acidic ethanol (pH value is 1) with the temperature of 2 ℃, soaking, and leaching for 2.5 hours; repeatedly extracting for 3 times, filtering with microfiltration membrane, mixing filtrates, and vacuum concentrating to obtain 92% (by weight) rose pigment glycoside concentrated solution; the dry rose flower is a dry corolla of the double-petal rose;

as shown in fig. 1: the rose flower liquid is prepared by using rose flower liquid preparation equipment: the rose flower liquid preparation equipment comprises a drying box body 1 and a movable trolley 2 arranged in the drying box body 1, wherein the drying box body 1 is provided with a sealing door, and the rose flower liquid preparation equipment also comprises a heat conduction oil furnace 3 for supplying heat to the drying box body, a heat conduction oil output pipeline 4, a heat conduction oil return pipeline 5 and at least 4 radiators 6 arranged in the drying box body 1, one end of the heat conduction oil output pipeline 4 is connected with a heat conduction oil output pipe of the heat conduction oil furnace 3, the other end of the heat conduction oil output pipeline is sequentially connected with the radiators 6 in series, one end of the heat conduction oil return pipeline 5 is connected with an oil outlet of the radiator 6 arranged at the tail end, and the other end of the; a thermometer (not shown in the attached drawings of the specification) and a hygrometer (not shown in the attached drawings of the specification) are also arranged on the drying box body 1; the rose flower liquid condensation and collection device is arranged at the top of the drying box body;

the rose flower liquid condensation collecting device comprises 2 condensers 7, a hot air circulation exhaust fan 8, an air exhaust pipeline section 9 and an air supply pipeline section 10, wherein the hot air circulation exhaust fan 8 is installed at the left side of a drying box body 1 by using a hot air circulation exhaust fan installation seat, the 2 condensers 7 are sequentially installed on a top plate of the drying box body 1, lower vertical pipeline sections are respectively installed at two sides of the axial lower bottom surface of the 2 condensers 7, and the other ends of the lower vertical pipeline sections respectively installed at two sides of the axial lower bottom surface of the 2 condensers 7 respectively sequentially penetrate through the top plate of the drying box body 1 and are longitudinally and fixedly installed on the top plate of the drying box body 1; the middle positions of the axial upper top surfaces of the 2 condensers 7 are respectively provided with an upper vertical pipeline section, the other ends of the upper vertical pipeline sections respectively arranged at the middle positions of the axial upper top surfaces of the 2 condensers 7 are respectively and fixedly connected with a horizontal pipeline section in a sealing way, one end of the air exhaust pipeline section 9 is fixedly connected with an air inlet of a hot air circulation exhaust fan 8 in a sealing way, and the other end of the air exhaust pipeline section is fixedly connected with the horizontal pipeline section respectively arranged at the middle positions of the axial upper top surfaces of the 2 condensers 7 in a sealing way; one end of the air supply pipeline section 10 is fixedly connected with an air outlet of the hot air circulation exhaust fan 8 in a sealing way, and the other end of the air supply pipeline section is fixedly connected with an air inlet arranged at the lower part of the side wall of the right side of the drying box body 1 in a sealing way; the rose flower liquid collecting device comprises a rose flower liquid discharging pipeline 11 with a vertical section in an S-shaped curve, a rose flower liquid collecting tank 12, a rose flower liquid discharging pipeline 11 with a vertical section in an S-shaped curve, a parallel pipeline section far away from the vertical section in an S-shaped curve and a vertical pipeline section close to the vertical section in an S-shaped curve, a parallel pipeline section far away from the vertical section in an S-shaped curve and a pipeline section close to the vertical section in an S-shaped curve, wherein the rose flower liquid discharging pipeline 11 with a vertical section in an S-shaped curve is fixedly connected with pipeline sections which are respectively arranged at the middle positions of the axial lower bottom surfaces of the 2 condensers 7 in a sealing manner, the end part of a section of vertical pipeline section with a vertical section which is S-shaped and is close to the vertical section, which is arranged on the rose flower liquid discharge pipeline 11 with the vertical section which is S-shaped, is inserted into a pot opening of a rose flower liquid collecting pot 12 which is arranged on one side of the drying box body 1 by using a supporting seat; the heat-conducting oil furnace, the installation of the heat-conducting oil furnace and the condenser are all completed by adopting the prior art;

the preparation process of the fresh rose flower liquid comprises the following steps:

step A: when the temperature in the drying box body 1 is regulated and controlled to be raised to 40 ℃, a sealing door of the drying box body 1 is opened, the movable trolley 2 filled with fresh rose flowers is pushed in, and the sealing door of the drying box body 1 is closed; a first working stage: the temperature of the drying box body 1 is set to be 50 ℃, the humidity value is set to be 50% RH, the heat conduction oil furnace 3 is started, the temperature in the drying box body 1 is increased, when the humidity value shows 50% RH, the hot air circulation exhaust fan 8 is opened, the 2 condensers 7 start to work, gaseous rose flower liquid is condensed and gathered to form liquid through the 2 condensers 7, and the liquid enters the rose flower liquid collecting tank 12 through the rose flower liquid discharge pipeline 11 with the S-shaped vertical section; a gas supply pipeline section 10 fixedly connected with a gas outlet of the hot air circulation exhaust fan 8 in a sealing way circularly conveys circulating gas into the drying box body 1 through a gas inlet arranged at the lower part of the side wall at the right side of the drying box body 1; when humidity value is less than 50% RH in the stoving box 1, heated air circulation air exhauster 8 closes, 2 condensers 7 stop working, and first working phase circulation is reciprocal 10 hours, when humidity value no longer reaches 50% RH in the stoving box 1, gets into the second working phase:

and a second working stage: the temperature in the drying box body 1 is set to be 60 ℃, the humidity value is set to be 45% RH, when the humidity value in the drying box body 1 shows 45% RH, the hot air circulation exhaust fan 8 is opened, the 2 condensers 7 start to work, the gaseous rose flower liquid is condensed and gathered by the 2 condensers 7 to form liquid, and the liquid enters the rose flower liquid collecting tank 12 through the rose flower liquid discharge pipeline 11 with the vertical section being S-shaped; a gas supply pipeline section 10 fixedly connected with a gas outlet of the hot air circulation exhaust fan 8 in a sealing way circularly conveys circulating gas into the drying box body 1 through a gas inlet arranged at the lower part of the side wall at the right side of the drying box body 1; when the humidity value in the drying box body 1 is lower than 45% RH, the hot air circulation exhaust fan 8 is closed, and the 2 condensers 7 stop working; the second working phase is circulated for 8 hours, and when the humidity does not reach 45% RH any more, the preparation process of the fresh rose flower liquid is finished;

and B, step: mixing the solutions, filtering with microfiltration membrane, sterilizing at ultrahigh temperature and ultraviolet ray, and storing in 316 stainless steel tank to obtain fresh rose solution;

the lemon juice is prepared by the following steps: taking 150 g of fresh lemon, peeling, putting into a juicer for juicing, filtering by using a microfiltration membrane, heating to 100 ℃, sterilizing, cooling and standing at normal temperature for later use.

A preparation method of rose anthocyanin skin-care fresh flower water is characterized by comprising the following steps: the method comprises the following steps:

A. respectively weighing 92% (weight percentage) of rose pigment glycoside concentrated solution, aloe extract, tremella polysaccharide, honey, vitamin C, vitamin E, lemon juice, betaine, hyaluronic acid, phenoxyethanol/ethylhexyl glycerin, birch juice, xanthan gum and fresh rose flower solution according to the weight part ratio for later use;

B. sequentially adding 92% (by weight) of rose pigment glycoside concentrated solution prepared in the step A, honey, vitamin E, betaine, aloe extract, tremella polysaccharide, hyaluronic acid, birch juice, xanthan gum and fresh rose flower solution into a stainless steel batching barrel, and stirring for 15 minutes clockwise and 15 minutes anticlockwise; adding vitamin C and lemon juice, and controlling the dosage of the vitamin C and the lemon juice to ensure that the pH value of the mixed solution added into the stainless steel batching barrel in the step B is between 5.5;

C. adding the phenoxyethanol/ethylhexyl glycerol prepared in the step A into the mixed solution prepared in the step B, and stirring for 15 minutes clockwise and anticlockwise respectively; and D, uniformly mixing the phenoxyethanol/ethylhexyl glycerin prepared in the step A and the mixed solution prepared in the step B, filtering by using a diaphragm pump, carrying out pasteurization in a sterile room, preparing the rose pigment glycoside skin moisturizer, and carrying out vacuum packaging, warehousing and normal-temperature storage.

Claims (2)

1. A rose pigment glycoside skin-care fresh flower water is characterized in that: the composition is prepared from the following raw materials in parts by weight: 90-92% (weight percentage) of rose pigment glycoside concentrated solution 5-10, aloe extract 2-5, tremella polysaccharide 0.5-3, honey 1-3, vitamin C0.5-1, vitamin E0.5-1, lemon juice 0.5-1, betaine 0.5-1, hyaluronic acid 0.1-0.5, phenoxyethanol/ethylhexyl glycerin 0.1-0.5, birch juice 2-5, xanthan gum 0.1-0.5, and fresh rose flower solution 85-90;

the rose anthocyanin concentrated solution is prepared by the following steps: taking 60% (weight percentage) of acidic ethanol (pH value is 1) as an extracting agent, taking 1 part of dried rose flower under the condition that the material-liquid ratio is 1:10-12 (weight portion ratio), taking 10-12 parts of 60% (weight percentage) of acidic ethanol (pH value is 1) and heating to 50-52 ℃, adding 1 part of dried rose flower into 10-12 parts of 60% (weight percentage) of acidic ethanol (pH value is 1) with the temperature of 50-52 ℃, soaking, and leaching for 2-2.5 hours; repeatedly extracting for 3 times, filtering with microfiltration membrane, mixing filtrates, and vacuum concentrating to obtain 90-92% (by weight) rose pigment glycoside concentrated solution; the dry rose flower is a dry corolla of the double-petal rose;

the rose flower liquid is prepared by using rose flower liquid preparation equipment: the rose flower liquid preparation equipment comprises a drying box body and a movable trolley arranged in the drying box body, wherein the drying box body is provided with a sealing door, and further comprises a heat conduction oil furnace, a heat conduction oil output pipeline, a heat conduction oil return pipeline and at least 4 radiators arranged in the drying box body, wherein the heat conduction oil furnace is used for supplying heat to the drying box body; a thermometer and a hygrometer are also arranged on the drying box body; the rose flower liquid condensation and collection device is arranged at the top of the drying box body;

the rose flower liquid condensation collecting device comprises 2 condensers, a hot air circulation exhaust fan, an air exhaust pipeline section and an air supply pipeline section, wherein the hot air circulation exhaust fan is installed at the left position of a drying box body by using a hot air circulation exhaust fan installation seat, the 2 condensers are sequentially installed on a top plate of the drying box body, lower vertical pipeline sections are respectively installed at two sides of the axial lower bottom surface of the 2 condensers, and the other ends of the lower vertical pipeline sections respectively installed at two sides of the axial lower bottom surface of the 2 condensers respectively sequentially penetrate through the top plate of the drying box body and are longitudinally and fixedly installed on the top plate of the drying box body; the middle positions of the axial upper top surfaces of the 2 condensers are respectively provided with an upper vertical pipeline section, the other ends of the upper vertical pipeline sections which are respectively arranged at the middle positions of the axial upper top surfaces of the 2 condensers are respectively and fixedly connected with a horizontal pipeline section in a sealing way, one end of the air exhaust pipeline section is fixedly connected with an air inlet of a hot air circulation exhaust fan in a sealing way, and the other end of the air exhaust pipeline section is fixedly connected with the horizontal pipeline section which is respectively and fixedly connected with the other ends of the upper vertical pipeline sections which are respectively arranged at the middle positions of the axial upper top surfaces of the; one end of the air supply pipeline section is fixedly connected with an air outlet of the hot air circulation air extractor in a sealing way, and the other end of the air supply pipeline section is fixedly connected with an air inlet arranged at the lower part of the side wall of the right side of the drying box body in a sealing way; the rose flower liquid collecting device comprises a rose flower liquid discharging pipeline with a vertical section in an S-shaped bend and a rose flower liquid collecting tank, wherein the rose flower liquid discharging pipeline with the vertical section in the S-shaped bend is provided with a parallel pipeline section away from the vertical section in the S-shaped bend and a vertical pipeline section close to the vertical section in the S-shaped bend; the heat-conducting oil furnace, the installation of the heat-conducting oil furnace and the condenser are all completed by adopting the prior art;

the preparation process of the fresh rose flower liquid comprises the following steps:

step A: when the temperature in the drying box body is regulated and controlled to be increased to 35-40 ℃, a sealing door of the drying box body is opened, the movable trolley filled with fresh rose flowers is pushed in, and the sealing door of the drying box body is closed; a first working stage: the temperature of the drying box body is set to be 35-50 ℃, the humidity value is set to be 50% RH, the heat conduction oil furnace is started, the temperature in the drying box body rises, when the humidity value shows 50% RH, the hot air circulation exhaust fan is opened, the 2 condensers start to work, the gaseous rose flower liquid is condensed and gathered to form liquid through the 2 condensers, and the liquid enters the rose flower liquid collecting tank through the rose flower liquid discharge pipeline with the S-shaped vertical section; the air supply pipeline section fixedly connected with the air outlet of the hot air circulation exhaust fan in a sealing way circularly conveys the circulating air into the drying box body through an air inlet arranged at the lower part of the side wall at the right side of the drying box body; when humidity numerical value is less than 50% RH in the drying cabinet, the heated air circulation air exhauster is closed, 2 condensers stop working, first working phase circulation is reciprocal 10 hours, when humidity numerical value no longer reaches 50% RH in the drying cabinet, gets into the second working phase:

and a second working stage: the temperature in the drying box is set to be 50-60 ℃, the humidity value is set to be 45% RH, when the humidity value in the drying box shows 45% RH, the hot air circulation exhaust fan is opened, the 2 condensers start to work, the gaseous rose flower liquid is condensed and gathered into liquid through the 2 condensers, and the liquid enters the rose flower liquid collecting tank through a rose flower liquid discharge pipeline with an S-shaped vertical section; the air supply pipeline section fixedly connected with the air outlet of the hot air circulation exhaust fan in a sealing way circularly conveys the circulating air into the drying box body through an air inlet arranged at the lower part of the side wall at the right side of the drying box body; when the humidity value in the drying box body is lower than 45% RH, the hot air circulation exhaust fan is closed, and the 2 condensers stop working; the second working phase is circulated for 8 hours, and when the humidity does not reach 45% RH any more, the preparation process of the fresh rose flower liquid is finished;

and B, step: mixing the solutions, filtering with microfiltration membrane, sterilizing at ultrahigh temperature and ultraviolet ray, and storing in 316 stainless steel tank to obtain fresh rose solution;

the lemon juice is prepared by the following steps: taking 100-150 g of fresh lemon, peeling, putting into a juicer for juicing, filtering with a microfiltration membrane, heating to 100 ℃, sterilizing, and cooling to normal temperature for later use.

2. The method for preparing rose pigment glycoside skin-care fresh flower water as claimed in claim 1, which is characterized in that: the method comprises the following steps:

A. respectively weighing 90-92% (by weight) of rose pigment glycoside concentrated solution, aloe extract, tremella polysaccharide, honey, vitamin C, vitamin E, lemon juice, betaine, hyaluronic acid, phenoxyethanol/ethylhexyl glycerin, birch juice, xanthan gum and fresh rose flower solution according to the weight parts for later use;

B. sequentially adding 90-92% (by weight) of rose pigment glycoside concentrated solution prepared in the step A, honey, vitamin E, betaine, aloe extract, tremella polysaccharide, hyaluronic acid, white birch juice, xanthan gum and fresh rose flower solution into a stainless steel batching barrel, and stirring for 10-15 minutes clockwise and 10-15 minutes anticlockwise; adding vitamin C and lemon juice, and controlling the dosage of vitamin C and lemon juice to ensure that the pH value of the mixed solution added into the stainless steel batching barrel in the step B is between 4.5 and 5.5;

C. adding the phenoxyethanol/ethylhexyl glycerol prepared in the step A into the mixed solution prepared in the step B, and stirring for 10-15 minutes clockwise and anticlockwise respectively; and D, uniformly mixing the phenoxyethanol/ethylhexyl glycerin prepared in the step A and the mixed solution prepared in the step B, filtering by using a diaphragm pump, carrying out pasteurization in a sterile room, preparing the rose pigment glycoside skin moisturizer, and carrying out vacuum packaging, warehousing and normal-temperature storage.

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