CN109498488A - A kind of ginseng moisture saver mask and the preparation method and application thereof - Google Patents
A kind of ginseng moisture saver mask and the preparation method and application thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The present invention provides a kind of ginseng moisture saver mask, is made of tetra- part A, B, C, D, and wherein A phase includes hydroxyethyl cellulose, esters of acrylic acid/C10-30 alkylol acrylamide acid esters cross-linked polymer, butanediol；B phase includes composition 1, composition 2, composition 3, composition 4, PEG/PPG-17/6 copolymer, parahydroxyacet-ophenone, 1,2- pentanediol；C phase includes sodium hydroxide, composition 5；D phase includes Sodium Hyaluronate, solubilizer and essence, wherein contain ginseng root extract in composition 5, active components of plants in its cooperative compositions 1-4, successively tetra- constituent part of A, B, C, D is mixed in such a way that substep mixes, stable, the good facial mask of moistening effect is formed, is with a wide range of applications.
Description
Technical field
The invention belongs to cosmetic field, it is related to a kind of moisture saver mask and the preparation method and application thereof, and in particular to a kind of
Ginseng moisture saver mask and the preparation method and application thereof.
Background technique
With the development and continuous improvement of people's living standards of social economy, requirement of the people for beauty is increasingly
Height, cosmetics type on the market are also further abundant.Cosmetics, which refer to, is embrocated or is sprayed on body surface (epidermis, head
Hair, lip, nail, tooth, mucous membrane etc.), can play cleaning, protection, reduce peculiar smell, maintain kilter any substance or
Preparation.In short, can achieve the purpose of personal hygiene and beautification by the processing of cosmetics complete set of programs.It is advised according to Darwin
Then, realize that the pursuit to beauty is a biological characteristic of biological evolution using cosmetics, animals and humans pass through evolution respectively
It visual signature and is realized using external tool.Face whether beauty be evaluate spouse value important biomolecule signal, and with suction
The judgement of the social properties such as gravitation, competitiveness, affinity and credit is associated.
Wherein, facial mask is a kind of beauty product with multiple efficacies, using the of short duration time for being covered on face, temporarily
Extraneous air and pollution is isolated, improves skin temperature, the pore expansion of skin promotes sweat gland secretion and metabolism, facial mask
In moisture or other functional components penetrate into the cuticula of epidermis, skin becomes soft, and making skin, light is flexible naturally.With
People's beauty and the transformation of consumption idea, facial mask enter the rapid growth phase, have very big development space.
Replenishing water and preserving moisture is the groundwork of skin nursing, and it is easy to appear moisture under the influence of by external environment for skin
Loss, and skin lacks enough water content and will result directly in that skin metabolism is abnormal and aging, wrinkle and color spot occur etc.
Etc. a series of skin problems.As it can be seen that it is also most important work that replenishing water and preserving moisture, which is the most basic of skin daily nursing, but how
Safely and effectively facial mask is the majority of consumers' concern the most for selection.More scientific researches are still dedicated to the makeup such as facial mask
The improvement of product, one of field are exactly to meet consumer demand using active skull cap components.Patent application
CN106420505A discloses a kind of Chinese medicinal plant composition, by 5 kinds of Astragalus membranacus, radix saposhnikoviae, Rhizoma Gastrodiae, pot marigold and silk tree groups
Split-phase interaction plays sensitivity of releiving, pacifies antipruritic, red detumescence of dispelling, quick rear the effect of repairing.Patent application CN108451856A
A kind of replenishing water and preserving moisture facial mask is disclosed, golden hairpin dendrobium extract, shrubby sophora extract, Echinacea angustifolia extract, lycium barbarum are utilized
The raw materials such as berry extract, aloe vera extract, chitosan and biological carbohydrate gum make stoste have maintenance skin, improve flesh
Skin is obscure, dark yellow, dry, oxidation and other effects.
Ginseng system Araliaceae-ginseng dry root, tonifying five zang organs vigour, determine soul, stop palpitate with fear, go at body spirit of taking shelter
It removes pathogenic factor, sharp liver improving eyesight, intelligence development are happy, take a good fit light macrobiosis for a long time.Modern medicine study show ginseng have it is anti-oxidant,
Anti-aging, anti-radiation, removing toxic substances, enhancing memory inhibit tumour growth, adjustment physiological function and enhancing immunity of organisms function to make
With.Currently, the main effective active matter found in ginseng has ginsenoside, organic acid and esters, amino acid, polysaccharide, gland
Glycosides, L-Glutimic acid, vitamins, microelement etc..Ginsenoside has moisture-keeping function to skin, is able to suppress tyrosinase
Activity and the effect for removing DPPH free radical.Patent application CN106309282A discloses a kind of ginseng beauty mask, is mentioned with ginseng
Taking liquid, Fresh Cucumber Juice, asparagus juice is active constituent, and the facial mask being prepared not only has moisturizing, health, beauty treatment, nourishes face
Function, and have the function of delaying senescence, enhance skin vitality.Patent application CN108158970A also discloses a kind of people
Join moisture saver mask comprising Skin Cell can be improved in ginseng extract and aloe barbadensis Miller leaf juice, the ginsenoside in ginseng
Antioxygenic activity, enhance the Scavenging activity of Skin Cell free radical, delayed the aging of skin, and aloe vera extract,
Its main component can be improved the effect of after-sun restorative, promoted antibacterial, replenishing water and preserving moisture, oil control and acne removal, pore refining, it is anti-oxidant,
Anti-aging, goes the multiple efficacies such as wrinkle at antiallergic reparation.
As it can be seen that application of the ginseng in the cosmetics such as facial mask is very extensive, but how to select suitable active factors
Compatibility is carried out, and cooperates corresponding auxiliary material, effect of the ginseng extract in terms of moisturizing is played to the maximum extent, is vast research and development
The direction of target and effort that personnel constantly pursue.
Summary of the invention
For the defect for solving the above-mentioned prior art, the present invention provides a kind of ginseng beauty mask, passes through addition various plants activity
Ingredient and ginseng root extract form good synergistic effect, form a kind of better ginseng moisture saver mask of replenishing water and preserving moisture effect.
The present invention provides a kind of ginseng moisture saver mask, by tetra- phase composition of A, B, C, D, wherein A phase include hydroxyethyl cellulose,
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, butanediol；B phase includes composition 1, composition 2, combination
Object 3, composition 4, PEG/PPG-17/6 copolymer, parahydroxyacet-ophenone, 1,2- pentanediol；C phase includes sodium hydroxide and combination
Object 5；D phase includes Sodium Hyaluronate, solubilizer and essence；
Wherein, the composition 1 includes water, glycerol, HERBA DENDROBII stem extraction, aloe barbadensis Miller leaf extract, kuh-seng
Root extract, lycium barbarum berry extract and Echinacea angustifolia extract, Phenoxyethanol, Sensiva SC50；
The composition 2 includes butanediol and quinine fungus extract；
The composition 3 includes butanediol, water, Astragalus membranacus root extract, windproof root extract, pot marigold extraction
Object, Flos Albiziae extract, Rhizoma Gastrodiae root extract
The composition 4 includes water, glycerol, dried tremella extract, Phenoxyethanol, Sensiva SC50；
The composition 5 includes water, glycerol and ginseng root extract；
The solubilizer is the mixed of coceth -7, PPG-1-PEG-9 laurel glycol ethers and Cremophor RH40
Close object.
Further, the ginseng moisture saver mask includes following components in parts by weight:
A phase: 0.01-0.50 parts of hydroxyethyl celluloses, 0.01-0.30 parts of acrylic acid (ester) classes/C10-30 alkylol acrylamide acid
Ester cross-linked polymer, 0.10-10.00 part butanediol；
B phase: 0.50-10.00 parts of compositions 1,0.50-10.00 parts of compositions 2,0.50-10.00 parts of compositions 3,0.50-
10.00 parts of compositions 4,0.05-2.00 parts of PEG/PPG-17/6 copolymers, 0.10-3.00 parts of parahydroxyacet-ophenones, 0.1-
10.00 part 1,2- pentanediol；
C phase: 0.25-0.75 parts of NaOH, 0.10-20.00 parts of compositions 5；
D phase: 0.01-0.50 parts of Sodium Hyaluronates, 0.05-1.50 parts of solubilizer, 0.01-0.30 parts of essence.
Further, the ginseng moisture saver mask includes following components in parts by weight:
A phase: 0.05-0.30 parts of hydroxyethyl celluloses, 0.05-0.20 parts of acrylic acid (ester) classes/C10-30 alkylol acrylamide acid
Ester cross-linked polymer, 0.50-8.00 part butanediol；
B phase: 1.00-8.00 parts of compositions 1,1.00-8.00 parts of compositions 2,1.00-8.00 parts of compositions 3,1.00-
8.00 parts of compositions 4,0.10-1.00 parts of PEG/PPG-17/6 copolymers, 0.50-2.00 parts of parahydroxyacet-ophenones, 1.00-8.00
Part 1,2- pentanediol；
C phase: 0.30-0.70 parts of NaOH, 1.00-15.00 parts of compositions 5；
D phase: 0.05-0.30 parts of Sodium Hyaluronates, 0.10-1.00 parts of solubilizer, 0.05-0.20 parts of essence.
Still further, the ginseng moisture saver mask includes following components in parts by weight:
A phase: 0.10-0.20 parts of hydroxyethyl celluloses, 0.10-0.15 parts of acrylic acid (ester) classes/C10-30 alkylol acrylamide acid
Ester cross-linked polymer, 1.00-5.00 part butanediol；
B phase: 3.00-5.00 parts of compositions 1,3.00-5.00 parts of compositions 2,3.00-5.00 parts of compositions 3,3.00-
5.00 parts of compositions 4,0.50-0.80 parts of PEG/PPG-17/6 copolymers, 1.00-1.50 parts of parahydroxyacet-ophenones, 3.00-5.00
Part 1,2- pentanediol；
C phase: 0.40-0.60 parts of NaOH, 5.00-10.00 parts of compositions 5；
D phase: 0.10-0.20 parts of Sodium Hyaluronates, 0.50-1.00 parts of solubilizer, 0.10-0.15 parts of essence.
Further, the composition 1 can be according to parts by weight, by 20 parts of glycerol, 64.3 parts of water, 6 parts of HERBA DENDROBII stems
Extract, 3 parts of aloe barbadensis Miller leaf extracts, 3 parts of kuh-seng root extracts, 2 parts of lycium barbarum berry extracts, 1 portion of purple coneflower
Extract, 0.63 part of Phenoxyethanol, 0.07 part of Sensiva SC50 are mixed；The vast gloomy production of Beijing Orient can also directly be bought
Product Lin Lan profit dew, including water, glycerol, HERBA DENDROBII stem extraction, aloe barbadensis Miller leaf extract, kuh-seng root extract, Ningxia
Fructus lycii berry extract, Echinacea angustifolia extract, Phenoxyethanol and Sensiva SC50.
Further, the composition 2 buys BASF product " LS 8865 ", and it includes butanediols and quinine fungus
Extract.
Further, the composition 3 can extract 80 parts of butanediols, 8 parts of water, 5 parts of pod astragalus roots according to parts by weight
Object, 3 parts of windproof root extracts, 2 parts of pot marigold flower extracts, 1 part of Flos Albiziae extract, 1 part of Rhizoma Gastrodiae root extract are mixed；
The vast gloomy product Shu Minjia of Beijing Orient can also be directly bought, including butanediol, water, Astragalus membranacus root extract, opoponax mention
Take object, pot marigold flower extract, Flos Albiziae extract, Rhizoma Gastrodiae root extract.
Further, the composition 4 can be according to parts by weight, by 92 parts of water, 2 parts of glycerol, 5 parts of dried tremella extracts, 0.9
Part Phenoxyethanol, 0.1 part of Sensiva SC50 are prepared, or directly buy the vast gloomy product " α-mannosan " of Beijing Orient,
It includes water, glycerol, dried tremella extract, Phenoxyethanol, Sensiva SC50s.
Further, the composition 5 is the vast gloomy product of Beijing Orient, including water, glycerol, ginseng root extract；It can also
To be prepared by the following method: ginseng extracting in water is added glycerol compounding in supernatant, after high-temperature sterilization, then
Adding preservative agent.
Still further, composition 5 is prepared by the following method: by ginseng palpus: pure water=1:15-17
Solid-liquid ratio extracts 2-3h under 80-85 DEG C of stirring, in filtrate: glycerol=100:10-15 ratio compounding, 88-93 DEG C of sterilizing
40-45min, add 0.6-1.0% Phenoxyethanol/Sensiva SC50 to get.
Further, the solubilizer is the product of Beijing member of Imperial Academy, including coceth -7, PPG-1-PEG-9 laurel
Glycol ethers and Cremophor RH40.
The present invention also provides the preparation methods of above-mentioned ginseng beauty mask, comprising the following steps:
(1) hydroxyethyl cellulose butanediol in A phase is fully dispersed, it is added to sprinkled with acrylic acid (ester) class/C10-30
In the water phase of alkylol acrylamide acid esters cross-linked polymer, it is uniformly mixed, obtains mixed solution 1；
(2) B phase materials are added in mixed solution 1 in proportion, are uniformly mixed, obtain mixed solution 2；
(3) sodium hydroxide is added in mixed solution 2 and is neutralized, add other raw materials in C phase, be uniformly mixed,
Obtain mixed solution 3；
(4) by scattered sodium hyaluronate solution preparatory in D phase, be added in mixed solution 3 and mix, then by solubilizer with
It is added, is uniformly mixed to get facial mask essence after essence mixing；
(5) by facial mask cloth be infiltrated in facial mask essence to get.
Further, in the step (1) that hydroxyethyl cellulose butanediol in A phase is fully dispersed, it is added to and is sprinkled with
In acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer water phase, it is warming up to 80-85 DEG C, 18-22r/min is stirred
20-40min is mixed, mixed solution 1 is obtained.
Further, after mixed solution being cooled to 48-53 DEG C in the step (2), B phase materials, 18-22r/ are added
Min is stirred evenly, and obtains mixed solution 2.
Further, it after solution 2 to be mixed is cooled to 43-47 DEG C in the step (3), is added during sodium hydroxide carries out
With add other raw materials, 18-22r/min in C phase and stir evenly, obtain mixed solution 3.
Further, after solution to be mixed is cooled to 38-42 DEG C in the step (4), by scattered matter preparatory in D phase
The sodium hyaluronate solution that percentage concentration is 0.5-2.0% is measured, is added in mixed solution 3 and mixes, then solubilizer and essence are mixed
It is added after conjunction, 18-22r/min stirs evenly to get facial mask essence.
Further, every facial mask cloth adds Essence 25-30g/ piece to carry out wetting immersion in the step (5).
The present invention also provides above-mentioned ginseng moisture saver mask to prepare the application in moisture saver mask.Beneficial effects of the present invention:
(1) present invention forms good synergistic effect by addition various plants active constituent and ginseng root extract, more
Skin condition is repaired in orientation, forms a kind of better ginseng moisture saver mask of replenishing water and preserving moisture effect, wherein composition 1 can assist in people
Conopsea extraction solve the problems, such as jointly dry skin, quinine fungus extract promote pore shrink, composition 3 pacify it is antipruritic,
Sensitive skin is takeed good care of, dried tremella extract is then " plant hyaluronic acid " effectively water lock moisturizing.
(2) all the components such as active constituent, auxiliary material are divided into 4 parts by the present invention, are first passed through A phase component and are prepared facial mask base
Material；Then addition guarantees that active constituent is sufficiently mixed uniformly in facial mask containing Supplementary active ingredients B phases such as compositions 1,2,3,4,
It is set preferably to play a role；PH value is first carried out before adding the C phase containing this main active constituent of ginseng root extract again
It adjusts, active factors in ginseng extract is avoided to be destroyed；The D phase containing Sodium Hyaluronate etc. is finally added, is formed and is stablized
System.Each operating procedure all carries out within specified temperatures, and the activity and system of each active constituent is effectively ensured
Stability.
Specific embodiment
1 ginseng moisture saver mask of embodiment and its preparation
It is specific the preparation method comprises the following steps:
(1) hydroxyethyl cellulose butanediol in A phase is fully dispersed, then by acrylic acid (ester) class/C10-30 alkanol
Acrylate crosspolymers are sprinkled on the water surface, and the hydroxyethyl cellulose butanediol solution after dispersion is added to sprinkled with acrylic acid
In (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer water phase, 80 DEG C are warming up to, 20r/min stirs 30min, obtains mixed
Close solution 1；
(2) after being cooled to 50 DEG C, B phase materials are added in mixed solution 1 in proportion, 20r/min is stirred evenly, and must be mixed
Solution 2；
(3) after being cooled to 45 DEG C, sodium hydroxide is added in mixed solution 2 and is neutralized, add composition in C phase
5,20r/min stir evenly, and obtain mixed solution 3；
(4) after solution to be mixed is cooled to 40 DEG C, by scattered mass percentage concentration preparatory in D phase be 1.0% it is saturating
Bright matter acid sodium solution is added in mixed solution 3 and mixes, then is added after solubilizer is mixed with essence, and 20r/min is stirred evenly；
(5) 38 DEG C are cooled to hereinafter, examining, discharging；
(6) it is aged, is filling to get facial mask essence after detection qualification；
(7) Essence 25-30g/ piece is added to carry out wetting immersion every facial mask cloth.
2 ginseng moisture saver mask of embodiment and preparation method thereof
It is specific the preparation method comprises the following steps:
(1) hydroxyethyl cellulose butanediol in A phase is fully dispersed, then by acrylic acid (ester) class/C10-30 alkanol
Acrylate crosspolymers are sprinkled on the water surface, and the hydroxyethyl cellulose butanediol solution after dispersion is added to sprinkled with acrylic acid
In (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer water phase, 85 DEG C are warming up to, 18r/min stirs 20min, obtains mixed
Close solution 1；
(2) after being cooled to 48 DEG C, B phase materials are added in mixed solution 1 in proportion, 18r/min is stirred evenly, and must be mixed
Solution 2；
(3) after being cooled to 43 DEG C, sodium hydroxide is added in mixed solution 2 and is neutralized, add composition in C phase
5,18r/min stir evenly, and obtain mixed solution 3；
(4) after solution to be mixed is cooled to 38 DEG C, by scattered mass percentage concentration preparatory in D phase be 0.5% it is saturating
Bright matter acid sodium solution is added in mixed solution 3 and mixes, then is added after solubilizer is mixed with essence, and 18r/min is stirred evenly；；
(5) it examines, discharge；
(6) it is aged, is filling to get facial mask essence after detection qualification；
(7) every facial mask cloth is added in 25-30g Essence and is impregnated, sealed package to obtain the final product.
3 ginseng moisture saver mask of embodiment and preparation method thereof
It is specific the preparation method comprises the following steps:
(1) hydroxyethyl cellulose butanediol in A phase is fully dispersed, then by acrylic acid (ester) class/C10-30 alkanol
Acrylate crosspolymers are sprinkled on the water surface, and the hydroxyethyl cellulose butanediol solution after dispersion is added to sprinkled with acrylic acid
In (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer water phase, 82 DEG C are warming up to, 22r/min stirs 40min, obtains mixed
Close solution 1；
(2) after being cooled to 53 DEG C, B phase materials are added in mixed solution 1 in proportion, 22r/min is stirred evenly, and must be mixed
Solution 2；
(3) after being cooled to 47 DEG C, sodium hydroxide is added in mixed solution 2 and is neutralized, add composition in C phase
5,22r/min stir evenly, and obtain mixed solution 3；
(4) after solution to be mixed is cooled to 42 DEG C, by scattered mass percentage concentration preparatory in D phase be 1.0% it is saturating
Bright matter acid sodium solution is added in mixed solution 3 and mixes, then is added after solubilizer is mixed with essence, and 22r/min is stirred evenly；；
(5) 38 DEG C are cooled to hereinafter, examining, discharging；
(6) it is aged, is filling to get facial mask essence after detection qualification；
(7) every facial mask cloth is immersed into 25-30g facial mask essence, sealed package to obtain the final product.
4 ginseng moisture saver mask of embodiment and preparation method thereof
Preparation method:
Composition 5 the preparation method comprises the following steps: according to ginseng must: pure water=1:15 solid-liquid ratio, 80 DEG C stirring under mentioned
3h is taken, in filtrate: glycerol=100:10 ratio compounding, 88 DEG C of sterilizing 45min add 0.6% Phenoxyethanol/Sensiva SC50,
To obtain the final product
Remaining is the same as embodiment 1.
5 ginseng moisture saver mask of embodiment and preparation method thereof
Preparation method:
Composition 5 the preparation method comprises the following steps:
Ginseng palpus: pure water=1:17 solid-liquid ratio extracts 2h under 85 DEG C of stirrings, by filtrate: glycerol=100:15
Ratio compounding, 93 DEG C of sterilizing 40min, add 1.0% Phenoxyethanol/Sensiva SC50 to get
Remaining is the same as embodiment 1.
6 ginseng moisture saver mask of embodiment and preparation method thereof
Preparation method:
Wherein composition 5 the preparation method comprises the following steps:
Ginseng palpus: pure water=1:16 solid-liquid ratio extracts 2h under 85 DEG C of stirrings, by filtrate: glycerol=100:13
Ratio compounding, 93 DEG C of sterilizing 40min, add 0.8% Phenoxyethanol/Sensiva SC50 to get
Remaining is the same as embodiment 1.
Comparative example 1 is free of the ginseng moisture saver mask and preparation method thereof of composition 1
In addition to without composition 1, remaining is with embodiment 1, specific formula
It is specific that the preparation method is the same as that of Example 1.
Ginseng moisture saver mask and its preparation of the comparative example 2 without composition 2
In addition to without composition 2, remaining is the same as embodiment 1
Ginseng moisture saver mask and its preparation of the comparative example 3 without composition 3
In addition to without composition 3, remaining is the same as embodiment 1
Preparation method: with embodiment 1.
Comparative example 4 is free of 4 ginseng beauty mask of composition and its preparation
In addition to without composition 4, remaining is the same as embodiment 1.
Preparation method: with embodiment 1.
The ginseng moisture saver mask and its preparation that the different preparation methods of comparative example 5 are prepared
Formula: with embodiment 1.
Preparation method: step (2) is cooled to 55 DEG C, remaining is the same as embodiment 1.
The ginseng moisture saver mask and its preparation that the different preparation methods of comparative example 6 are prepared
Formula: without outside NaOH, remaining is the same as embodiment 1.
Preparation method: NaOH is not added and adjusts outside pH for step (3), remaining is the same as embodiment 1.
Effect example different people joins moisture saver mask efficacy assessments
1-6 of the embodiment of the present invention, comparative example are tested referring to QB/T 4256-2011 " cosmetics moisture-keeping efficacy evaluation guide "
Skin moisture content MMV value and percutaneous water loss amount TEWL value after when the ginseng moisture saver mask of 1-6 preparation.
1.1 test crowds:
Subject 31 are randomly selected, using inside of cranking arm as test zone, according to cycle labeling principle to survey before test
Examination region is marked, and acquires initial value according to marking serial numbers, numerical value when being denoted as 0h, then carrying out sample according to application method makes
With the data at corresponding time point, finally carry out data processing after acquisition sample use, it was therefore concluded that.
(1) crowd's inclusion criteria is tested:
1. the good male of other physical conditions of whole body, women, age are random；
2. medical treatment and health status meet the standard of being included in
3. without cosmetic allergic contact dermatitis history；
4. treatment does not take corticosteroid hormone, antibiotic, tretinoin medicines or receives other anti-acne drugs for first 2 weeks
Object treatment；
5. not doing laser beautifying or Chemical peeling in nearly 2 years；
6. no logic taboo；
7. having read and having signed on informed consent form before the study.
(2) crowd's exclusion criteria is tested:
1. gestation or breast feeding women；
2. the planned pregnancy of readme；Contraceptives person is reluctant or cannot be used to female volunteers with fecundity；
3. having allergy or highly sensitive risk person to cosmetics；
4. nearly one week using antihistamine or it is one month nearly in use immunosuppressor person；
5. recipient site applies any anti-inflammatory drug person in nearly two months；
6. subject is cured person with the clinical end of inflammatory dermatoses, or is receiving the asthma treated or other chronic respiratories
Systemic disease patient；
7. the person that receives anticancer chemotherapy in nearly 6 months；
8. immune deficiency or autoimmune disease patient or insulin-dependent diabetes mellitus patient or constitution are highly sensitive
Person；
9. non-aspiration participates in or cannot complete specified content person by test requirements document
(3) exit and (fall off) standard:
1. subject is lost to follow-up, initiative exits；
2. compliance is poor, product cannot be used according to quantity on time；It cannot follow-up as required；
3. using other anti-acne therapeutic drugs in research process；
4. occurring directly affecting the new disease of clinical state assessment, including skin disease during entire research；
5. there is serious disease person during entire research；
6. pregnant subject during research；
7. not being resistant to this researcher；
8. there is serious adverse reaction SAE person during entire research
1.2 test zones: test sample is cut into 3cm*3cm size and is put on subject's group test zone by laboratory technician
In (crank arm inside), sticks to take off after facial mask is massaged into absorption after 15min and be paid a return visit.
1.3 test environment: 22 ± 2 DEG C of temperature；50 ± 5%RH of relative humidity
1.4 return visit times: first test skin area is tested using preceding, 0h data is denoted as, sticks 15min and take face off
Film is massaged into 1h, 2h, 4h progress repetition measurement after absorption.It is tested using not applying sample surface diaphragm area as blank.
1.5 experimental result
1 different people of table joins moisture saver mask skin moisture content MMV value result
Note: wherein compared to the blank group, P < 0.05 *, representing has significant difference；P < 0.05 * is represented with extremely aobvious
Write sex differernce；Different letters, which represent, between same row has significant difference, P < 0.05.
Ginseng beauty mask provided by the invention has good moistening effect it can be seen from 1 data of table, after having used 1h
Skin moisture content reaches peak value, and water content is apparently higher than the blank group of unused facial mask, also above comparative example 1-6 group, fills
The bright the present inventor that defends oneself, which joins moisture saver mask, can effectively improve the water content of skin, wherein have good collaboration between each component
Effect lacks the moisturizing effect that any of them component influences whether facial mask, and temperature and pH in the preparation process of facial mask
Control also have a large impact on the effect of facial mask.
2 different people of table joins the percutaneous water loss amount TEWL value result of moisture saver mask
Note: wherein compared to the blank group, P < 0.05 *, representing has significant difference；P < 0.05 * is represented with extremely aobvious
Write sex differernce；Different letters, which represent, between same row has significant difference, P < 0.05.
Percutaneous moisture loss TEWL value is smaller, represents that moisture loss is fewer, and water lock ability is stronger；Conversely, water lock ability is got over
It is weak.Table 2 reduces moisture flowing water statistics indicate that ginseng moisture saver mask provided by the invention can preferably lock the moisture of skin,
Wherein best with the effect of embodiment 1 and 6, the ginseng beauty mask that comparative example 1-6 is provided is good without facial mask water lock ability of the present invention.
Above-mentioned detailed description is illustrating for one of them possible embodiments of the present invention, the embodiment not to
The scope of the patents of the invention is limited, all equivalence enforcements or change without departing from carried out by the present invention are intended to be limited solely by the technology of the present invention
In the range of scheme.
Claims (10)
1. a kind of ginseng moisture saver mask, by tetra- phase composition of A, B, C, D, which is characterized in that the A phase include hydroxyethyl cellulose,
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, butanediol；B phase includes composition 1, composition 2, combination
Object 3, composition 4, PEG/PPG-17/6 copolymer, parahydroxyacet-ophenone, 1,2- pentanediol；C phase includes sodium hydroxide, composition
5；D phase includes Sodium Hyaluronate, solubilizer and essence；
Wherein, the composition 1 is mentioned including water, glycerol, HERBA DENDROBII stem extraction, aloe barbadensis Miller leaf extract, radix sophorae
Take object, lycium barbarum berry extract and Echinacea angustifolia extract, Phenoxyethanol, Sensiva SC50；
The composition 2 includes butanediol and quinine fungus extract；
The composition 3 includes butanediol, water, Astragalus membranacus root extract, windproof root extract, pot marigold flower extract, closes
Joyous flower extract, Rhizoma Gastrodiae root extract；
The composition 4 includes water, glycerol, dried tremella extract, Phenoxyethanol, Sensiva SC50；
The composition 5 includes water, glycerol and ginseng root extract；
The solubilizer is the mixture of coceth -7, PPG-1-PEG-9 laurel glycol ethers and Cremophor RH40.
2. ginseng moisture saver mask according to claim 1, which is characterized in that the ginseng moisture saver mask includes following weight
The component of part:
A phase: 0.01-0.50 parts of hydroxyethyl celluloses, 0.01-0.30 parts of acrylic acid (ester) classes/C10-30 alkylol acrylamide acid esters are handed over
Linked polymer, 0.10-10.00 part butanediol；
B phase: 0.50-10.00 parts of compositions 1,0.50-10.00 parts of compositions 2,0.50-10.00 parts of compositions 3,0.50-
10.00 parts of compositions 4,0.05-2.00 parts of PEG/PPG-17/6 copolymers, 0.10-3.00 parts of parahydroxyacet-ophenones, 0.1-
10.00 part 1,2- pentanediol；
C phase: 0.25-0.75 parts of NaOH, 0.10-20.00 parts of compositions 5；
D phase: 0.01-0.50 parts of Sodium Hyaluronates, 0.05-1.50 parts of solubilizer, 0.01-0.30 parts of essence.
3. ginseng moisture saver mask according to claim 2, which is characterized in that the ginseng moisture saver mask includes following weight
The component of part:
A phase: 0.05-0.30 parts of hydroxyethyl celluloses, 0.05-0.20 parts of acrylic acid (ester) classes/C10-30 alkylol acrylamide acid esters are handed over
Linked polymer, 0.50-8.00 part butanediol；
B phase: 1.00-8.00 parts of compositions 1,1.00-8.00 parts of compositions 2,1.00-8.00 parts of compositions 3,1.00-8.00 parts
Composition 4,0.10-1.00 parts of PEG/PPG-17/6 copolymers, 0.50-2.00 parts of parahydroxyacet-ophenones, 1.00-8.00 parts of 1,2-
Pentanediol；
C phase: 0.30-0.70 parts of NaOH, 1.00-15.00 parts of compositions 5；
D phase: 0.05-0.30 parts of Sodium Hyaluronates, 0.10-1.00 parts of solubilizer, 0.05-0.20 parts of essence.
4. ginseng moisture saver mask according to claim 1-3, which is characterized in that the composition 5 passes through following
What method was prepared: ginseng extracting in water is added glycerol compounding in supernatant, then plus PEHG, sterilize to obtain the final product.
5. the preparation method of any one of claim 1-4 ginseng beauty mask a kind of, comprising the following steps:
(1) hydroxyethyl cellulose butanediol in A phase is fully dispersed, it is added to sprinkled with acrylic acid (ester) class/C10-30 alkanol
In the water phase of acrylate crosspolymers, it is uniformly mixed, obtains mixed solution 1；
(2) B phase materials are added in mixed solution 1 in proportion, are uniformly mixed, obtain mixed solution 2；
(3) sodium hydroxide is added in mixed solution 2 and is neutralized, add other raw materials in C phase, be uniformly mixed, obtain mixed
Close solution 3；
(4) essence is added after being dispersed in water solubilizer in D phase, forms mixed liquor and is added in mixed solution 3, is then added pre-
First scattered sodium hyaluronate solution is uniformly mixed to get facial mask essence；
(5) by facial mask cloth be infiltrated in facial mask essence to get.
6. preparation method according to claim 5, which is characterized in that by hydroxyethyl cellulose in A phase in the step (1)
It is fully dispersed with butanediol, it is added to sprinkled in acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer water phase,
It is warming up to 80-85 DEG C, 18-22r/min stirs 20-40min, obtains mixed solution 1.
7. preparation method according to claim 5, which is characterized in that mixed solution is cooled to 48- in the step (2)
After 53 DEG C, B phase materials are added, 18-22r/min is stirred evenly, and obtains mixed solution 2.
8. preparation method according to claim 5, which is characterized in that solution 2 to be mixed is cooled in the step (3)
After 43-47 DEG C, sodium hydroxide is added and is neutralized, adds other raw materials, 18-22r/min in C phase and stirs evenly, must mix
Solution 3.
9. preparation method according to claim 5, which is characterized in that solution to be mixed is cooled to 38- in the step (4)
After 42 DEG C, it is molten that mixing is added in the sodium hyaluronate solution for being 0.5-2.0% by scattered mass percentage concentration preparatory in D phase
It mixes in liquid 3, then is added after solubilizer is mixed with essence, 18-22r/min stirs evenly to get facial mask essence.
10. any one of any one of the claim 1-4 facial mask or claim 5-9 preparation method is prepared facial mask and exists
Prepare the application in moisture saver mask.
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| CN111110606A (en) * | 2020-02-26 | 2020-05-08 | 广东省粤企产业创新研究院 | Skin-moistening composition, preparation method thereof and skin-moistening emulsion |
| CN111529464A (en) * | 2020-05-20 | 2020-08-14 | 广东创美抗衰老研究有限公司 | Moisturizing cream suitable for diabetic patients |
| CN112569147A (en) * | 2019-09-28 | 2021-03-30 | 广州市中通生化制品有限公司 | Anti-allergy composition, anti-allergy cream and preparation method of anti-allergy composition |
| CN112675110A (en) * | 2021-01-08 | 2021-04-20 | 厦门力嘉诚生物科技有限公司 | Graphene ginseng mask and preparation method thereof |
| CN117653566A (en) * | 2023-11-16 | 2024-03-08 | 广州艾玫格生物科技有限公司 | Extraction composition containing medicinal layer porus and application thereof |
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Application publication date: 20190322 |