CN109363981A - A kind of plant amino acid shampoo - Google Patents
A kind of plant amino acid shampoo Download PDFInfo
- Publication number
- CN109363981A CN109363981A CN201811158964.3A CN201811158964A CN109363981A CN 109363981 A CN109363981 A CN 109363981A CN 201811158964 A CN201811158964 A CN 201811158964A CN 109363981 A CN109363981 A CN 109363981A
- Authority
- CN
- China
- Prior art keywords
- amino acid
- orange peel
- dried orange
- plant amino
- sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 150000001413 amino acids Chemical class 0.000 title claims abstract description 64
- 239000002453 shampoo Substances 0.000 title claims abstract description 59
- 239000000284 extract Substances 0.000 claims abstract description 59
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000004094 surface-active agent Substances 0.000 claims abstract description 24
- 229930003944 flavone Natural products 0.000 claims abstract description 23
- 235000011949 flavones Nutrition 0.000 claims abstract description 23
- 150000002213 flavones Chemical class 0.000 claims abstract description 21
- 238000002360 preparation method Methods 0.000 claims abstract description 16
- 239000000463 material Substances 0.000 claims abstract description 12
- 150000005846 sugar alcohols Polymers 0.000 claims abstract description 11
- 239000004064 cosurfactant Substances 0.000 claims abstract description 10
- 239000003755 preservative agent Substances 0.000 claims abstract description 9
- 230000002335 preservative effect Effects 0.000 claims abstract description 9
- 239000002562 thickening agent Substances 0.000 claims abstract description 8
- 229940024606 amino acid Drugs 0.000 claims description 58
- 235000001014 amino acid Nutrition 0.000 claims description 58
- 241000196324 Embryophyta Species 0.000 claims description 36
- 238000000605 extraction Methods 0.000 claims description 25
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 24
- 239000002904 solvent Substances 0.000 claims description 24
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 22
- -1 glutamic acid TEA salt Chemical class 0.000 claims description 22
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
- 239000000706 filtrate Substances 0.000 claims description 18
- 239000002994 raw material Substances 0.000 claims description 13
- 244000060011 Cocos nucifera Species 0.000 claims description 11
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- 235000019441 ethanol Nutrition 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 8
- 229920000289 Polyquaternium Polymers 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
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- 229940045944 sodium lauroyl glutamate Drugs 0.000 claims description 6
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical group [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 claims description 6
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 5
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 claims description 5
- 125000002811 oleoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])/C([H])=C([H])\C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 5
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- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 4
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- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 claims description 4
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- HXKKHQJGJAFBHI-UHFFFAOYSA-N 1-aminopropan-2-ol Chemical compound CC(O)CN HXKKHQJGJAFBHI-UHFFFAOYSA-N 0.000 claims description 3
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- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
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- BIVBRWYINDPWKA-VLQRKCJKSA-L Glycyrrhizinate dipotassium Chemical compound [K+].[K+].O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@H]1CC[C@]2(C)[C@H]3C(=O)C=C4[C@@H]5C[C@](C)(CC[C@@]5(CC[C@@]4(C)[C@]3(C)CC[C@H]2C1(C)C)C)C(O)=O)C([O-])=O)[C@@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O BIVBRWYINDPWKA-VLQRKCJKSA-L 0.000 claims description 2
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- WSDISUOETYTPRL-UHFFFAOYSA-N dmdm hydantoin Chemical compound CC1(C)N(CO)C(=O)N(CO)C1=O WSDISUOETYTPRL-UHFFFAOYSA-N 0.000 claims description 2
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- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 2
- 241001080929 Zeugopterus punctatus Species 0.000 description 2
- 229930013930 alkaloid Natural products 0.000 description 2
- 150000003797 alkaloid derivatives Chemical class 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000005187 foaming Methods 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- 230000003648 hair appearance Effects 0.000 description 2
- 210000003128 head Anatomy 0.000 description 2
- 235000008216 herbs Nutrition 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 231100000022 skin irritation / corrosion Toxicity 0.000 description 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- 210000000952 spleen Anatomy 0.000 description 2
- 239000012086 standard solution Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 2
- 239000000341 volatile oil Substances 0.000 description 2
- OYINQIKIQCNQOX-UHFFFAOYSA-M 2-hydroxybutyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCC(O)C[N+](C)(C)C OYINQIKIQCNQOX-UHFFFAOYSA-M 0.000 description 1
- OTTPFCJTQXRWHO-UHFFFAOYSA-N 3-(2,3-dichloroanilino)cyclohex-2-en-1-one Chemical compound ClC1=CC=CC(NC=2CCCC(=O)C=2)=C1Cl OTTPFCJTQXRWHO-UHFFFAOYSA-N 0.000 description 1
- 206010063409 Acarodermatitis Diseases 0.000 description 1
- 206010002198 Anaphylactic reaction Diseases 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 239000004166 Lanolin Substances 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241001093501 Rutaceae Species 0.000 description 1
- 241000447727 Scabies Species 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 206010040914 Skin reaction Diseases 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- KTHUPQRVVIDEPB-RGMNGODLSA-N [K].C(CC)N[C@@H](CCO)C(=O)O Chemical compound [K].C(CC)N[C@@H](CCO)C(=O)O KTHUPQRVVIDEPB-RGMNGODLSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000002390 adhesive tape Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 230000036783 anaphylactic response Effects 0.000 description 1
- 208000003455 anaphylaxis Diseases 0.000 description 1
- 238000010171 animal model Methods 0.000 description 1
- 230000003266 anti-allergic effect Effects 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical group [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000001408 fungistatic effect Effects 0.000 description 1
- 239000011086 glassine Substances 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000003845 household chemical Substances 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- MGIYRDNGCNKGJU-UHFFFAOYSA-N isothiazolinone Chemical compound O=C1C=CSN1 MGIYRDNGCNKGJU-UHFFFAOYSA-N 0.000 description 1
- 229940039717 lanolin Drugs 0.000 description 1
- 235000019388 lanolin Nutrition 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 208000030208 low-grade fever Diseases 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 125000001419 myristoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- HLERILKGMXJNBU-UHFFFAOYSA-N norvaline betaine Chemical compound CCCC(C([O-])=O)[N+](C)(C)C HLERILKGMXJNBU-UHFFFAOYSA-N 0.000 description 1
- 239000003002 pH adjusting agent Substances 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 208000005687 scabies Diseases 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 230000035483 skin reaction Effects 0.000 description 1
- 231100000430 skin reaction Toxicity 0.000 description 1
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- JAJWGJBVLPIOOH-IZYKLYLVSA-M sodium taurocholate Chemical compound [Na+].C([C@H]1C[C@H]2O)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC(=O)NCCS([O-])(=O)=O)C)[C@@]2(C)[C@@H](O)C1 JAJWGJBVLPIOOH-IZYKLYLVSA-M 0.000 description 1
- 238000002798 spectrophotometry method Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 229940117986 sulfobetaine Drugs 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Pharmacology & Pharmacy (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pain & Pain Management (AREA)
- Rheumatology (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to daily-use chemical industry technical field, a kind of plant amino acid shampoo and preparation method thereof is specifically disclosed, the plant amino acid shampoo includes: amino acid surfactant: 10~40%；Cosurfactant: 5~15%；Conditioner: 0.2~3%；Thickener: 0~4%；Dried orange peel extracts: 0.1~5%；Polyalcohol: 0~5%；Preservative: 0.02~0.5%；Surplus is water；The weight percentage of flavones is 70~95% in the dried orange peel extracts.The present invention uses amino acid type surfactant, mild pro-skin substantially reduces stimulation and injury to scalp, it is poor that nontraditional amino acid surfactant soil release performance as caused by surface-active difference is overcome simultaneously, the unstable disadvantage of foam, dried orange peel extracts are additionally used as functional component, ingredient is relatively easy, material is easy to obtain, not only property is mild for its obtained hair washing product, it can be while anti-inflammatory antibacterial, scalp of releiving, alleviating external environment to hair injury, the moist nursing for taking into account hair makes the hair after washing keep submissive.
Description
Technical field
The invention belongs to daily-use chemical industry technical field, it is related to a kind of plant amino acid shampoo, more particularly to a kind of containing old
Amino acid shampoo of bark extract and preparation method thereof.
Background technique
China's hair washing market for water is that personal care market development is earliest, one of most fast market, shampoo production and sale
Amount has accounted for first of the whole world.Shampoo mainly based on surfactant compound made of, with cleaning people scalp and hair,
And keep the product of its beauty function.Currently on the market most shampoo be all using sulfate surfactant, although
Strong cleaning force, but they are higher, bigger to the irritation of scalp with the residual quantity on hair in scalp, correct scared scale
There are certain harmful effects.As the improvement of people's living standards, mild, safety product is increasingly by the blueness of people
It looks at, has gradually appeared the hair washing product using amino acid surfactant as primary surfactant now.The amino acid table of low stimulation
Face activating agent substitutes traditional Sulfates surfactant, greatly reduces shampoo to the irritation of scalp, degreasing power is kept away
Exempt from the problems such as causing the inflammation of sensitive scalp.Most amino acid surfactants have mild cleaning force, wash rear hair
A softer and smoother touch degree is preferable, but foam is not easy to rinse, and soil release performance is poor, hair conditioning is inadequate, therefore seeks surface-active in shampoo
Proportion between agent is to reach preferable dirt-removing power as key problem.
Inadequate for the scalability of shampoo, many shampoos are added some traditional Chinese medicine ingredients at present, and Chinese medical extract at
Point various, drug effect is complicated, and the irritation taste of Chinese medical extract greatly reduces the use feeling of shampoo, meanwhile, Chinese materia medica preparation is given birth to
Production. art is complicated, and effect is single and anti-inflammatory fungistatic effect is weak.Therefore, develop a kind of ingredient is simple, effect is excellent, strong cleaning force,
The mild plant amino acid shampoo of performance is very important.
Summary of the invention
It is an object of the invention in view of the above problems, provide the anti-inflammatory antibacterial, scalp of releiving of one kind, alleviate the external world
Environment injures hair, while having the plant amino acid shampoo of excellent foam and detergency.
The purpose of the present invention is achieved through the following technical solutions: a kind of plant amino acid shampoo, including following weight point
Several raw materials:
Amino acid surfactant: 10~40%；
Cosurfactant: 5~15%；
Conditioner: 0.2~3%；
Thickener: 0~4%；
Dried orange peel extracts: 0.1~5%；
Polyalcohol: 0~5%；
Preservative: 0.02~0.5%；
Surplus is water；
The weight percentage of flavones is 70~95% in the dried orange peel extracts.
The preparations of the dried orange peel extracts the following steps are included:
(1) weigh and crush dried orange peel: claim dried orange peel is crushed, sieving；
(2) it extracts: smashed dried orange peel in step (1) being added in Extraction solvent and is impregnated, and dried orange peel and Extraction solvent is added
The citric acid of gross mass 0.1~0.5%, while being aided with ultrasound, and be heated to 50~60 DEG C and extract, extraction 2~3 times, every time
2~3h, filtering, filtrate merge, be concentrated under reduced pressure into Extraction solvent amount be 10%~20% when, obtain filtrate；
(3) dry: filtrate obtained in step (2) is freeze-dried to get dried orange peel extracts.
The Extraction solvent is that mass fraction is at least one of 30~50% ethyl alcohol, ethylene glycol, propylene glycol.
The dried orange peel is a kind of integration of drinking and medicinal herbs in China from rutaceae orange and its mature pericarp of variety
Chinese traditional herbs, bitter, pungent, warm-natured, return lung, the spleen channel have regulating qi-flowing for strengthening spleen, eliminating dampness and eliminating phlegm effect.Medicinal material is divided into " old
Skin " and " citrus chachiensis hortorum ", wherein with the quality of " citrus chachiensis hortorum " be it is excellent, in " citrus chachiensis hortorum " again using Xinhui tangerine peel as genunie medicinal materials.Dried orange peel
It is to strip pericarp by winning ripening fruits, made of sun drying or low temperature drying, air-dry time is usually 1 year or more.Dried orange peel
In containing the chemical components such as flavone compound, alkaloid, volatile oil, polysaccharide and a variety of the essential trace elements of the human bodys, have
It is anti-oxidant, anti-inflammatory, antiallergy and it is antitumor the effects of, pharmaceutically having been widely used and Utilization prospects.At present by dried orange peel
It is used as medicine or is used in household chemicals for more in food, but seldom.Multicomponent acts synergistically in dried orange peel extracts, can inhibit
Scalp pruritus nourishes root of hair, allows the tough health of healthy hair, submissive glossy.
The dried orange peel extracts are Xinhui tangerine peel extract.
The amino acid surfactant is sodium lauroyl glutamate, lauroyl glutamate potassium, cocoyl paddy
Propylhomoserin potassium, sodium cocoyl glutamate, cocoyl disodium glutamate, cocoyl glutamic acid TEA salt, myristoyl paddy ammonia
Sour potassium, myristoyl sodium glutamate, sodium methyl cocoyl taurate, cocoyl alanine TEA salt, cocoamido
The combination of one or more of sodium propionate, cocoyl Sodium Glycinate, sodium lauroyl sarcosine.
The cosurfactant is combined selected from one or more of glycine betaine, alkyl glycosides, alkanolamide class.
The betaines are Cocoamidopropyl betaine, lauroylamidopropyl betaine, coco betaine, laurel
One or more of base glycine betaine, lauryl hydroxy sulfo lycine, cocamidopropyl propyl amide hydroxyl sulfo betaine.
The alkyl glycosides is lauryl glucoside, in cocoyl glucoside, octyl glucoside, myristyl glucoside
It is one or more of
The alkanolamide class is coconut oleoyl amine MEA, coconut oleoyl amine DEA, lauramide DEA, stearmide DEA, coconut oleoyl amine
One or more of MIPA, coconut oleoyl amine DIPA, coconut oleoyl amine methyl MEA, cetyl-PG hydroxyethyl palmitamide.
The conditioner is cation guar gum, polyquaternium and one of silicone oil or vegetable fat or combinations thereof.
Preferably, the polyquaternium is hexadecyltrimethylammonium chloride, polyquaternium -7, Polyquaternium-10, poly- season
One of ammonium salt -67, polyquaternium -39, palmitamide hydroxypropyltrimonium chloride or combinations thereof.
Preferably, the cation guar gum is guar hydroxypropyltrimonium ammonium chloride, cassia gum Hydroxyproyl Trimethyl
One of ammonium chloride.
Preferably, the vegetable fat is one of camellia seed oil, oil of ginger, wheat-germ oil.
The polyalcohol is the one or more of pungent glycol, pentanediol, butanediol, Sensiva SC50, dipropylene glycol.Institute
Stating polyalcohol has certain bacteriostasis, can reduce the dosage of preservative.
The thickener be card wave, acrylic acid esters co-polymer, carboxymethyl cellulose, hydroxyethyl cellulose, xanthan gum,
One or more of PEG-120 methyl dioleate.
The plant amino acid shampoo, further include pearling agent, chelating agent, PH regulator, dipotassium glycyrrhizinate, in essence
It is at least one.
The chelating agent be selected from one of disodium ethylene diamine tetraacetate, tetrasodium ethylenediamine tetraacetate, Etidronic Acid or
Several combinations；It is preferred that disodium ethylene diamine tetraacetate.
The PH regulator is citric acid, tartaric acid, sulfonic acid, triethanolamine.
The preservative is Phenoxyethanol, sodium benzoate, methylparaben, propylben, DMDM hydantoin, methyl
The combination of one or more of isothiazolinone, methylchloroisothiazandnone, iodopropynyl butyl formate.
A kind of preparation method of plant amino acid shampoo is claimed in the present invention simultaneously, comprising the following steps:
(1) conditioner is mixed at room temperature with about 5~15% water, is slowly stirred, is uniformly dispersed, be heated to 50~70 DEG C, obtains molten
Liquid A；
(2) thickener is pre-dissolved with 5~15% water, is slowly stirred, is uniformly dispersed, obtains solution B；
(3) chelating agent is added in remaining water, amino acid surfactant, supplementary table is sequentially added after being warming up to 50~65 DEG C
Face activating agent, polyalcohol, stir evenly, and add solution A and solution B, stir 5~10 minutes, heat preservation to whole material dissolutions；
(4) the remaining material including dried orange peel extracts is added after being cooled to 35~45 DEG C, stirs evenly, is finally adjusted with PH
Agent adjusts pH.
The present invention has the advantages that
1. the present invention uses amino acid type surfactant, mild pro-skin substantially reduces stimulation and injury to scalp, simultaneously
Nontraditional amino acid table is overcome by proportion optimizing with the use of cosurfactant using amino acid type surfactant
Activating agent soil release performance as caused by surface-active difference in face is poor, the unstable disadvantage of foam, and amino acid surfactant is also
With no anaphylaxis, even if child, pregnant woman or sensibility hair quality can be applicable in.
2. present invention employs dried orange peel extracts as functional component, ingredient is relatively easy, and material is easy to obtain, and obtains
Not only property is mild for the hair washing product arrived, can anti-inflammatory antibacterial, scalp of releiving, alleviate external environment to hair injure while,
The moist nursing for taking into account hair makes the hair after washing keep submissive.
3. plant amino acid shampoo of the present invention, simple production process are suitable for large-scale production, have a vast market
Prospect.
The invention will be further described by the following examples.
Specific embodiment
The technical solution used in the present invention is: a kind of plant amino acid shampoo, by the raw material group of following weight fraction
At:
Amino acid surfactant: 10~40%；
Cosurfactant: 5~15%；
Conditioner: 0.2~3%；
Thickener: 0~4%；
Dried orange peel extracts: 0.1~5%；
Polyalcohol: 0~5%；
Preservative: 0.02~0.5%；
Surplus is water；
The weight percentage of flavones is 70~95% in the dried orange peel extracts.
Flavones total amount is high in the content of dried orange peel extracts in the present invention, to hair can play anti-inflammatory antibacterial, scalp of releiving,
Alleviate the effect that injure to hair of external environment, and also contains a small amount of alkaloid, volatile oil, polysaccharide and micro- in dried orange peel extracts
Secondary element, these multicomponents synergistic effect, correct micromicro play the role of moist, submissive synergy.
The measurement of flavones content is first to prepare flavones content-absorbance (A) by reference substance of rutin in dried orange peel extracts
Standard curve checks in corresponding flavones content by standard curve by the A value of measurement, and the specific test method is as follows:
(1) spectrophotometry of standard sample is established
0.0997g rutoside standard sample accurately is weighed in beaker, adds methanol to dissolve in 40 DEG C of water-bath low-grade fevers, after being cooled to room temperature
It is placed in 100ml volumetric flask, adds methanol to scale, shake up.Accurate measuring 10ml, which is placed in 100ml volumetric flask, is diluted with water to quarter
Degree, shakes up the standard solution to get 0.100mg/ml.
(2) foundation of standard curve
Accurate measuring standard solution 0ml, 0.5ml, 1.0ml, 2.0ml, 3.0ml, 4.0ml, 5.0ml adds in 10ml volumetric flask
Enter distilled water and be settled to 5ml, 5% sodium nitrite solution 0.3ml is added, shakes up, after placing 6~8 minutes, 10% nitric acid is added
0.3 ml of aluminum solutions, shakes up, and after placing 6~8 minutes, adds 1mol/L sodium hydroxide solution 4ml, distilled water is added to be diluted to quarter
Degree, shakes up, and places 20 minutes, its absorbance of survey, is averaged for parallel 3 times in 500nm at, makes standard curve.
(3) in dried orange peel extracts general flavone content measurement
Dried orange peel extracts 0.1g is weighed, with methanol constant volume into 100 ml volumetric flasks, takes 1.0 ml of sample liquid in 10ml volumetric flask
In, according to the method for step (2), its absorbance is surveyed everywhere in 500nm, is calculated according to the standard curve that step (2) obtains old
The content of flavones in bark extract.
The preparations of the dried orange peel extracts the following steps are included:
(1) weigh and crush dried orange peel: claim dried orange peel is crushed, sieving；
(2) it extracts: smashed dried orange peel in step (1) being added in Extraction solvent and is impregnated, and dried orange peel and Extraction solvent is added
The citric acid of gross mass 0.1~0.5%, while being aided with ultrasound, and be heated to 50~60 DEG C and extract, extraction 2~3 times, every time
2~3h, filtering, filtrate merge, be concentrated under reduced pressure into Extraction solvent amount be 10%~20% when, obtain filtrate；
(3) dry: filtrate obtained in step (2) is freeze-dried to get dried orange peel extracts.
The Extraction solvent is that mass fraction is at least one of 30~50% ethyl alcohol, ethylene glycol, propylene glycol.
Preferably, the Extraction solvent is the mixture of ethyl alcohol and ethylene glycol or ethyl alcohol and propylene glycol, ethyl alcohol and ethylene glycol
Or the mass ratio of ethyl alcohol and propylene glycol is 5:1~2:1.
Preferably, the dried orange peel extracts are Xinhui tangerine peel extract.
The storage time of the dried orange peel is 3~6 years.
The power of the ultrasound is 200~500W.
The solid-liquid ratio of the dried orange peel and the Extraction solvent are as follows: 1:10~1:50.
Preferably, the solid-liquid ratio of the dried orange peel and the Extraction solvent are as follows: 1:20~1:30.
Preferably, the amino acid surfactant is sodium lauroyl glutamate, sodium cocoyl glutamate, methyl
At least one of cocoyl sodium taurocholate.
Preferably, the amino acid surfactant is sodium lauroyl glutamate or methyl cocoyl taurine
Sodium and sodium cocoyl glutamate compounding, sodium lauroyl glutamate or sodium methyl cocoyl taurate and cocoyl paddy
The mass ratio of propylhomoserin sodium is 7:2~1:1.
Preferably, the cosurfactant is that lauryl glucoside and Cocoamidopropyl betaine compound, laurel
The mass ratio of base glucoside and Cocoamidopropyl betaine is 3:1~1:1.
In a preferred embodiment of the present invention, the plant amino acid shampoo includes the group of following weight percent
Point:
Sodium lauroyl glutamate or sodium methyl cocoyl taurate: 10~25%；
Sodium cocoyl glutamate: 3~15%；
Lauryl glucoside: 3~10%；
Cocoamidopropyl betaine: 1~5%；
Alkanolamide 1~5%；
Conditioner: 0.2~3%；
Polyalcohol: 0~5%；
Dried orange peel extracts: 0.1~5%；
Preservative: 0.02~0.5%；
EDETATE SODIUM: 0.05~0.2%；
Essence: appropriate；
Surplus is water.
A kind of preparation method of plant amino acid shampoo of the present invention, preparation process are as follows: (1) at room temperature by conditioner
The mixing of about 5~15% water, is slowly stirred, is uniformly dispersed, be heated to 50~60 DEG C, obtain solution A；(2) add in remaining water
Enter EDETATE SODIUM, amino acid surfactant, cosurfactant sequentially added after being warming up to 50~65 DEG C, is stirred evenly,
Polyalcohol is added, is stirred 5~10 minutes, heat preservation to whole material dissolutions；(3) dried orange peel is added after being cooled to 35~45 DEG C to extract
Object, preservative, essence, stir evenly, and finally adjust pH with pH adjusting agent.
Below with reference to embodiment, the invention will be further described.
Embodiment 1:
A kind of plant amino acid shampoo, raw material composition such as the following table 1:
The raw material of 1 plant amino acid shampoo of table forms
The preparations of dried orange peel extracts of the invention the following steps are included:
(1) weigh and crush Xinhui tangerine peel: claim Xinhui tangerine peel 1g is crushed, sieving；
(2) extract: it is to impregnate in 50% Extraction solvent that smashed dried orange peel in step (1), which is added to 20ml mass fraction, is mentioned
Solvent is taken to be made of ethyl alcohol and ethylene glycol, mass ratio 3:1, and the citric acid of 0.1g is added, while being aided with ultrasound, and add
Heat is extracted to 55 DEG C, extract 3 times, each 2h, filtering, filtrate merge, be concentrated under reduced pressure into Extraction solvent amount be 10% when, obtain
Filtrate；
(3) dry: filtrate obtained in step (2) is freeze-dried to get flaxen dried orange peel extracts.
The measurement of flavones content is first to prepare flavones content-absorbance (A) by reference substance of rutin in dried orange peel extracts
Standard curve checks in corresponding flavones content by standard curve by the A value of measurement, in the dried orange peel extracts by above-mentioned preparation
The content of flavones is 83.2%.
Embodiment 2:
A kind of plant amino acid shampoo, raw material composition such as the following table 2:
The raw material of 2 plant amino acid shampoo of table forms
The preparations of dried orange peel extracts of the invention the following steps are included:
(1) weigh and crush Xinhui tangerine peel: claim Xinhui tangerine peel 1g is crushed, sieving；
(2) extract: it is to impregnate in 50% Extraction solvent that smashed dried orange peel in step (1), which is added to 30ml mass fraction, is mentioned
Solvent is taken to be made of ethyl alcohol and propylene glycol, mass ratio 5:1, and the citric acid of 0.1g is added, while being aided with ultrasound, and add
Heat is extracted to 60 DEG C, extract 3 times, each 3h, filtering, filtrate merge, be concentrated under reduced pressure into Extraction solvent amount be 15% when, obtain
Filtrate；
(3) dry: filtrate obtained in step (2) is freeze-dried to get flaxen dried orange peel extracts.
The measurement of flavones content is first to prepare flavones content-absorbance (A) by reference substance of rutin in dried orange peel extracts
Standard curve checks in corresponding flavones content by standard curve by the A value of measurement, in the dried orange peel extracts by above-mentioned preparation
The content of flavones is 90.6%.
Embodiment 3:
A kind of plant amino acid shampoo, raw material composition such as the following table 3:
The raw material of 3 plant amino acid shampoo of table forms
The preparations of dried orange peel extracts of the invention the following steps are included:
(1) weigh and crush Xinhui tangerine peel: claim Xinhui tangerine peel 1g is crushed, sieving；
(2) extract: it is to impregnate in 40% Extraction solvent that smashed dried orange peel in step (1), which is added to 25ml mass fraction, is mentioned
Solvent is taken to be made of ethyl alcohol and propylene glycol, mass ratio 3:1, and the citric acid of 0.08g is added, while being aided with ultrasound, and
60 DEG C are heated to extract, extract 3 times, each 3h, filtering, filtrate merge, be concentrated under reduced pressure into Extraction solvent amount be 10% when,
Obtain filtrate；
(3) dry: filtrate obtained in step (2) is freeze-dried to get flaxen dried orange peel extracts.
The measurement of flavones content is first to prepare flavones content-absorbance (A) by reference substance of rutin in dried orange peel extracts
Standard curve checks in corresponding flavones content by standard curve by the A value of measurement, in the dried orange peel extracts by above-mentioned preparation
The content of flavones is 86.9%.
Comparative example 1:
A kind of plant amino acid shampoo, raw material composition such as the following table 4:
The raw material of 4 plant amino acid shampoo of table forms
Comparative example 1: containing only amino acid surfactant sodium methyl cocoyl taurate and cosurfactant cocounut oil acyl
Amine propyl betaine and coconut oleoyl amine MIPA.
Comparative example 2:
A kind of amino acid shampoo is free of dried orange peel extracts, raw material composition such as the following table 5:
The raw material of 5 plant amino acid shampoo of table forms
Test case 1: skin irritation/corrosion test
Tested material: the plant amino acid shampoo that embodiment 1-3 and comparative example 1-2 are prepared；
Experimental animal: healthy rabbits 50, weight 80-220g are chosen, half male and half female；
Test side's content: before test about for 24 hours, cutting off a hair for rabbit back backbone two sides, do not damage epidermis, and removing gross area is 3cm
×3cm.It takes each 0.5g of shampoo to be directly applied on skin, is then covered with two layers of gauze (2.5cm × 2.5cm) and one layer of glassine paper
Lid, with immobilization with adhesive tape, other side skin is as control.Shampoo is removed after application 4h, and washes away residual tested material with clear water, is gone
Except 1,24, the 48 and 72h observation recipient site local skin reaction after tested material, " cosmetics safety technical specification " (2015 is pressed
Year version) skin irritation/corrosion test carries out dermoreaction scoring, and synthesis is carried out with the average value that animal subject integrates and is commented
Valence, and observe other side effects effect in addition to irritation.
Test result: each observing time point top mean value < 0.5 in test belongs to nonirritant, that is, skin irritation
Test result are as follows: nonirritant.Therefore plant amino acid shampoo provided by the invention is milder to skin, it is nontoxic non-stimulated.
Test case 2: foam height and stability
It is measured according to GB13173-2008, the method is as follows: shampoo prepared by Example 1-3, comparative example 1 and comparative example 2
Each 2.5g is dissolved with 150mg/kg hard water respectively, is transferred in 1000mL volumetric flask, and be diluted to scale, shakes up.It again will be molten
Liquid is placed in (40 ± 0.5) DEG C water bath with thermostatic control and is aged, total time 30min since adding water-soluble sample, is then surveyed with Roche foam meter
Determine foam height, is shown in Table 6.
6 foam parameters of table
As shown in Table 6, the initial foam height of plant amino acid shampoo prepared by the present invention is about 16cm, and comparative example 1
Foaming characteristic and foam stability are poorer than the effect of the amino acid shampoo prepared of embodiment of the present invention 1-3, illustrate offer of the present invention
The mutual compatibility of amino acid surfactant can enhance foaming characteristic, test also measured were the height of foam after 5min, finds this hair
Bright embodiment 1-3 hair washing water bubble is more stable.
Test case 3: detergency ability
Test method: greasy dirt is made in 50g lanolin and the stirring of 1g charcoal powder；Then same human hair is used into 20% lauryl alcohol sulphur
It cleans 10 minutes in acid sodium solution vibrating machine, is rinsed well after taking-up using clear water, hair dryer is blown to constant weight (W), is equally divided into 5
Then greasy dirt is applied on topknot (every beam 0.1g greasy dirt) by group, every group of 5 beams, be air-dried at room temperature placement 48 hours, then weigh
(W1), it is dissolved in using 0.5g shampoo in the water that 100ml hardness is 250mg/L, is put into topknot, vibrating machine is cleaned 30 minutes, taken
Out, it is washed till non-foam with clear water, hair dryer is blown to constant weight, weighs (W2), calculate decontamination rate.Decontamination rate=(W1-W2)/(W1-W)
× 100%, specific it is as shown in the table；
7 shampoo decontamination rate of table
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 |
| Decontamination rate (%) | 90.1 | 89.3 | 87.8 | 70.2 | 87.6 |
As can be seen from Table 7, strong using shampoo dirt-removing power made from 1-3 of the embodiment of the present invention.
Test case 4:
The effect of evaluating the plant amino acid shampoo and comparative sample 1-2 of embodiment 1-3 using points-scoring system.Experimental subjects is year
50 volunteers that age is 18~40 years old, every group of 10 people, male to female ratio 1:1, according to phase when volunteer uses hair washing water sample
The hair washing of same method, every kind of shampoo is continuous with two weeks respectively, and hair washing is primary every three days, according to the feeling of oneself to shampoo
Score, scoring using 5 points of systems, 1 point to be worst, 3 points are moderate, 5 points be it is best, score more high effect is better.Various uses
Effect assessment average mark result is listed in the table below 8:
Shampoo made from 1-3 of the embodiment of the present invention, it is clearly smooth with rear hair, it is easy to comb, deep layer is takeed good care of and nourished impaired
Hair quality, not plus the use feeling of the comparative example 2 of dried orange peel extracts is not good enough.
Test case 5: the test of anti-dandruff and itching-relieving effect
Selection has head to itch and 25 to 55 years old triers of dandruff problem male 20 people, 40 people of female, is randomly divided into two groups, every group of male 10
People, 20 people of female.Two groups use hair washing in embodiment 3,2 shampoo of comparative example every two days primary respectively, and statistics uses after two weeks
As a result.As a result it is listed in the table below.Standards of grading: 5 points are no dandruff, and 4 points are the greyish white rough scales of small flakes, and 3 points are small
To median size chip, 2 points for the loose big and thin chip being connected of scalp, 1 point is divided for big tackness chip 1.Not scabies
Itch 5 points, itch 4 is divided sometimes for part, and often itch 3 is divided for part, and itch 2 is divided all over the face, and seriously itch 1 is divided all over the face.
By result as it can be seen that plant amino acid hair washing water energy of the invention effectively improves head and itches and dandruff problem.
Claims (10)
1. a kind of plant amino acid shampoo, which is characterized in that the raw material including following weight fraction:
Amino acid surfactant: 10~40%；
Cosurfactant: 5~15%；
Conditioner: 0.2~3%；
Thickener: 0~4%；
Dried orange peel extracts: 0.1~5%；
Polyalcohol: 0~5%；
Preservative: 0.02~0.5%；
Surplus is water；
The weight percentage of flavones is 70~95% in the dried orange peel extracts.
2. plant amino acid shampoo according to claim 1, it is characterized in that: the preparation of the dried orange peel extracts include with
Lower step:
(1) weigh and crush dried orange peel: claim dried orange peel is crushed, sieving；
(2) it extracts: smashed dried orange peel in step (1) being added in Extraction solvent and is impregnated, and dried orange peel and Extraction solvent is added
The citric acid of gross mass 0.1~0.5%, while being aided with ultrasound, and be heated to 50~60 DEG C and extract, extraction 2~3 times, every time
2~3h, filtering, filtrate merge, be concentrated under reduced pressure into Extraction solvent amount be 10%~20% when, obtain filtrate；
(3) dry: filtrate obtained in step (2) is freeze-dried to get dried orange peel extracts.
3. plant amino acid shampoo according to claim 2, it is characterized in that: it is 30 that the Extraction solvent, which is mass fraction,
The combination of one or both of~50% ethyl alcohol, ethylene glycol, propylene glycol.
4. plant amino acid shampoo according to claim 1, it is characterized in that: the amino acid surfactant is
Sodium lauroyl glutamate, lauroyl glutamate potassium, cocoyl potassium glutamate, sodium cocoyl glutamate, cocoyl
Disodium glutamate, cocoyl glutamic acid TEA salt, myristoyl potassium glutamate, myristoyl sodium glutamate, methyl cocoyl
Acyl taurines sodium, cocoyl alanine TEA salt, cocoamido sodium propionate, cocoyl Sodium Glycinate, lauroyl flesh
The combination of one or more of propylhomoserin sodium.
5. plant amino acid shampoo according to claim 1, it is characterized in that: the cosurfactant is selected from beet
The combination of one or more of alkali, alkyl glycosides, alkanolamide class.
6. plant amino acid shampoo according to claim 5, it is characterized in that: the betaines are cocamidopropyl propyl amide
Glycine betaine, lauroylamidopropyl betaine, coco betaine, lauryl betaine, lauryl hydroxy sulfo lycine, cocounut oil acyl
One or more of amine hydroxysultaine；
The alkyl glycosides is one of lauryl glucoside, cocoyl glucoside, octyl glucoside, myristyl glucoside
Or it is several；
The alkanolamide class is coconut oleoyl amine MEA, coconut oleoyl amine DEA, lauramide DEA, stearmide DEA, coconut oleoyl amine
One or more of MIPA, coconut oleoyl amine DIPA, coconut oleoyl amine methyl MEA, cetyl-PG hydroxyethyl palmitamide.
7. plant amino acid shampoo according to claim 1, it is characterized in that: the conditioner be cation guar gum,
Polyquaternium and one of silicone oil or vegetable fat or combinations thereof.
8. plant amino acid shampoo according to claim 7, it is characterized in that: the polyquaternium is cetyl front three
Ammonium chloride, polyquaternium -7, Polyquaternium-10, Polyquaternium-67, polyquaternium -39, palmitamide oxypropyl trimethyl chlorine
Change one of ammonium or combinations thereof；
The cation guar gum is guar hydroxypropyltrimonium ammonium chloride, one in cassia gum hydroxypropyl-trimethyl ammonium chloride
Kind；
The vegetable fat is one of camellia seed oil, oil of ginger, wheat-germ oil.
9. plant amino acid shampoo according to claim 1, it is characterized in that: the polyalcohol be pungent glycol, pentanediol,
The one or more of butanediol, Sensiva SC50, dipropylene glycol；
The thickener is card wave, acrylic acid esters co-polymer, carboxymethyl cellulose, hydroxyethyl cellulose, xanthan gum, PEG-
One or more of 120 methyl dioleates；
The plant amino acid shampoo, further include pearling agent, chelating agent, PH regulator, dipotassium glycyrrhizinate, in essence at least
It is a kind of；
The chelating agent is selected from one or more of disodium ethylene diamine tetraacetate, tetrasodium ethylenediamine tetraacetate, Etidronic Acid
Combination；It is preferred that disodium ethylene diamine tetraacetate；
The PH regulator is citric acid, tartaric acid, sulfonic acid, triethanolamine；
The preservative is Phenoxyethanol, sodium benzoate, methylparaben, propylben, DMDM hydantoin, the different thiophene of methyl
The combination of one or more of oxazoline ketone, methylchloroisothiazandnone, iodopropynyl butyl formate.
10. -9 a kind of preparation method of plant amino acid shampoo according to claim 1, which is characterized in that including following
Step:
(1) conditioner is mixed at room temperature with about 5~15% water, is slowly stirred, is uniformly dispersed, be heated to 50~70 DEG C, obtains molten
Liquid A；
(2) thickener is pre-dissolved with 5~15% water, is slowly stirred, is uniformly dispersed, obtains solution B；
(3) chelating agent is added in remaining water, amino acid surfactant, supplementary table is sequentially added after being warming up to 50~65 DEG C
Face activating agent, polyalcohol, stir evenly, and add solution A and solution B, stir 5~10 minutes, heat preservation to whole material dissolutions；
(4) the remaining material including dried orange peel extracts is added after being cooled to 35~45 DEG C, stirs evenly, is finally adjusted with PH
Agent adjusts pH.
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| CN112773751A (en) * | 2021-01-12 | 2021-05-11 | 吴维碧 | Infant shampoo and preparation method thereof |
| CN112999114A (en) * | 2021-02-04 | 2021-06-22 | 拉芳家化股份有限公司 | Hair care shampoo containing perfume slow-release particles |
| CN113545995A (en) * | 2020-04-23 | 2021-10-26 | 北京罗氏化妆品有限责任公司 | Formula of amino acid shampoo without silicone oil |
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