CN1879599A - Shampoo containing plant extracts - Google Patents
Shampoo containing plant extracts Download PDFInfo
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- CN1879599A CN1879599A CNA2006100783609A CN200610078360A CN1879599A CN 1879599 A CN1879599 A CN 1879599A CN A2006100783609 A CNA2006100783609 A CN A2006100783609A CN 200610078360 A CN200610078360 A CN 200610078360A CN 1879599 A CN1879599 A CN 1879599A
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- CN
- China
- Prior art keywords
- shampoo
- extract
- leaf
- plant extract
- fructus citri
- Prior art date
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- Granted
Links
- 239000002453 shampoo Substances 0.000 title claims abstract description 37
- 239000000419 plant extract Substances 0.000 title claims abstract description 27
- 239000000284 extract Substances 0.000 claims abstract description 26
- 229930003935 flavonoid Natural products 0.000 claims abstract description 16
- 150000002215 flavonoids Chemical class 0.000 claims abstract description 16
- 235000017173 flavonoids Nutrition 0.000 claims abstract description 16
- 239000004094 surface-active agent Substances 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 9
- 239000000686 essence Substances 0.000 claims abstract description 7
- 239000000049 pigment Substances 0.000 claims abstract description 7
- 239000008367 deionised water Substances 0.000 claims abstract description 5
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 36
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical class [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 21
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical class CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 20
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 18
- -1 polyethylene Polymers 0.000 claims description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 15
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 12
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 12
- QZXSMBBFBXPQHI-UHFFFAOYSA-N N-(dodecanoyl)ethanolamine Chemical compound CCCCCCCCCCCC(=O)NCCO QZXSMBBFBXPQHI-UHFFFAOYSA-N 0.000 claims description 9
- 238000000605 extraction Methods 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 8
- BTBJBAZGXNKLQC-UHFFFAOYSA-N ammonium lauryl sulfate Chemical compound [NH4+].CCCCCCCCCCCCOS([O-])(=O)=O BTBJBAZGXNKLQC-UHFFFAOYSA-N 0.000 claims description 7
- 229940063953 ammonium lauryl sulfate Drugs 0.000 claims description 7
- 230000002421 anti-septic effect Effects 0.000 claims description 7
- 244000060011 Cocos nucifera Species 0.000 claims description 6
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 6
- 239000004698 Polyethylene Substances 0.000 claims description 6
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 6
- 125000002252 acyl group Chemical group 0.000 claims description 6
- 230000001476 alcoholic effect Effects 0.000 claims description 6
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 6
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 6
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 6
- 150000001768 cations Chemical class 0.000 claims description 6
- 239000003208 petroleum Substances 0.000 claims description 6
- 229920000573 polyethylene Polymers 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000011734 sodium Substances 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 239000011780 sodium chloride Substances 0.000 claims description 6
- 229910021653 sulphate ion Inorganic materials 0.000 claims description 6
- 239000002202 Polyethylene glycol Substances 0.000 claims description 5
- 238000005119 centrifugation Methods 0.000 claims description 5
- 230000006837 decompression Effects 0.000 claims description 5
- 238000004821 distillation Methods 0.000 claims description 5
- 239000000706 filtrate Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 229940100242 glycol stearate Drugs 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 229920001223 polyethylene glycol Polymers 0.000 claims description 5
- 229920002907 Guar gum Polymers 0.000 claims description 3
- 239000000665 guar gum Substances 0.000 claims description 3
- 229960002154 guar gum Drugs 0.000 claims description 3
- 235000010417 guar gum Nutrition 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 10
- 239000006260 foam Substances 0.000 abstract description 9
- 230000002708 enhancing effect Effects 0.000 abstract description 7
- 230000036039 immunity Effects 0.000 abstract description 6
- 201000000849 skin cancer Diseases 0.000 abstract description 5
- 230000001954 sterilising effect Effects 0.000 abstract description 5
- 208000001840 Dandruff Diseases 0.000 abstract description 4
- 239000001100 (2S)-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)chroman-4-one Substances 0.000 abstract description 3
- 239000001606 7-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2S,3R,4R,5R,6S)-3,4,5-trihydroxy-6-methyloxan-2-yl]oxyoxan-2-yl]oxy-5-hydroxy-2-(4-hydroxyphenyl)chroman-4-one Substances 0.000 abstract description 3
- 244000089795 Clausena lansium Species 0.000 abstract description 3
- 235000008738 Clausena lansium Nutrition 0.000 abstract description 3
- QUQPHWDTPGMPEX-UHFFFAOYSA-N Hesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(COC4C(C(O)C(O)C(C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-UHFFFAOYSA-N 0.000 abstract description 3
- 208000003251 Pruritus Diseases 0.000 abstract description 3
- QUQPHWDTPGMPEX-UTWYECKDSA-N aurantiamarin Natural products COc1ccc(cc1O)[C@H]1CC(=O)c2c(O)cc(O[C@@H]3O[C@H](CO[C@@H]4O[C@@H](C)[C@H](O)[C@@H](O)[C@H]4O)[C@@H](O)[C@H](O)[C@H]3O)cc2O1 QUQPHWDTPGMPEX-UTWYECKDSA-N 0.000 abstract description 3
- APSNPMVGBGZYAJ-GLOOOPAXSA-N clematine Natural products COc1cc(ccc1O)[C@@H]2CC(=O)c3c(O)cc(O[C@@H]4O[C@H](CO[C@H]5O[C@@H](C)[C@H](O)[C@@H](O)[C@H]5O)[C@@H](O)[C@H](O)[C@H]4O)cc3O2 APSNPMVGBGZYAJ-GLOOOPAXSA-N 0.000 abstract description 3
- VUYDGVRIQRPHFX-UHFFFAOYSA-N hesperidin Natural products COc1cc(ccc1O)C2CC(=O)c3c(O)cc(OC4OC(COC5OC(O)C(O)C(O)C5O)C(O)C(O)C4O)cc3O2 VUYDGVRIQRPHFX-UHFFFAOYSA-N 0.000 abstract description 3
- QUQPHWDTPGMPEX-QJBIFVCTSA-N hesperidin Chemical compound C1=C(O)C(OC)=CC=C1[C@H]1OC2=CC(O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]4[C@@H]([C@H](O)[C@@H](O)[C@H](C)O4)O)O3)O)=CC(O)=C2C(=O)C1 QUQPHWDTPGMPEX-QJBIFVCTSA-N 0.000 abstract description 3
- 229940025878 hesperidin Drugs 0.000 abstract description 3
- 229930019673 naringin Natural products 0.000 abstract description 3
- DFPMSGMNTNDNHN-ZPHOTFPESA-N naringin Chemical compound O[C@@H]1[C@H](O)[C@@H](O)[C@H](C)O[C@H]1O[C@H]1[C@H](OC=2C=C3O[C@@H](CC(=O)C3=C(O)C=2)C=2C=CC(O)=CC=2)O[C@H](CO)[C@@H](O)[C@@H]1O DFPMSGMNTNDNHN-ZPHOTFPESA-N 0.000 abstract description 3
- 229940052490 naringin Drugs 0.000 abstract description 3
- ARGKVCXINMKCAZ-UHFFFAOYSA-N neohesperidine Natural products C1=C(O)C(OC)=CC=C1C1OC2=CC(OC3C(C(O)C(O)C(CO)O3)OC3C(C(O)C(O)C(C)O3)O)=CC(O)=C2C(=O)C1 ARGKVCXINMKCAZ-UHFFFAOYSA-N 0.000 abstract description 3
- 229930182486 flavonoid glycoside Natural products 0.000 abstract description 2
- 150000007955 flavonoid glycosides Chemical class 0.000 abstract description 2
- 235000001759 Citrus maxima Nutrition 0.000 abstract 2
- 244000276331 Citrus maxima Species 0.000 abstract 2
- 206010020751 Hypersensitivity Diseases 0.000 abstract 1
- 206010061218 Inflammation Diseases 0.000 abstract 1
- 208000000453 Skin Neoplasms Diseases 0.000 abstract 1
- 208000026935 allergic disease Diseases 0.000 abstract 1
- 230000007815 allergy Effects 0.000 abstract 1
- 230000004054 inflammatory process Effects 0.000 abstract 1
- 230000007803 itching Effects 0.000 abstract 1
- 239000003755 preservative agent Substances 0.000 abstract 1
- 230000002335 preservative effect Effects 0.000 abstract 1
- 230000003405 preventing effect Effects 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 10
- 239000000243 solution Substances 0.000 description 9
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 8
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 5
- 230000003110 anti-inflammatory effect Effects 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 230000002265 prevention Effects 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 4
- 230000003266 anti-allergic effect Effects 0.000 description 4
- 230000001139 anti-pruritic effect Effects 0.000 description 4
- 239000003908 antipruritic agent Substances 0.000 description 4
- 210000004761 scalp Anatomy 0.000 description 4
- 238000010008 shearing Methods 0.000 description 4
- 201000008261 skin carcinoma Diseases 0.000 description 4
- 238000004659 sterilization and disinfection Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 102220470372 Thymosin beta-10_K12A_mutation Human genes 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 238000010790 dilution Methods 0.000 description 3
- 239000012895 dilution Substances 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 230000006870 function Effects 0.000 description 3
- 239000003292 glue Substances 0.000 description 3
- 239000008233 hard water Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 239000003945 anionic surfactant Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 230000003648 hair appearance Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 208000000044 Amnesia Diseases 0.000 description 1
- 208000031091 Amnestic disease Diseases 0.000 description 1
- 206010002660 Anoxia Diseases 0.000 description 1
- 241000976983 Anoxia Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010006458 Bronchitis chronic Diseases 0.000 description 1
- 206010007191 Capillary fragility Diseases 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010021143 Hypoxia Diseases 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 241001464837 Viridiplantae Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 230000006986 amnesia Effects 0.000 description 1
- 230000007953 anoxia Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 210000000748 cardiovascular system Anatomy 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 208000007451 chronic bronchitis Diseases 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses shampoo containing plant extracts, which comprises a surfactant, a foam booster, a tackifier, a pearling agent, a conditioner, a preservative, a pigment, essence and deionized water, and is characterized in that: the shampoo also contains a shaddock leaf and/or Chinese wampee leaf extract, wherein the shaddock leaf and Chinese wampee leaf extract accounts for 0.05-15.0% of the weight of the shampoo. The shampoo disclosed by the invention is rich in flavonoid substances such as naringin, hesperidin and flavonoid glycoside, and can achieve the effects of sterilizing, relieving itching, stopping dandruff, resisting inflammation and allergy, preventing skin cancer, enhancing immunity and the like.
Description
Technical field
The present invention relates to a kind of shampoo that contains plant extract.
Background technology
Along with the raising of people's living standard, also more and more higher to the prescription of shampoo.Originally, as long as shampoo satisfies clean of people's requirement, but along with growth in the living standard, it is straight smooth that people require to wash the back hair at leisure, anti-dandruff or the like, nowadays, along with the trend of naturalization, nutrient laden and the curative effectization of international hair shampoo article, more and more be subjected to the favor of consumer with the composite shampoo of the natural Chinese medicinal herb, plant extraction liquid and the natural nutriment that have no side effect, have curative effect and Nutrition.
Summary of the invention
The object of the present invention is to provide a kind of shampoo that contains plant extract, its mature production technology, product is easy to use, gentle, non-stimulated, foam enriches, smooth elegant with the back hair, skin is totally comfortable, and have sterilization, antipruritic, end functions such as bits, antiinflammatory, antiallergic and prevention skin carcinoma, enhancing immunity, be the Mobyneb shampoo that integrates clean, hair care and skin and complexion improving.
For achieving the above object, the present invention adopts following technical scheme:
A kind of shampoo that contains plant extract of the present invention, it comprises surfactant, suds booster, viscosifier, pearling agent, conditioner, antiseptic, pigment, essence, deionized water, also contain leaf of Fructus Citri grandis and/or Folium clausenae lansii extract in the described shampoo, the percentage by weight that described plant extract accounts for shampoo is 0.05~15.0%.
The extracting method of leaf of Fructus Citri grandis of the present invention and Folium clausenae lansii extract is: get leaf of Fructus Citri grandis and Folium clausenae lansii defat with petroleum ether after-filtration, obtain defat leaf of Fructus Citri grandis and Folium clausenae lansii; To the alcoholic solution that wherein adds 70%, under 80 ℃ of constant temperature, refluxed 6 hours, cooled and filtered is concentrated to 1/7 volume with the filtrate decompression distillation, with isopyknic water-saturated n-butanol extraction, getting the distilling under reduced pressure of n-butyl alcohol phase is concentrated to and is the thick time cooling of brown, the dissolve with methanol solution of adding 80% adds acetone again and fully vibrates centrifugation, dry pale yellow powder shape extract, i.e. flavonoid material.
Surfactant of the present invention is selected from one or more combination of ammonium lauryl sulfate, Sodium Alcohol Ether Sulphate or fat alcohol polyethylene ether ammonium sulfate.
Suds booster of the present invention and viscosifier are selected from one or more combination of coconut monoethanolamide, cocoanut oil diethan olamide, Oleum Cocois acyl group CAB or sodium chloride.
Pearling agent of the present invention is a polyethylene glycol stearate diester.
Conditioner of the present invention is selected from one or more combination of cation guar gum, polyquaternary ammonium salt-39 or polyquaternium-7.
Antiseptic of the present invention is an isothiazolone magnesium sulfate.
Leaf of Fructus Citri grandis is rich in the plain material of multiple flavonoid such as naringin, hesperidin, they have unique armaticity and significant pharmacotoxicological effect, can prevent and treat the disease and the chronic bronchitis of cardiovascular system, also have cough-relieving, relieving asthma eliminate the phlegm, anti-capillary fragility, anti-inflammatory and effects such as irritated active, antibacterial, anticancer, antioxidation, blood circulation promoting and enhancing immunity.And be rich in flavonoid glycoside in the Folium clausenae lansii, treatment diabetes, anoxia, amnesia etc. are had significant curative effect.
The present invention extracts the active ingredient of leaf of Fructus Citri grandis and Folium clausenae lansii and is applied in the shampoo, reach the sterilization of high-efficient and lasting ground, antipruritic, end bits, antiinflammatory, the purpose of antiallergic and prevention skin carcinoma and enhancing immunity, again in conjunction with anion surfactant and other surfactants, make product easy to use, gentle, non-stimulated, foam is abundant, smooth elegant with the back hair, skin is totally comfortable, and has a sterilization, antipruritic, end bits, antiinflammatory, antiallergic, and prevention skin carcinoma, functions such as enhancing immunity are clean of collection, hair care and skin and complexion improving are in the Mobyneb shampoo of one.
The ammonium lauryl sulfate that the present invention selects to use is K12 ammonium salt (ALSA), belongs to mild acidulous anion surfactant.Foam is abundant, and zest is little, and viscosity is big, easily flushing.
Polyoxyethylenated alcohol sodium sulfate is soluble in water, has good decontamination, emulsifying, foam performance and anti-performance of hard water, and biological degradability is good.AESA has good washing detergency ability and biological degradability, and anti-hard water is strong, in hard water, promptly is when having a large amount of dirts to exist, also to have good foaming characteristic.Foam is abundant, fine and smooth, and gives hair soft with easy combing sense with skin is smooth and comfort.
Surfactant of the present invention aspect is selected ammonium lauryl sulfate (K12A), Sodium Alcohol Ether Sulphate (AES) or fat alcohol polyethylene ether ammonium sulfate (AESA) for use; With coconut monoethanolamide (CMEA), cocoanut oil diethan olamide (6501) and Oleum Cocois acyl group CAB (CAB) or sodium chloride is suds booster and viscosifier, play a part foam enhancing, surely the bubble and tackify.Selecting polyethylene glycol stearate diester for use is pearling agent, gives the product pearl effect.With cation pawl that glue (C-14-S), polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 is conditioner, further improves the sensation after washing.Antiseptic is selected isothiazolone magnesium sulfate for use.Good product performance after these compositions are composite, bubble soon, also have the ability of certain bacteria growing inhibiting, keep the soft and smooth of the normal function of skin and hair quality, do not damage hair quality.
The batch process production method is adopted in the production procedure that contains the shampoo of plant extract of the present invention.
In mixing kettle, heat up earlier surfactant ammonium lauryl sulfate (K12A), Sodium Alcohol Ether Sulphate (AES) or the dissolvings such as (AESA) of fat alcohol polyethylene ether ammonium sulfate, then add pearlescent flake, dissolving, be warmed up to 84~87 ℃, water with about 3% disperses your glue of cation pawl the back to add, then temperature is raised to 85~87 ℃, polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 after the water dilution of adding about 3%, because the system under the high temperature is very rare, and polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 are very thick, disperse polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 to disperse with enough big shearing force, and rare system can't provide enough big shearing force, disperses so polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 dilution add easily.Cool to about 70 ℃; add coconut monoethanolamide (CMEA), cocoanut oil diethan olamide (6501) and raw materials such as Oleum Cocois acyl group CAB (CAB) or sodium chloride then successively; add plant extract (flavonoid), essence and pigment when stirring is cooled to 40 ℃ of left and right sides, stir.
The shampoo sample that contains plant extract of the present invention meets national body lotion QB1994 standard through the light industrial goods supervision and inspection station check of Guangdong Bureau of Technical Supervision.Through the check of Guangdong health and epidemic prevention station, its every index meets the sanitary quality standard and the security requirement of national regulation fully.
The shampoo that contains plant extract of the present invention, walk the road of green plants comprehensive exploitation, from leaf of Fructus Citri grandis and Folium clausenae lansii, extract flavonoid materials such as naringin, hesperidin and Clausena lansium (Lour.) Skeels glycoside, have sterilization, antipruritic, only bits, antiinflammatory, antiallergic and effects such as prevention skin carcinoma and enhancing immunity.Shampoo performance gentleness of the present invention, foam are abundant, and be clearly comfortable, integrates clean, hair care, skin and complexion improving, through many batches on probation, effect is fine, does not have any untoward reaction.
The specific embodiment
The extraction and the evaluation of embodiment 1 leaf of Fructus Citri grandis extract
Take by weighing fresh leaf of Fructus Citri grandis 50 gram, clean, dry and pulverizes afterwards standby; With filtering with buchner funnel behind the defat with petroleum ether, obtain the defat leaf of Fructus Citri grandis; The defat leaf of Fructus Citri grandis is placed the 500ml boiling flask, shake up to the alcoholic solution 350ml that wherein adds 70% then, under 80 ℃ of constant temperature, refluxed 6 hours with Rotary Evaporators, filter with buchner funnel the cooling back, the filtrate decompression distillation is concentrated to 50ml, with isopyknic water-saturated n-butanol extraction, getting the distilling under reduced pressure of n-butyl alcohol phase is concentrated to and is the thick time cooling of brown, add 80% methanol solution 3ml dissolving, adding acetone 40ml more fully vibrates, centrifugation, oven dry promptly gets pale yellow powder shape extract, and wherein flavonoids content is 50%.
Test experience: extract and dense ammonia, magnesium powder/hydrochloric acid reaction produce feature yellow fluorescence and dark pink respectively, and judging above-mentioned leaf of Fructus Citri grandis extract qualitatively is flavonoids.
Details are as follows for flavonoids qualitative experiment scheme:
1, dense ammonia react:
Extract is dissolved with small amount of ethanol, point is on silica gel H (5%CMC is a binding agent) plate, use petroleum ether respectively: ethyl acetate=2: 1, chloroform: methanol=10: 1, ethyl acetate: acetone=10: 1 chromatographies, smoked on the strong aqua ammonia layer, place immediately under the fluorescent lamp, produce 3~4 bright yellow fluorescence speckles.
2, hydrochloric acid, magnesium powder reaction:
The alcoholic solution 1ml that gets extract adds magnesium powder in test tube an amount of, and the concentrated hydrochloric acid number droplet of reinjecting (1 time add) is dark pink at the foam place.
3, there is characteristic absorption the ultra-violet (UV) band of extract about 250nm.
4, extract is the pale yellow powder shape, has hydrophilic to a certain degree.
The extraction and the evaluation of embodiment 2 Folium clausenae lansii extracts
1, gets fresh Folium clausenae lansii 1000 gram, clean, dry and pulverizes afterwards standby;
2, with filtering with buchner funnel behind the defat with petroleum ether, obtain the defat Folium clausenae lansii;
3, the defat Folium clausenae lansii is placed the boiling flask of 5L, shake up to the alcoholic solution 3.5L that wherein adds 70% then, under 80 ℃ of constant temperature, refluxed 6 hours, filter with buchner funnel the cooling back, the filtrate decompression distillation is concentrated to 500ml, with isopyknic water-saturated n-butanol extraction, getting the distilling under reduced pressure of n-butyl alcohol phase is concentrated to and is the thick time cooling of brown, the methanol solution 30ml dissolving of adding 80%, adding 400ml acetone more fully vibrates, centrifugation, oven dry promptly gets pale yellow powder shape extract, and wherein flavonoids content is 50%.
4, test experience: extract and dense ammonia, magnesium powder/hydrochloric acid reaction produce feature yellow fluorescence and dark pink respectively, judge that qualitatively the said extracted thing is the flavonoids in leaf of Fructus Citri grandis or the Folium clausenae lansii.
Flavonoids qualitative experiment scheme is with embodiment 1.
The extraction and the evaluation of embodiment 3 leaf of Fructus Citri grandis and Folium clausenae lansii extract
1, gets fresh leaf of Fructus Citri grandis and Folium clausenae lansii totally 1000 grams, clean, dry and pulverizes afterwards standby;
2, with filtering with buchner funnel behind the defat with petroleum ether, obtain defat leaf of Fructus Citri grandis and Folium clausenae lansii;
3, defat leaf of Fructus Citri grandis and Folium clausenae lansii are placed the boiling flask of 5L, shake up to the alcoholic solution 3.5L that wherein adds 70% then, under 80 ℃ of constant temperature, refluxed 6 hours, filter with buchner funnel the cooling back, the filtrate decompression distillation is concentrated to 500ml, with isopyknic water-saturated n-butanol extraction, getting the distilling under reduced pressure of n-butyl alcohol phase is concentrated to and is the thick time cooling of brown, the methanol solution 30ml dissolving of adding 80%, add 400ml acetone again and fully vibrate, centrifugation, oven dry promptly gets pale yellow powder shape extract, wherein, flavonoids content is 50%.
4, test experience: extract and dense ammonia, magnesium powder/hydrochloric acid reaction produce feature yellow fluorescence and dark pink respectively, judge that qualitatively the said extracted thing is the flavonoids in leaf of Fructus Citri grandis and the Folium clausenae lansii.
Flavonoids qualitative experiment scheme is with embodiment 1.
The preparation of embodiment 4-7 shampoo
The shampoo that contains plant extract of the present invention, comprise surfactant, suds booster, viscosifier, pearling agent, conditioner, antiseptic, pigment, essence, deionized water, also containing plant extract, is the flavonoid material that extracts from leaf of Fructus Citri grandis and/or Folium clausenae lansii; The percentage by weight of described plant extract is 0.05~15.0.
Concrete preparation method is as follows:
In mixing kettle, heat up earlier surfactant ammonium lauryl sulfate (K12A), Sodium Alcohol Ether Sulphate (AES) or the dissolvings such as (AESA) of fat alcohol polyethylene ether ammonium sulfate, then add the pearling agent polyethylene glycol stearate diester, dissolving, be warmed up to 84~87 ℃, water with about 3% disperses your glue of cation pawl the back to add, then temperature is raised to 85~87 ℃, add polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 after 3% left and right sides water dilutes, (because the system under the high temperature is very rare, and polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 are very thick, disperse polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 to disperse with enough big shearing force, and rare system can't provide enough big shearing force, disperses so polyquaternary ammonium salt-7 (M550) and polyquaternary ammonium salt-39 dilution add easily.) cool to about 70 ℃; add coconut monoethanolamide (CMEA), cocoanut oil diethan olamide (6501) and raw materials such as Oleum Cocois acyl group CAB (CAB) or sodium chloride then successively; add plant extract, essence and pigment when stirring is cooled to 40 ℃ of left and right sides, stir.
Concrete proportioning such as following table, the plant extract in its invading the exterior in the proportioning 1,2,3 and 4 be corresponding embodiment 1,2,3 and 4 plant extracts that prepare respectively.
Embodiment 4 | Embodiment 5 | Embodiment 6 | Embodiment 7 | ||
Composition | Proportioning 1 (weight %) | Proportioning 2 (weight %) | Proportioning 3 (weight %) | Proportioning 4 (weight %) | |
Plant extract | 0.05 | 5.0 | 10.0 | 15.0 | |
Surfactant | Ammonium lauryl sulfate (25%) | 15.0 | 8.0 | 0 | 0 |
Sodium Alcohol Ether Sulphate (70%) | 5.0 | 7.0 | 0 | 9.0 | |
Fat alcohol polyethylene ether ammonium sulfate (70%) | 0 | 6.0 | 10.0 | 7.0 | |
Suds booster and viscosifier | Coconut monoethanolamide | 0 | 1.5 | 2.0 | 0 |
Cocoanut oil diethan olamide | 1.5 | 0 | 1.8 | 2.0 | |
Oleum Cocois acyl group CAB | 1.6 | 1.7 | 1.5 | 0 | |
Sodium chloride | In right amount | In right amount | In right amount | In right amount | |
Pearling agent | Polyethylene glycol stearate diester | 1.7 | 1.5 | 1.8 | 2.0 |
Conditioner | Cation guar gum | 0 | 0.5 | 0 | 0.5 |
Polyquaternary ammonium salt-39 | 3.0 | 0 | 3.5 | 3.3 | |
Polyquaternium-7 | 2.3 | 2.5 | 0 | 1.9 | |
Antiseptic | Isothiazolone magnesium sulfate | 0.1 | 0.1 | 0.1 | 0.1 |
Pigment | In right amount | In right amount | In right amount | In right amount | |
Essence | In right amount | In right amount | In right amount | In right amount | |
Deionized water | To 100.0 | To 100.0 | To 100.0 | To 100.0 |
Embodiment 8 trial effects that contain the shampoo of plant extract of the present invention
Object of study: scalp itch, dandruff is many, scalp is irritated, subinflammatory people, is divided into four experimental grouies, establishes a normal control group again, every group of each 50 people, wherein male 20 people, women 30 people.
Trial scheme:
Four experimental grouies every day 1-2 time, used 1 month continuously respectively with the shampoo hair washing of embodiment of the invention 4-7 preparation.
The normal control group every day 1-2 time, is used January continuously with the common shampoo hair washing on the market.
Experimental result:
Experimental group one | Experimental group two | Experimental group three | Experimental group four | The normal control group | |
Alleviate | 38 | 40 | 35 | 33 | 0 |
Obviously improve | 7 | 8 | 11 | 15 | 0 |
Invalid | 5 | 2 | 4 | 2 | 0 |
Worsen | 0 | 0 | 0 | 0 | 0 |
The result shows:
For scalp itch, dandruff is many, scalp is irritated, subinflammatory user, the life-time service shampoo that contains plant extract of the present invention has obvious effects.
The present invention is not limited to above-mentioned preferred forms, and other any identical with the present invention or akin products that anyone draws under enlightenment of the present invention all drop within protection scope of the present invention.
Claims (7)
1, a kind of shampoo that contains plant extract, it comprises surfactant, suds booster, viscosifier, pearling agent, conditioner, antiseptic, pigment, essence, deionized water, it is characterized in that: also contain leaf of Fructus Citri grandis and/or Folium clausenae lansii extract in the described shampoo, the percentage by weight that described leaf of Fructus Citri grandis and/or Folium clausenae lansii extract account for shampoo is 0.05~15.0%.
2, the shampoo that contains plant extract as claimed in claim 1, it is characterized in that: the extracting method of described leaf of Fructus Citri grandis and Folium clausenae lansii extract is: get leaf of Fructus Citri grandis and/or Folium clausenae lansii defat with petroleum ether after-filtration, obtain defat leaf of Fructus Citri grandis and/or Folium clausenae lansii; To the alcoholic solution that wherein adds 70%, under 80 ℃ of constant temperature, refluxed 6 hours, cooled and filtered is concentrated to 1/7 volume with the filtrate decompression distillation, with isopyknic water-saturated n-butanol extraction, getting the distilling under reduced pressure of n-butyl alcohol phase is concentrated to and is the thick time cooling of brown, the dissolve with methanol solution of adding 80% adds acetone again and fully vibrates centrifugation, dry pale yellow powder shape extract, i.e. flavonoid material.
3, the shampoo that contains plant extract as claimed in claim 1 or 2 is characterized in that: described surfactant is selected from one or more combination of ammonium lauryl sulfate, Sodium Alcohol Ether Sulphate or fat alcohol polyethylene ether ammonium sulfate.
4, the shampoo that contains plant extract as claimed in claim 1 or 2 is characterized in that: described suds booster and viscosifier are selected from one or more combination of coconut monoethanolamide, cocoanut oil diethan olamide, Oleum Cocois acyl group CAB or sodium chloride.
5, the shampoo that contains plant extract as claimed in claim 1 or 2 is characterized in that: described pearling agent is a polyethylene glycol stearate diester.
6, the shampoo that contains plant extract as claimed in claim 1 or 2 is characterized in that: described conditioner is selected from one or more combination of cation guar gum, polyquaternary ammonium salt-39 or polyquaternium-7.
7, the shampoo that contains plant extract as claimed in claim 1 or 2 is characterized in that: described antiseptic is an isothiazolone magnesium sulfate.
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