CN104758215A - Wudalianchi dryopteris fragrans mineral spring effervescent tablet and preparation method thereof - Google Patents
Wudalianchi dryopteris fragrans mineral spring effervescent tablet and preparation method thereof Download PDFInfo
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Abstract
Disclosed is a Wudalianchi dryopteris fragrans mineral spring effervescent tablet and a preparation method thereof, relating to dryopteris fragrans mineral spring effervescent tablets. The invention aims to solve the problems that the effective components of the conventional Wudalianchi dryopteris fragrans are not fully extracted, the efficacy cannot be effectively exerted, and the application effect is not good; and the existing bath products can not effectively improve skin diseases caused by bacterial and fungal infections, and the bath products applying antibiotics and corticosteroids have great harm to the body and the skin. The composition is prepared from 5-30 parts by mass of drynaria fragrans extract, 5-20 parts by mass of drynaria fragrans mineral water extract, 5-20 parts by mass of drynaria fragrans mineral mud powder, 5-50 parts by mass of an acid source, 5-50 parts by mass of an alkali source, 2-20 parts by mass of a lubricant, 0.1-50 parts by mass of a filler and 0.1-5 parts by mass of essential oil. The preparation method comprises the following steps: extracting dryopteris fragrans, mineral water extract and volcanic mud powder; mixing with acid source, alkali source, lubricant and filler.
Description
Technical field
The present invention relates to health bath product field, particularly a kind of Dryopteris fragrans (L.) Schott mineral spring effervescent tablet.
Background technology
The dermatosis that bacterial fungus infects is current commonly encountered diseases, frequently-occurring disease, it is inconvenient and painful greatly to bring to patient, because it easily recurs repeatedly, and life-time service antibiotic or corticosteroids medicine have larger harm to health and skin, cannot be solved the problem by simple bathing, bring very large puzzlement to people's life.
Dryopteris fragrans (L.) Schott medicinal history is long, and physiologically active is comparatively strong, and Popular Utilization is extensive.Be mainly used in treating the diseases such as various dermatosis and arthritis.Local chronicle according to Wudalianchi is recorded, and moved in local resident and just learn to utilize Dryopteris fragrans (L.) Schott decocting liquid to treat various dermatosis, especially to psoriatic therapeutic effect highly significant before the centuries.Local resident is considered as Dryopteris fragrans (L.) Schott " dermopathic jinx ".The medical value that spring is washed in Wudalianchi is very high, especially to treat dermatosis and arthritis is the most remarkable, annual have the person of recuperating that comes because of respect for the fame in a large number and visitor to come here to carry out health care of recuperating, and it is consistent that the health-care effect that spring bathes is washed in effect and the Wudalianchi of Wudalianchi Dryopteris fragrans (L.) Schott.
Summary of the invention
The present invention is that mainly to solve the extracts active ingredients of existing Wudalianchi Dryopteris fragrans (L.) Schott insufficient, and effect can not effectively play, and effect is not good; And existing bath article effectively can not improve antibacterial, the skin disease that fungal infection causes, the bath article of application antibiotic and corticosteroids has the problem of very major injury to health and skin, and provides Wudalianchi Dryopteris fragrans (L.) Schott mineral spring effervescent tablet and preparation method thereof.
Wudalianchi of the present invention Dryopteris fragrans (L.) Schott mineral spring effervescent tablet, it is be made up of 5 ~ 30 parts of Wudalianchi Dryopteris fragrans (L.) Schott extracts, 5 ~ 20 parts of Wudalianchi heavy carbonic mineral water extracts, 5 ~ 20 parts of Wudalianchi Volcanic sludge powder, 5 ~ 50 acid sources, 5-50 part alkali source, 2-20 part lubricant, 0.1-50 part filler and 0.1-5 part quintessence oils by mass fraction.
Wudalianchi of the present invention Dryopteris fragrans (L.) Schott mineral spring effervescent tablet preparation method, it carries out according to following steps:
One, after the Dryopteris fragrans (L.) Schott to more than 5cm that lava plateau, Wudalianchi grows being gathered, place shady and cool ventilation place natural drying, 20 orders are crushed to pulverizer after drying, be that 95% ethanol extracts according to the ratio of solid-to-liquid ratio 1:30 with volumn concentration, extraction time is 2 hours, extraction time 2 times, is lyophilized into powder after collecting extract concentrating under reduced pressure for subsequent use, collects residue for subsequent use simultaneously;
Two, with the residue that the Wudalianchi heavy carbonic mineral water through manganese sand aeration removing ferrimanganic is collected according to the ratio extraction step one of solid-to-liquid ratio 1:30, extraction time is 2 hours, extraction time 2 times, is lyophilized into Powdered for subsequent use after extract concentrating under reduced pressure;
Three, Wudalianchi Dryopteris fragrans (L.) Schott extract is namely obtained by after the freeze-dried powder of the freeze-dried powder of step one extract and step 2 extract in mass ratio 1:1 mixing;
Four, by Wudalianchi heavy carbonic mineral water after concentrating under reduced pressure, be lyophilized into powder, pulverize after cross 80 mesh sieves, obtain wudalianchi minerals extract;
Five, Wudalianchi Volcanic sludge, gathers the high-quality sludge of Wudalianchi Yaoquanshan sludge band underground 30cm ~ 100cm soil layer, pulverized 800 mesh sieves, and obtained Wudalianchi Volcanic sludge powder after drying in the shade;
Six, by acid source, alkali source, lubricant and filler, pulverized 80 mesh sieves, in mass ratio after 4:4:2:1 mixing, added 0.1 ~ 5 part of quintessence oil, then temperature be less than 26 DEG C, humidity under being the condition being less than 40% obtained powders A for subsequent use;
Seven, by after above-mentioned Wudalianchi Dryopteris fragrans (L.) Schott extract, Wudalianchi mineral spring extract, Wudalianchi Volcanic sludge powder and powders A in mass ratio 2:2:1:5 mixing, adding mass percentage is 1.5% dehydrated alcohol, make granule, after tabletting and get final product, Wudalianchi Dryopteris fragrans (L.) Schott mineral spring effervescent tablet.
The present invention comprises following beneficial effect:
The present invention extracts Wudalianchi Dryopteris fragrans (L.) Schott respectively with Wudalianchi heavy carbonic mineral water and 95% ethanol respectively, obtain its extract, namely save the water extraction part of Dryopteris fragrans (L.) Schott conventional use effective site, turn increase 95% ethanol extraction part of very strong fungistatic effect.The present invention extracts in Dryopteris fragrans (L.) Schott process and has used the natural heavy carbonic mineral water in Wudalianchi, this mineral water not only has the multiple trace element useful to human body, and wherein have a large amount of bicarbonate radicals, extraction ratio and the dissolubility of effective ingredient phloroglucinol derivatives material can be increased, extracts active ingredients efficiency is improved, the volcanic slurry powder added in the mineral spring effervescent tablet of the present invention's development and disintegrating agent effectively can increase the dissolubility of Dryopteris fragrans (L.) Schott fat-soluble active ingredient in water, the Wudalianchi Volcanic sludge powder added, because the loose structure of its uniqueness and adsorptivity better can make Effervescent tablet disintegration, shorten disintegration time, make disintegrate uniform and stable.Disintegrate can be higher the hardness of improvement effervescent tablet and the sticking phenomenon that reduces in effervescent tablet preparation process.
The present invention Wudalianchi is distinctive among the peoplely often has medical herbs Dryopteris fragrans (L.) Schott to be primary raw material, research is aided with appropriate effervescent and is developed into effervescent tablet by experiment, and add Wudalianchi heavy carbonic mineral spring extract, with volcanic slurry powder, to psoriasis, tinea manus and pedis, acne, beriberi, foot odor, the various skin diseases such as dermatitis all have good Prevention health-care effect.
Dryopteris fragrans (L.) Schott is made the effervescent tablet conveniently utilizing and carry by the present invention; resource utilization is improved; people use convenient, not only to psoriasis, and tinea manus and pedis; acne; the various skin diseases such as dermatitis all have improves effect preferably, and can anti-inflammation, and deodorization is antipruritic; the Wudalianchi heavy carbonic mineral spring extract added and sludge extract can bring to skin more fully protects and nourishes, and more can improve skin-protection and health-care effect of effervescent tablet.
Detailed description of the invention
Detailed description of the invention one: the Wudalianchi Dryopteris fragrans (L.) Schott mineral spring effervescent tablet of present embodiment, it is be made up of 5 ~ 30 parts of Wudalianchi Dryopteris fragrans (L.) Schott extracts, 5 ~ 20 parts of Wudalianchi heavy carbonic mineral water extracts, 5 ~ 20 parts of Wudalianchi Volcanic sludge powder, 5 ~ 50 acid sources, 5-50 part alkali source, 2-20 part lubricant, 0.1-50 part filler and 0.1-5 part quintessence oils by mass fraction.
Detailed description of the invention two: present embodiment and detailed description of the invention one unlike: described acid source is fumaric acid, citric acid, tartaric acid, adipic acid, malic acid one or more be mixed by any ratio.Other is identical with detailed description of the invention one.
Detailed description of the invention three: present embodiment and detailed description of the invention one are that one or more in sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, calcium carbonate are mixed by any ratio unlike: described alkali source.Other is identical with detailed description of the invention one.
Detailed description of the invention four: present embodiment and detailed description of the invention one unlike: described lubricant is Macrogol 4000, polyethylene glycol 6000, sodium lauryl sulphate, and one or more in hard magnesium, micropowder silica gel, sodium stearyl fumarate are mixed by any ratio.Other is identical with detailed description of the invention one.
Detailed description of the invention five: present embodiment and detailed description of the invention one are that one or more in dextrin, beta cyclodextrin, glucose, mannitol are mixed by any ratio unlike: described filler.Other is identical with detailed description of the invention one.
Detailed description of the invention six: the Wudalianchi Dryopteris fragrans (L.) Schott mineral spring effervescent tablet preparation method of present embodiment, it carries out according to following steps:
One, after the Dryopteris fragrans (L.) Schott to more than 5cm that lava plateau, Wudalianchi grows being gathered, place shady and cool ventilation place natural drying, 20 orders are crushed to pulverizer after drying, be that 95% ethanol extracts according to the ratio of solid-to-liquid ratio 1:30 with volumn concentration, extraction time is 2 hours, extraction time 2 times, is lyophilized into powder after collecting extract concentrating under reduced pressure for subsequent use, collects residue for subsequent use simultaneously;
Two, with the residue that the Wudalianchi heavy carbonic mineral water through manganese sand aeration removing ferrimanganic is collected according to the ratio extraction step one of solid-to-liquid ratio 1:30, extraction time is 2 hours, extraction time 2 times, is lyophilized into Powdered for subsequent use after extract concentrating under reduced pressure;
Three, Wudalianchi Dryopteris fragrans (L.) Schott extract is namely obtained by after the freeze-dried powder of the freeze-dried powder of step one extract and step 2 extract in mass ratio 1:1 mixing;
Four, by Wudalianchi heavy carbonic mineral water after concentrating under reduced pressure, be lyophilized into powder, pulverize after cross 80 mesh sieves, obtain wudalianchi minerals extract;
Five, Wudalianchi Volcanic sludge, gathers the high-quality sludge of Wudalianchi Yaoquanshan sludge band underground 30cm ~ 100cm soil layer, pulverized 800 mesh sieves, and obtained Wudalianchi Volcanic sludge powder after drying in the shade;
Six, by acid source, alkali source, lubricant and filler, pulverized 80 mesh sieves, in mass ratio after 4:4:2:1 mixing, added 0.1 ~ 5 part of quintessence oil, then temperature be less than 26 DEG C, humidity under being the condition being less than 40% obtained powders A for subsequent use;
Seven, by after above-mentioned Wudalianchi Dryopteris fragrans (L.) Schott extract, Wudalianchi mineral spring extract, Wudalianchi Volcanic sludge powder and powders A in mass ratio 2:2:1:5 mixing, adding mass percentage is 1.5% dehydrated alcohol, make granule, after tabletting and get final product, Wudalianchi Dryopteris fragrans (L.) Schott mineral spring effervescent tablet.
Detailed description of the invention seven: present embodiment and detailed description of the invention six unlike: the Wudalianchi heavy carbonic mineral water removing ferrimanganic through manganese sand aeration refers to: get wudalianchi minerals, by air aeration method, aeration 4h is carried out to wudalianchi minerals, leave standstill 72h, leave and take supernatant, to drain bottom precipitation, namely obtain the wudalianchi minerals after removing ferrum and manganese.Other is identical with detailed description of the invention six.
Experiment 1: Wudalianchi heavy carbonic mineral water and the research of distilled water extraction Dryopteris fragrans (L.) Schott extraction comparison.
Powder (20 order) 20g totally 10 parts after the pulverizing of accurate measuring Dryopteris fragrans (L.) Schott, respectively with the Wudalianchi heavy carbonic mineral water of manganese sand aeration removing ferrimanganic, Dryopteris fragrans (L.) Schott is extracted according to the ratio of solid-to-liquid ratio 1:30 with distilled water, extraction time is 2 hours, extraction time 2 times, extract concentrate drying, to constant weight, weighs the weight of dry thing, compares the weight result of two kinds of water extract as following table 1.
Table 1 Wudalianchi heavy carbonic mineral water and distilled water extraction Dryopteris fragrans (L.) Schott contrast experiment
As can be seen from Table 1, with the quality average out to 0.74g of the Dryopteris fragrans (L.) Schott extract of Wudalianchi heavy carbonic mineral water extraction.With the quality average out to of the Dryopteris fragrans (L.) Schott of distilled water extraction
Experiment 2: add sludge powder and do not add the comparative study of sludge powder to phloroglucinol dissolution rate in the Dryopteris fragrans (L.) Schott effervescent tablet of Wudalianchi.
Get the Dryopteris fragrans (L.) Schott mineral bath sheet adding 10% volcanic slurry powder developed and each 5 of the Dryopteris fragrans (L.) Schott mineral bath sheet not adding sludge powder, bath sheet contains total phloroglucinol of 1%, bath sheet is put in 500ml distilled water, after its complete disintegrate, bathe the content of phloroglucinol constituents in sheet aqueous solution with prison blue BB salt colour developing determined by ultraviolet spectrophotometry and calculate dissolution as following table 2.
The measurement of table 2 Wudalianchi Dryopteris fragrans (L.) Schott effervescent tablet phloroglucinol dissolution
As known from Table 2, the dissolution adding the Dryopteris fragrans (L.) Schott effervescent tablet phloroglucinol of Wu Da Lian chi sludge powder obviously increases, dissolution before not adding is on average 77.26%, and the dissolution not adding the phloroglucinol of the Dryopteris fragrans (L.) Schott effervescent tablet of Wu Da Lian chi sludge powder on average only has 57.90%.
For understanding the result of use of Wudalianchi Dryopteris fragrans (L.) Schott effervescent tablet prepared by the present invention, investigation on probation has widely been carried out with the Wudalianchi Dryopteris fragrans (L.) Schott effervescent tablet of the form of questionnaire survey to preparation, trier 100 people, wherein male 48 people, women 52 people, the oldest 53 years old, minimum 18 years old, about 32 years old mean age, the symptom that trier had dry, coarse, tinea, acne, chilblain in various degree or is chapped from the cold before volcano on probation cold spring bath sheet.Regain effective questionnaire 96 parts altogether after on probation, 96 triers use this product result of use to the indices of sensation of taking a shower, curative effect of disease, stimulation allergy after 4 weeks, and the result of self evaluation is as follows:
Table 3 product beta test statistical effect table
As shown in Table 3:
1, shower sensation: the trier of 52.08% takes a shower and feels good, the trier of 26.04% takes a shower sensation better;
2, skin condition: the trier of 51.04% has moderate to improve, and the trier of 20.83% has clear improvement;
3, allergy is stimulated: non-stimulated irritated example.
As can be seen from the result of the self assessment of trier, Wudalianchi Dryopteris fragrans (L.) Schott effervescent tablet has sensation of well taking a shower, and has good improvement result to the dermatosis of user, does not find that product produces stimulation allergic phenomena to trier.Show according to survey result: Wudalianchi Dryopteris fragrans (L.) Schott effervescent tablet effectively utilizes antibacterial active component and sludge powder, mineral water effective ingredient and the various active nutrient substance of Wudalianchi Dryopteris fragrans (L.) Schott, the disease problems that can improve skin can make again entirety conditioning and the maintenance of skin, better increase skin resistance, the composition of mineral spring and sludge more easily discharges the antibacterial active component of Dryopteris fragrans (L.) Schott simultaneously, be absorbed by the skin, make trier can enjoy the double effects of well take a shower sensation and disease curing health.
Claims (7)
1. Wudalianchi Dryopteris fragrans (L.) Schott mineral spring effervescent tablet, is characterized in that it is be made up of 5 ~ 30 parts of Wudalianchi Dryopteris fragrans (L.) Schott extracts, 5 ~ 20 parts of Wudalianchi heavy carbonic mineral water extracts, 5 ~ 20 parts of Wudalianchi Volcanic sludge powder, 5 ~ 50 acid sources, 5-50 part alkali source, 2-20 part lubricant, 0.1-50 part filler and 0.1-5 part quintessence oils by mass fraction.
2. Wudalianchi according to claim 1 Dryopteris fragrans (L.) Schott mineral spring effervescent tablet, it is characterized in that described acid source is fumaric acid, citric acid, tartaric acid, adipic acid, malic acid one or more be mixed by any ratio.
3. Wudalianchi according to claim 1 Dryopteris fragrans (L.) Schott mineral spring effervescent tablet, is characterized in that described alkali source is that one or more in sodium carbonate, sodium bicarbonate, potassium carbonate, potassium bicarbonate, calcium carbonate are mixed by any ratio.
4. Wudalianchi according to claim 1 Dryopteris fragrans (L.) Schott mineral spring effervescent tablet, it is characterized in that described lubricant is Macrogol 4000, polyethylene glycol 6000, sodium lauryl sulphate, hard magnesium, micropowder silica gel are hard, one or more in acyl fumaric acid sodium are mixed by any ratio.
5. Wudalianchi according to claim 1 Dryopteris fragrans (L.) Schott mineral spring effervescent tablet, is characterized in that described filler is that one or more in dextrin, beta cyclodextrin, glucose, mannitol are mixed by any ratio.
6. prepare Wudalianchi according to claim 1 Dryopteris fragrans (L.) Schott mineral spring effervescent tablet, it is characterized in that it carries out according to following steps:
One, after the Dryopteris fragrans (L.) Schott to more than 5cm that lava plateau, Wudalianchi grows being gathered, place shady and cool ventilation place natural drying, 20 orders are crushed to pulverizer after drying, be that 95% ethanol extracts according to the ratio of solid-to-liquid ratio 1:30 with volumn concentration, extraction time is 2 hours, extraction time 2 times, is lyophilized into powder after collecting extract concentrating under reduced pressure for subsequent use, collects residue for subsequent use simultaneously;
Two, with the residue that the Wudalianchi heavy carbonic mineral water through manganese sand aeration removing ferrimanganic is collected according to the ratio extraction step one of solid-to-liquid ratio 1:30, extraction time is 2 hours, extraction time 2 times, is lyophilized into Powdered for subsequent use after extract concentrating under reduced pressure;
Three, Wudalianchi Dryopteris fragrans (L.) Schott extract is namely obtained by after the freeze-dried powder of the freeze-dried powder of step one extract and step 2 extract in mass ratio 1:1 mixing;
Four, by Wudalianchi heavy carbonic mineral water after concentrating under reduced pressure, be lyophilized into powder, pulverize after cross 80 mesh sieves, obtain wudalianchi minerals extract;
Five, Wudalianchi Volcanic sludge, gathers the high-quality sludge of Wudalianchi Yaoquanshan sludge band underground 30cm ~ 100cm soil layer, pulverized 800 mesh sieves, and obtained Wudalianchi Volcanic sludge powder after drying in the shade;
Six, by acid source, alkali source, lubricant and filler, pulverized 80 mesh sieves, in mass ratio after 4:4:2:1 mixing, added 0.1 ~ 5 part of quintessence oil, then temperature be less than 26 DEG C, humidity under being the condition being less than 40% obtained powders A for subsequent use;
Seven, by after above-mentioned Wudalianchi Dryopteris fragrans (L.) Schott extract, Wudalianchi mineral spring extract, Wudalianchi Volcanic sludge powder and powders A in mass ratio 2:2:1:5 mixing, adding mass percentage is 1.5% dehydrated alcohol, make granule, after tabletting and get final product, Wudalianchi Dryopteris fragrans (L.) Schott mineral spring effervescent tablet.
7. the preparation method of Wudalianchi according to claim 6 Dryopteris fragrans (L.) Schott mineral spring effervescent tablet, it is characterized in that the Wudalianchi heavy carbonic mineral water through manganese sand aeration removing ferrimanganic refers to: get wudalianchi minerals, by air aeration method, aeration 4h is carried out to wudalianchi minerals, leave standstill 72h, leave and take supernatant, to drain bottom precipitation, namely obtain the wudalianchi minerals after removing ferrum and manganese.
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Cited By (2)
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| CN107693404A (en) * | 2017-11-03 | 2018-02-16 | 黑龙江省科学院火山与矿泉研究所 | Slime hair mask and method for preparing slime hair mask cap by using slime hair mask |
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| CN103239368A (en) * | 2013-05-21 | 2013-08-14 | 黑龙江省科学院火山与矿泉研究所 | Volcano cold spring bath tablet and preparation method thereof |
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| CN103239368A (en) * | 2013-05-21 | 2013-08-14 | 黑龙江省科学院火山与矿泉研究所 | Volcano cold spring bath tablet and preparation method thereof |
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Cited By (3)
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| CN106721692A (en) * | 2016-11-17 | 2017-05-31 | 黑龙江省科学院火山与矿泉研究所 | Instant Wudalianchi recarbonic mineral water fruit juice beverage and preparation method thereof |
| CN106721692B (en) * | 2016-11-17 | 2020-10-27 | 黑龙江省科学院火山与矿泉研究所 | Instant Wudalianchi recarbonic mineral water fruit juice beverage and preparation method thereof |
| CN107693404A (en) * | 2017-11-03 | 2018-02-16 | 黑龙江省科学院火山与矿泉研究所 | Slime hair mask and method for preparing slime hair mask cap by using slime hair mask |
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