CN107693404A - Slime hair mask and method for preparing slime hair mask cap by using slime hair mask - Google Patents
Slime hair mask and method for preparing slime hair mask cap by using slime hair mask Download PDFInfo
- Publication number
- CN107693404A CN107693404A CN201711072123.6A CN201711072123A CN107693404A CN 107693404 A CN107693404 A CN 107693404A CN 201711072123 A CN201711072123 A CN 201711072123A CN 107693404 A CN107693404 A CN 107693404A
- Authority
- CN
- China
- Prior art keywords
- parts
- volcanic mud
- water
- hair
- soluble
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
-
- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D44/00—Other cosmetic or toiletry articles, e.g. for hairdressers' rooms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D44/00—Other cosmetic or toiletry articles, e.g. for hairdressers' rooms
- A45D2044/007—Devices for determining the condition of hair or skin or for selecting the appropriate cosmetic or hair treatment
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/87—Application Devices; Containers; Packaging
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Biotechnology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
A slime hair mask and a method for preparing a slime hair mask cap by using the slime hair mask relate to a hair mask and a method for preparing the slime hair mask cap by using the slime hair mask. The invention aims to solve the problems that active ingredients in volcanic mud are damaged in the prior art, the active ingredients of the prepared hairdressing and hair care products are easy to damage, and the existing products on the market have unobvious effects on dandruff removal and hair loss. The slime hair mask is prepared from deionized water, a Wudalianchi frozen primary slime extract, a Wudalianchi heavy carbonic acid mineral water extract, linseed oil, malus wallichiana oil, hydrolyzed collagen, corn modified starch, docosyltrimethylammonium chloride, linoleamidopropyl dimethyl 2, 3-dipropyl propyl ammonium chloride, hydroxyethyl cellulose, dryopteris fragrans extract, polyquaternary ammonium salt-10, levorotatory vitamin C, vitamin E, citric acid and ethylparaben. The preparation method comprises the following steps: weighing raw materials, sequentially adding the weighed raw materials, stirring and mixing, and sealing the slime hair film into a hair film cap.
Description
Technical field
Film and the method using its preparation hair film cap are sent out the present invention relates to a kind of.
Background technology
Wudalianchi Volcanic sludge is that eruption is scattered in low-lying place before more than 300 years, the immersion through the mineral water several years,
The byproduct of the colcanism formed under biology, chemical action and Redox Condition, is natural aging sludge, is to answer
System treasures resource.Wudalianchi Volcanic sludge is applied primarily to paste mask in beauty treatment fields at present, and product type also compares
It is more single.
Because Wudalianchi Volcanic sludge is chronically at freezing state, for wherein active nutrient component preservation create it is non-
Chang Youliang condition, therefore, using the activity that Wudalianchi Volcanic mud carries out focusing on protecting it precious during product development into
Point.And in the preparation for send out membrane component, prior art can make it that the active component in volcanic mud is destroyed, and be made simultaneously
Hair-dressing and hair care product under air or illumination condition active component easily destroyed, performance is not sufficiently stable, and causes volcanic mud
Maximally utilizing for resource is not obtained in hairdressing and hair care art, causes the waste of resource, and existing anti-dandruff product needs
To use more than the 7th day, just start to show anti-dandruff effect, after user disables 5 days, dandruff continued growth, and use existing
There are anti-hair loss products hair loss effect and unobvious, it is only less than 20% to reduce alopecia rate.
The content of the invention
It can cause that the active component in volcanic mud is destroyed the invention solves prior art, while manufactured hairdressing is protected
Hair product active component under air or illumination condition easily destroyed, and commercially available prod to anti-dandruff and Anti-hair loss effect not
The problem of obvious, and a kind of sludge hair film is provided and prepares the method for sludge hair film cap using it.
A kind of sludge hair film is primary by 50 parts~70 parts deionized waters, 10 parts~20 parts Wudalianchi frosts in parts by weight
Sludge extract, 10 parts~20 parts Wudalianchi heavy carbonic mineral spring water extracts, 1 part~5 portions linseed oil, 1 part~5 parts Qiong Ya
Malus spectabilis oil, 1 part~5 parts Hydrolyzed Collagens, 1 part~5 parts maize modified starch, 0.5 part~5 parts behenyl chlorine
Change ammonium, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyls ammonium chlorides, 1 part~3 parts hydroxyethyl celluloses,
0.5 part~2 parts dryopteris fragrans extracts, 0.5 part~2 parts Polyquaternium-10s, 0.1 part~1 part L-vitamin C, 0.1 part~1
Part vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part ethyl hydroxy benzoate are prepared.
Carried out according to the following steps using a kind of method of sludge hair film preparation sludge hair film cap：
First, weigh：50 parts~70 parts deionized waters, 10 parts~20 parts Wudalianchi frost primary ores are weighed in parts by weight
Mud extract, 10 parts~20 parts Wudalianchi heavy carbonic mineral spring water extracts, 1 part~5 portions linseed oil, 1 part~5 parts Qiong Yahai
Chinese bush cherry oil, 1 part~5 parts Hydrolyzed Collagens, 1 part~5 parts maize modified starch, 0.5 part~5 parts behentrimonium chlorides
Ammonium, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyls ammonium chlorides, 1 part~3 parts hydroxyethyl celluloses, 0.5
Part~2 parts of dryopteris fragrans extracts, 0.5 part~2 parts Polyquaternium-10s, 0.1 part~1 part L-vitamin C, 0.1 part~1 part
Vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part ethyl hydroxy benzoate；
Described 50 parts~70 parts of deionized waters, 10 parts~20 parts Wudalianchis frost primary slime extracts, 10 parts~
20 parts of Wudalianchi heavy carbonic mineral spring water extracts, 1 part~5 parts maize modified starch, 0.5 part~5 parts docosyl front threes
Ammonium chloride, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyls ammonium chlorides and 1 part~3 parts hydroxy ethyl fibers
Element composition phase A；
Described 1 part~5 portions of linseed oil, 1 part~5 parts fine jade precipice Malus spectabilis oil and 0.5 part~2 parts Polyquaternium-10 compositions
Phase B；
Described 1 part~5 parts of Hydrolyzed Collagens, 0.5 part~2 parts dryopteris fragrans extracts, 0.1 part~1 part left-handed dimension
Raw plain C, 0.1 part~1 part vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part ethyl hydroxy benzoate composition phase C；
2nd, phase A and phase B are separately heated to temperature as 40 DEG C~50 DEG C, then low whipping speed be 300r/min~
Under conditions of 500r/min, phase B is added to stirring 10min~30min in phase A, obtains mixture, thing temperature to be mixed is down to
During room temperature, low whipping speed be 400r/min~600r/min under conditions of, into mixture add phase C and stir 5min~
10min, sludge hair film is obtained, sludge hair film is sealed into the cavity of hair film cap, that is, obtain sludge hair film cap；
Described hair film cap includes outer layer, internal layer and silica gel check valve；Cavity is formed between described outer layer and internal layer, it is interior
Layer lower surface is uniformly arranged multiple silica gel check valves, and silica gel check valve is connected with cavity, between silica gel check valve and cavity
Provided with diaphragm seal；The material of described outer layer, internal layer and silica gel check valve is the silica gel material of full shading；
Described silica gel check valve is made up of the first trapezoidal portion, the second trapezoidal portion and domed ends；First trapezoidal portion
One end end face is connected with one end end face in the second trapezoidal portion, and the other end in the second trapezoidal portion is provided with domed ends, hemisphere
Shape end is provided with opening, is open when applying process without external force, in the presence of silica gel material pretightning force, opening is close all the time
Envelope, it is open when there is external force to apply process, opening open.
The beneficial effects of the invention are as follows：
1st, the present invention, which realizes it and optimized with sludge component, combines and occurs synergy and reach its hair care function
Maximization, and in order to realize the complete performance of the stability and effect during use of hair film formulation, having invented one kind can be with
The packaging of matched application.
2nd, the state of dry hair and bifurcated can be effectively improved after use, deep layer, which is nourished, repairs hair scale piece, energy after use
Enough make hair more submissive glossy, and play the unique effects of the hair care anticreep of volcanic slurry.In addition, the present invention
Auxiliary package can realize keep in dark place, oxidizable composition applies the application in hair care and nourishing product.
3rd, constituent part in film is sent out due to formula sludge and is easily changed chemical property under air and illumination, hair is made
To depositing and using there is higher requirement after film, cause many compositions for having excellent activity to hair care hairdressing to be used in and match somebody with somebody
Fang Zhong.In order to solve this problem, the invention provides one kind to pack, and material is the silica gel material of soft, frivolous and full shading,
With good ductility, property is stable, safety, is not chemically reacted with internal component, and is readily extruded, and less residue is not
Easily waste.Profile is the shape of double-deck bathing cap, and there is Design of Screw Thread outside, is advantageous to the force of hand.Inside is cavity, will be had
The hair film of unstable chemical active ingredient is filling wherein, and a number of silica gel check valve is designed in the side for pressing close to scalp, often
The relatively thin diaphragm seal of material is provided with inside individual silica gel check valve.When use, hair film cap is worn on the head, passes through squeezing for hand
Pressure force, breaks through inner sealing film by the hair film in cavity, because the domed ends of silica gel check valve are provided with opening, opening
When applying process without external force, in the presence of silica gel material pretightning force, opening seals all the time, and being open is having external force to apply
Cheng Shi, opening open, therefore, when being exerted a force by the extruding of hand, opening open, sludge hair film extrude from silica gel check valve and
Hair contacts, and because the part that silica gel check valve protrudes can give scalp massage, therefore, passes through in the case where wearing hair film cap
The massage and rubbing of hand, hair film is completely attached to hair, to reach abundant massage, wear massage and ensure that air-isolation, and
And the temperature of scalp is kept, stimulate circulation, finally rinsed well with clear water.It is pre- in silica gel material when stopping force
In the presence of clamp force, opening is sealed all the time, and therefore, the hair film of extrusion will not be sucked in bathing cap by silica gel check valve again.Meanwhile this
Pack it is closed the entrance of light and air is avoided using space, while also result in a certain degree of heat insulation situation, make head
The temperature of hair is higher, promote head blood circulation and hair film in nutritional ingredient by hair and the degree of absorption of scalp.
4th, as a result this hair film is shown through crowd's test experiments：50 triers think that this product hair film is smeared after use
After be readily cleaned, the state of dry hair and bifurcated can be effectively improved, deep layer, which is nourished, repairs hair scale piece, and head can be made after use
The more submissive easily comb of hair, cleaning is flexible and is greatly improved rich in healthy glow, grease, itch, and uses rear non-stimulated mistake
Quick property.
5th, the sludge hair film trier that prepared by the present invention is still kept for the long period do not perplexed by dandruff in 5 days after disabling, and is tried
User just shows the effect of control dandruff well since using the 2nd day, illustrates that product prepared by the present invention can substantially change
Kind dandruff problem.
6th, 56 days using after product of the present invention, and during comb hair, hair loss hair loss significantly reduces, the hair loss 129 during by being not used
Reduce to 37, reduce alopecia 71.3%, and using after 7 days with regard to significant effect.
Brief description of the drawings
Fig. 1 is the structural representation of present invention hair film cap；
Fig. 2 is the sectional view of present invention hair film cap；
Fig. 3 is the structural representation of silica gel check valve.
Embodiment
Embodiment one：A kind of sludge of present embodiment hair film in parts by weight by 50 parts~70 parts deionized waters,
10 parts~20 parts Wudalianchis frost primary slime extracts, 10 parts~20 parts Wudalianchi heavy carbonic mineral spring water extracts, 1 part
~5 portions of linseed oil, 1 part~5 parts fine jade precipice Malus spectabilis oil, 1 part~5 parts Hydrolyzed Collagens, 1 part~5 parts maize modified starch,
0.5 part~5 parts INCROQUAT TMC-80s, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyl chlorine
Change ammonium, 1 part~3 parts hydroxyethyl celluloses, 0.5 part~2 parts dryopteris fragrans extracts, 0.5 part~2 parts Polyquaternium-10s, 0.1
Part~1 part of L-vitamin C, 0.1 part~1 part vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part oxybenzene second
Ester is prepared.
The beneficial effect of present embodiment is：1st, present embodiment realize its optimized with sludge component combine it is concurrent
It is raw to act synergistically to reach the maximization of its hair care function, and in order to realize effect during the stability of hair film formulation and use
Complete performance, invented it is a kind of can be with the packaging of matched application.
2nd, the state of dry hair and bifurcated can be effectively improved after use, deep layer, which is nourished, repairs hair scale piece, energy after use
Enough make hair more submissive glossy, and play the unique effects of the hair care anticreep of volcanic slurry.In addition, this embodiment party
The auxiliary package of formula can realize keep in dark place, oxidizable composition applies the application in hair care and nourishing product.
3rd, constituent part in film is sent out due to present embodiment formula sludge and is easily changed chemical property under air and illumination, made
To depositing and using there is higher requirement after into hair film, many compositions for having excellent activity to hair care hairdressing are caused to be employed
In formula.In order to solve this problem, present embodiments provide for one kind to pack, and material is soft, frivolous and full shading
Silica gel material, there is good ductility, property is stable, safety, is not chemically reacted with internal component, and is readily extruded,
Less residue is not easy to waste.Profile is the shape of double-deck bathing cap, and there is Design of Screw Thread outside, is advantageous to the force of hand.Inside is
Cavity 4, the hair film with unstable chemical active ingredient is filling wherein, and a number of silicon is designed in the side for pressing close to scalp
Glue check valve 3, each inside of silica gel check valve 3 are provided with the relatively thin diaphragm seal 5 of material.When use, hair film cap is worn over head
On, exerted a force by the extruding of hand, the hair film in cavity 4 is broken through into inner sealing film 5, due to the hemispherical of silica gel check valve 3
End 3-3 is provided with opening, is open when applying process without external force, in the presence of silica gel material pretightning force, opening is all the time
Sealing, it is open when there is external force to apply process, opening open, therefore, and when being exerted a force by the extruding of hand, opening open, sludge
Hair film is extruded from silica gel check valve 3 to be contacted with hair, because the part that silica gel check valve 3 protrudes can give scalp massage, because
This, wear send out film cap in the case of by the massage and rubbing of hand, hair film is completely attached to hair, with reach fully by
Rub, wear massage and ensure that air-isolation, and keep the temperature of scalp, stimulate circulation, finally rinsed well with clear water
.When stopping force, in the presence of silica gel material pretightning force, opening seals all the time, therefore, the hair film of extrusion will not again by
Silica gel check valve 3 is sucked in bathing cap.Meanwhile this packaging is closed that the entrance of light and air is avoided using space, while also make
Into a certain degree of heat insulation situation, make the temperature of hair higher, promote head blood circulation and hair film in nutrition into
Divide by hair and the degree of absorption of scalp.
4th, as a result this hair film is shown through crowd's test experiments：50 triers think that this product hair film is smeared after use
After be readily cleaned, the state of dry hair and bifurcated can be effectively improved, deep layer, which is nourished, repairs hair scale piece, and head can be made after use
The more submissive easily comb of hair, cleaning is flexible and is greatly improved rich in healthy glow, grease, itch, and uses rear non-stimulated mistake
Quick property.
5th, the sludge hair film trier that prepared by present embodiment is still kept for the long period do not perplexed by dandruff in 5 days after disabling,
And trier just shows the effect of control dandruff well since using the 2nd day, illustrate product prepared by present embodiment
It can obviously improve dandruff problem.
6th, 56 days using after present embodiment product, and during comb hair, hair loss hair loss significantly reduces, hair loss during by being not used
129 are reduced to 37, reduce alopecia 71.3%, and using after 7 days with regard to significant effect.
Embodiment two：Present embodiment is unlike embodiment one：Described Wudalianchi frost
Primary slime extract is prepared according to the following steps：
First, the preparation of volcanic mud water-soluble extracting liquid：
1., Wudalianchi Volcanic sludge is placed in ultra low temperature freezer and freezed, be subsequently placed in temperature for -80 DEG C~-
It is freeze-dried in 55 DEG C of vacuum freeze drier, obtains volcanic slurry freeze-dried powder；2., rotating speed be 1100r/min~
Under conditions of 1200r/min, volcanic slurry freeze-dried powder is well mixed with water, mud mixture is obtained, then mixes muddy water
Thing is placed in ultrasonic extractor, prolonged agitation, under conditions of supersonic frequency is 25kHz~40kHz, extraction 45min~
60min, obtain upper strata suspension and sediment；Described volcanic slurry freeze-dried powder and the mass ratio of water are 1:(20~25)；③、
By 2. sediment that step obtains by step 2. ultrasonic extraction 2 times~3 times, upper strata suspension and extraction water-soluble extracting liquid are obtained
Volcanic mud afterwards；4., combining step 2. and step 3. gained upper strata suspension, filter upper strata suspension, that is, obtain volcanic mud
Water-soluble extracting liquid；
2nd, the preparation of volcanic mud alcohol-soluble extract solution：
Volcanic mud after extraction water-soluble extracting liquid is added to the ethanol water that mass percent is 25%~70%
In, ultrasonic 30min~40min, then using reduced-pressure backflow 60min~80min, it is 50 DEG C~70 DEG C to depressurize temperature control,
Suspension is obtained, filters suspension, that is, obtains extracting the volcanic mud and volcanic mud alcohol-soluble extract solution after alcohol-soluble extract solution；
Volcanic mud after described extraction water-soluble extracting liquid and the ethanol water that mass percent is 25%~70%
Mass ratio be 1:(3~5)；
3rd, the preparation of volcanic mud oil-soluble extract solution：
Under agitation, the volcanic mud after extraction alcohol-soluble extract solution is stirred, the volcano to be stirred
Mud, then grease is weighed in parts by weight, described grease is by 5 parts~10 portions apricot kernel oils, 10 parts~15 parts olive oil, 5 parts~10
Part shea butter, 5 parts~10 parts grape-kernel oils, 2 parts~4 parts saualanes, 5 parts~10 parts ethoxylated dodecyl alcohol sodium sulphates,
13 parts~15 parts lauryl sodium sulfate, 1 part~2 parts cocamidopropyl betaines and 2 parts~5 parts alkylolamides groups
Into；First by 5 parts~10 portions apricot kernel oils, 10 parts~15 parts olive oil, 5 parts~10 parts shea butters, 5 parts~10 parts grape pips
Oil, the mixing of 2 parts~4 parts saualanes, obtain fat A, then by 5 parts~10 parts ethoxylated dodecyl alcohol sodium sulphates, 13 parts~
15 parts of lauryl sodium sulfate, 1 part~2 parts cocamidopropyl betaines and 2 parts~5 parts alkylolamides mixing, are obtained
Grease B, under agitation, fat A and grease B are added sequentially in the volcanic mud that stirs, obtained after adding grease
Volcanic mud, then will add the volcanic mud after grease and be placed on constant-temperature table and carry out concussion extraction, the temperature of constant-temperature table is
30 DEG C~40 DEG C, concussion frequency is 200rpm~300rpm, and extraction time is 3h~4h, obtains upper oil phase suspension, i.e., fiery
Minishanny oil-soluble extract solution；The mass ratio of volcanic mud and grease after described extraction alcohol-soluble extract solution is 1:(30~35)；
3rd, volcanic mud water-soluble extracting liquid, volcanic mud alcohol-soluble extract solution and volcanic mud oil-soluble extract solution are mixed, obtained
Primary slime extract is freezed to Wudalianchi；The matter of described volcanic mud water-soluble extracting liquid and volcanic mud alcohol-soluble extract solution
Measure ratio 1:(0.5~0.8)；The mass ratio 1 of described volcanic mud water-soluble extracting liquid and volcanic mud oil-soluble extract solution:(0.5~
0.8).It is other identical with embodiment one.
Because the active ingredient in sludge has unstability to heat, and the active ingredient of sludge is very precious, existing
Percolation is carried out at normal temperatures and pressures, and extraction effect can not be complete, therefore improves this part to active ingredient in volcanic mud
The link of extraction.Ensure to realize the extraction of composition under conditions of low temperature and high pressure, improve out one kind enable to it is wherein effective
The method that ingredient solubility is maximum, does not carry out Dynamic Extraction at destroyed temperature, this is also the reason of thermally labile component extraction
Think state, improve the utilization rate of sludge.
Decompression extraction can control Extracting temperature in suitable lower temperature, prevent active component extraction process high temperature
Under be decomposed destruction, moreover it is possible to reduce impurity and the stripping quantity of other compositions, and sludge oil-soluble composition is mainly organic acid esters
Class.Existing water-soluble and oil soluble extract completely can not come out extracts active ingredients.
Embodiment three：Unlike one of present embodiment and embodiment one or two：Described five are big
Even pond heavy carbonic mineral spring water extract is prepared according to the following steps：Wudalianchi heavy carbonic mineral water is first passed through into manganese sand, so
Afterwards under conditions of pressure is 0.1MPa~0.2MPa, by the filter membrane that aperture is 0.1 μm~3 μm, then by five after filtering
Dalian pond heavy carbonic mineral water stands 18h~24h, is finally concentrated under reduced pressure into dry, that is, obtains Wudalianchi heavy carbonic mineral spring water extraction
Take thing.It is other identical with embodiment one or two.
Embodiment four：Unlike one of present embodiment and embodiment one to three：Described androconium
Hair fern extract is prepared according to the following steps：
First, dryopteris fragrans are spontaneously dried and is crushed to the mesh of 30 mesh~40 with pulverizer, be 95% with volumn concentration
Ethanol according to solid-to-liquid ratio 1:The ratio of (20~25) is extracted, and extraction time is 1h~1.5h, extraction time 3 times~4 times,
Collect after extract is concentrated under reduced pressure and be lyophilized into powder, while collect residue, obtain the freeze-dried powder A and residue of extract；
2nd, with water according to solid-to-liquid ratio 1:The residue obtained in the ratio extraction step one of (20~25), extraction time 1h
~1.5h, extraction time 3 times~4 times, extract is lyophilized into powder after being concentrated under reduced pressure, and obtains the freeze-dried powder B of extract；
3rd, by the freeze-dried powder A of extract and the freeze-dried powder B in mass ratio 1 of extract:(0.5~0.8) mix, obtain perfume (or spice)
Shield-fern extract.It is other identical with embodiment one to three.
Embodiment five：Present embodiment is illustrated with reference to Fig. 1 to Fig. 3, present embodiment utilizes a kind of sludge
The method of hair film preparation sludge hair film cap is carried out according to the following steps：
First, weigh：50 parts~70 parts deionized waters, 10 parts~20 parts Wudalianchi frost primary ores are weighed in parts by weight
Mud extract, 10 parts~20 parts Wudalianchi heavy carbonic mineral spring water extracts, 1 part~5 portions linseed oil, 1 part~5 parts Qiong Yahai
Chinese bush cherry oil, 1 part~5 parts Hydrolyzed Collagens, 1 part~5 parts maize modified starch, 0.5 part~5 parts behentrimonium chlorides
Ammonium, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyls ammonium chlorides, 1 part~3 parts hydroxyethyl celluloses, 0.5
Part~2 parts of dryopteris fragrans extracts, 0.5 part~2 parts Polyquaternium-10s, 0.1 part~1 part L-vitamin C, 0.1 part~1 part
Vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part ethyl hydroxy benzoate；
Described 50 parts~70 parts of deionized waters, 10 parts~20 parts Wudalianchis frost primary slime extracts, 10 parts~
20 parts of Wudalianchi heavy carbonic mineral spring water extracts, 1 part~5 parts maize modified starch, 0.5 part~5 parts docosyl front threes
Ammonium chloride, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyls ammonium chlorides and 1 part~3 parts hydroxy ethyl fibers
Element composition phase A；
Described 1 part~5 portions of linseed oil, 1 part~5 parts fine jade precipice Malus spectabilis oil and 0.5 part~2 parts Polyquaternium-10 compositions
Phase B；
Described 1 part~5 parts of Hydrolyzed Collagens, 0.5 part~2 parts dryopteris fragrans extracts, 0.1 part~1 part left-handed dimension
Raw plain C, 0.1 part~1 part vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part ethyl hydroxy benzoate composition phase C；
2nd, phase A and phase B are separately heated to temperature as 40 DEG C~50 DEG C, then low whipping speed be 300r/min~
Under conditions of 500r/min, phase B is added to stirring 10min~30min in phase A, obtains mixture, thing temperature to be mixed is down to
During room temperature, low whipping speed be 400r/min~600r/min under conditions of, into mixture add phase C and stir 5min~
10min, sludge hair film is obtained, sludge hair film is sealed into the cavity 4 of hair film cap, that is, obtain sludge hair film cap；
Described hair film cap includes outer layer 1, internal layer 2 and silica gel check valve 3；Formed between described outer layer 1 and internal layer 2 empty
Chamber 4, the lower surface of internal layer 2 is uniformly arranged multiple silica gel check valves 3, and silica gel check valve 3 is connected with cavity 4, silica gel check valve 3
Diaphragm seal 5 is provided between cavity 4；The material of described outer layer 1, internal layer 2 and silica gel check valve 3 is the silica gel material of full shading
Matter；
Described silica gel check valve 3 is made up of the first trapezoidal portion 3-1, the second trapezoidal portion 3-2 and domed ends 3-3；The
One trapezoidal portion 3-1 one end end face is connected with the second trapezoidal portion 3-2 one end end face, the second trapezoidal portion 3-2 other end
Opening is provided with provided with domed ends 3-3, domed ends 3-3, is open when applying process without external force, due to silica gel material
In the presence of pretightning force, opening seals all the time, is open when there is external force to apply process, opening open.
Embodiment six：Present embodiment is unlike embodiment five：Five described in step 1 are big
Lian Chi frost primary slime extracts are prepared according to the following steps：
First, the preparation of volcanic mud water-soluble extracting liquid：
1., Wudalianchi Volcanic sludge is placed in ultra low temperature freezer and freezed, be subsequently placed in temperature for -80 DEG C~-
It is freeze-dried in 55 DEG C of vacuum freeze drier, obtains volcanic slurry freeze-dried powder；2., rotating speed be 1100r/min~
Under conditions of 1200r/min, volcanic slurry freeze-dried powder is well mixed with water, mud mixture is obtained, then mixes muddy water
Thing is placed in ultrasonic extractor, prolonged agitation, under conditions of supersonic frequency is 25kHz~40kHz, extraction 45min~
60min, obtain upper strata suspension and sediment；Described volcanic slurry freeze-dried powder and the mass ratio of water are 1:(20~25)；③、
By 2. sediment that step obtains by step 2. ultrasonic extraction 2 times~3 times, upper strata suspension and extraction water-soluble extracting liquid are obtained
Volcanic mud afterwards；4., combining step 2. and step 3. gained upper strata suspension, filter upper strata suspension, that is, obtain volcanic mud
Water-soluble extracting liquid；
2nd, the preparation of volcanic mud alcohol-soluble extract solution：
Volcanic mud after extraction water-soluble extracting liquid is added to the ethanol water that mass percent is 25%~70%
In, ultrasonic 30min~40min, then using reduced-pressure backflow 60min~80min, it is 50 DEG C~70 DEG C to depressurize temperature control,
Suspension is obtained, filters suspension, that is, obtains extracting the volcanic mud and volcanic mud alcohol-soluble extract solution after alcohol-soluble extract solution；
Volcanic mud after described extraction water-soluble extracting liquid and the ethanol water that mass percent is 25%~70%
Mass ratio be 1:(3~5)；
3rd, the preparation of volcanic mud oil-soluble extract solution：
Under agitation, the volcanic mud after extraction alcohol-soluble extract solution is stirred, the volcano to be stirred
Mud, then grease is weighed in parts by weight, described grease is by 5 parts~10 portions apricot kernel oils, 10 parts~15 parts olive oil, 5 parts~10
Part shea butter, 5 parts~10 parts grape-kernel oils, 2 parts~4 parts saualanes, 5 parts~10 parts ethoxylated dodecyl alcohol sodium sulphates,
13 parts~15 parts lauryl sodium sulfate, 1 part~2 parts cocamidopropyl betaines and 2 parts~5 parts alkylolamides groups
Into；First by 5 parts~10 portions apricot kernel oils, 10 parts~15 parts olive oil, 5 parts~10 parts shea butters, 5 parts~10 parts grape pips
Oil, the mixing of 2 parts~4 parts saualanes, obtain fat A, then by 5 parts~10 parts ethoxylated dodecyl alcohol sodium sulphates, 13 parts~
15 parts of lauryl sodium sulfate, 1 part~2 parts cocamidopropyl betaines and 2 parts~5 parts alkylolamides mixing, are obtained
Grease B, under agitation, fat A and grease B are added sequentially in the volcanic mud that stirs, obtained after adding grease
Volcanic mud, then will add the volcanic mud after grease and be placed on constant-temperature table and carry out concussion extraction, the temperature of constant-temperature table is
30 DEG C~40 DEG C, concussion frequency is 200rpm~300rpm, and extraction time is 3h~4h, obtains upper oil phase suspension, i.e., fiery
Minishanny oil-soluble extract solution；The mass ratio of volcanic mud and grease after described extraction alcohol-soluble extract solution is 1:(30~35)；
3rd, volcanic mud water-soluble extracting liquid, volcanic mud alcohol-soluble extract solution and volcanic mud oil-soluble extract solution are mixed, obtained
Primary slime extract is freezed to Wudalianchi；The matter of described volcanic mud water-soluble extracting liquid and volcanic mud alcohol-soluble extract solution
Measure ratio 1:(0.5~0.8)；The mass ratio 1 of described volcanic mud water-soluble extracting liquid and volcanic mud oil-soluble extract solution:(0.5~
0.8).It is other identical with embodiment five.
Embodiment seven：Unlike one of present embodiment and embodiment five or six：Institute in step 1
The Wudalianchi heavy carbonic mineral spring water extract stated is prepared according to the following steps：Wudalianchi heavy carbonic mineral water is first passed through
Manganese sand,, then will filtering by the filter membrane that aperture is 0.1 μm~3 μm then under conditions of pressure is 0.1MPa~0.2MPa
Wudalianchi heavy carbonic mineral water afterwards stands 18h~24h, is finally concentrated under reduced pressure into dry, that is, obtains Wudalianchi heavy carbonic ore deposit
Spring extract.It is other identical with embodiment five or six.
Embodiment eight：Unlike one of present embodiment and embodiment five to seven：Institute in step 1
The dryopteris fragrans extract stated is prepared according to the following steps：
First, dryopteris fragrans are spontaneously dried and is crushed to the mesh of 30 mesh~40 with pulverizer, be 95% with volumn concentration
Ethanol according to solid-to-liquid ratio 1:The ratio of (20~25) is extracted, and extraction time is 1h~1.5h, extraction time 3 times~4 times,
Collect after extract is concentrated under reduced pressure and be lyophilized into powder, while collect residue, obtain the freeze-dried powder A and residue of extract；
2nd, with water according to solid-to-liquid ratio 1:The residue obtained in the ratio extraction step one of (20~25), extraction time 1h
~1.5h, extraction time 3 times~4 times, extract is lyophilized into powder after being concentrated under reduced pressure, and obtains the freeze-dried powder B of extract；
3rd, by the freeze-dried powder A of extract and the freeze-dried powder B in mass ratio 1 of extract:(0.5~0.8) mix, obtain perfume (or spice)
Shield-fern extract.It is other identical with embodiment five to seven.
Embodiment nine：Unlike one of present embodiment and embodiment five to eight：Institute in step 2
The upper surface of outer layer 1 for the hair film cap stated is provided with screw thread.It is other identical with embodiment five to eight.
Embodiment ten：Unlike one of present embodiment and embodiment five to nine described in step 2
The material of diaphragm seal 5 be preservative film.It is other identical with embodiment five to nine.
Beneficial effects of the present invention are verified using following examples：
Embodiment one：
A kind of sludge hair film described in the present embodiment is former by 60 parts of deionized waters, 15 parts of Wudalianchi frosts in parts by weight
Rawore mud extract, 15 parts of Wudalianchi heavy carbonic mineral spring water extracts, 3 portions of linseed oil, 3 parts of fine jade precipice Malus spectabilis oil, 3 parts of hydrolysis
Collagen, 3 parts of maize modified starch, 3 parts of INCROQUAT TMC-80s, 3 parts of linseed oil amido propyl dimethyl 2,
3- dihydroxypropyls ammonium chloride, 2 parts of hydroxyethyl celluloses, 1 part of dryopteris fragrans extract, 1 part of Polyquaternium-10,0.5 part of left-handed dimension
Raw plain C, 0.5 part of vitamin E, 0.05 part of citric acid and 0.05 part of ethyl hydroxy benzoate are prepared；
Carried out according to the following steps using a kind of method of sludge hair film preparation sludge hair film cap：
First, weigh：60 parts of deionized waters, 15 parts of Wudalianchi frost primary slime extracts, 15 are weighed in parts by weight
Part Wudalianchi heavy carbonic mineral spring water extract, 3 portions of linseed oil, 3 parts of fine jade precipice Malus spectabilis oil, 3 parts of Hydrolyzed Collagens, 3 parts of jade
Rice modified starch, 3 parts of INCROQUAT TMC-80s, 3 parts of linseed oil amido propyl dimethyl 2,3- dihydroxypropyl chlorinations
Ammonium, 2 parts of hydroxyethyl celluloses, 1 part of dryopteris fragrans extract, 1 part of Polyquaternium-10,0.5 part of L-vitamin C, 0.5 part of dimension
Raw plain E, 0.05 part of citric acid and 0.05 part of ethyl hydroxy benzoate；
Described 60 parts of deionized waters, 15 parts of Wudalianchis frost primary slime extracts, 15 parts of Wudalianchi heavy carbonics
Mineral spring water extract, 3 parts of maize modified starch, 3 parts of INCROQUAT TMC-80s, 3 parts of linseed oil amido propyl diformazans
Base 2,3- dihydroxypropyls ammonium chloride and 2 parts of hydroxyethyl cellulose composition phase A；
Described 3 portions of linseed oil, 3 parts of fine jade precipice Malus spectabilis oil and 1 part of Polyquaternium-10 composition phase B；
Described 3 parts of Hydrolyzed Collagens, 1 part of dryopteris fragrans extract, 0.5 part of L-vitamin C, 0.5 part of vitamin
E, 0.05 part of citric acid and 0.05 part of ethyl hydroxy benzoate composition phase C；
2nd, phase A and phase B are separately heated to temperature as 45 DEG C, will under conditions of then low whipping speed is 400r/min
Phase B is added in phase A and stirs 20min, obtains mixture, when thing temperature to be mixed is down to room temperature, low whipping speed 500r/
Under conditions of min, phase C is added into mixture and stirs 8min, obtain sludge hair film, sludge hair film is sealed to hair film cap
In cavity 4, that is, obtain sludge hair film cap；
Described hair film cap includes outer layer 1, internal layer 2 and silica gel check valve 3；Formed between described outer layer 1 and internal layer 2 empty
Chamber 4, the lower surface of internal layer 2 is uniformly arranged multiple silica gel check valves 3, and silica gel check valve 3 is connected with cavity 4, silica gel check valve 3
Diaphragm seal 5 is provided between cavity 4；The material of described outer layer 1, internal layer 2 and silica gel check valve 3 is the silica gel material of full shading
Matter；
Described silica gel check valve 3 is made up of the first trapezoidal portion 3-1, the second trapezoidal portion 3-2 and domed ends 3-3；The
One trapezoidal portion 3-1 one end end face is connected with the second trapezoidal portion 3-2 one end end face, the second trapezoidal portion 3-2 other end
Opening is provided with provided with domed ends 3-3, domed ends 3-3, is open when applying process without external force, due to silica gel material
In the presence of pretightning force, opening seals all the time, is open when there is external force to apply process, opening open.
Wudalianchi frost primary slime extract described in step 1 is prepared according to the following steps：
First, the preparation of volcanic mud water-soluble extracting liquid：
1., Wudalianchi Volcanic sludge is placed in ultra low temperature freezer and freezed, it is -70 DEG C true to be subsequently placed in temperature
It is freeze-dried in vacuum freecing-dry machine, obtains volcanic slurry freeze-dried powder；2., rotating speed be 1150r/min under conditions of, will
Volcanic slurry freeze-dried powder is well mixed with water, obtains mud mixture, then mud mixture is placed in ultrasonic extractor, hold
Continuous agitation, under conditions of supersonic frequency is 40kHz, 55min is extracted, obtains upper strata suspension and sediment；Described volcano
The mass ratio of sludge freeze-dried powder and water is 1:20；3., by 2. sediment that step obtains by step 2. ultrasonic extraction 3 times, obtain
Volcanic mud after upper strata suspension and extraction water-soluble extracting liquid；4., combining step 2. and step 3. gained upper strata suspension,
Upper strata suspension is filtered, that is, obtains volcanic mud water-soluble extracting liquid；
2nd, the preparation of volcanic mud alcohol-soluble extract solution：
Volcanic mud after extraction water-soluble extracting liquid is added in the ethanol water that mass percent is 60%, ultrasound
35min, then using reduced-pressure backflow 70min, it is 60 DEG C to depressurize temperature control, obtains suspension, filters suspension, that is, obtains
Extract the volcanic mud and volcanic mud alcohol-soluble extract solution after alcohol-soluble extract solution；
Quality of the volcanic mud with mass percent for 60% ethanol water after described extraction water-soluble extracting liquid
Than for 1:4；
3rd, the preparation of volcanic mud oil-soluble extract solution：
Under agitation, the volcanic mud after extraction alcohol-soluble extract solution is stirred, the volcano to be stirred
Mud, then grease is weighed in parts by weight, described grease is 8 portions of apricot kernel oils, 13 parts of olive oil, 8 parts of shea butters, 8 portions of grapes
Seed oil, 3 parts of saualanes, 8 parts of ethoxylated dodecyl alcohol sodium sulphates, 14 parts of lauryl sodium sulfate, 1.5 parts of cocamidopropyls third
Base glycine betaine and 4 parts of alkylolamides compositions；First by 8 portions of apricot kernel oils, 13 parts of olive oil, 8 parts of shea butters, 8 parts of grape pips
Oil, 3 parts of saualane mixing, obtain fat A, then by 8 parts of ethoxylated dodecyl alcohol sodium sulphates, 14 parts of dodecyl sulphates
Sodium, 1.5 parts of cocamidopropyl betaines and 4 parts of alkylolamides mixing, obtain grease B, under agitation, by grease
A and grease B is added sequentially in the volcanic mud that stirs, obtains the volcanic mud added after grease, after then adding grease
Volcanic mud be placed on constant-temperature table and carry out concussion extraction, the temperature of constant-temperature table is 35 DEG C, and concussion frequency is 300rpm, is extracted
Time is 3.5h, obtains upper oil phase suspension, i.e. volcanic mud oil-soluble extract solution；After described extraction alcohol-soluble extract solution
The mass ratio of volcanic mud and grease is 1:35；
3rd, volcanic mud water-soluble extracting liquid, volcanic mud alcohol-soluble extract solution and volcanic mud oil-soluble extract solution are mixed, obtained
Primary slime extract is freezed to Wudalianchi；The matter of described volcanic mud water-soluble extracting liquid and volcanic mud alcohol-soluble extract solution
Measure ratio 1:0.8；The mass ratio 1 of described volcanic mud water-soluble extracting liquid and volcanic mud oil-soluble extract solution:0.8.
Wudalianchi heavy carbonic mineral spring water extract described in step 1 is prepared according to the following steps：By Wudalianchi
Heavy carbonic mineral water first passes through manganese sand, then under conditions of pressure is 0.15MPa, by the filter membrane that aperture is 1 μm, then will
Wudalianchi heavy carbonic mineral water after filtering stands 22h, is finally concentrated under reduced pressure into dry, that is, obtains Wudalianchi heavy carbonic mineral spring
Water extract；
Dryopteris fragrans extract described in step 1 is prepared according to the following steps：
First, dryopteris fragrans are spontaneously dried and is crushed to 35 mesh with pulverizer, with the ethanol that volumn concentration is 95%
According to solid-to-liquid ratio 1:20 ratio is extracted, extraction time 1h, extraction time 4 times, is collected after extract is concentrated under reduced pressure and is frozen
Powder is done into, while collects residue, obtains the freeze-dried powder A and residue of extract；
2nd, with water according to solid-to-liquid ratio 1:The residue obtained in 20 ratio extraction step one, extraction time 1h, extraction time
Number 4 times, extract is lyophilized into powder after being concentrated under reduced pressure, and obtains the freeze-dried powder B of extract；
3rd, by the freeze-dried powder A of extract and the freeze-dried powder B in mass ratio 1 of extract:0.5 mixing, obtains dryopteris fragrans and carries
Take thing；
The upper surface of outer layer 1 of hair film cap described in step 2 is provided with screw thread；The material of diaphragm seal 5 described in step 2
For preservative film.
50 triers of selection send out film 3 months using sludge manufactured in the present embodiment, use once within every 3 days, according to everyone
Hair length, from 5mL~10mL, application method is specially after trier has one's hair wash, according to the different choice of itself hair amount
The hair film cap of injection different capabilities sludge hair film is worn on head, is exerted a force by the extruding of hand, the sludge in cavity 4 is sent out into film
Inner sealing film 5 is broken through, sludge is sent out into film extrusion from the silica gel check valve 3 of hair film cap is contacted with hair, and film cap is sent out wearing
In the case of by the massage and rubbing of hand, after hair film is completely attached to 3min~5min with hair, pluck hair film cap, use clear water
Rinse well, the application method of anti-dandruff measure of merit and Anti-hair loss measure of merit is identical below.In the form of survey
Carry out effect research to sludge manufactured in the present embodiment hair film, the wherein people of trier male 20, the people of women 30, the oldest 65
Year, minimum 10 years old, trier is to using the compliance after this product, elasticity, gloss, hair quality state, moisturizing, grease, itch, thorn
Swash the indices such as anaphylaxis to be evaluated：50 triers think that this product hair film is readily cleaned after smearing after use, energy
The state of dry hair and bifurcated is enough effectively improved, deep layer, which is nourished, repairs hair scale piece, can make hair more submissive after use
Easily comb, cleaning is flexible and is greatly improved rich in healthy glow, grease, itch, and uses rear non-stimulated anaphylaxis.
Anti-dandruff measure of merit：Utilize the sludge in product on the basis of China on the market well-known product W salable and embodiment
Hair film D is contrasted, and trier (totally 40, every 1 group of 5 people) is the bob male for having dandruff worried.Professional teacher is to two kinds
Product does half a head experiment, is then rinsed out with identical and enough water, when half a head is using hair film manufactured in the present embodiment, according to
Particular case prepares the hair film cap suitable for half a head, according to the hair length of half a head, from the hair film of different capabilities sludge hair film
Cap is worn on half a head, and the slime product sent out in film cap is directly expressed to the side of pretest completely, is wearing hair film cap
In the case of by the massage and rubbing of hand, after hair film is completely attached to 3min~5min with hair, pluck hair film cap, rushed with clear water
Wash clean.The trier for participating in evaluating will fix half a head and use W samples, and another side uses the sludge hair film D in embodiment,
Continuous use 14 days, is tracked 5 days again after stopping using.Dandruff feelings before using daily by 18 professional teachers to every trier
Condition is tracked evaluation marking, and (10 points are that dandruff is seldom, and 0 point is that dandruff is special
Seriously), dandruff score value of the average as the same day, test result are as shown in table 1：
As shown in Table 1, sludge hair film D trier manufactured in the present embodiment still keeps the long period for 5 days not by head after disabling
Bits puzzlement, and control sample W trier is used, after disabling 5 days, dandruff continues to perplex trier.And the present embodiment product
Trier just show the effect of control dandruff well since using the 2nd day, trier using control sample W is from making
With more than the 7th day, just start to show and the 2nd day anti-dandruff effect of identical of the present embodiment.It follows that the present embodiment product exists
Anti-dandruff aspect has a clear superiority compared with market situation of selling well hit product W, illustrates that product manufactured in the present embodiment can obviously improve
Dandruff problem.
The hair test of anticreep effect：Entered using product on the basis of China on the market commercially available prod and the sludge hair film in embodiment
Row contrast, choose 50 triers and participate in experiment, trier's age between 30 years old~55 years old, belongs to alopecia seborrheica, alopecia areata
With physiologic alopecia etc., the other diseases of this observation result may not be influenceed, not used similar anti-product-stripping mechanism in 1 month, and
Completion observation etc. can voluntarily be coordinated on request.Furthermore, it is contemplated that seasonal factor, experiment selection is carried out in winter-spring season.Trier
The people of test group 25 and the people of control group 25 are randomly divided into, the trier of test group, uses the Hair-loss-preventingshampoo shampoo of the present embodiment, control
The trier of group, using commercially available prod as reference, and test group uses identical program and time with control group.Daily
Divide 3 combing hairs in the morning, afternoon and evening, collect the hair to come off and record radical, its integer is taken after obtaining average value.By 56 days
After experiment, statistics, its result sees below table 2.
Table 2
| Time day | It is several with the product alopecia of the present embodiment | It is several with commercially available prod alopecia |
| 0 | 129 | 112 |
| 7 | 114 | 108 |
| 14 | 91 | 106 |
| 21 | 87 | 105 |
| 28 | 82 | 98 |
| 35 | 74 | 96 |
| 42 | 63 | 96 |
| 49 | 51 | 95 |
| 56 | 37 | 94 |
As shown in Table 2,56 days using after the present embodiment product, and during comb hair, hair loss hair loss significantly reduces, during by being not used
Hair loss 129 is reduced to 37, reduces alopecia 71.3%, and using after 7 days with regard to significant effect.And imitated using commercially available prod hair loss
Fruit and unobvious, the hair loss 112 during by being not used are reduced to 94, alopecia 16.1% are reduced, it follows that comparing commercially available production
Product, the present embodiment product can obviously improve alopecia effect.
Claims (10)
1. a kind of sludge sends out film, it is characterised in that a kind of sludge hair film in parts by weight by 50 parts~70 parts deionized waters, 10 parts
~20 parts of Wudalianchi frost primary slime extracts, 10 parts~20 parts Wudalianchi heavy carbonic mineral spring water extracts, 1 part~5
Portion linseed oil, 1 part~5 parts fine jade precipice Malus spectabilis oil, 1 part~5 parts Hydrolyzed Collagens, 1 part~5 parts maize modified starch, 0.5 part
~5 parts of INCROQUAT TMC-80s, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyls ammonium chlorides,
1 part~3 parts hydroxyethyl celluloses, 0.5 part~2 parts dryopteris fragrans extracts, 0.5 part~2 parts Polyquaternium-10s, 0.1 part~1
Part L-vitamin C, 0.1 part~1 part vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part ethyl hydroxy benzoate system
It is standby to form.
2. a kind of sludge hair film according to claim 1, it is characterised in that described Wudalianchi frost primary slime carries
Thing is taken to prepare according to the following steps：
First, the preparation of volcanic mud water-soluble extracting liquid：
1., Wudalianchi Volcanic sludge is placed in ultra low temperature freezer and freezed, be subsequently placed in temperature as -80 DEG C~-55 DEG C
Vacuum freeze drier in be freeze-dried, obtain volcanic slurry freeze-dried powder；2., rotating speed be 1100r/min~
Under conditions of 1200r/min, volcanic slurry freeze-dried powder is well mixed with water, mud mixture is obtained, then mixes muddy water
Thing is placed in ultrasonic extractor, prolonged agitation, under conditions of supersonic frequency is 25kHz~40kHz, extraction 45min~
60min, obtain upper strata suspension and sediment；Described volcanic slurry freeze-dried powder and the mass ratio of water are 1:(20~25)；③、
By 2. sediment that step obtains by step 2. ultrasonic extraction 2 times~3 times, upper strata suspension and extraction water-soluble extracting liquid are obtained
Volcanic mud afterwards；4., combining step 2. and step 3. gained upper strata suspension, filter upper strata suspension, that is, obtain volcanic mud
Water-soluble extracting liquid；
2nd, the preparation of volcanic mud alcohol-soluble extract solution：
Volcanic mud after extraction water-soluble extracting liquid is added in the ethanol water that mass percent is 25%~70%, surpassed
Sound 30min~40min, then using reduced-pressure backflow 60min~80min, it is 50 DEG C~70 DEG C to depressurize temperature control, is hanged
Supernatant liquid, suspension is filtered, that is, obtain extracting the volcanic mud and volcanic mud alcohol-soluble extract solution after alcohol-soluble extract solution；
Matter of the volcanic mud with mass percent for 25%~70% ethanol water after described extraction water-soluble extracting liquid
Amount is than being 1:(3~5)；
3rd, the preparation of volcanic mud oil-soluble extract solution：
Under agitation, the volcanic mud after extraction alcohol-soluble extract solution is stirred, the volcanic mud to be stirred, then
Grease is weighed in parts by weight, and described grease is by 5 parts~10 portions apricot kernel oils, 10 parts~15 parts olive oil, 5 parts~10 parts breast wood
Fruit oil, 5 parts~10 parts grape-kernel oils, 2 parts~4 parts saualanes, 5 parts~10 parts ethoxylated dodecyl alcohol sodium sulphates, 13 parts~
15 parts of lauryl sodium sulfate, 1 part~2 parts cocamidopropyl betaines and 2 parts~5 parts alkylolamides compositions；First
By 5 parts~10 portions apricot kernel oils, 10 parts~15 parts olive oil, 5 parts~10 parts shea butters, 5 parts~10 parts grape-kernel oils, 2 parts~4
Part saualane mixing, obtains fat A, then by 5 parts~10 parts ethoxylated dodecyl alcohol sodium sulphates, 13 parts~15 parts dodecanes
Base sodium sulphate, 1 part~2 parts cocamidopropyl betaines and 2 parts~5 parts alkylolamides mixing, obtain grease B, are stirring
Under the conditions of mixing, fat A and grease B are added sequentially in the volcanic mud that stirs, obtain the volcanic mud added after grease, so
The volcanic mud after addition grease is placed on constant-temperature table afterwards and carries out concussion extraction, the temperature of constant-temperature table is 30 DEG C~40 DEG C,
Concussion frequency is 200rpm~300rpm, and extraction time is 3h~4h, obtains upper oil phase suspension, i.e. volcanic mud oil-soluble carries
Take liquid；The mass ratio of volcanic mud and grease after described extraction alcohol-soluble extract solution is 1:(30~35)；
3rd, volcanic mud water-soluble extracting liquid, volcanic mud alcohol-soluble extract solution and volcanic mud oil-soluble extract solution are mixed, obtains five
Dalian pond freezes primary slime extract；The mass ratio of described volcanic mud water-soluble extracting liquid and volcanic mud alcohol-soluble extract solution
1:(0.5~0.8)；The mass ratio 1 of described volcanic mud water-soluble extracting liquid and volcanic mud oil-soluble extract solution:(0.5~
0.8)。
A kind of 3. sludge hair film according to claim 1, it is characterised in that described Wudalianchi heavy carbonic mineral spring water extraction
Thing is taken to prepare according to the following steps：Wudalianchi heavy carbonic mineral water is first passed through into manganese sand, then pressure be 0.1MPa~
Under conditions of 0.2MPa, by the filter membrane that aperture is 0.1 μm~3 μm, then by the Wudalianchi heavy carbonic mineral water after filtering
18h~24h is stood, is finally concentrated under reduced pressure into dry, that is, obtains Wudalianchi heavy carbonic mineral spring water extract.
4. a kind of sludge hair film according to claim 1, it is characterised in that described dryopteris fragrans extract is by following
Prepared by step：
First, dryopteris fragrans are spontaneously dried and is crushed to the mesh of 30 mesh~40 with pulverizer, with the second that volumn concentration is 95%
Alcohol is according to solid-to-liquid ratio 1:The ratio of (20~25) is extracted, and extraction time is 1h~1.5h, extraction time 3 times~4 times, is collected
Extract is lyophilized into powder after being concentrated under reduced pressure, while collects residue, obtains the freeze-dried powder A and residue of extract；
2nd, with water according to solid-to-liquid ratio 1:The residue obtained in the ratio extraction step one of (20~25), extraction time be 1h~
1.5h, extraction time 3 times~4 times, extract is lyophilized into powder after being concentrated under reduced pressure, and obtains the freeze-dried powder B of extract；
3rd, by the freeze-dried powder A of extract and the freeze-dried powder B in mass ratio 1 of extract:(0.5~0.8) mix, obtain androconium hair
Fern extract.
5. utilize a kind of method of sludge hair film preparation sludge hair film cap described in claim 1, it is characterised in that utilize one kind
The method of sludge hair film preparation sludge hair film cap is carried out according to the following steps：
First, weigh：50 parts~70 parts deionized waters are weighed in parts by weight, 10 parts~20 parts Wudalianchi frost primary slimes carry
Take thing, 10 parts~20 parts Wudalianchi heavy carbonic mineral spring water extracts, 1 part~5 portions linseed oil, 1 part~5 parts fine jade precipice Malus spectabilis
Oil, 1 part~5 parts Hydrolyzed Collagens, 1 part~5 parts maize modified starch, 0.5 part~5 parts behentrimonium chlorides
Ammonium, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyls ammonium chlorides, 1 part~3 parts hydroxyethyl celluloses, 0.5
Part~2 parts of dryopteris fragrans extracts, 0.5 part~2 parts Polyquaternium-10s, 0.1 part~1 part L-vitamin C, 0.1 part~1 part
Vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part ethyl hydroxy benzoate；
Described 50 parts~70 parts of deionized waters, 10 parts~20 parts Wudalianchis frost primary slime extracts, 10 parts~20 parts
Wudalianchi heavy carbonic mineral spring water extract, 1 part~5 parts maize modified starch, 0.5 part~5 parts behenyl chlorine
Change ammonium, 0.5 part~5 parts linseed oil amido propyl dimethyl 2,3- dihydroxypropyls ammonium chlorides and 1 part~3 parts hydroxyethyl cellulose groups
Into phase A；
Described 1 part~5 portions of linseed oil, 1 part~5 parts fine jade precipice Malus spectabilis oil and 0.5 part~2 parts Polyquaternium-10 composition phase B；
Described 1 part~5 parts of Hydrolyzed Collagens, 0.5 part~2 parts dryopteris fragrans extracts, 0.1 part~1 part L-vitamin
C, 0.1 part~1 part vitamin E, 0.01 part~0.1 part citric acid and 0.01 part~0.1 part ethyl hydroxy benzoate composition phase C；
2nd, phase A and phase B are separately heated to temperature as 40 DEG C~50 DEG C, then low whipping speed is 300r/min~500r/
Under conditions of min, phase B is added to stirring 10min~30min in phase A, obtains mixture, thing temperature to be mixed is down to room temperature
When, under conditions of low whipping speed is 400r/min~600r/min, phase C is added into mixture and stirs 5min~10min,
Sludge hair film is obtained, sludge hair film is sealed into the cavity (4) of hair film cap, that is, obtains sludge hair film cap；
Described hair film cap includes outer layer (1), internal layer (2) and silica gel check valve (3)；Between described outer layer (1) and internal layer (2)
Cavity (4) is formed, internal layer (2) lower surface is uniformly arranged multiple silica gel check valves (3), and silica gel check valve (3) and cavity (4) phase
Connection, is provided with diaphragm seal (5) between silica gel check valve (3) and cavity (4)；Described outer layer (1), internal layer (2) and silica gel are unidirectional
The material of valve (3) is the silica gel material of full shading；
Described silica gel check valve (3) is by the first trapezoidal portion (3-1), the second trapezoidal portion (3-2) and domed ends (3-3) group
Into；One end end face of first trapezoidal portion (3-1) is connected with one end end face of the second trapezoidal portion (3-2), the second trapezoidal portion (3-2)
Other end be provided with domed ends (3-3), domed ends (3-3) are provided with opening, be open without external force apply process
When, in the presence of silica gel material pretightning force, opening seals all the time, is open when there is external force to apply process, opening open.
6. a kind of method according to claim 5 that film preparation sludge hair film cap is sent out using sludge, it is characterised in that step
Wudalianchi frost primary slime extract described in one is prepared according to the following steps：
First, the preparation of volcanic mud water-soluble extracting liquid：
1., Wudalianchi Volcanic sludge is placed in ultra low temperature freezer and freezed, be subsequently placed in temperature as -80 DEG C~-55 DEG C
Vacuum freeze drier in be freeze-dried, obtain volcanic slurry freeze-dried powder；2., rotating speed be 1100r/min~
Under conditions of 1200r/min, volcanic slurry freeze-dried powder is well mixed with water, mud mixture is obtained, then mixes muddy water
Thing is placed in ultrasonic extractor, prolonged agitation, under conditions of supersonic frequency is 25kHz~40kHz, extraction 45min~
60min, obtain upper strata suspension and sediment；Described volcanic slurry freeze-dried powder and the mass ratio of water are 1:(20~25)；③、
By 2. sediment that step obtains by step 2. ultrasonic extraction 2 times~3 times, upper strata suspension and extraction water-soluble extracting liquid are obtained
Volcanic mud afterwards；4., combining step 2. and step 3. gained upper strata suspension, filter upper strata suspension, that is, obtain volcanic mud
Water-soluble extracting liquid；
2nd, the preparation of volcanic mud alcohol-soluble extract solution：
Volcanic mud after extraction water-soluble extracting liquid is added in the ethanol water that mass percent is 25%~70%, surpassed
Sound 30min~40min, then using reduced-pressure backflow 60min~80min, it is 50 DEG C~70 DEG C to depressurize temperature control, is hanged
Supernatant liquid, suspension is filtered, that is, obtain extracting the volcanic mud and volcanic mud alcohol-soluble extract solution after alcohol-soluble extract solution；
Matter of the volcanic mud with mass percent for 25%~70% ethanol water after described extraction water-soluble extracting liquid
Amount is than being 1:(3~5)；
3rd, the preparation of volcanic mud oil-soluble extract solution：
Under agitation, the volcanic mud after extraction alcohol-soluble extract solution is stirred, the volcanic mud to be stirred, then
Grease is weighed in parts by weight, and described grease is by 5 parts~10 portions apricot kernel oils, 10 parts~15 parts olive oil, 5 parts~10 parts breast wood
Fruit oil, 5 parts~10 parts grape-kernel oils, 2 parts~4 parts saualanes, 5 parts~10 parts ethoxylated dodecyl alcohol sodium sulphates, 13 parts~
15 parts of lauryl sodium sulfate, 1 part~2 parts cocamidopropyl betaines and 2 parts~5 parts alkylolamides compositions；First
By 5 parts~10 portions apricot kernel oils, 10 parts~15 parts olive oil, 5 parts~10 parts shea butters, 5 parts~10 parts grape-kernel oils, 2 parts~4
Part saualane mixing, obtains fat A, then by 5 parts~10 parts ethoxylated dodecyl alcohol sodium sulphates, 13 parts~15 parts dodecanes
Base sodium sulphate, 1 part~2 parts cocamidopropyl betaines and 2 parts~5 parts alkylolamides mixing, obtain grease B, are stirring
Under the conditions of mixing, fat A and grease B are added sequentially in the volcanic mud that stirs, obtain the volcanic mud added after grease, so
The volcanic mud after addition grease is placed on constant-temperature table afterwards and carries out concussion extraction, the temperature of constant-temperature table is 30 DEG C~40 DEG C,
Concussion frequency is 200rpm~300rpm, and extraction time is 3h~4h, obtains upper oil phase suspension, i.e. volcanic mud oil-soluble carries
Take liquid；The mass ratio of volcanic mud and grease after described extraction alcohol-soluble extract solution is 1:(30~35)；
3rd, volcanic mud water-soluble extracting liquid, volcanic mud alcohol-soluble extract solution and volcanic mud oil-soluble extract solution are mixed, obtains five
Dalian pond freezes primary slime extract；The mass ratio of described volcanic mud water-soluble extracting liquid and volcanic mud alcohol-soluble extract solution
1:(0.5~0.8)；The mass ratio 1 of described volcanic mud water-soluble extracting liquid and volcanic mud oil-soluble extract solution:(0.5~
0.8)。
7. a kind of method according to claim 5 that film preparation sludge hair film cap is sent out using sludge, it is characterised in that step
Wudalianchi heavy carbonic mineral spring water extract described in one is prepared according to the following steps：By Wudalianchi heavy carbonic mineral water
Manganese sand is first passed through, is 0.1 μm~3 μm of filter membrane by aperture, then then under conditions of pressure is 0.1MPa~0.2MPa
Wudalianchi heavy carbonic mineral water after filtering is stood into 18h~24h, is finally concentrated under reduced pressure into dry, that is, obtains Wudalianchi weight
Carbonic acid mineral spring water extract.
8. a kind of method according to claim 5 that film preparation sludge hair film cap is sent out using sludge, it is characterised in that step
Dryopteris fragrans extract described in one is prepared according to the following steps：
First, dryopteris fragrans are spontaneously dried and is crushed to the mesh of 30 mesh~40 with pulverizer, with the second that volumn concentration is 95%
Alcohol is according to solid-to-liquid ratio 1:The ratio of (20~25) is extracted, and extraction time is 1h~1.5h, extraction time 3 times~4 times, is collected
Extract is lyophilized into powder after being concentrated under reduced pressure, while collects residue, obtains the freeze-dried powder A and residue of extract；
2nd, with water according to solid-to-liquid ratio 1:The residue obtained in the ratio extraction step one of (20~25), extraction time be 1h~
1.5h, extraction time 3 times~4 times, extract is lyophilized into powder after being concentrated under reduced pressure, and obtains the freeze-dried powder B of extract；
3rd, by the freeze-dried powder A of extract and the freeze-dried powder B in mass ratio 1 of extract:(0.5~0.8) mix, obtain androconium hair
Fern extract.
9. a kind of method according to claim 5 that film preparation sludge hair film cap is sent out using sludge, it is characterised in that step
Outer layer (1) upper surface of hair film cap described in two is provided with screw thread.
10. a kind of method according to claim 5 that film preparation sludge hair film cap is sent out using sludge, it is characterised in that step
The material of diaphragm seal (5) described in two is preservative film.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711072123.6A CN107693404A (en) | 2017-11-03 | 2017-11-03 | Slime hair mask and method for preparing slime hair mask cap by using slime hair mask |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711072123.6A CN107693404A (en) | 2017-11-03 | 2017-11-03 | Slime hair mask and method for preparing slime hair mask cap by using slime hair mask |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107693404A true CN107693404A (en) | 2018-02-16 |
Family
ID=61177836
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711072123.6A Pending CN107693404A (en) | 2017-11-03 | 2017-11-03 | Slime hair mask and method for preparing slime hair mask cap by using slime hair mask |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107693404A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110478282A (en) * | 2019-09-11 | 2019-11-22 | 黑龙江省科学院火山与矿泉研究所 | A kind of multi-functional volcanic slurry cleaning mud film and preparation method thereof and application method |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2166632Y (en) * | 1993-08-05 | 1994-06-01 | 黎亘 | Hair-care cap with function of curing bare hair |
| US5850636A (en) * | 1997-12-31 | 1998-12-22 | Reuven; Michelle G. | Heatable hair cap |
| CN203353914U (en) * | 2013-04-26 | 2013-12-25 | 林权飞 | Flushing-free hair washing cap containing traditional Chinese medicine shampoo |
| CN104643511A (en) * | 2013-12-30 | 2015-05-27 | 郑智英 | Steam Hair Pack Using Head Heat And Heat-generating Beauty Solution |
| CN104666128A (en) * | 2015-03-16 | 2015-06-03 | 黑龙江省科学院火山与矿泉研究所 | Volcanic mud essence spray mask and preparation method thereof |
| CN104758215A (en) * | 2015-04-09 | 2015-07-08 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi dryopteris fragrans mineral spring effervescent tablet and preparation method thereof |
| CN206491439U (en) * | 2016-09-30 | 2017-09-15 | 许广南 | Yi Zhong treatment oil caps |
-
2017
- 2017-11-03 CN CN201711072123.6A patent/CN107693404A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2166632Y (en) * | 1993-08-05 | 1994-06-01 | 黎亘 | Hair-care cap with function of curing bare hair |
| US5850636A (en) * | 1997-12-31 | 1998-12-22 | Reuven; Michelle G. | Heatable hair cap |
| CN203353914U (en) * | 2013-04-26 | 2013-12-25 | 林权飞 | Flushing-free hair washing cap containing traditional Chinese medicine shampoo |
| CN104643511A (en) * | 2013-12-30 | 2015-05-27 | 郑智英 | Steam Hair Pack Using Head Heat And Heat-generating Beauty Solution |
| CN104666128A (en) * | 2015-03-16 | 2015-06-03 | 黑龙江省科学院火山与矿泉研究所 | Volcanic mud essence spray mask and preparation method thereof |
| CN104758215A (en) * | 2015-04-09 | 2015-07-08 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi dryopteris fragrans mineral spring effervescent tablet and preparation method thereof |
| CN206491439U (en) * | 2016-09-30 | 2017-09-15 | 许广南 | Yi Zhong treatment oil caps |
Non-Patent Citations (6)
| Title |
|---|
| 中国职工疗养协会组: "《职工疗休养手册》", 31 May 2006, 杭州出版社 * |
| 国家药典委员会: "《中华人民共和国药典临床用药须知》", 30 September 2017, 中国医药科技出版社 * |
| 广州市发歌精细化工有限公司: ""威莱雅火山泥矿物修复精华发膜"", 《国产非特殊用途化妆品备案服务平台（HTTP://125.35.6.80:8181/FTBAN/FW.JSP）》 * |
| 广州市白云区龙归雅丽丝日用化妆品厂: ""海曼火山泥发膜"", 《国产非特殊用途化妆品备案服务平台（HTTP://125.35.6.80:8181/FTBAN/FW.JSP）》 * |
| 张彦龙: "《药用植物香鳞毛蕨药效物质基础的研究》", 30 November 2006, 哈尔滨工程大学出版社 * |
| 邱水红等: "《英语时文悦读》", 29 February 2008, 山东科学技术出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110478282A (en) * | 2019-09-11 | 2019-11-22 | 黑龙江省科学院火山与矿泉研究所 | A kind of multi-functional volcanic slurry cleaning mud film and preparation method thereof and application method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105560097B (en) | A kind of fresh peony flower ferment and its preparation method and application | |
| CN104546653A (en) | Skin moisturizer containing rose ferment | |
| CN103830155B (en) | A kind of betaplex gentle cleansing milk | |
| CN103550131B (en) | Pure natural hair care hair color shampoo and preparation method thereof | |
| CN106420524A (en) | Anti-hair-loss and hair-promotion traditional Chinese medicine composition as well as preparation method and application thereof | |
| CN104383114A (en) | Traditional Chinese medicine composition and liquid shampoo for preventing alopecia, and preparation method of traditional Chinese medicine composition | |
| CN103392827A (en) | Moringa leaf preserved bean curd | |
| CN103844189A (en) | Appetizing cedrela sinensis fine dried noodles and preparation method thereof | |
| CN105832590A (en) | Washing-caring two-in-one hair health-caring product | |
| CN103550101B (en) | There is plant extraction liquid and the application thereof of tender white moisturizing effect | |
| CN106619384A (en) | Shampoo-conditioning fluid | |
| CN110420161A (en) | It is a kind of with antipruritic and skin makeup function toner and preparation method thereof | |
| CN107693404A (en) | Slime hair mask and method for preparing slime hair mask cap by using slime hair mask | |
| CN103536524B (en) | Hair blackening and growing shampoo and preparation method thereof | |
| CN104887602B (en) | Jasmine hair washing face washing liquid | |
| CN101933614A (en) | Method for preparing oviductus ranae granules | |
| CN103947950B (en) | A kind of red compound health rice cake and processing method thereof | |
| CN106214557A (en) | The preparation method of purely-natural liquid shampoo | |
| CN108703918A (en) | It is a kind of to have effects that anti-dandruff shampoo and preparation method thereof | |
| CN101536969B (en) | Salt Chinese herbal medicine paste shampoo | |
| CN101683313A (en) | Trichosanthes anguina (mongloian snakegourd) washing skin protection series | |
| CN107821954A (en) | Sesame paste cappelletti | |
| CN105878152A (en) | Pasty bath salt containing punica granatum fruit extract | |
| CN111821239A (en) | A hair blackening shampoo containing herba Gynostemmatis extract and its preparation method | |
| CN105411985A (en) | Whitening and moisturizing mask |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180216 |