CN104666128A - Volcanic mud essence spray mask and preparation method thereof - Google Patents
Volcanic mud essence spray mask and preparation method thereof Download PDFInfo
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- CN104666128A CN104666128A CN201510114742.1A CN201510114742A CN104666128A CN 104666128 A CN104666128 A CN 104666128A CN 201510114742 A CN201510114742 A CN 201510114742A CN 104666128 A CN104666128 A CN 104666128A
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Abstract
A volcanic mud essence spray mask and a preparation method thereof relate to a mask and a preparation method thereof. The invention aims to solve the problems that the existing volcanic mud mask feels drier and drier in the using process, the fit degree with the skin is poor, and effective components cannot be completely conducted into the skin and cannot be completely utilized. The volcanic mud essence spray mask is prepared from volcanic mud essence, lanolin, lauric acid, lauryl trimethyl ammonium chloride and ethyl perfluorobutyl ether. The preparation method comprises the following steps: mixing lanolin, lauric acid and lauryl trimethyl ammonium chloride to obtain a mixture, adding the mixture into the volcanic mud essence, uniformly stirring and dispersing, adding ethyl perfluorobutyl ether, uniformly stirring, and then filling into a spray tank to obtain the volcanic mud essence spray mask. The invention relates to a volcanic mud essence spray mask and a preparation method thereof.
Description
Technical field
The present invention relates to a kind of facial film and preparation method thereof.
Background technology
Volcanic mud is because being rich in various trace elements, mineral and organic acid, there is high health care and cosmetology function, be widely used in various skin-protection product at present, wherein maximum is exactly volcanic mud facial film, Main Morphology is volcanic mud powder facial film and volcanic mud cream pack, volcanic mud effect to skin extra-nutrition material and deep layer cleaning can be played, in use because moisture constantly evaporates, can feel more and more dry, and make the laminating degree of part volcanic mud and skin more and more bad, thus make the effective ingredient of the top layer volcanic mud contacted with air can not be conducted into skin completely, do not reach and utilize completely.Volcanic mud in addition much can by the potentiality excavated as a kind of skincare material of pure natural, the essence substance how obtained in volcanic mud is still one piece of market shortcoming, and selects the powerful novel skin care item of performance preferably all volcanic muds elite also urgently to develop.
Summary of the invention
The present invention will solve in the use procedure of existing volcanic mud facial film because moisture constantly evaporates, can feel more and more dry, and make the laminating degree of part volcanic mud and skin more and more bad, thus make the effective ingredient of the top layer volcanic mud contacted with air can not be conducted into skin completely, do not reach the problem utilized completely, and a kind of volcanic mud elite spraying facial film and preparation method thereof is provided.
A kind of volcanic mud elite spraying facial film of the present invention is prepared from by 25 parts ~ 75 parts volcanic mud elite, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids, 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides and 5 parts ~ 15 parts ethyl perfluorobutyl ether by weight;
Described volcanic mud elite is mixed by 10 parts ~ 12 parts volcanic mud oil-soluble extracting solution and 40 parts ~ 45 parts volcanic mud water-soluble extracting liquids by weight;
Described volcanic mud water-soluble extracting liquid is prepared according to the following steps: 1., at rotating speed be under the condition of 800r/min ~ 1000r/min, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 20kHz ~ 30kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit; Described moisture content is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:(20 ~ 30); 2., by step 1. in deposit by step 1. supersound extraction 2 times ~ 3 times, the volcanic mud after obtaining upper strata suspension and extracting water-soluble extracting liquid; 3., combining step 1. and the upper strata suspension of step 2. gained, namely obtain volcanic mud water-soluble extracting liquid;
Described volcanic mud oil-soluble extracting solution is prepared according to the following steps: under agitation, volcanic mud after extracting water-soluble extracting liquid is stirred, obtain the volcanic mud stirred, take oils and fats by weight again, described oils and fats is 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat, 5 parts ~ 8 parts squalanes, 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides compositions, first by 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat and 5 parts ~ 8 parts squalane mixing, obtain fat A, then by 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides mixing, obtain oils and fats B, under agitation, fat A and oils and fats B are joined in the volcanic mud stirred successively, obtain the volcanic mud after adding oils and fats, then be placed in and constant-temperature table carry out concussion by adding the volcanic mud after oils and fats and extract, the temperature of constant-temperature table is 30 DEG C ~ 50 DEG C, concussion frequency is 100rpm ~ 300rpm, extraction time is 2h ~ 4h, obtain upper oil phase suspension, i.e. volcanic mud oil-soluble extracting solution,
Volcanic mud after described extraction water-soluble extracting liquid and the mass ratio of oils and fats are 1:(25 ~ 35).
The preparation method of a kind of volcanic mud elite spraying facial film of the present invention is carried out according to the following steps:
One, take: take 25 parts ~ 75 parts volcanic mud elite, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids, 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides and 5 parts ~ 15 parts ethyl perfluorobutyl ether by weight;
Described volcanic mud elite is mixed by 10 parts ~ 12 parts volcanic mud oil-soluble extracting solution and 40 parts ~ 45 parts volcanic mud water-soluble extracting liquids by weight;
Described volcanic mud water-soluble extracting liquid is prepared according to the following steps: 1., at rotating speed be under the condition of 800r/min ~ 1000r/min, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 20kHz ~ 30kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit; Described moisture content is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:(20 ~ 30); 2., by step 1. in deposit by step 1. supersound extraction 2 times ~ 3 times, the volcanic mud after obtaining upper strata suspension and extracting water-soluble extracting liquid; 3., combining step 1. and the upper strata suspension of step 2. gained, namely obtain volcanic mud water-soluble extracting liquid;
Described volcanic mud oil-soluble extracting solution is prepared according to the following steps: under agitation, volcanic mud after extracting water-soluble extracting liquid is stirred, obtain the volcanic mud stirred, take oils and fats by weight again, described oils and fats is 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat, 5 parts ~ 8 parts squalanes, 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides compositions, first by 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat and 5 parts ~ 8 parts squalane mixing, obtain fat A, then by 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides mixing, obtain oils and fats B, under agitation, fat A and oils and fats B are joined in the volcanic mud stirred successively, obtain the volcanic mud after adding oils and fats, then be placed in and constant-temperature table carry out concussion by adding the volcanic mud after oils and fats and extract, the temperature of constant-temperature table is 30 DEG C ~ 50 DEG C, concussion frequency is 100rpm ~ 300rpm, extraction time is 2h ~ 4h, obtain upper oil phase suspension, i.e. volcanic mud oil-soluble extracting solution,
Volcanic mud after described extraction water-soluble extracting liquid and the mass ratio of oils and fats are 1:(25 ~ 35);
Two, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids are mixed with 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides, obtain mixture, then mixture is joined in volcanic mud elite, and be that under the condition of 1000r/min ~ 2000r/min, dispersed with stirring is even at rotating speed, then 5 parts ~ 15 parts ethyl perfluorobutyl ether are added, load in aerosol can after rotating speed is stir under the condition of 1000r/min ~ 2000r/min, namely obtain volcanic mud elite spraying facial film.
The invention has the beneficial effects as follows:
1, in volcanic mud elite aqueous phase leaching process, ultrasound wave is utilized to realize improving the extraction ratio of water soluble ingredient in the process do not heated, utilize orthogonal experiment to set optimum extraction condition, prevent process tediously long in the loss of active component in volcanic mud and traditional extraction.
2, in volcanic mud elite oil phase extracts, utilize compound water-soluble grease to take on extractant, in process, use constant-temperature table to realize fully contacting and extraction of volcanic mud and water-soluble grease.
3, this facial film adopts biphase suspension, because through volcanic mud molecular weight that is ultrasonic and that remain in after shaking in aqueous phase and oil phase, with skin contact after more easily can act on skin surface, waste that face causes that what before improving, volcanic mud cream pack was thick be coated in and airtight, uncomfortable sense organ.
4, add foaming agent when realizing volcanic mud elite to the importing of skin, because ever-increasing foam produces Bohr effect at face, after realizing, Rhizoma Atractylodis Macrocephalae China is absorbed greatly.
Specific embodiments
Specific embodiments one: present embodiment is that a kind of volcanic mud elite spraying facial film is prepared from by 25 parts ~ 75 parts volcanic mud elite, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids, 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides and 5 parts ~ 15 parts ethyl perfluorobutyl ether by weight;
Described volcanic mud elite is mixed by 10 parts ~ 12 parts volcanic mud oil-soluble extracting solution and 40 parts ~ 45 parts volcanic mud water-soluble extracting liquids by weight;
Described volcanic mud water-soluble extracting liquid is prepared according to the following steps: 1., at rotating speed be under the condition of 800r/min ~ 1000r/min, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 20kHz ~ 30kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit; Described moisture content is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:(20 ~ 30); 2., by step 1. in deposit by step 1. supersound extraction 2 times ~ 3 times, the volcanic mud after obtaining upper strata suspension and extracting water-soluble extracting liquid; 3., combining step 1. and the upper strata suspension of step 2. gained, namely obtain volcanic mud water-soluble extracting liquid;
Described volcanic mud oil-soluble extracting solution is prepared according to the following steps: under agitation, volcanic mud after extracting water-soluble extracting liquid is stirred, obtain the volcanic mud stirred, take oils and fats by weight again, described oils and fats is 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat, 5 parts ~ 8 parts squalanes, 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides compositions, first by 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat and 5 parts ~ 8 parts squalane mixing, obtain fat A, then by 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides mixing, obtain oils and fats B, under agitation, fat A and oils and fats B are joined in the volcanic mud stirred successively, obtain the volcanic mud after adding oils and fats, then be placed in and constant-temperature table carry out concussion by adding the volcanic mud after oils and fats and extract, the temperature of constant-temperature table is 30 DEG C ~ 50 DEG C, concussion frequency is 100rpm ~ 300rpm, extraction time is 2h ~ 4h, obtain upper oil phase suspension, i.e. volcanic mud oil-soluble extracting solution,
Volcanic mud after described extraction water-soluble extracting liquid and the mass ratio of oils and fats are 1:(25 ~ 35).
In this detailed description of the invention 2. in by step 1. in deposit by step 1. supersound extraction specifically to carry out according to the following steps for 2 times ~ 3 times: a, at rotating speed be 800r/min ~ 1000r/min condition under, deposit is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 20kHz ~ 30kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit; B, repetition a2 time ~ 3 times; Described deposit and the mass ratio of water are 1:(20 ~ 30).
The beneficial effect of present embodiment is: 1, in volcanic mud elite aqueous phase leaching process, ultrasound wave is utilized to realize improving the extraction ratio of water soluble ingredient in the process do not heated, utilize orthogonal experiment to set optimum extraction condition, prevent process tediously long in the loss of active component in volcanic mud and traditional extraction.
2, in volcanic mud elite oil phase extracts, utilize compound water-soluble grease to take on extractant, in process, use constant-temperature table to realize fully contacting and extraction of volcanic mud and water-soluble grease.
3, this facial film adopts biphase suspension, because through volcanic mud molecular weight that is ultrasonic and that remain in after shaking in aqueous phase and oil phase, with skin contact after more easily can act on skin surface, waste that face causes that what before improving, volcanic mud cream pack was thick be coated in and airtight, uncomfortable sense organ.
4, add foaming agent when realizing volcanic mud elite to the importing of skin, because ever-increasing foam produces Bohr effect at face, after realizing, Rhizoma Atractylodis Macrocephalae China is absorbed greatly.
Detailed description of the invention two: the preparation method of a kind of volcanic mud elite spraying facial film described in present embodiment, specifically carry out according to following steps:
One, take: take 25 parts ~ 75 parts volcanic mud elite, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids, 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides and 5 parts ~ 15 parts ethyl perfluorobutyl ether by weight;
Described volcanic mud elite is mixed by 10 parts ~ 12 parts volcanic mud oil-soluble extracting solution and 40 parts ~ 45 parts volcanic mud water-soluble extracting liquids by weight;
Described volcanic mud water-soluble extracting liquid is prepared according to the following steps: 1., at rotating speed be under the condition of 800r/min ~ 1000r/min, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 20kHz ~ 30kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit; Described moisture content is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:(20 ~ 30); 2., by step 1. in deposit by step 1. supersound extraction 2 times ~ 3 times, the volcanic mud after obtaining upper strata suspension and extracting water-soluble extracting liquid; 3., combining step 1. and the upper strata suspension of step 2. gained, namely obtain volcanic mud water-soluble extracting liquid;
Described volcanic mud oil-soluble extracting solution is prepared according to the following steps: under agitation, volcanic mud after extracting water-soluble extracting liquid is stirred, obtain the volcanic mud stirred, take oils and fats by weight again, described oils and fats is 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat, 5 parts ~ 8 parts squalanes, 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides compositions, first by 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat and 5 parts ~ 8 parts squalane mixing, obtain fat A, then by 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides mixing, obtain oils and fats B, under agitation, fat A and oils and fats B are joined in the volcanic mud stirred successively, obtain the volcanic mud after adding oils and fats, then be placed in and constant-temperature table carry out concussion by adding the volcanic mud after oils and fats and extract, the temperature of constant-temperature table is 30 DEG C ~ 50 DEG C, concussion frequency is 100rpm ~ 300rpm, extraction time is 2h ~ 4h, obtain upper oil phase suspension, i.e. volcanic mud oil-soluble extracting solution,
Volcanic mud after described extraction water-soluble extracting liquid and the mass ratio of oils and fats are 1:(25 ~ 35);
Two, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids are mixed with 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides, obtain mixture, then mixture is joined in volcanic mud elite, and be that under the condition of 1000r/min ~ 2000r/min, dispersed with stirring is even at rotating speed, then 5 parts ~ 15 parts ethyl perfluorobutyl ether are added, load in aerosol can after rotating speed is stir under the condition of 1000r/min ~ 2000r/min, namely obtain volcanic mud elite spraying facial film.
In this detailed description of the invention step one 2. in by step 1. in deposit by step 1. supersound extraction specifically to carry out according to the following steps for 2 times ~ 3 times: a, at rotating speed be 800r/min ~ 1000r/min condition under, deposit is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 20kHz ~ 30kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit; B, repetition a2 time ~ 3 times; Described deposit and the mass ratio of water are 1:(20 ~ 30).
The beneficial effect of present embodiment is: 1, in volcanic mud elite aqueous phase leaching process, ultrasound wave is utilized to realize improving the extraction ratio of water soluble ingredient in the process do not heated, utilize orthogonal experiment to set optimum extraction condition, prevent process tediously long in the loss of active component in volcanic mud and traditional extraction.
2, in volcanic mud elite oil phase extracts, utilize compound water-soluble grease to take on extractant, in process, use constant-temperature table to realize fully contacting and extraction of volcanic mud and water-soluble grease.
3, this facial film adopts biphase suspension, because through volcanic mud molecular weight that is ultrasonic and that remain in after shaking in aqueous phase and oil phase, with skin contact after more easily can act on skin surface, waste that face causes that what before improving, volcanic mud cream pack was thick be coated in and airtight, uncomfortable sense organ.
4, add foaming agent when realizing volcanic mud elite to the importing of skin, because ever-increasing foam produces Bohr effect at face, after realizing, Rhizoma Atractylodis Macrocephalae China is absorbed greatly.
Detailed description of the invention three: present embodiment and detailed description of the invention two difference are: the moisture content described in step one is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:25.Other is identical with detailed description of the invention two.
Detailed description of the invention four: one of present embodiment and detailed description of the invention two or three difference is: be under the condition of 800r/min ~ 1000r/min at rotating speed in step one, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 25kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit.Other is identical with detailed description of the invention two or three.
Detailed description of the invention five: one of present embodiment and detailed description of the invention two to four difference is: be placed in and constant-temperature table carry out concussion by adding the volcanic mud after oils and fats and extract in step one, the temperature of constant-temperature table is 40 DEG C, concussion frequency is 200rpm, and extraction time is 2h ~ 4h.Other is identical with detailed description of the invention two to four.
Adopt following verification experimental verification effect of the present invention:
Embodiment one:
Volcanic mud elite spraying facial film is prepared from by 50 parts of volcanic mud elite, 2 parts of lanolines, 10 parts of lauric acids, 5 parts of lauryl trimethyl ammonium chlorides and 10 parts of ethyl perfluorobutyl ether by weight.
The preparation method of described volcanic mud elite spraying facial film is carried out according to the following steps:
One, take: take 50 parts of volcanic mud elite, 2 parts of lanolines, 10 parts of lauric acids, 5 parts of lauryl trimethyl ammonium chlorides and 10 parts of ethyl perfluorobutyl ether by weight;
Described volcanic mud elite is mixed by 12 parts of volcanic mud oil-soluble extracting solution and 45 parts of volcanic mud water-soluble extracting liquids by weight;
Described volcanic mud water-soluble extracting liquid is prepared according to the following steps: 1., at rotating speed be under the condition of 900r/min, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 25kHz in supersonic frequency, extract 30min, obtain upper strata suspension and deposit; Described moisture content is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:25; 2., by step 1. in deposit by step 1. supersound extraction 2 times, the volcanic mud after obtaining upper strata suspension and extracting water-soluble extracting liquid; 3., combining step 1. and the upper strata suspension of step 2. gained, namely obtain volcanic mud water-soluble extracting liquid;
Described volcanic mud oil-soluble extracting solution is prepared according to the following steps: under agitation, volcanic mud after extracting water-soluble extracting liquid is stirred, obtain the volcanic mud stirred, take oils and fats by weight again, described oils and fats is 5 portions of almond oil, 10 parts of olive oil, 5 portions of Oleum Cocois, 5 parts of babassu oil fat, 5 parts of squalanes, 5 parts of polyoxyethylene lauryl ether sodium sulfate, 10 parts of sodium lauryl sulphates, 1 part of cocamidopropyl betaine and 2 parts of alkylolamides compositions, first by 5 portions of almond oil, 10 parts of olive oil, 5 portions of Oleum Cocois, 5 parts of babassu oil fat and 5 parts of squalane mixing, obtain fat A, then by 5 parts of polyoxyethylene lauryl ether sodium sulfate, 10 parts of sodium lauryl sulphates, 1 part of cocamidopropyl betaine and 2 parts of alkylolamides mixing, obtain oils and fats B, under agitation, fat A and oils and fats B are joined in the volcanic mud stirred successively, obtain the volcanic mud after adding oils and fats, then be placed in and constant-temperature table carry out concussion by adding the volcanic mud after oils and fats and extract, the temperature of constant-temperature table is 40 DEG C, concussion frequency is 200rpm, extraction time is 3h, obtain upper oil phase suspension, i.e. volcanic mud oil-soluble extracting solution,
Volcanic mud after described extraction water-soluble extracting liquid and the mass ratio of oils and fats are 1:30;
Two, 2.5 parts of lanolines, 12.5 parts of lauric acids are mixed with 7.5 parts of lauryl trimethyl ammonium chlorides, obtain mixture, then mixture is joined in volcanic mud elite, and be that under the condition of 2000r/min, dispersed with stirring is even at rotating speed, then 15 parts of ethyl perfluorobutyl ether are added, load in aerosol can after rotating speed is stir under the condition of 2000r/min, namely obtain volcanic mud elite spraying facial film.
To volcanic mud elite spraying facial film test prepared by the present embodiment, method of testing is carried out according to the following steps:
Volcanic mud elite spraying facial film is the product being directly used in skin, the value of product is decided by sensory effects such as comfort levels, in order to understand the result of use of volcanic mud elite spraying facial film prepared by the present embodiment, with the form of questionnaire survey, investigation on probation is widely carried out to volcanic mud elite spraying facial film prepared by the present embodiment, trier 100 people, wherein male 19 people, women 81 people, the oldest 50 years old, minimum 18 years old, about 30 years old mean age, 93 parts are regained altogether after on probation, 93 triers use after this product breathability, comfortableness, assimilation effect, use film wettability after 15min and use the result of use evaluation of indices of film laminating degree after 15min, test result is as shown in table 1:
As seen from table: 1, breathability: the trier of 73.13% feels that breathability is fine, and the trier of 15.05% feels that breathability is better;
2, comfortableness: the trier of 78.50% feels that comfortableness is fine, and the trier of 17.20% feels that comfortableness is better;
3, assimilation effect: the trier of 70.97% feels that assimilation effect is fine, and the trier of 20.43% feels that assimilation effect is better;
4, film wettability after 15min is used: the trier of 81.72% feels that wettability is fine, and the trier of 6.45% feels that wettability is better;
5, film laminating degree after 15min is used: the trier of 80.64% feels that laminating degree is fine, and the trier of 11.83% feels that laminating degree is better;
6, allergy is stimulated: non-stimulated irritated example.
As can be seen from the result of the self assessment of trier, after volcanic mud elite spraying facial film uses 15min, still there is good wettability and laminating degree, thus there is good breathability and comfortableness, therefore, make the effective ingredient of the top layer volcanic mud contacted with air can be conducted into skin completely, reach and utilize completely, good absorbing effect, and do not find that product produces stimulation allergic phenomena to trier.
Claims (5)
1. a volcanic mud elite spraying facial film, is characterized in that volcanic mud elite spraying facial film is prepared from by 25 parts ~ 75 parts volcanic mud elite, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids, 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides and 5 parts ~ 15 parts ethyl perfluorobutyl ether by weight;
Described volcanic mud elite is mixed by 10 parts ~ 12 parts volcanic mud oil-soluble extracting solution and 40 parts ~ 45 parts volcanic mud water-soluble extracting liquids by weight;
Described volcanic mud water-soluble extracting liquid is prepared according to the following steps: 1., at rotating speed be under the condition of 800r/min ~ 1000r/min, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 20kHz ~ 30kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit; Described moisture content is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:(20 ~ 30); 2., by step 1. in deposit by step 1. supersound extraction 2 times ~ 3 times, the volcanic mud after obtaining upper strata suspension and extracting water-soluble extracting liquid; 3., combining step 1. and the upper strata suspension of step 2. gained, namely obtain volcanic mud water-soluble extracting liquid;
Described volcanic mud oil-soluble extracting solution is prepared according to the following steps: under agitation, volcanic mud after extracting water-soluble extracting liquid is stirred, obtain the volcanic mud stirred, take oils and fats by weight again, described oils and fats is 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat, 5 parts ~ 8 parts squalanes, 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides compositions, first by 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat and 5 parts ~ 8 parts squalane mixing, obtain fat A, then by 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides mixing, obtain oils and fats B, under agitation, fat A and oils and fats B are joined in the volcanic mud stirred successively, obtain the volcanic mud after adding oils and fats, then be placed in and constant-temperature table carry out concussion by adding the volcanic mud after oils and fats and extract, the temperature of constant-temperature table is 30 DEG C ~ 50 DEG C, concussion frequency is 100rpm ~ 300rpm, extraction time is 2h ~ 4h, obtain upper oil phase suspension, i.e. volcanic mud oil-soluble extracting solution,
Volcanic mud after described extraction water-soluble extracting liquid and the mass ratio of oils and fats are 1:(25 ~ 35).
2. preparation a kind of volcanic mud elite spraying facial film according to claim 1, is characterized in that the preparation method of a kind of volcanic mud elite spraying facial film is carried out according to the following steps:
One, take: take 25 parts ~ 75 parts volcanic mud elite, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids, 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides and 5 parts ~ 15 parts ethyl perfluorobutyl ether by weight;
Described volcanic mud elite is mixed by 10 parts ~ 12 parts volcanic mud oil-soluble extracting solution and 40 parts ~ 45 parts volcanic mud water-soluble extracting liquids by weight;
Described volcanic mud water-soluble extracting liquid is prepared according to the following steps: 1., at rotating speed be under the condition of 800r/min ~ 1000r/min, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 20kHz ~ 30kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit; Described moisture content is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:(20 ~ 30); 2., by step 1. in deposit by step 1. supersound extraction 2 times ~ 3 times, the volcanic mud after obtaining upper strata suspension and extracting water-soluble extracting liquid; 3., combining step 1. and the upper strata suspension of step 2. gained, namely obtain volcanic mud water-soluble extracting liquid;
Described volcanic mud oil-soluble extracting solution is prepared according to the following steps: under agitation, volcanic mud after extracting water-soluble extracting liquid is stirred, obtain the volcanic mud stirred, take oils and fats by weight again, described oils and fats is 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat, 5 parts ~ 8 parts squalanes, 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides compositions, first by 5 parts ~ 12.5 portions almond oil, 10 parts ~ 15 parts olive oil, 5 parts ~ 15 portions Oleum Cocois, 5 parts ~ 15 parts babassu oil fat and 5 parts ~ 8 parts squalane mixing, obtain fat A, then by 5 parts ~ 10 parts polyoxyethylene lauryl ether sodium sulfate, 10 parts ~ 12.5 parts sodium lauryl sulphates, 1 part ~ 2 parts cocamidopropyl betaine and 2 parts ~ 5 parts alkylolamides mixing, obtain oils and fats B, under agitation, fat A and oils and fats B are joined in the volcanic mud stirred successively, obtain the volcanic mud after adding oils and fats, then be placed in and constant-temperature table carry out concussion by adding the volcanic mud after oils and fats and extract, the temperature of constant-temperature table is 30 DEG C ~ 50 DEG C, concussion frequency is 100rpm ~ 300rpm, extraction time is 2h ~ 4h, obtain upper oil phase suspension, i.e. volcanic mud oil-soluble extracting solution,
Volcanic mud after described extraction water-soluble extracting liquid and the mass ratio of oils and fats are 1:(25 ~ 35);
Two, 2 parts ~ 2.5 parts lanolines, 5 parts ~ 12.5 parts lauric acids are mixed with 2 parts ~ 7.5 parts lauryl trimethyl ammonium chlorides, obtain mixture, then mixture is joined in volcanic mud elite, and be that under the condition of 1000r/min ~ 2000r/min, dispersed with stirring is even at rotating speed, then 5 parts ~ 15 parts ethyl perfluorobutyl ether are added, load in aerosol can after rotating speed is stir under the condition of 1000r/min ~ 2000r/min, namely obtain volcanic mud elite spraying facial film.
3. the preparation method of a kind of volcanic mud elite spraying facial film according to claim 2, is characterized in that the moisture content described in step one is less than the volcanic mud dry powder of 5% and the mass ratio of water is 1:25.
4. the preparation method of a kind of volcanic mud elite spraying facial film according to claim 2, to it is characterized in that in step one under rotating speed is the condition of 800r/min ~ 1000r/min, volcanic mud dry powder moisture content being less than 5% is mixed homogeneously with water, obtain mud mixture, then mud mixture is placed in ultrasonic extractor, be under the condition of 25kHz in supersonic frequency, extract 25min ~ 35min, obtain upper strata suspension and deposit.
5. the preparation method of a kind of volcanic mud elite spraying facial film according to claim 2, it is characterized in that being placed in and constant-temperature table carrying out concussion by adding the volcanic mud after oils and fats and extract in step one, the temperature of constant-temperature table is 40 DEG C, and concussion frequency is 200rpm, and extraction time is 2h ~ 4h.
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| CN104983609A (en) * | 2015-06-11 | 2015-10-21 | 珀莱雅化妆品股份有限公司 | Spraying type mask and preparation method thereof |
| CN107375081A (en) * | 2017-08-04 | 2017-11-24 | 兰新全 | Replenishing water and preserving moisture is releived toner and preparation method thereof |
| CN107496319A (en) * | 2017-08-04 | 2017-12-22 | 兰新全 | Moisturizing whitening is releived essence lotion and preparation method thereof |
| CN107536791A (en) * | 2017-08-04 | 2018-01-05 | 兰新全 | A kind of deep layer cleaning mud mask and preparation method thereof |
| CN107693404A (en) * | 2017-11-03 | 2018-02-16 | 黑龙江省科学院火山与矿泉研究所 | Slime hair mask and method for preparing slime hair mask cap by using slime hair mask |
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