CN106265266A - A kind of containing chlorophyllous Shu Min bath gel - Google Patents

A kind of containing chlorophyllous Shu Min bath gel Download PDF

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Publication number
CN106265266A
CN106265266A CN201610737365.1A CN201610737365A CN106265266A CN 106265266 A CN106265266 A CN 106265266A CN 201610737365 A CN201610737365 A CN 201610737365A CN 106265266 A CN106265266 A CN 106265266A
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bath gel
parts
shu min
thallus
chlorophyllous
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CN106265266B (en
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陈松彬
易萍
倪彦艳
刘杰森
张爱萍
李小翠
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Guangdong Kewei Biological Technology Co Ltd
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Guangdong Kewei Biological Technology Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20—Halogens; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42—Amides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
    • A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86—Polyethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005—Antimicrobial preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/005—Preparations for sensitive skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42—Colour properties
    • A61K2800/43—Pigments; Dyes
    • A61K2800/436—Interference pigments, e.g. Iridescent, Pearlescent

Abstract

The present invention relates to a kind of containing chlorophyllous Shu Min bath gel, belong to technical field of cosmetic preparation.In order to overcome the deficiencies in the prior art, the present invention provides a kind of containing chlorophyllous Shu Min bath gel, the preparation technology of this Shu Min bath gel includes three steps of prescription dispensing of the chlorophyllous extraction of Thallus Laminariae (Thallus Eckloniae), the preparation of Chinese medicine essence and Shu Min bath gel, the Shu Min bath gel stable in properties obtained of preparation, moisturizing whitening effect is notable, and overcome the conventional poor stability containing chlorophyllous Shu Min bath gel and the technical deficiency of allergy, therefore there is good market prospect.

Description

A kind of containing chlorophyllous Shu Min bath gel
Technical field
The present invention relates to a kind of containing chlorophyllous Shu Min bath gel, belong to technical field of cosmetic preparation.
Background technology
Bath gel, also known as bath oil, bath foam, be a kind of modern common cleaning supplies, the invention master of bath oil If for sense of touch and effect of replacing tradition cleaning soap, not having as soap hard during bath oil contact people's skin The sensation of watchman's wooden clapper watchman's wooden clapper, some manufacturers even release the bath oil of effective in cure or special fragrance so that many people go after like a flock of ducks.The most also There are child's bath oil, male's bath oil, baby body wash etc., a feast for the eyes.In recent years, owing to bath gel product employing relatively Many additives, there is redness, the allergic symptoms such as pain of itching after using, drastically influence consumption in bath gel products a lot of on market Person's confidence to product.Along with green product degree of concern is gradually increased by people, natural environmental-protective type additive cosmetics are Become current main direction of studying.
Chlorophyll is the Primary Actor of photosynthesis of plant, and its content is assessment phytomass, volume of production and health The physical signs of degree etc..Chlorophyll is a kind of good natural pigment, and has refreshing and detoxicating, moisturizing, opposing radiation etc. to make The important nutrient substance by, a kind of uniqueness of being present in green plants, starts gradually to be applied to cosmetic field.Natural Chlorophyll is water insoluble, easily decomposes under the conditions of heat, light, oxygen etc., and chlorophyllous extraction and preparation difficulty are relatively greatly, make After Shu Min bath gel apt to deteriorate, so when plant chlorophyll extracts must to different disposal under the conditions of chlorophyllous stability enter Row research.
Chinese invention patent application CN104055724A discloses the preparation method of a kind of technology of Momordica Charantia L. chlorophyll face mask cream, its bag Include following steps: 1) extraction of technology of Momordica Charantia L. chlorophyll: 1.1) get the raw materials ready: Fructus Momordicae charantiae is pulled an oar, filtering residue；1.2) alcohol steep；1.3) Concentrate；1.4) petroleum ether extraction；1.5) it is concentrated in vacuo dry, obtains technology of Momordica Charantia L. chlorophyll standby；2) technology of Momordica Charantia L. chlorophyll face mask cream Preparation: 2.1) expect: two Plurol Oleique CC497s 3～4；Stearic acid 1～2；Hexadecanol 4～5；Glycerol 6～7；Oleum Ricini 8～9； Chlorophyll 0.5～1；The Pseudobulbus Bletillae (Rhizoma Bletillae) 10～12；Margarita powder 10～12；Sorbester p18 2～3；Polysorbate60 2～3；Starch 1～2；Three carboxymethyls Sodium cellulosate 8～10；Vitamin E 0.3～0.5；Water 50～60；2.2) oil mixture is prepared；2.3) aqueous phase mixing is prepared Thing；2.4) technology of Momordica Charantia L. chlorophyll face mask cream it is mixed to form.It is published in 2010 " development of leaves of hyacinth verdazulene face mask cream " with water Calabash chlorophyll is principle active component, be then aided with two Plurol Oleique CC497s, stearic acid, hexadecanol, glycerol, Oleum Ricini, Chlorophyll, the Pseudobulbus Bletillae (Rhizoma Bletillae) are object of study and the reciprocal action that considers between them have developed a kind of leaves of hyacinth verdazulene face mask cream, tool Standby certain shelf characteric and cosmetic result.Patent application 200810104962.6 discloses a kind of chlorophyllin copper complex sodium baby moistening Bath gel, it is using chlorophyllin copper complex sodium as one of main composition, and its primary raw material includes chlorophyllin copper complex sodium, milk, cocos nucifera oil Amido propyl betaine, cocos nucifera oil both sexes sodium acetate, Fructus Citri Limoniae flavoring orange essence and water, this functional bath gel has multiple efficacies, But it is the form of chlorophyllide, it is difficult to play effect of chlorophyllous skin moistening and whitening.
Above-mentioned prior art discloses chlorophyll or its salt has had the use for cosmetics to report as effective ingredient, But most products function is more single, and there is a lot of user still can produce the allergic symptoms such as pruritus herpes in use process, It is difficult to meet the women demand to Shu Min bath gel of liking to be beautiful on existing market.Based on this, the present invention provides a kind of containing chlorophyll Shu Min bath gel, it not only has good moistening effect, and is possible to prevent skin allergy, has good antibiotic and sterilizing Effect.
Summary of the invention
In order to overcome above-mentioned the deficiencies in the prior art, the present invention provides a kind of containing chlorophyllous Shu Min bath gel and system thereof Preparation Method, its preparation nature is stable, and antibiotic and sterilizing effect is notable, and overcomes routine containing chlorophyllous Shu Min bath gel The allergic symptom existed, therefore has good market prospect.
The present invention is achieved through the following technical solutions above-mentioned technique effect:
A kind of containing chlorophyllous Shu Min bath gel, its preparation method specifically includes following steps:
1) the chlorophyllous extraction of Thallus Laminariae (Thallus Eckloniae): take Thallus Laminariae (Thallus Eckloniae) in darkroom and be placed in Webster blender pulverizing and obtain Thallus Laminariae (Thallus Eckloniae) powder, toward Thallus Laminariae (Thallus Eckloniae) The mixed solvent adding Thallus Laminariae (Thallus Eckloniae) opaque amount 5-6 times weight in powder carries out ultrasonic extraction, and concussion shakes up, and controls Extracting temperature and is 43-56 DEG C, control supersonic frequency 250-350Hz of ultrasound wave, by extracting solution frozen centrifugation after extracting 1.5-3.5 hour continuously, Centrifugal rotational speed is 2000-4000rpm, obtains supernatant, add magnesium chloride and potassium chloride makes in supernatant after centrifugal 10-15min The concentration of magnesium ion and the concentration of potassium ion are respectively 0.08 μ g/mL and 0.5 μ g/mL, i.e. can get Thallus Laminariae (Thallus Eckloniae) chlorophyll solution, its Described in the mixed solvent that mixed solvent is methanol, n-butyl alcohol and petroleum ether, by volume, methanol: n-butyl alcohol: petroleum ether is 1:0.2-0.4:0.5-0.8；
2) preparation of Chinese medicine essence: accurately weigh 10-12 part Herba Portulacae, 15-18 part Herba Menthae, 12-14 part Flos Chrysanthemi Indici, 5- Being ground into 80-100 mesh after 7 parts of fragrant citrus seed mixing, be added thereto to 80% ethanol solution of 8 times of weight, controlling Extracting temperature is 80-90 DEG C of reflux, extract, 40-60min, obtains Chinese medicine extraction liquid；Chinese medicine extraction liquid is joined in distillator, 40-55 DEG C of decompression Ethanol is distilled off, i.e. can get Chinese medicine essence；
3) prepared by Shu Min bath gel: join in emulsifying pot by 0.4-0.6 part hydroxyethyl cellulose, and stirring is warming up to 75- 80 DEG C, homogenizing 3min, after material dissolution homogeneous transparent, sequentially add 28-32 part amino acid surfactant, 1.0-3.0 Part coconut oleoyl amine DEA, 14-16 part NT-D55,0.8-1.2 part 3237DS pearly-lustre grain stirring, to whole material dissolutions, is incubated 10min After when being cooled to 70 DEG C, add the most scattered 7.5-8.5 part acrylic copolymer, after stirring, be cooled to 35 DEG C, Successively in mixed liquor add 1.8-2.2 part Glucam E-20,16-24 part Thallus Laminariae (Thallus Eckloniae) chlorophyll, 35-40 part Chinese medicine essence, 0.3-0.7 part drosophila melanogaster antimicrobial peptide, 0.3-0.5 part essence；Carry out middle inspection by Nacl regulation product viscosity, filter out after the assay was approved Material, obtains containing chlorophyllous Shu Min bath gel.Preparation method containing chlorophyllous Shu Min bath gel as above, wherein Described step 1) in mixed solvent, by volume, methanol: n-butyl alcohol: petroleum ether is preferably 1:0.3:0.7, this mixed solvent The Thallus Laminariae (Thallus Eckloniae) chlorophyll content of lower extraction is the highest, for the improvement best results of skin.
The preparation method containing chlorophyllous Shu Min bath gel as above, wherein said step 2) in Chinese medicine essence Raw material of preparing be: 11 portions of Herba Portulacaes, 16 portions of Herba Menthaes, 13 parts of Flos Chrysanthemi Indicis, 6 parts of fragrant citrus seeds.Chinese medicine elite under this combination matching After liquid mixes with Thallus Laminariae (Thallus Eckloniae) chlorophyll solution, the chlorophyllous stability of Thallus Laminariae (Thallus Eckloniae) is higher, and more can play its collaborative U.S. after the two mixing Hold whitening effect.
The preparation method containing chlorophyllous Shu Min bath gel as above, described step 3) comprise the steps: by 0.5 part of hydroxyethyl cellulose joins in emulsifying pot, and stirring is warming up to 78 DEG C, homogenizing 3min, after material dissolution homogeneous transparent, Sequentially add 30 parts of amino acid surfactants, 2.0 parts of coconut oleoyl amine DEA, 15 parts of NT-D55,1.0 parts of 3237DS pearly-lustre grains Stir to whole material dissolutions, when being cooled to 70 DEG C after insulation 10min, add 8.0 parts of the most scattered acrylic copolymer Thing, is cooled to 35 DEG C after stirring, add in mixed liquor successively 2.0 parts of Glucam E-20,18 parts of Thallus Laminariae (Thallus Eckloniae) chlorophylls, 38 Part Chinese medicine essence, 0.4 part of drosophila melanogaster antimicrobial peptide, 0.4 part of essence；Middle inspection is carried out, after the assay was approved by Nacl regulation product viscosity Filter discharging, obtain containing chlorophyllous Shu Min bath gel.The present invention is also claimed and directly obtains according to above-mentioned preparation method Shu Min bath gel.
Prepare Shu Min bath gel according to the method described above and there is good beauty treatment and eliminating spot whitening effect, the embodiment of the present invention 4 show, from the stability of product, comparative example 1, the instability of product of comparative example 2, this shows to add wherein Enter metal ion and Chinese medicine essence can affect the stability of product Determination of Chlorophyll.Add metal ion and Chinese medicine elite The stability of the product of liquid is preferable.From whitening and freckle effect, the whitening effect of embodiment of the present invention product and dispelling Speckle effect is preferable, and trier not only makes skin present moist, tender, smooth, refrigerant sensation with this product of rear reflection, and has Well sun-screening function, can alleviate speckle on pachylosis, desalination face.It is better than prior art comparative example 4, is also significantly better than Shu Min bath gel that Thallus Laminariae (Thallus Eckloniae) chlorophyll is made separately as effective ingredient and Chinese medicine essence are as relaxing that effective ingredient is made Quick bath gel, this shows that two groups of compositions have notable synergism in terms of brightening, dispelling spots, dispelling.Wherein with comparative example 2 correspondence Product effect is best, for optimum embodiment.Based on this, the present invention is also claimed described containing chlorophyllous Shu Min bath gel Application in preparing brightening, dispelling spots, dispelling product.
The present invention compared with prior art has a following technical advantage:
1) stability of product is more preferable.Experiment shows, adds metal ion and middle YAOJING in Thallus Laminariae (Thallus Eckloniae) chlorophyll solution China's liquid can affect the stability of product Determination of Chlorophyll.Add the stability of product of metal ion and Chinese medicine essence relatively Good.
2) there is good brightening, dispelling spots, dispelling effect and antiallergic effect.From whitening and freckle effect, the present invention is real Execute the whitening effect of example product and freckle effect be preferable, trier with this product of rear reflection not only make skin present moist, Tender, smooth, refrigerant sensation, and have good sun-screening function, speckle on pachylosis, desalination face can be alleviated.Its effect is better than Prior art products.Product of the present invention has significant antiallergic effect, and user occurs that the probability of allergic symptom is 0, this table Bright, reasonable recipe of the present invention, additive is safe and reliable, has good application prospect.
3) Thallus Laminariae (Thallus Eckloniae) chlorophyll and Chinese medicine essence have notable synergism in terms of whitening and speckle dispelling.Shu Min of the present invention takes a shower Dew is substantially better than Shu Min bath gel and Chinese medicine essence that Thallus Laminariae (Thallus Eckloniae) chlorophyll makes separately as effective ingredient as effectively becoming Dividing the Shu Min bath gel made, this shows that two groups of compositions have notable synergism in terms of brightening, dispelling spots, dispelling.Wherein real to contrast The product effect executing example 2 correspondence is best, for optimum embodiment.
Detailed description of the invention
Further describe the present invention below by way of specific embodiment, but described embodiment never in any form restriction are the most specially The protection domain of profit.
Embodiment 1
A kind of containing chlorophyllous Shu Min bath gel, its preparation method specifically includes following steps:
1) the chlorophyllous extraction of Thallus Laminariae (Thallus Eckloniae): take Thallus Laminariae (Thallus Eckloniae) in darkroom and be placed in Webster blender pulverizing and obtain Thallus Laminariae (Thallus Eckloniae) powder, toward Thallus Laminariae (Thallus Eckloniae) The mixed solvent adding Thallus Laminariae (Thallus Eckloniae) 5 times of weight of opaque amount in powder carries out ultrasonic extraction, and concussion shakes up, and controlling Extracting temperature is 43 DEG C, control supersonic frequency 250Hz of ultrasound wave, after extracting 1.5 hours continuously by extracting solution frozen centrifugation, centrifugal rotational speed be 2000rpm, after centrifugal 10min supernatant, in supernatant, add magnesium chloride and potassium chloride make the concentration of magnesium ion and potassium from The concentration of son is respectively 0.08 μ g/mL and 0.5 μ g/mL, i.e. can get Thallus Laminariae (Thallus Eckloniae) chlorophyll solution, wherein said mixed solvent, By volume, methanol: n-butyl alcohol: petroleum ether is 1:0.2:0.5；
2) preparation of Chinese medicine essence: accurately weighing 10 portions of Herba Portulacaes, 15 portions of Herba Menthaes, 12 parts of Flos Chrysanthemi Indicis, 5 parts of fragrant citrus seeds mix Being ground into 80 mesh after conjunction, be added thereto to 80% ethanol solution of 8 times of weight, controlling Extracting temperature is 80 DEG C of reflux, extract, 40min, obtains Chinese medicine extraction liquid；Being joined by Chinese medicine extraction liquid in distillator, 40 DEG C of decompressions are distilled off ethanol, the most available Chinese medicine essence；
3) prepared by Shu Min bath gel: join in emulsifying pot by 0.4 part of hydroxyethyl cellulose, and stirring is warming up to 75 DEG C, all Matter 3min, after material dissolution homogeneous transparent, sequentially add 28 parts of amino acid surfactants, 1.0 parts of coconut oleoyl amine DEA, 14 parts of NT-D55,0.8-1.2 part 3237DS pearly-lustre grain stirrings, to whole material dissolutions, when being cooled to 70 DEG C after insulation 10min, add Enter the most scattered 7.5 part acrylic copolymer, after stirring, be cooled to 35 DEG C, in mixed liquor, add 1.8 successively Part Glucam E-20,16 parts of Thallus Laminariae (Thallus Eckloniae) chlorophylls, 35 parts of Chinese medicine essences, 0.3 part of drosophila melanogaster antimicrobial peptide, 0.3 part of essence；Use Nacl Regulation product viscosity carries out middle inspection, filters discharging after the assay was approved, obtains containing chlorophyllous Shu Min bath gel.
Embodiment 2
A kind of containing chlorophyllous Shu Min bath gel, its preparation method specifically includes following steps:
1) the chlorophyllous extraction of Thallus Laminariae (Thallus Eckloniae): take Thallus Laminariae (Thallus Eckloniae) in darkroom and be placed in Webster blender pulverizing and obtain Thallus Laminariae (Thallus Eckloniae) powder, toward Thallus Laminariae (Thallus Eckloniae) The mixed solvent adding Thallus Laminariae (Thallus Eckloniae) 6 times of weight of opaque amount in powder carries out ultrasonic extraction, and concussion shakes up, and controlling Extracting temperature is 50 DEG C, control supersonic frequency 300Hz of ultrasound wave, after extracting 2.5 hours continuously by extracting solution frozen centrifugation, centrifugal rotational speed be 3000rpm, after centrifugal 15min supernatant, in supernatant, add magnesium chloride and potassium chloride make the concentration of magnesium ion and potassium from The concentration of son is respectively 0.08 μ g/mL and 0.5 μ g/mL, i.e. can get Thallus Laminariae (Thallus Eckloniae) chlorophyll solution, wherein said mixed solvent, By volume, methanol: n-butyl alcohol: petroleum ether is 1:0.3:0.7；
2) preparation of Chinese medicine essence: accurately weighing 11 portions of Herba Portulacaes, 16 portions of Herba Menthaes, 13 parts of Flos Chrysanthemi Indicis, 6 parts of fragrant citrus seeds mix Being ground into 100 mesh after conjunction, be added thereto to 80% ethanol solution of 8 times of weight, controlling Extracting temperature is 85 DEG C of reflux, extract, 50min, obtains Chinese medicine extraction liquid；Being joined by Chinese medicine extraction liquid in distillator, 48 DEG C of decompressions are distilled off ethanol, the most available Chinese medicine essence；
3) prepared by Shu Min bath gel: join in emulsifying pot by 0.5 part of hydroxyethyl cellulose, and stirring is warming up to 78 DEG C, all Matter 3min, after material dissolution homogeneous transparent, sequentially add 30 parts of amino acid surfactants, 2.0 parts of coconut oleoyl amine DEA, 15 parts of NT-D55,1.0 parts of 3237DS pearly-lustre grain stirrings, to whole material dissolutions, when being cooled to 70 DEG C after insulation 10min, add pre- 8.0 parts of the most scattered acrylic copolymers, are cooled to 35 DEG C after stirring, add 2.0 parts successively in mixed liquor Glucam E-20,18 parts of Thallus Laminariae (Thallus Eckloniae) chlorophylls, 38 parts of Chinese medicine essences, 0.4 part of drosophila melanogaster antimicrobial peptide, 0.4 part of essence；Adjust with Nacl Joint product viscosity carries out middle inspection, filters discharging after the assay was approved, obtains containing chlorophyllous Shu Min bath gel.
Embodiment 3
A kind of containing chlorophyllous Shu Min bath gel, its preparation method specifically includes following steps:
1) the chlorophyllous extraction of Thallus Laminariae (Thallus Eckloniae): take Thallus Laminariae (Thallus Eckloniae) in darkroom and be placed in Webster blender pulverizing and obtain Thallus Laminariae (Thallus Eckloniae) powder, toward Thallus Laminariae (Thallus Eckloniae) The mixed solvent adding Thallus Laminariae (Thallus Eckloniae) 6 times of weight of opaque amount in powder carries out ultrasonic extraction, and concussion shakes up, and controlling Extracting temperature is 56 DEG C, control supersonic frequency 350Hz of ultrasound wave, after extracting 3.5 hours continuously by extracting solution frozen centrifugation, centrifugal rotational speed be 4000rpm, after centrifugal 15min supernatant, in supernatant, add magnesium chloride and potassium chloride make the concentration of magnesium ion and potassium from The concentration of son is respectively 0.08 μ g/mL and 0.5 μ g/mL, i.e. can get Thallus Laminariae (Thallus Eckloniae) chlorophyll solution, wherein said mixed solvent, By volume, methanol: n-butyl alcohol: petroleum ether is 1:0.4:0.8；
2) preparation of Chinese medicine essence: accurately weigh 12 portions of Herba Portulacaes, 18 portions of Herba Menthaes, 14 parts of Flos Chrysanthemi Indicis, 5-7 part fragrant citrus seed Being ground into 100 mesh after mixing, be added thereto to 80% ethanol solution of 8 times of weight, controlling Extracting temperature is 90 DEG C of reflux, extract, 60min, obtains Chinese medicine extraction liquid；Being joined by Chinese medicine extraction liquid in distillator, 55 DEG C of decompressions are distilled off ethanol, the most available Chinese medicine essence；
3) prepared by Shu Min bath gel: join in emulsifying pot by 0.6 part of hydroxyethyl cellulose, and stirring is warming up to 80 DEG C, all Matter 3min, after material dissolution homogeneous transparent, sequentially add 32 parts of amino acid surfactants, 3.0 parts of coconut oleoyl amine DEA, 16 parts of NT-D55,1.2 parts of 3237DS pearly-lustre grain stirrings, to whole material dissolutions, when being cooled to 70 DEG C after insulation 10min, add pre- 8.5 parts of the most scattered acrylic copolymers, are cooled to 35 DEG C after stirring, add 2.2 parts successively in mixed liquor Glucam E-20,24 parts of Thallus Laminariae (Thallus Eckloniae) chlorophylls, 40 parts of Chinese medicine essences, 0.7 part of drosophila melanogaster antimicrobial peptide, 0.5 part of essence；Adjust with Nacl Joint product viscosity carries out middle inspection, filters discharging after the assay was approved, obtains containing chlorophyllous Shu Min bath gel.
Comparative example 1
Preparation method is with the embodiment of the present invention 2, and difference is step 1) in do not add magnesium chloride and potassium chloride.
Comparative example 2
Preparation method is with the embodiment of the present invention 2, and difference is to omit step 2), step 3) in do not add Chinese medicine essence. Comparative example 3
Preparation method is with the embodiment of the present invention 2, and difference is to omit step 1), step 3) in do not add Thallus Laminariae (Thallus Eckloniae) chlorophyll.
Comparative example 4
The plain edition chlorophyllin copper complex sodium baby moistening prepared according to patent application 200810104962.6 embodiment 1 is washed one's hair Bath lotion.
Stability and beauty treatment brightening, dispelling spots, dispelling measure of merit in embodiment 4 chlorophyll of the present invention facial film
Comparing embodiment 1-3, obtained by comparative example 1-4, chlorophyllous stability and the beauty treatment of Shu Min bath gel increase White freckle effect, wherein beauty treatment whitening effect employing " ++++" " +++ ", " ++ " "+" represent its effect difference.Allergy rate is for using Person occurs that allergic symptom crowd accounts for the percentage rate of user, and allergic symptom includes redness, pruritus or herpes.The user of bath gel Method is: product carrying out human body skin and smears test, every kind of Shu Min bath gel number of trying out is 20 people, and the time was four weeks. Experimental result is as shown in table 1.
Stability Allergy rate Whitening effect
Embodiment 1 Stable 0 +++
Embodiment 2 Stable 0 ++++
Embodiment 3 Stable 0 +++
Comparative example 1 Unstable 0 +++
Comparative example 2 Unstable 7% ++
Comparative example 3 Stable 10% +
Comparative example 4 - 5% ++
As can be seen from Table 1, from the stability of product, comparative example 1, the shakiness of product of comparative example 2 Fixed, this shows be added thereto to metal ion and can affect the stability of product Determination of Chlorophyll, wherein with Chinese medicine essence Add metal ion and preferable with the stability of the product of Chinese medicine essence.From allergic symptom and freckle effect, this The whitening effect of inventive embodiments product is preferable, and trier not only makes skin present moist, tender, light with this product of rear reflection Sliding, refrigerant sensation, and have good sun-screening function, speckle on pachylosis, desalination face can be alleviated.It is better than prior art contrast Embodiment 4, is also significantly better than Shu Min bath gel and Chinese medicine essence work that Thallus Laminariae (Thallus Eckloniae) chlorophyll is made separately as effective ingredient The Shu Min bath gel made for effective ingredient, this shows that two groups of compositions have notable synergism in terms of brightening, dispelling spots, dispelling.Wherein Product effect with comparative example 2 correspondence is best, for optimum embodiment.Meanwhile, product of the present invention has significant antiallergic Effect, user occurs that the probability of allergic symptom is 0, and this shows, reasonable recipe of the present invention, and additive is safe and reliable, has very Good application prospect.

Claims (4)

1. one kind contains chlorophyllous Shu Min bath gel, it is characterised in that its preparation method specifically includes following steps:
1) the chlorophyllous extraction of Thallus Laminariae (Thallus Eckloniae): darkroom takes Thallus Laminariae (Thallus Eckloniae) be placed in Webster blender pulverizing obtain Thallus Laminariae (Thallus Eckloniae) powder, in Thallus Laminariae (Thallus Eckloniae) powder The mixed solvent adding Thallus Laminariae (Thallus Eckloniae) opaque amount 5-6 times weight carries out ultrasonic extraction, and concussion shakes up, and control Extracting temperature is 43-56 DEG C, control supersonic frequency 250-350Hz of ultrasound wave, by extracting solution frozen centrifugation after extracting 1.5-3.5 hour continuously, centrifugal turn Speed is 2000-4000rpm, obtains supernatant, add magnesium chloride and potassium chloride makes magnesium ion in supernatant after centrifugal 10-15min Concentration and the concentration of potassium ion be respectively 0.08 μ g/mL and 0.5 μ g/mL, i.e. can get Thallus Laminariae (Thallus Eckloniae) chlorophyll solution, wherein said The mixed solvent that mixed solvent is methanol, n-butyl alcohol and petroleum ether, by volume, methanol: n-butyl alcohol: petroleum ether is 1:0.2- 0.4:0.5-0.8；
2) preparation of Chinese medicine essence: accurately weigh 10-12 part Herba Portulacae, 15-18 part Herba Menthae, 12-14 part Flos Chrysanthemi Indici, 5-7 part Being ground into 80-100 mesh after the mixing of fragrant citrus seed, be added thereto to 80% ethanol solution of 8 times of weight, control Extracting temperature is 80- 90 DEG C of reflux, extract, 40-60min, obtain Chinese medicine extraction liquid；Being joined by Chinese medicine extraction liquid in distillator, 40-55 DEG C of decompression is steamed Evaporate removing ethanol, i.e. can get Chinese medicine essence；
3) prepared by Shu Min bath gel: join in emulsifying pot by 0.4-0.6 part hydroxyethyl cellulose, and stirring is warming up to 75-80 DEG C, Homogenizing 3min, after material dissolution homogeneous transparent, sequentially adds 28-32 part amino acid surfactant, 1.0-3.0 part cocos nucifera oil The stirring of amide DEA, 14-16 part NT-D55,0.8-1.2 part 3237DS pearly-lustre grain, to whole material dissolutions, is lowered the temperature after insulation 10min During to 70 DEG C, add the most scattered 7.5-8.5 part acrylic copolymer, after stirring, be cooled to 35 DEG C, successively to Mixed liquor adds 1.8-2.2 part Glucam E-20,16-24 part Thallus Laminariae (Thallus Eckloniae) chlorophyll, 35-40 part Chinese medicine essence, 0.3-0.7 Part drosophila melanogaster antimicrobial peptide, 0.3-0.5 part essence；Carry out middle inspection by Nacl regulation product viscosity, filter discharging after the assay was approved, to obtain final product Containing chlorophyllous Shu Min bath gel.
The most according to claim 1 containing chlorophyllous Shu Min bath gel, it is characterised in that described step 1) in mixing Solvent, by volume, methanol: n-butyl alcohol: petroleum ether is 1:0.3:0.7.
The most according to claim 1 containing chlorophyllous Shu Min bath gel, it is characterised in that described step 2) in YAOJING The raw material of preparing of China's liquid is: 11 portions of Herba Portulacaes, 16 portions of Herba Menthaes, 13 parts of Flos Chrysanthemi Indicis, 6 parts of fragrant citrus seeds.
The most according to claim 1 containing chlorophyllous Shu Min bath gel, it is characterised in that described step 3) include as follows Step: join in emulsifying pot by 0.5 part of hydroxyethyl cellulose, stirring is warming up to 78 DEG C, and homogenizing 3min treats that material dissolution is uniform After transparent, sequentially add 30 parts of amino acid surfactants, 2.0 parts of coconut oleoyl amine DEA, 15 parts of NT-D55,1.0 parts of 3237DS The stirring of pearly-lustre grain, to whole material dissolutions, when being cooled to 70 DEG C after insulation 10min, adds 8.0 parts of the most scattered acrylic acid Analog copolymer, is cooled to 35 DEG C after stirring, add 2.0 parts of Glucam E-20,18 parts of Thallus Laminariae (Thallus Eckloniae) leaves successively green in mixed liquor Element, 38 parts of Chinese medicine essences, 0.4 part of drosophila melanogaster antimicrobial peptide, 0.4 part of essence；Carrying out middle inspection by Nacl regulation product viscosity, inspection is closed Filter discharging after lattice, obtain containing chlorophyllous Shu Min bath gel.
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106619319A (en) * 2017-02-08 2017-05-10 广东科玮生物技术股份有限公司 Antibacterial peptide-containing shower gel with function of relieving itching, and preparation method of shower gel
CN107550840A (en) * 2017-09-30 2018-01-09 曹美兰 A kind of antiallergy face moisture-keeping emulsion
CN110585099A (en) * 2019-10-12 2019-12-20 福建省梦娇兰日用化学品有限公司 Baby moisturizing and nourishing shower gel prepared by plant chlorophyll centrifugal extraction technology

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CN101564373A (en) * 2008-04-25 2009-10-28 北京健健康康生物技术有限公司 Sodium copper chlorophyll baby moistening bath and preparation method thereof
CN105380842A (en) * 2015-11-19 2016-03-09 湖南叶姿国际植物化妆品有限公司 Black tea shower gel

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Publication number Priority date Publication date Assignee Title
CN101564373A (en) * 2008-04-25 2009-10-28 北京健健康康生物技术有限公司 Sodium copper chlorophyll baby moistening bath and preparation method thereof
CN105380842A (en) * 2015-11-19 2016-03-09 湖南叶姿国际植物化妆品有限公司 Black tea shower gel

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106619319A (en) * 2017-02-08 2017-05-10 广东科玮生物技术股份有限公司 Antibacterial peptide-containing shower gel with function of relieving itching, and preparation method of shower gel
CN106619319B (en) * 2017-02-08 2019-09-20 广东科玮生物技术股份有限公司 A kind of itching-relieving shower dew and preparation method thereof containing antibacterial peptide
CN107550840A (en) * 2017-09-30 2018-01-09 曹美兰 A kind of antiallergy face moisture-keeping emulsion
CN110585099A (en) * 2019-10-12 2019-12-20 福建省梦娇兰日用化学品有限公司 Baby moisturizing and nourishing shower gel prepared by plant chlorophyll centrifugal extraction technology

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