CN102935056B

CN102935056B - Slime sun screen and preparation method thereof

Info

Publication number: CN102935056B
Application number: CN201210519524.2A
Authority: CN
Inventors: 王希英; 谢振华; 方振兴
Original assignee: INSTITUTE OF VOLCANO AND SPRING OF HEILONGJIANG ACADEMY OF SCIENCES
Current assignee: INSTITUTE OF VOLCANO AND SPRING OF HEILONGJIANG ACADEMY OF SCIENCES
Priority date: 2012-12-06
Filing date: 2012-12-06
Publication date: 2014-08-27
Anticipated expiration: 2032-12-06
Also published as: CN102935056A

Abstract

A mineral mud sun screen and a preparation method thereof relate to a sun screen and a preparation method thereof. The invention aims to solve the problem that the emulsification system of cosmetics is damaged by directly adding mineral components into the existing make-up base. The invention relates to a slime isolation cream which is prepared by emulsifying and homogenizing a Wudalianchi volcanic slime extract, squalane, butanediol, titanium dioxide, isononyl isononanoate, polydimethylsiloxane, cyclopentadimethylsiloxane, betaine, cetyl PEG/PPG-10/1 polydimethylsiloxane, silica dimethylsilylate, a ginkgo leaf extract, a chamomile extract, bisabolol, allantoin, methylparaben, propylparaben, phenoxyethanol, sodium chloride, essence, CI77288 and treated Wudalianchi mineral water. The method comprises the following steps: firstly, preparing materials; secondly, preparing an oil phase mixture; thirdly, preparing a water phase mixture; fourthly, emulsification; and fifthly, mixing and stirring. The method is used for preparing the slime isolation cream.

Description

A kind of sludge sun screen and preparation method thereof

Technical field

The present invention relates to a kind of sun screen and preparation method thereof.

Background technology

Wudalianchi Volcanic sludge is natural volcanic slurry, by forming through high temperature, high pressure, naturally calm volcano particle matter and subsoil water immersion, it is multiple to the useful element of human body and mineral that it contains calcium, magnesium, potassium, silicon, ferrum, sulfur etc. after testing, potassium in mineral, sodium, magnesium, calcium plasma energy infiltration skin top layer, some even can antioxidation, combine antagonism with oxygen molecule destroys the free radical of protein and infringement skin gene, can play the effect of supplementary, enhancing and balanced skin.Wudalianchi minerals is the famous volcano cold spring of China, belong to the siliceous heavy carbonic magnesium of ferrum calcium type mineral water, it is not only natural, pure, health, do not pollute, and the calcium that contains multiple needed by human, magnesium, potassium, sodium, ferrum, the macroelements such as manganese and strontium, zinc, lithium, nickel, copper, the trace element such as cobalt, the trace element that it contains is suitable with human body requirements proportional quantities, the optimal supplement of body trace element, and wudalianchi minerals can be cured, can drink, can bathe, both can be used as medical mineral water, can be used as again beverage mineral water, can match in excellence or beauty with domestic and international famous mineral water, it is rare precious mineral resource.

Wudalianchi minerals and Wudalianchi Volcanic sludge contain the several mineral materials composition useful to human skin, but these useful compositions are directly added in sun screen, can increase the ionic strength of cosmetics, electrical conductivity and pH value raise, destroy the emulsification system of cosmetics, cause cosmetics series unstable, above reason has limited wudalianchi minerals and the application of Wudalianchi Volcanic sludge in cosmetics.

Summary of the invention

The present invention will solve the direct mineral composition that adds in existing sun screen can destroy the emulsification system problem of cosmetics, and a kind of sludge sun screen and preparation method thereof is provided.

A kind of sludge sun screen of the present invention, it is characterized in that sludge sun screen is by weight percentage by 8% ~ 10% Wudalianchi Volcanic sludge extract, 3% ~ 5% squalane, 5% ~ 10% butanediol, 2.5% ~ 3% titanium dioxide, 5% ~ 10% isononyl isononanoate, 3% ~ 3.5% polydimethylsiloxane, 0.5% ~ 2% ring five polydimethylsiloxane, 1.5% ~ 2.5% betanin, 0.5% ~ 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% ~ 5% dimetylsilyl SiClx stone, 1.5% ~ 2.5% Folium Ginkgo extract, 1.5% ~ 2.5% Anthemis nobilis flower extract, 1% ~ 3% bisabolol, 3% ~ 5% allantoin, 0.05% ~ 0.5% methyl hydroxybenzoate, 0.05% ~ 0.5% propyl hydroxybenzoate, 1.5% ~ 2.5% phenoxyethanol, 0.5% ~ 2% sodium chloride, 0.01% ~ 0.05% essence, 0.01% ~ 0.05%CI772889 and surplus are that wudalianchi minerals after treatment forms through emulsifying homogeneous.

A preparation method for sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 8% ~ 10% Wudalianchi Volcanic sludge extract, 3% ~ 5% squalane, 5% ~ 10% butanediol, 2.5% ~ 3% titanium dioxide, 5% ~ 10% isononyl isononanoate, 3% ~ 3.5% polydimethylsiloxane, 0.5% ~ 2% ring five polydimethylsiloxane, 1.5% ~ 2.5% betanin, 0.5% ~ 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% ~ 5% dimetylsilyl SiClx stone, 1.5% ~ 2.5% Folium Ginkgo extract, 1.5% ~ 2.5% Anthemis nobilis flower extract, 1% ~ 3% bisabolol, 3% ~ 5% allantoin, 0.05% ~ 0.5% methyl hydroxybenzoate, 0.05% ~ 0.5% propyl hydroxybenzoate, 1.5% ~ 2.5% phenoxyethanol, 0.5% ~ 2% sodium chloride, 0.01% ~ 0.05% essence, 0.01% ~ 0.05%CI772889 and surplus are wudalianchi minerals after treatment, two, prepare oil mixture: 3% ~ 5% squalane, 2.5% ~ 3% titanium dioxide, 5% ~ 10% isononyl isononanoate, 3% ~ 3.5% polydimethylsiloxane, 0.5% ~ 2% ring five polydimethylsiloxane, 1.5% ~ 2.5% betanin, 0.5% ~ 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% ~ 5% dimetylsilyl SiClx stone, 0.05% ~ 0.5% methyl hydroxybenzoate and 0.05% ~ 0.5% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 70 DEG C ~ 85 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 5% ~ 10% butanediol, 1% ~ 3% bisabolol, 3% ~ 5% allantoin, 1.5% ~ 2.5% phenoxyethanol, 0.5% ~ 2% sodium chloride and surplus that step 1 is prepared are wudalianchi minerals mix homogeneously after treatment and are heated to 70 DEG C ~ 85 DEG C from room temperature, obtain aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 5min ~ 10min under the condition of 1800 revs/min ~ 2000 revs/min in speed, is cooled to 40 DEG C ~ 60 DEG C, obtains mixed solution, five, mix and blend: 8% ~ 10% Wudalianchi Volcanic sludge extract, 1.5% ~ 2.5% Folium Ginkgo extract, 1.5% ~ 2.5% Anthemis nobilis flower extract, 0.01% ~ 0.05%CI77288 and 0.01% ~ 0.05% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 10min ~ 20min under the condition of 80 revs/min ~ 100 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Advantage of the present invention: the sludge sun screen that, prepared by the present invention has added Wudalianchi Volcanic sludge extract and wudalianchi minerals after treatment, remove the oxidizable composition of ferrum, manganese in mineral water by aeration, reduce ionic strength, electrical conductivity, by orthogonal experimental formula, determine consumption, reach stable emulsification system; Two, the sludge sun screen that prepared by the present invention, as the protective barrier between skin and color make-up, stops the infringement of color make-up to skin; Three, the sludge sun screen that prepared by the present invention, as unique skin conditioner, is adjusted the colour of skin, makes the normal color coloured silk of its color and luster closer to skin; Four, the active component in the sludge sun screen that prepared by the present invention can strengthen skin resistance, and isolation ultraviolet is also repaired the infringement that ultraviolet causes; Five, in the sludge sun screen that prepared by the present invention, contain several mineral materials and organic acid, can strengthen skin immunization power; Six, the chemical composition in the sludge sun screen that prepared by the present invention is ionic condition, active high, penetration is strong, easily see through skin and enter in body and have an effect; Seven, the sludge sun screen that prepared by the present invention has heigh antioxidation effect, can repair because ultraviolet tans by the sun impaired skin protein, makes the colour of skin no longer obscure and partially yellow, and can balance acid-base scale of skin, makes skin reach delicate, healthy naturalness; Eight, the sludge sun screen that prepared by the present invention has been widened Wu Da Lian chi sludge, mineral water new application, has brought larger economic benefit and social benefit; Nine, the preparation method technique of sludge sun screen of the present invention is simple, easy to operate.

Detailed description of the invention

Detailed description of the invention one: a kind of sludge sun screen of present embodiment is by weight percentage by 8% ~ 10% Wudalianchi Volcanic sludge extract, 3% ~ 5% squalane, 5% ~ 10% butanediol, 2.5% ~ 3% titanium dioxide, 5% ~ 10% isononyl isononanoate, 3% ~ 3.5% polydimethylsiloxane, 0.5% ~ 2% ring five polydimethylsiloxane, 1.5% ~ 2.5% betanin, 0.5% ~ 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% ~ 5% dimetylsilyl SiClx stone, 1.5% ~ 2.5% Folium Ginkgo extract, 1.5% ~ 2.5% Anthemis nobilis flower extract, 1% ~ 3% bisabolol, 3% ~ 5% allantoin, 0.05% ~ 0.5% methyl hydroxybenzoate, 0.05% ~ 0.5% propyl hydroxybenzoate, 1.5% ~ 2.5% phenoxyethanol, 0.5% ~ 2% sodium chloride, 0.01% ~ 0.05% essence, 0.01% ~ 0.05%CI772889 and surplus are that wudalianchi minerals after treatment forms through emulsifying homogeneous.

Cetyl PEG/PPG ~ 10/1 polydimethylsiloxane described in present embodiment is a kind of emulsifying agent.

CI772889 described in present embodiment is a kind of colorant, and Chinese is chrome oxide green.

Sludge sun screen described in present embodiment is stable emulsification system.

Sludge sun screen described in present embodiment, as the protective barrier between skin and color make-up, stops the infringement of color make-up to skin.

Sludge sun screen described in present embodiment, as unique skin conditioner, is adjusted the colour of skin, makes the normal color of its color and luster closer to skin.

Active component in sludge sun screen described in present embodiment can strengthen skin resistance, and isolation ultraviolet is also repaired the infringement that ultraviolet causes.

In sludge sun screen described in present embodiment, contain several mineral materials and organic acid, can strengthen skin immunization power.

Chemical composition in sludge sun screen described in present embodiment is ionic condition, active high, penetration is strong, easily see through skin and enter in body and have an effect.

Sludge sun screen described in present embodiment has heigh antioxidation effect, can repair because ultraviolet tans by the sun impaired skin protein, makes the colour of skin no longer obscure and partially yellow, and can balance acid-base scale of skin, makes skin reach delicate, healthy naturalness.

Sludge sun screen described in present embodiment has been widened Wu Da Lian chi sludge, mineral water new application, has brought larger economic benefit and social benefit.

Detailed description of the invention two: present embodiment is different from detailed description of the invention one: described wudalianchi minerals after treatment obtains by following processing: 1. remove ferrum and manganese: adopt air aeration method aerator to carry out aeration 4h to Wudalianchi Yuan Shui (natural mineral water that Wudalianchi gushes out naturally), leave standstill 72h, leave and take supernatant, the bottom precipitation of draining, obtains removing the Wudalianchi Yuan Shui after ferrum and manganese; 2. degerming and filtration: the former water in Wudalianchi after removal ferrum and the manganese that 1. step is obtained, through pipeline disinfection by ultraviolet light, filters by filtering with microporous membrane device, obtains wudalianchi minerals after treatment.Other are identical with detailed description of the invention one.

Wudalianchi minerals described in present embodiment belongs to the siliceous carbonic acid heavy carbonate of ferrum magnesium calcium type natural mineral water, contains more element and mineral, and the wherein about 40mg/L of ferrous content meets the very easily oxidized generation precipitation of air.

Detailed description of the invention three: present embodiment is different from one of detailed description of the invention one or two: described Wudalianchi Volcanic sludge extract completes according to the following steps: 1. remove foreign material: first the foreign material in Wudalianchi Volcanic sludge are removed, then be divided into the clod that diameter is 5cm ~ 8cm, after drying in the shade, obtain removing the clod after foreign material; 2. prepare micropowder: the clod coarse-cracking machine after the removal foreign material that 1. step is obtained is broken into the clod granule that diameter is 5mm ~ 10mm, then shift and put in super fine machine, charging rate be 1400 ~ 1500 revs/min, distinguished and admirable be to pulverize under the condition of 1800 ~ 2000 revs/min, grain size of micropowder is 300 order ~ 600 orders, obtains dry sludge powder; 3. extract: wudalianchi minerals after treatment is added in dry sludge powder, the mass ratio of wudalianchi minerals after treatment and dry sludge powder is 20:1, pH is adjusted to 5.0 ~ 7.0 with hydrochloric acid or sodium hydroxide, stir, place 24h, get supernatant, obtain the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge; Then adopting white oil is solvent, white oil solvent is added in dry sludge powder, the mass ratio of white oil solvent and dry sludge powder is 20:1, soak at room temperature 24h, leave standstill 24h, get supernatant, obtain Wudalianchi Volcanic sludge oil-soluble composition extracting solution, be finally 5:1 mixing and stirring in mass ratio by the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge and Wudalianchi Volcanic sludge oil-soluble composition extracting solution, obtain Wudalianchi Volcanic sludge extract.Other are identical with detailed description of the invention one or two.

Detailed description of the invention four: the preparation method of a kind of sludge sun screen of present embodiment, specifically completes according to the following steps:

Sludge sun screen prepared by present embodiment has added Wudalianchi Volcanic sludge extract and wudalianchi minerals after treatment, remove the oxidizable composition of ferrum, manganese in mineral water by aeration, reduce ionic strength, electrical conductivity, by orthogonal experimental formula, determine consumption, reach stable emulsification system.

Sludge sun screen prepared by present embodiment, as the protective barrier between skin and color make-up, stops the infringement of color make-up to skin.

Sludge sun screen prepared by present embodiment, as unique skin conditioner, is adjusted the colour of skin, makes the normal color of its color and luster closer to skin.

Active component in sludge sun screen prepared by present embodiment can strengthen skin resistance, and isolation ultraviolet is also repaired the infringement that ultraviolet causes.

In sludge sun screen prepared by present embodiment, contain several mineral materials and organic acid, can strengthen skin immunization power.

Chemical composition in sludge sun screen prepared by present embodiment is ionic condition, active high, penetration is strong, easily see through skin and enter in body and have an effect.

Sludge sun screen prepared by present embodiment has heigh antioxidation effect, can repair because ultraviolet tans by the sun impaired skin protein, makes the colour of skin no longer obscure and partially yellow, and can balance acid-base scale of skin, makes skin reach delicate, healthy naturalness.

Sludge sun screen prepared by present embodiment has been widened Wu Da Lian chi sludge, mineral water new application, has brought larger economic benefit and social benefit.

The preparation method technique of present embodiment sludge sun screen is simple, easy to operate.

Detailed description of the invention five: present embodiment is different from detailed description of the invention four: the wudalianchi minerals after treatment described in step 1 obtains by following processing: 1. remove ferrum and manganese: adopt air aeration method aerator to carry out aeration 4h to Wudalianchi Yuan Shui (natural mineral water that Wudalianchi gushes out naturally), leave standstill 72h, leave and take supernatant, the bottom precipitation of draining, obtains removing the Wudalianchi Yuan Shui after ferrum and manganese; 2. degerming and filtration: the former water in Wudalianchi after removal ferrum and the manganese that 1. step is obtained, through pipeline disinfection by ultraviolet light, filters by filtering with microporous membrane device, obtains wudalianchi minerals after treatment.Other are identical with detailed description of the invention four.

Detailed description of the invention six: present embodiment is different from one of detailed description of the invention four or five: the Wudalianchi Volcanic sludge extract described in step 1 completes according to the following steps: 1. remove foreign material: first the foreign material in Wudalianchi Volcanic sludge are removed, then be divided into the clod that diameter is 5cm ~ 8cm, after drying in the shade, obtain removing the clod after foreign material; 2. prepare micropowder: the clod coarse-cracking machine after the removal foreign material that 1. step is obtained is broken into the clod granule that diameter is 5mm ~ 10mm, then shift and put in super fine machine, charging rate be 1400 revs/min ~ 1500 revs/min, distinguished and admirable be to pulverize under the condition of 1800 revs/min ~ 2000 revs/min, grain size of micropowder is 300 order ~ 600 orders, obtains dry sludge powder; 3. extract: wudalianchi minerals after treatment is added in dry sludge powder, the mass ratio of wudalianchi minerals after treatment and dry sludge powder is 20:1, pH is adjusted to 5.0 ~ 7.0 with hydrochloric acid or sodium hydroxide, stir, place 24h, get supernatant, obtain the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge; Then adopting white oil is solvent, white oil solvent is added in dry sludge powder, the mass ratio of white oil solvent and dry sludge powder is 20:1, soak at room temperature 24h, leave standstill 24h, get supernatant, obtain Wudalianchi Volcanic sludge oil-soluble composition extracting solution, be finally 5:1 mixing and stirring in mass ratio by the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge and Wudalianchi Volcanic sludge oil-soluble composition extracting solution, obtain Wudalianchi Volcanic sludge extract.Other are identical with detailed description of the invention four or five.

Detailed description of the invention seven: present embodiment is different from one of detailed description of the invention four to six: 3% ~ 5% squalane of in step 2, step 1 being prepared, 2.5% ~ 3% titanium dioxide, 5% ~ 10% isononyl isononanoate, 3% ~ 3.5% polydimethylsiloxane, 0.5% ~ 2% ring five polydimethylsiloxane, 1.5% ~ 2.5% betanin, 0.5% ~ 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% ~ 5% dimetylsilyl SiClx stone, 0.05% ~ 0.5% methyl hydroxybenzoate and 0.05% ~ 0.5% propyl hydroxybenzoate mix and blend are also heated to 75 DEG C ~ 80 DEG C from room temperature, obtain oil mixture.Other are identical with one of detailed description of the invention four to six.

Detailed description of the invention eight: present embodiment is different from one of detailed description of the invention four to seven: 5% ~ 10% butanediol, 1% ~ 3% bisabolol, 3% ~ 5% allantoin, 1.5% ~ 2.5% phenoxyethanol, 0.5% ~ 2% sodium chloride and the surplus in step 3, step 1 prepared are wudalianchi minerals mix homogeneously after treatment and are heated to 75 DEG C ~ 80 DEG C from room temperature, obtain aqueous mixture.Other are identical with one of detailed description of the invention four to seven.

Detailed description of the invention nine: present embodiment is different from one of detailed description of the invention four to eight: the oil mixture in step 4, step 2 being obtained adds in the aqueous mixture that step 3 obtains, be emulsifying homogeneous 6min ~ 8min under the condition of 1800 revs/min ~ 2000 revs/min in speed, be cooled to 45 DEG C ~ 50 DEG C, obtain mixed solution.Other are identical with one of detailed description of the invention four to eight.

Adopt following verification experimental verification effect of the present invention:

Test one: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 8% Wudalianchi Volcanic sludge extract, 3% squalane, 5% butanediol, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 1% bisabolol, 3% allantoin, 0.05% methyl hydroxybenzoate, 0.05% propyl hydroxybenzoate, 1.5% phenoxyethanol, 0.5% sodium chloride, 0.01% essence, 0.01%CI772889 and 59.88% wudalianchi minerals after treatment, two, prepare oil mixture: 3% squalane, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 0.05% methyl hydroxybenzoate and the 0.05% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 5% butanediol, 1% bisabolol, 3% allantoin, 1.5% phenoxyethanol, 0.5% sodium chloride and the 59.88% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 5min under the condition of 1800 revs/min in speed, is cooled to 40 DEG C, obtains mixed solution, five, mix and blend: 8% Wudalianchi Volcanic sludge extract, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 0.01%CI77288 and 0.01% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 10min under the condition of 80 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

The described wudalianchi minerals after treatment of this test obtains by following processing: 1. remove ferrum and manganese: adopt air aeration method aerator to carry out aeration 4h to Wudalianchi Yuan Shui (natural mineral water that Wudalianchi gushes out naturally), leave standstill 72h, leave and take supernatant, the bottom precipitation of draining, obtains removing the Wudalianchi Yuan Shui after ferrum and manganese; 2. degerming and filtration: the former water in Wudalianchi after removal ferrum and the manganese that 1. step is obtained, through pipeline disinfection by ultraviolet light, filters by filtering with microporous membrane device, obtains wudalianchi minerals after treatment.

The described Wudalianchi Volcanic sludge extract of this test completes according to the following steps: 1. remove foreign material: first the foreign material in Wudalianchi Volcanic sludge are removed, then be divided into the clod that diameter is 5cm ~ 8cm, after drying in the shade, obtain removing the clod after foreign material; 2. prepare micropowder: the clod coarse-cracking machine after the removal foreign material that 1. step is obtained is broken into the clod granule that diameter is 5mm ~ 10mm, then shift and put in super fine machine, charging rate be 1400 revs/min, distinguished and admirable be to pulverize under the condition of 1800 revs/min, grain size of micropowder is 300 order ~ 600 orders, obtains dry sludge powder; 3. extract: wudalianchi minerals after treatment is added in dry sludge powder, the mass ratio of wudalianchi minerals after treatment and dry sludge powder is 20:1, pH is adjusted to 6.0 with hydrochloric acid or sodium hydroxide, stir, place 24h, get supernatant, obtain the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge; Then adopting white oil is solvent, white oil solvent is added in dry sludge powder, the mass ratio of white oil solvent and dry sludge powder is 20:1, soak at room temperature 24h, leave standstill 24h, get supernatant, obtain Wudalianchi Volcanic sludge oil-soluble composition extracting solution, be finally 5:1 mixing and stirring in mass ratio by the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge and Wudalianchi Volcanic sludge oil-soluble composition extracting solution, obtain Wudalianchi Volcanic sludge extract.

Test two: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 10% Wudalianchi Volcanic sludge extract, 5% squalane, 10% butanediol, 3% titanium dioxide, 10% isononyl isononanoate, 3.5% polydimethylsiloxane, 2% ring five polydimethylsiloxane, 2.5% betanin, 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 5% dimetylsilyl SiClx stone, 2.5% Folium Ginkgo extract, 2.5% Anthemis nobilis flower extract, 3% bisabolol, 5% allantoin, 0.5% methyl hydroxybenzoate, 0.5% propyl hydroxybenzoate, 2.5% phenoxyethanol, 2% sodium chloride, 0.05% essence, 0.05%CI772889 and 27.4% wudalianchi minerals after treatment, two, prepare oil mixture: 5% squalane, % titanium dioxide, 10% isononyl isononanoate, 3.5% polydimethylsiloxane, 2% ring five polydimethylsiloxane, 2.5% betanin, 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 5% dimetylsilyl SiClx stone, 0.5% methyl hydroxybenzoate and the 0.5% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 85 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 10% butanediol, 3% bisabolol, 5% allantoin, 2.5% phenoxyethanol, 2% sodium chloride and the 27.4% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 85 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 10min under the condition of 2000 revs/min in speed, is cooled to 60 DEG C, obtains mixed solution, five, mix and blend: 10% Wudalianchi Volcanic sludge extract, 2.5% Folium Ginkgo extract, 2.5% Anthemis nobilis flower extract, 0.05%CI77288 and 0.05% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 20min under the condition of 100 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Test three: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 5% Wudalianchi Volcanic sludge extract, 3% squalane, 5% butanediol, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 1% bisabolol, 3% allantoin, 0.05% methyl hydroxybenzoate, 0.05% propyl hydroxybenzoate, 1.5% phenoxyethanol, 0.5% sodium chloride, 0.01% essence, 0.01%CI772889 and 62.88% wudalianchi minerals after treatment, two, prepare oil mixture: 3% squalane, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 0.05% methyl hydroxybenzoate and the 0.05% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 5% butanediol, 1% bisabolol, 3% allantoin, 1.5% phenoxyethanol, 0.5% sodium chloride and the 62.88% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 5min under the condition of 1800 revs/min in speed, is cooled to 40 DEG C, obtains mixed solution, five, mix and blend: 5% Wudalianchi Volcanic sludge extract, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 0.01%CI77288 and 0.01% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 10min under the condition of 80 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Test four: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 15% Wudalianchi Volcanic sludge extract, 5% squalane, 10% butanediol, 3% titanium dioxide, 10% isononyl isononanoate, 3.5% polydimethylsiloxane, 2% ring five polydimethylsiloxane, 2.5% betanin, 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 5% dimetylsilyl SiClx stone, 2.5% Folium Ginkgo extract, 2.5% Anthemis nobilis flower extract, 3% bisabolol, 5% allantoin, 0.5% methyl hydroxybenzoate, 0.5% propyl hydroxybenzoate, 2.5% phenoxyethanol, 2% sodium chloride, 0.05% essence, 0.05%CI772889 and 22.4% wudalianchi minerals after treatment, two, prepare oil mixture: 5% squalane, % titanium dioxide, 10% isononyl isononanoate, 3.5% polydimethylsiloxane, 2% ring five polydimethylsiloxane, 2.5% betanin, 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 5% dimetylsilyl SiClx stone, 0.5% methyl hydroxybenzoate and the 0.5% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 85 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 10% butanediol, 3% bisabolol, 5% allantoin, 2.5% phenoxyethanol, 2% sodium chloride and the 22.4% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 85 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 10min under the condition of 2000 revs/min in speed, is cooled to 60 DEG C, obtains mixed solution, five, mix and blend: 15% Wudalianchi Volcanic sludge extract, 2.5% Folium Ginkgo extract, 2.5% Anthemis nobilis flower extract, 0.05%CI77288 and 0.05% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 20min under the condition of 100 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Test five: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 25% Wudalianchi Volcanic sludge extract, 5% squalane, 10% butanediol, 3% titanium dioxide, 10% isononyl isononanoate, 3.5% polydimethylsiloxane, 2% ring five polydimethylsiloxane, 2.5% betanin, 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 5% dimetylsilyl SiClx stone, 2.5% Folium Ginkgo extract, 2.5% Anthemis nobilis flower extract, 3% bisabolol, 5% allantoin, 0.5% methyl hydroxybenzoate, 0.5% propyl hydroxybenzoate, 2.5% phenoxyethanol, 2% sodium chloride, 0.05% essence, 0.05%CI772889 and 12.4% wudalianchi minerals after treatment, two, prepare oil mixture: 5% squalane, % titanium dioxide, 10% isononyl isononanoate, 3.5% polydimethylsiloxane, 2% ring five polydimethylsiloxane, 2.5% betanin, 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 5% dimetylsilyl SiClx stone, 0.5% methyl hydroxybenzoate and the 0.5% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 85 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 10% butanediol, 3% bisabolol, 5% allantoin, 2.5% phenoxyethanol, 2% sodium chloride and the 12.4% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 85 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 10min under the condition of 2000 revs/min in speed, is cooled to 60 DEG C, obtains mixed solution, five, mix and blend: 25% Wudalianchi Volcanic sludge extract, 2.5% Folium Ginkgo extract, 2.5% Anthemis nobilis flower extract, 0.05%CI77288 and 0.05% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 20min under the condition of 100 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Test six: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 30% Wudalianchi Volcanic sludge extract, 3% squalane, 5% butanediol, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 1% bisabolol, 3% allantoin, 0.05% methyl hydroxybenzoate, 0.05% propyl hydroxybenzoate, 1.5% phenoxyethanol, 0.5% sodium chloride, 0.01% essence, 0.01%CI772889 and 37.88% wudalianchi minerals after treatment, two, prepare oil mixture: 3% squalane, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 0.05% methyl hydroxybenzoate and the 0.05% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 5% butanediol, 1% bisabolol, 3% allantoin, 1.5% phenoxyethanol, 0.5% sodium chloride and the 37.88% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 5min under the condition of 1800 revs/min in speed, is cooled to 40 DEG C, obtains mixed solution, five, mix and blend: 30% Wudalianchi Volcanic sludge extract, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 0.01%CI77288 and 0.01% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 10min under the condition of 80 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Test seven: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 35% Wudalianchi Volcanic sludge extract, 3% squalane, 5% butanediol, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 1% bisabolol, 3% allantoin, 0.05% methyl hydroxybenzoate, 0.05% propyl hydroxybenzoate, 1.5% phenoxyethanol, 0.5% sodium chloride, 0.01% essence, 0.01%CI772889 and 32.88% wudalianchi minerals after treatment, two, prepare oil mixture: 3% squalane, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 0.05% methyl hydroxybenzoate and the 0.05% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 5% butanediol, 1% bisabolol, 3% allantoin, 1.5% phenoxyethanol, 0.5% sodium chloride and the 32.88% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 5min under the condition of 1800 revs/min in speed, is cooled to 40 DEG C, obtains mixed solution, five, mix and blend: 35% Wudalianchi Volcanic sludge extract, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 0.01%CI77288 and 0.01% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 10min under the condition of 80 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Test eight: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 50% Wudalianchi Volcanic sludge extract, 3% squalane, 5% butanediol, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 1% bisabolol, 3% allantoin, 0.05% methyl hydroxybenzoate, 0.05% propyl hydroxybenzoate, 1.5% phenoxyethanol, 0.5% sodium chloride, 0.01% essence, 0.01%CI772889 and 17.88% wudalianchi minerals after treatment, two, prepare oil mixture: 3% squalane, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 0.05% methyl hydroxybenzoate and the 0.05% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 5% butanediol, 1% bisabolol, 3% allantoin, 1.5% phenoxyethanol, 0.5% sodium chloride and the 17.88% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 5min under the condition of 1800 revs/min in speed, is cooled to 40 DEG C, obtains mixed solution, five, mix and blend: 50% Wudalianchi Volcanic sludge extract, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 0.01%CI77288 and 0.01% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 10min under the condition of 80 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Test nine: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 60% Wudalianchi Volcanic sludge extract, 3% squalane, 5% butanediol, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 1% bisabolol, 3% allantoin, 0.05% methyl hydroxybenzoate, 0.05% propyl hydroxybenzoate, 1.5% phenoxyethanol, 0.5% sodium chloride, 0.01% essence, 0.01%CI772889 and 7.88% wudalianchi minerals after treatment, two, prepare oil mixture: 3% squalane, 2.5% titanium dioxide, 5% isononyl isononanoate, 3% polydimethylsiloxane, 0.5% ring five polydimethylsiloxane, 1.5% betanin, 0.5% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2% dimetylsilyl SiClx stone, 0.05% methyl hydroxybenzoate and the 0.05% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 5% butanediol, 1% bisabolol, 3% allantoin, 1.5% phenoxyethanol, 0.5% sodium chloride and the 7.88% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 70 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 5min under the condition of 1800 revs/min in speed, is cooled to 40 DEG C, obtains mixed solution, five, mix and blend: 60% Wudalianchi Volcanic sludge extract, 1.5% Folium Ginkgo extract, 1.5% Anthemis nobilis flower extract, 0.01%CI77288 and 0.01% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 10min under the condition of 80 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

Test ten: a kind of preparation method of sludge sun screen, specifically completes according to the following steps:

One, prepare material: prepare by weight percentage 9% Wudalianchi Volcanic sludge extract, 4% squalane, 8% butanediol, 3% titanium dioxide, 8% isononyl isononanoate, 3% polydimethylsiloxane, 2% ring five polydimethylsiloxane, 2% betanin, 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 3% dimetylsilyl SiClx stone, 2% Folium Ginkgo extract, 2% Anthemis nobilis flower extract, 2% bisabolol, 4% allantoin, 0.5% methyl hydroxybenzoate, 0.5% propyl hydroxybenzoate, 2% phenoxyethanol, 1% sodium chloride, 0.05% essence, 0.05%CI772889 and 40.9% wudalianchi minerals after treatment, two, prepare oil mixture: 4% squalane, 3% titanium dioxide, 8% isononyl isononanoate, 3% polydimethylsiloxane, 2% ring five polydimethylsiloxane, 2% betanin, 3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 3% dimetylsilyl SiClx stone, 0.5% methyl hydroxybenzoate and the 0.5% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 75 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 8% butanediol, 2% bisabolol, 4% allantoin, 2% phenoxyethanol, 1% sodium chloride and the 40.9% wudalianchi minerals mix homogeneously after treatment that step 1 is prepared is also heated to 75 DEG C from room temperature, obtains aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 10min under the condition of 2000 revs/min in speed, is cooled to 50 DEG C, obtains mixed solution, five, mix and blend: 9% Wudalianchi Volcanic sludge extract, 2% Folium Ginkgo extract, 2% Anthemis nobilis flower extract, 0.05%CI77288 and 0.05% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 20min under the condition of 100 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen.

The stability of sludge sun screens prepared by employing heatproof, low temperature resistant test demonstration test one to test ten:

1, heatproof test: first test one to the sludge sun screens of test ten preparations are placed to 24h in temperature is the calorstat of 40 ± 1 DEG C, then test one to the sludge sun screen of test ten preparations is taken out from calorstat, recover room temperature condition, place 24h, observe sludge sun screen and have or not oil-water separation phenomenon.

2, low temperature resistant test: first test one to the sludge sun screens of test ten preparations are placed to 24h in temperature is the refrigerator of-4 DEG C ~-11 DEG C, then test one to the sludge sun screen of test ten preparations is taken out from refrigerator, recover room temperature condition, place 24h, observe sludge sun screen without oil-water separation phenomenon.

Table 1

As can be seen from Table 1, the sludge sun screen of test one, test two and test ten preparations is stable, and test three to the sludge sun screen of test nine preparations is unsettled.

For understanding the result of use of the sludge sun screen prepared of the present invention, form with questionnaire survey has been carried out investigation on probation widely to testing the sludge sun screen of ten preparations, trier 100 people, wherein male 22 people, women 78 people, the oldest 51 years old, minimum 18 years old, about 32 years old mean age, regain altogether 95 parts of effective questionnaires.95 triers use this product after 4 weeks to isolation color make-up, isolate the result of use of the indices of dirty air, isolation ultraviolet, whitening nutrition and safety, stimulation allergy, the result of self evaluation is as follows:

Table 2

Name

Sex

Age

Isolation color make-up

Isolate dirty air

Isolation ultraviolet

Whitening nutrition

Stimulate irritated

Li Hang

Female

48

Moderate isolation

Obviously isolation

Obviously whitening is moistened

Nothing

Jia Feng

Man

35

—

Moderate isolation

Moderate whitening is moistened

Nothing

Chi Ming

Man

29

—

Moderate isolation

Moderate whitening is moistened

Nothing

Wang Jinrong

Female

45

Moderate isolation

Obviously whitening is moistened

Nothing

Wang Xuli

Female

25

Obviously isolation

Moderate whitening is moistened

Nothing

Huang Wei

Female

46

Moderate isolation

Moderate whitening is moistened

Nothing

Lin Shuan

Female

34

Moderate isolation

Moderate whitening is moistened

Nothing

Bo Yexia

Female

24

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Li Fengyun

Female

29

Moderate isolation

Obviously isolation

Obviously whitening is moistened

Nothing

White jade

Female

21

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Guo Min

Female

26

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Yang Jing

Female

28

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Liu Jiru

Female

35

Moderate isolation

Moderate whitening is moistened

Nothing

Liu Guohong

Man

33

—

Moderate isolation

Nothing

Yu Shuling

Female

43

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

David Gosset

Female

39

Moderate isolation

Obviously isolation

Moderate isolation

Obviously whitening is moistened

Nothing

Blog article people

Man

35

—

Moderate isolation

Moderate whitening is moistened

Nothing

Xu Lihua

Female

39

Moderate isolation

Moderate whitening is moistened

Nothing

Thousand is red

Female

26

Obviously isolation

Moderate isolation

Nothing

Liu Yan

Female

24

Obviously isolation

Moderate whitening is moistened

Nothing

Wang Haiyun

Female

18

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

SHIWEI

Man

37

—

Moderate isolation

Moderate whitening is moistened

Nothing

Li Wei

Female

32

Moderate isolation

Obviously isolation

Obviously whitening is moistened

Nothing

Cui Yongfan

Man

28

—

Moderate isolation

Nothing

Moderate whitening is moistened

Nothing

Zhuan Lihua

Female

31

Moderate isolation

Moderate whitening is moistened

Nothing

Zhou Lihai

Man

24

—

Moderate isolation

Moderate whitening is moistened

Nothing

Li Yingji

Female

31

Moderate isolation

Obviously isolation

Obviously whitening is moistened

Nothing

Yu Bo

Female

36

Moderate isolation

Moderate whitening is moistened

Nothing

Hao Hong

Female

26

Obviously isolation

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Han Xuesong

Female

40

Moderate isolation

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Tang Jing

Female

23

Moderate isolation

Moderate whitening is moistened

Nothing

Su Jie

Female

50

Moderate isolation

Obviously whitening is moistened

Nothing

Zhang Jinxia

Female

46

Moderate isolation

Moderate whitening is moistened

Nothing

Liu Zhongmin

Female

31

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Zhou Yajin

Female

33

Moderate isolation

Nothing

Wang Zhenlan

Female

35

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Han Yongzhu

Female

28

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Sun Guojiang

Man

26

—

Obviously isolation

Nothing

Moderate whitening is moistened

Nothing

Liu Yan

Female

35

Moderate isolation

Obviously whitening is moistened

Nothing

Wang Meng

Female

25

Obviously isolation

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Shi Wei

Female

41

Nothing

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Ren Lijun

Female

19

Moderate isolation

Obviously isolation

Obviously whitening is moistened

Nothing

The LUXIANG tinkling of pieces of jade

Female

31

Moderate isolation

Moderate whitening is moistened

Nothing

Cui Xiulan

Female

21

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Li Hua

Female

26

Obviously isolation

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Meng Qingxin

Female

32

?

Moderate isolation

Obviously whitening is moistened

Nothing

Liu Lijuan

Female

20

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Good fortune army

Man

25

—

Obviously isolation

Nothing

Moderate whitening is moistened

Nothing

Guo Hongyan

Female

32

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Gao Hui

Female

37

Moderate isolation

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Li Xin

Female

27

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

The little capital of the ancient state of Chu of Shao

Female

46

Nothing

Moderate isolation

Moderate whitening is moistened

Nothing

Yang Lixin

Female

50

Moderate isolation

Obviously whitening is moistened

Nothing

Liu Li

Female

31

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Cui Hai and

Female

32

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Li Zefang

Female

49

Moderate isolation

Nothing

Moderate whitening is moistened

Nothing

Zheng Kunlan

Female

51

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

He Fengyun

Female

51

Moderate isolation

Obviously isolation

Obviously whitening is moistened

Nothing

Wang Xiuling

Female

32

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Li Tongguang

Man

26

—

Obviously isolation

Moderate isolation

Nothing

Chen Baoling

Female

20

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Ni Chunjuan

Female

21

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Chen Shengli

Man

36

—

Moderate isolation

Obviously whitening is moistened

Nothing

Han Chunhong

Female

21

Moderate isolation

Obviously isolation

Nothing

Moderate whitening is moistened

Nothing

MAMEI

Female

39

Moderate isolation

Moderate whitening is moistened

Nothing

Jia Xuehong

Female

26

Obviously isolation

Moderate isolation

Obviously isolation

Moderate whitening is moistened

Nothing

Song Xuemei

Female

22

Moderate isolation

Obviously whitening is moistened

Nothing

Li Xiuli

Female

50

Moderate isolation

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Wang Lihong

Female

38

Moderate isolation

Moderate whitening is moistened

Nothing

Gao Ting

Female

26

Moderate isolation

Moderate whitening is moistened

Nothing

Marvin's

Man

30

—

Moderate isolation

Nothing

Moderate whitening is moistened

Nothing

Liu Huijun

Female

36

?

Moderate isolation

Moderate whitening is moistened

Nothing

Du Chunsheng

Man

45

—

Moderate isolation

Moderate whitening is moistened

Nothing

Liu Zhen

Female

39

Nothing

Obviously isolation

Moderate isolation

Obviously whitening is moistened

Nothing

Zhu Hua

Female

35

Moderate isolation

Moderate whitening is moistened

Nothing

Duan Yucheng

Female

22

Obviously isolation

Moderate isolation

Nothing

Moderate whitening is moistened

Nothing

Li Liyan

Female

42

Moderate isolation

Moderate whitening is moistened

Nothing

Li Yu

Female

35

Moderate isolation

Obviously isolation

Moderate isolation

Obviously whitening is moistened

Nothing

Li Li

Female

25

Moderate isolation

Moderate whitening is moistened

Nothing

Fan Xiuying

Female

42

Moderate isolation

Moderate whitening is moistened

Nothing

Dan Fengchun

Female

30

Obviously isolation

Moderate isolation

Nothing

Wang Chunying

Female

41

Moderate isolation

Obviously isolation

Moderate isolation

Obviously whitening is moistened

Nothing

Zhang Jiaming

Man

23

—

Moderate isolation

Nothing

Zhao Yurong

Female

20

?

Moderate isolation

Obviously whitening is moistened

Nothing

Du Jun

Man

18

—

Moderate isolation

Moderate whitening is moistened

Nothing

Wei Hongqiang

Man

34

—

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Zhou Yujun

Man

45

—

Moderate isolation

Moderate whitening is moistened

Nothing

Zhang Yong

Man

36

—

Moderate isolation

Moderate whitening is moistened

Nothing

Qu Dianyu

Female

22

Moderate isolation

Moderate whitening is moistened

Nothing

Zhang Yunlong

Man

28

—

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

Wu Jun

Man

36

—

Moderate isolation

Moderate whitening is moistened

Nothing

Yu Yongli

Man

45

—

Moderate isolation

Moderate whitening is moistened

Nothing

Wu Hua

Female

49

Nothing

Moderate isolation

Nothing

Brilliant ripple

Female

20

Moderate isolation

Moderate whitening is moistened

Nothing

Zheng Xifeng

Female

26

Moderate isolation

Obviously isolation

Moderate isolation

Moderate whitening is moistened

Nothing

As shown in Table 2,

1, isolation color make-up: 67.56% women trier has moderate isolation effect, and 27.02% women trier has obvious isolation effect;

2, isolate dirty air: 74.73% trier has moderate isolation effect, 25.26% trier has obvious isolation effect;

3, isolation ultraviolet: 71.57% trier has moderate isolation effect, and 21.05% trier has obvious isolation effect;

4, whitening nutrition: 73.68% trier has moderate whitening moisturizing effect, 18.94% trier has obvious whitening moisturizing effect;

5, stimulate allergy: non-stimulated irritated example.

Can find out from the result of trier's self assessment, sludge sun screen to isolation color make-up, isolate the problem such as dirty air, isolation ultraviolet, whitening nutrition and have isolation effect and whitening moisturizing effect in various degree, do not find that product produces stimulation allergic phenomena to trier.Show according to survey result: sludge extracting solution, mineral water effective ingredient and various active nutrient substance that sludge sun screen effectively utilizes; reach entirety conditioning and the maintenance of skin; better increase the ability of skin opposing color make-up, dirty air; the effective ingredient of sludge sun screen is more easily absorbed by the skin simultaneously, makes skin obtain protection and the moist dual cosmetic result of whitening.

Claims

1. a sludge sun screen, it is characterized in that sludge sun screen is by weight percentage by 8%～10% Wudalianchi Volcanic sludge extract, 3%～5% squalane, 5%～10% butanediol, 2.5%～3% titanium dioxide, 5%～10% isononyl isononanoate, 3%～3.5% polydimethylsiloxane, 0.5%～2% ring five polydimethylsiloxane, 1.5%～2.5% betanin, 0.5%～3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2%～5% dimetylsilyl SiClx stone, 1.5%～2.5% Folium Ginkgo extract, 1.5%～2.5% Anthemis nobilis flower extract, 1%～3% bisabolol, 3%～5% allantoin, 0.05%～0.5% methyl hydroxybenzoate, 0.05%～0.5% propyl hydroxybenzoate, 1.5%～2.5% phenoxyethanol, 0.5%～2% sodium chloride, 0.01%～0.05% essence, 0.01%～0.05%CI77288 and surplus are that wudalianchi minerals after treatment forms through emulsifying homogeneous,

Described wudalianchi minerals after treatment obtains by following processing: 1. remove ferrum and manganese: adopt air aeration method aerator to carry out aeration 4h to Wudalianchi Yuan Shui, leave standstill 72h, leave and take supernatant, the bottom precipitation of draining, obtains removing the Wudalianchi Yuan Shui after ferrum and manganese; 2. degerming and filtration: the former water in Wudalianchi after removal ferrum and the manganese that 1. step is obtained, through pipeline disinfection by ultraviolet light, filters by filtering with microporous membrane device, obtains wudalianchi minerals after treatment;

Described Wudalianchi Volcanic sludge extract completes according to the following steps: 1. remove foreign material: first the foreign material in Wudalianchi Volcanic sludge are removed, then be divided into the clod that diameter is 5cm～8cm, after drying in the shade, obtain removing the clod after foreign material; 2. prepare micropowder: the clod coarse-cracking machine after the removal foreign material that 1. step is obtained is broken into the clod granule that diameter is 5mm～10mm, then be transferred in super fine machine, charging rate be 1400 revs/min～1500 revs/min, distinguished and admirable be to pulverize under the condition of 1800 revs/min～2000 revs/min, grain size of micropowder is 300 order～600 orders, obtains dry sludge powder; 3. extract: wudalianchi minerals after treatment is added in dry sludge powder, the mass ratio of wudalianchi minerals after treatment and dry sludge powder is 20:1, pH is adjusted to 5.0～7.0 with hydrochloric acid or sodium hydroxide, stir, place 24h, get supernatant, obtain the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge; Then adopting white oil is solvent, white oil solvent is added in dry sludge powder, the mass ratio of white oil solvent and dry sludge powder is 20:1, soak at room temperature 24h, leave standstill 24h, get supernatant, obtain Wudalianchi Volcanic sludge oil-soluble composition extracting solution, be finally 5:1 mixing and stirring in mass ratio by the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge and Wudalianchi Volcanic sludge oil-soluble composition extracting solution, obtain Wudalianchi Volcanic sludge extract.

2. the preparation method of a kind of sludge sun screen as claimed in claim 1, is characterized in that the preparation method of sludge sun screen completes according to the following steps:

One, prepare material: prepare by weight percentage 8%～10% Wudalianchi Volcanic sludge extract, 3%～5% squalane, 5%～10% butanediol, 2.5%～3% titanium dioxide, 5%～10% isononyl isononanoate, 3%～3.5% polydimethylsiloxane, 0.5%～2% ring five polydimethylsiloxane, 1.5%～2.5% betanin, 0.5%～3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2%～5% dimetylsilyl SiClx stone, 1.5%～2.5% Folium Ginkgo extract, 1.5%～2.5% Anthemis nobilis flower extract, 1%～3% bisabolol, 3%～5% allantoin, 0.05%～0.5% methyl hydroxybenzoate, 0.05%～0.5% propyl hydroxybenzoate, 1.5%～2.5% phenoxyethanol, 0.5%～2% sodium chloride, 0.01%～0.05% essence, 0.01%～0.05%CI77288 and surplus are wudalianchi minerals after treatment, two, prepare oil mixture: 3%～5% squalane, 2.5%～3% titanium dioxide, 5%～10% isononyl isononanoate, 3%～3.5% polydimethylsiloxane, 0.5%～2% ring five polydimethylsiloxane, 1.5%～2.5% betanin, 0.5%～3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2%～5% dimetylsilyl SiClx stone, 0.05%～0.5% methyl hydroxybenzoate and 0.05%～0.5% propyl hydroxybenzoate mix and blend that step 1 is prepared is also heated to 70 DEG C～85 DEG C from room temperature, obtains oil mixture, three, prepare aqueous mixture: 5%～10% butanediol, 1%～3% bisabolol, 3%～5% allantoin, 1.5%～2.5% phenoxyethanol, 0.5%～2% sodium chloride and surplus that step 1 is prepared are wudalianchi minerals mix homogeneously after treatment and are heated to 70 DEG C～85 DEG C from room temperature, obtain aqueous mixture, four, emulsifying: the oil mixture that step 2 is obtained adds in the aqueous mixture that step 3 obtains, is emulsifying homogeneous 5min～10min under the condition of 1800 revs/min～2000 revs/min in speed, is cooled to 40 DEG C～60 DEG C, obtains mixed solution, five, mix and blend: 8%～10% Wudalianchi Volcanic sludge extract, 1.5%～2.5% Folium Ginkgo extract, 1.5%～2.5% Anthemis nobilis flower extract, 0.01%～0.05%CI77288 and 0.01%～0.05% essence that step 1 is prepared adds in the mixed solution that step 4 obtains, low whipping speed is to stir 10min～20min under the condition of 80 revs/min～100 revs/min, be cooled to discharging after room temperature, obtain sludge sun screen,

Wudalianchi minerals after treatment described in step 1 obtains by following processing: 1. remove ferrum and manganese: adopt air aeration method aerator to carry out aeration 4h to Wudalianchi Yuan Shui, leave standstill 72h, leave and take supernatant, the bottom precipitation of draining, obtains removing the Wudalianchi Yuan Shui after ferrum and manganese; 2. degerming and filtration: the former water in Wudalianchi after removal ferrum and the manganese that 1. step is obtained, through pipeline disinfection by ultraviolet light, filters by filtering with microporous membrane device, obtains wudalianchi minerals after treatment;

Wudalianchi Volcanic sludge extract described in step 1 completes according to the following steps: 1. remove foreign material: first the foreign material in Wudalianchi Volcanic sludge are removed, then be divided into the clod that diameter is 5cm～8cm, after drying in the shade, obtain removing the clod after foreign material; 2. prepare micropowder: the clod coarse-cracking machine after the removal foreign material that 1. step is obtained is broken into the clod granule that diameter is 5mm～10mm, then be transferred in super fine machine, charging rate be 1400 revs/min～1500 revs/min, distinguished and admirable be to pulverize under the condition of 1800 revs/min～2000 revs/min, grain size of micropowder is 300 order～600 orders, obtains dry sludge powder; 3. extract: wudalianchi minerals after treatment is added in dry sludge powder, the mass ratio of wudalianchi minerals after treatment and dry sludge powder is 20:1, pH is adjusted to 5.0～7.0 with hydrochloric acid or sodium hydroxide, stir, place 24h, get supernatant, obtain the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge; Then adopting white oil is solvent, white oil solvent is added in dry sludge powder, the mass ratio of white oil solvent and dry sludge powder is 20:1, soak at room temperature 24h, leave standstill 24h, get supernatant, obtain Wudalianchi Volcanic sludge oil-soluble composition extracting solution, be finally 5:1 mixing and stirring in mass ratio by the water soluble ingredient extracting solution of Wudalianchi Volcanic sludge and Wudalianchi Volcanic sludge oil-soluble composition extracting solution, obtain Wudalianchi Volcanic sludge extract.

3. the preparation method of a kind of sludge sun screen according to claim 2, it is characterized in that 3%～5% squalane of in step 2, step 1 being prepared, 2.5%～3% titanium dioxide, 5%～10% isononyl isononanoate, 3%～3.5% polydimethylsiloxane, 0.5%～2% ring five polydimethylsiloxane, 1.5%～2.5% betanin, 0.5%～3% cetyl PEG/PPG-10/1 polydimethylsiloxane, 2%～5% dimetylsilyl SiClx stone, 0.05%～0.5% methyl hydroxybenzoate and 0.05%～0.5% propyl hydroxybenzoate mix and blend are also heated to 75 DEG C～80 DEG C from room temperature, obtain oil mixture.

4. the preparation method of a kind of sludge sun screen according to claim 2, it is characterized in that 5%～10% butanediol, 1%～3% bisabolol, 3%～5% allantoin, 1.5%～2.5% phenoxyethanol, 0.5%～2% sodium chloride and the surplus in step 3, step 1 prepared are wudalianchi minerals mix homogeneously after treatment and are heated to 75 DEG C～80 DEG C from room temperature, obtain aqueous mixture.

5. the preparation method of a kind of sludge sun screen according to claim 2, it is characterized in that the oil mixture in step 4, step 2 being obtained adds in the aqueous mixture that step 3 obtains, be emulsifying homogeneous 6min～8min under the condition of 1800 revs/min～2000 revs/min in speed, be cooled to 45 DEG C～50 DEG C, obtain mixed solution.