CN104523563A - Diatom mask and preparation method thereof - Google Patents
Diatom mask and preparation method thereof Download PDFInfo
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- CN104523563A CN104523563A CN201510011800.8A CN201510011800A CN104523563A CN 104523563 A CN104523563 A CN 104523563A CN 201510011800 A CN201510011800 A CN 201510011800A CN 104523563 A CN104523563 A CN 104523563A
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Abstract
The invention belongs to the living field of cosmetics, and particularly relates to a diatom mask and a preparation method of the diatom mask. The diatom mask comprises diatom crusts, a moisturizing agent, a thickening agent, a traditional Chinese medicine extract, honey, a preservative, a desensitizer and the balance of water, all of which are prepared according to parts by weight, wherein the particle size of the diatom crusts ranges from 10 nm to 500 nm, and the traditional Chinese medicine extract is one or a mixture of two or more of radix angelicae, bletilla striata, liquorice, bighead atractylodes rhizome, angelica sinensis, honeysuckle, sophora flower buds, radix astragali and pseudo-ginseng. With the diatom crusts with a powerful adsorption function as the main matrix, the diatom mask achieves an excellent cleansing effect and can deeply cleanse the skin and easily adsorb redundant fat and blackheads. Meanwhile, because a large amount of mask water is contained in holes of the diatom crusts, oil and water secretion of the skin can be efficiently regulated and balanced. Furthermore, the traditional Chinese medicine is added in the diatom mask for whitening, and the traditional Chinese medicine and the diatom crusts supplement each other to achieve the effect of nursing the skin together.
Description
Technical field
The invention belongs to field of cosmetic life, be specifically related to a kind of diatom facial film and preparation method thereof.
Background technology
Facial film is a kind of cosmetics and skincare product applied on the face, current facial film generally only has the effect of whitening and skin moistening, not sterilization, antiinflammatory and antioxidative effect, some facial film is in order to strengthen cosmetic result, also add some chemical substance to human health wherein, as plumbous and hydrargyrum, this kind of facial film of life-time service can affect the healthy of people.
Cell wall from dead diatom can be accumulated on sea bed as huge siliceous mineral reserve, thickly reach 1400m, consequent diatom test owing to having the string premium properties such as light weight, porous, high-strength, wear-resisting, insulation, adiabatic, absorption and chemically stable, and is widely used in the industries such as metallurgy, chemical industry, electric power, agricultural, chemical fertilizer, building materials heat insulating products.On the other hand, the interest of the three dimensional structure of diatom test has caused nano materials research person, because the meticulous crepis of diatom can be used for the diatom metal pattern setting up nanotechnology.Also result in people to the research of diatom test at cosmetic field simultaneously.
Summary of the invention
The invention provides a kind of diatom facial film, have potent adsorption function, can receive fine, soft fur hole Bergamot Mint Extract by deep layer cleaning, moisture content is high, and moisturizing performance is all good.
The technical solution used in the present invention is as follows: a kind of diatom facial film and preparation method thereof, be made up of each component of following parts by weight: diatom shell 20-80 part, wetting agent 1-20 part, thickening agent 1-10 part, Chinese medicine extract 5-25 part, Mel 1-10 part, antiseptic 0.1-1 part, anti-sensitizer 0.1-1 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described Chinese medicine extract is one or more the mixture in the Radix Angelicae Dahuricae, the Pseudobulbus Bletillae (Rhizoma Bletillae), Radix Glycyrrhizae, the Rhizoma Atractylodis Macrocephalae, Radix Angelicae Sinensis, Flos Lonicerae, the Flos Sophorae Immaturus, the Radix Astragali, Radix Notoginseng.
Further, the present invention is made up of each component of following parts by weight: diatom shell 20-50 part, wetting agent 1-15 part, thickening agent 1-10 part, Chinese medicine extract 5-20 part, Mel 1-10 part, antiseptic 0.1-1 part, anti-sensitizer 0.1-1 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described Chinese medicine extract is one or more the mixture in the Radix Angelicae Dahuricae, the Pseudobulbus Bletillae (Rhizoma Bletillae), Radix Glycyrrhizae, the Rhizoma Atractylodis Macrocephalae, Radix Angelicae Sinensis.
Further, the present invention is made up of each component of following parts by weight: diatom shell 25-50 part, wetting agent 1-10 part, thickening agent 1-10 part, Chinese medicine extract 5-20 part, Mel 1-10 part, antiseptic 0.1-1 part, anti-sensitizer 0.1-1 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described Chinese medicine extract is one or more the mixture in Flos Lonicerae, the Flos Sophorae Immaturus, the Radix Astragali, Radix Notoginseng.
Further, the present invention also comprises quintessence oil, and described quintessence oil is 0.01-1 part.
Further, wetting agent of the present invention is butanediol or propylene glycol or glycerol or sorbitol.
Further, thickening agent of the present invention is hydroxy methocel or polyvinylpyrrolidone or 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers or polyacrylamide/C13-C14 isoparaffin/laureth-7.
Further, Chinese medicine extract preparation method of the present invention: above-mentioned Chinese medicine is cleaned and dries, pulverize, add 1-5 times of water soaking 2 hours, in 60-120 DEG C of soak by water 1-2 hour, filter to get filtrate, medicinal residues add 1-2 times of water, be 60-150 DEG C decoct 30-60 minute in temperature, filter to get filtrate, merging filtrate, filtrate is after adsorption bleaching, concentrated.
Further, present invention also offers the preparation method of diatom facial film, be added in reaction pot A by diatom shell, Chinese medicine extract, control temperature is 50 DEG C-80 DEG C, stirs 30min-120min; The water of surplus is heated to 50 DEG C-80 DEG C in prewired pot B, then adds wetting agent, thickening agent and Mel successively and stir; Being transferred to by material in prewired pot B answers in pot A again, and Keep agitation 30min-120min, then cools to 20 DEG C-50 DEG C; Add antiseptic, anti-sensitizer and quintessence oil again, stir 10min-120min, cooling discharging obtains diatom facial film.
The present invention adopts diatom test to be main matrix, the adsorption function that diatom test is powerful, shows excellent clean skin effect, can help skin deep layer cleaning, easily withhold excessive oils and fats and blackhead.Meanwhile, diatom test aperture stores a large amount of facial film moisture content, helps efficient conditioning balance skin profit to secrete.The present invention additionally uses Chinese medicine whitening, complements each other with diatom test, the common effect playing adjustment skin.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further elaborated.
embodiment 1
Diatom shell 40 parts, butanediol 10 parts, hydroxy methocel 2 parts, the Chinese medicine extract Radix Angelicae Dahuricae, the Pseudobulbus Bletillae (Rhizoma Bletillae), Radix Glycyrrhizae and the Rhizoma Atractylodis Macrocephalae have 6 parts altogether, Mel 8 parts, P-hydroxybenzoic acid 0.5 part, octyldodecanol 0.1 part, quintessence oil 0.05 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described diatom shell extracts and obtains from kieselguhr.
The method for preparing extractive of the described Radix Angelicae Dahuricae, the Pseudobulbus Bletillae (Rhizoma Bletillae), Radix Glycyrrhizae and the Rhizoma Atractylodis Macrocephalae: above-mentioned Chinese medicine is cleaned and dries, pulverize, add 1-5 times of water soaking 2 hours, in 60-120 DEG C of soak by water 1-2 hour, filter to get filtrate, medicinal residues add 1-2 times of water, be 60-150 DEG C in temperature and decoct 30-60 minute, filter to get filtrate, merging filtrate, filtrate is after adsorption bleaching, concentrated.
The preparation process of diatom facial film: be added in reaction pot A by the extract of diatom shell 40 parts, the Radix Angelicae Dahuricae, the Pseudobulbus Bletillae (Rhizoma Bletillae), Radix Glycyrrhizae and the Rhizoma Atractylodis Macrocephalae, control temperature is 50 DEG C-80 DEG C, stirs 30min-120min; The water of surplus is heated to 50 DEG C-80 DEG C in prewired pot B, then adds butanediol 10 parts, hydroxy methocel 2 parts and Mel 8 parts successively and stir; Being transferred to by material in prewired pot B answers in pot A again, and Keep agitation 30min-120min, then cools to 20 DEG C-50 DEG C; Add P-hydroxybenzoic acid 0.5 part, octyldodecanol 0.1 part and quintessence oil 0.05 part again, stir 10min-120min, cooling discharging obtains diatom facial film.
embodiment 2
Diatom shell 60 parts, sorbitol 8 parts, polyvinylpyrrolidone 2 parts, Chinese medicine extract Flos Lonicerae, the Flos Sophorae Immaturus have 5 parts altogether, Mel 8 parts, P-hydroxybenzoic acid 0.5 part, octyldodecanol 0.1 part, quintessence oil 0.05 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described diatom shell extracts and obtains from kieselguhr.
The method for preparing extractive of described Flos Lonicerae, the Flos Sophorae Immaturus: above-mentioned Chinese medicine is cleaned and dries, pulverize, add 1-5 times of water soaking 2 hours, in 60-120 DEG C of soak by water 1-2 hour, filter to get filtrate, medicinal residues add 1-2 times of water, be 60-150 DEG C in temperature and decoct 30-60 minute, filter to get filtrate, merging filtrate, filtrate is after adsorption bleaching, concentrated.
The preparation process of diatom facial film: be added in reaction pot A by the extract 5 parts of diatom shell 60 parts, Flos Lonicerae, the Flos Sophorae Immaturus, control temperature is 50 DEG C-80 DEG C, stirs 30min-120min; The water of surplus is heated to 50 DEG C-80 DEG C in prewired pot B, then adds glycerol 8 parts, polyvinylpyrrolidone 2 parts and Mel 8 parts successively and stir; Being transferred to by material in prewired pot B answers in pot A again, and Keep agitation 30min-120min, then cools to 20 DEG C-50 DEG C; Add P-hydroxybenzoic acid 0.5 part, octyldodecanol 0.1 part and quintessence oil 0.05 part again, stir 10min-120min, cooling discharging obtains diatom facial film.
embodiment 3
Diatom shell 55 parts, glycerol 8 parts, polyvinylpyrrolidone 1 part, the Chinese medicine extract Radix Astragali, Radix Notoginseng have 8 parts altogether, Mel 8 parts, P-hydroxybenzoic acid 0.5 part, octyldodecanol 0.2 part, quintessence oil 0.05 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described diatom shell extracts and obtains from kieselguhr.
The method for preparing extractive of the described Radix Astragali, Radix Notoginseng: above-mentioned Chinese medicine is cleaned and dries, pulverize, add 1-5 times of water soaking 2 hours, in 60-120 DEG C of soak by water 1-2 hour, filter to get filtrate, medicinal residues add 1-2 times of water, be 60-150 DEG C in temperature and decoct 30-60 minute, filter to get filtrate, merging filtrate, filtrate is after adsorption bleaching, concentrated.
The preparation process of diatom facial film: be added in reaction pot A by the extract 5 parts of diatom shell 55 parts, the Radix Astragali, Radix Notoginseng, control temperature is 50 DEG C-80 DEG C, stirs 30min-120min; The water of surplus is heated to 50 DEG C-80 DEG C in prewired pot B, then adds glycerol 8 parts, polyvinylpyrrolidone 1 part and Mel 8 parts successively and stir; Being transferred to by material in prewired pot B answers in pot A again, and Keep agitation 30min-120min, then cools to 20 DEG C-50 DEG C; Add P-hydroxybenzoic acid 0.5 part, octyldodecanol 0.2 part and quintessence oil 0.05 part again, stir 10min-120min, cooling discharging obtains diatom facial film.
embodiment 4
Diatom shell 30 parts, butanediol 5 parts, polyvinylpyrrolidone 3 parts, the Chinese medicine extract Radix Astragali, Radix Notoginseng have 8 parts altogether, Mel 5 parts, MIT 0.5 part, octyldodecanol 0.2 part, quintessence oil 0.05 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described diatom shell extracts and obtains from kieselguhr.
The method for preparing extractive of the described Radix Astragali, Radix Notoginseng: above-mentioned Chinese medicine is cleaned and dries, pulverize, add 1-5 times of water soaking 2 hours, in 60-120 DEG C of soak by water 1-2 hour, filter to get filtrate, medicinal residues add 1-2 times of water, be 60-150 DEG C in temperature and decoct 30-60 minute, filter to get filtrate, merging filtrate, filtrate is after adsorption bleaching, concentrated.
The preparation process of diatom facial film: be added in reaction pot A by the extract 8 parts of diatom shell 30 parts, the Radix Astragali, Radix Notoginseng, control temperature is 50 DEG C-80 DEG C, stirs 30min-120min; The water of surplus is heated to 50 DEG C-80 DEG C in prewired pot B, then adds butanediol 5 parts, polyvinylpyrrolidone 3 parts and Mel 5 parts successively and stir; Being transferred to by material in prewired pot B answers in pot A again, and Keep agitation 30min-120min, then cools to 20 DEG C-50 DEG C; Add MIT 0.5 part, octyldodecanol 0.2 part and quintessence oil 0.05 part again, stir 10min-120min, cooling discharging obtains diatom facial film.
In order to verify safety of the present invention, sample prepared by embodiment 1-4 is all sent to third party and detects detection of skin zest, the skin irritation test of continuous 10 days does with white mice in testing agency, all there is not red and swollen and edema phenomenon in the skin of result display white mice, third party testing agency, according to the repeatedly intact skin irritant test skin irritation strength grading standard in " Disposable Sanitary Accessory sanitary standard " (GB15979-2002), is nonirritant material to the sample conclusion prepared by embodiment 1-4.
In order to verify microorganism of the present invention and heavy metal index, the application is sent to third party through the present invention and detects company and detect, and after testing, meets national cosmetic 20007 specification, specifically in table 1:
Result of use: select 100 volunteers, 50 is experimental group, and another 50 is matched group, experimental group selects the product of the present embodiment 2, matched group directly selects water in contrast, and evaluation criterion is based on naked eyes viewing, and blackhead, tamper pimple and dull-looking skin are primary evaluation standard.Concrete outcome is as follows in table 2:
Compare from the use group of table 2 and matched group, standard variance P < 0.01, illustrates the evident in efficacy of this facial film.
The above; it is only most preferred embodiment of the present invention; not any pro forma restriction is done to the present invention; any those of ordinary skill in the art; do not departing under technical solution of the present invention ambit; utilize the method content of above-mentioned announcement to make many possible variations and modification to technical solution of the present invention, all belong to the scope of claims protection.
Claims (8)
1. a diatom facial film, it is characterized in that: be made up of each component of following parts by weight: diatom shell 20-80 part, wetting agent 1-20 part, thickening agent 1-10 part, Chinese medicine extract 5-25 part, Mel 1-10 part, antiseptic 0.1-1 part, anti-sensitizer 0.1-1 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described Chinese medicine extract is one or more the mixture in the Radix Angelicae Dahuricae, the Pseudobulbus Bletillae (Rhizoma Bletillae), Radix Glycyrrhizae, the Rhizoma Atractylodis Macrocephalae, Radix Angelicae Sinensis, Flos Lonicerae, the Flos Sophorae Immaturus, the Radix Astragali, Radix Notoginseng.
2. a kind of diatom facial film according to claim 1, is characterized in that: be made up of each component of following parts by weight:
Diatom shell 20-50 part, wetting agent 1-15 part, thickening agent 1-10 part, Chinese medicine extract 5-20 part, Mel 1-10 part, antiseptic 0.1-1 part, anti-sensitizer 0.1-1 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described Chinese medicine extract is one or more the mixture in the Radix Angelicae Dahuricae, the Pseudobulbus Bletillae (Rhizoma Bletillae), Radix Glycyrrhizae, the Rhizoma Atractylodis Macrocephalae, Radix Angelicae Sinensis.
3. a kind of diatom facial film according to claim 1, is characterized in that: be made up of each component of following parts by weight:
Diatom shell 25-50 part, wetting agent 1-10 part, thickening agent 1-10 part, Chinese medicine extract 5-20 part, Mel 1-10 part, antiseptic 0.1-1 part, anti-sensitizer 0.1-1 part, excess water, described diatom shell particle diameter is 10nm-500nm, and described Chinese medicine extract is one or more the mixture in Flos Lonicerae, the Flos Sophorae Immaturus, the Radix Astragali, Radix Notoginseng.
4. a kind of diatom facial film according to claims 1 to 3, is characterized in that: also comprise quintessence oil, described quintessence oil is 0.01-1 part.
5. a kind of diatom facial film according to Claims 1-4, is characterized in that: described wetting agent is butanediol or propylene glycol or glycerol or sorbitol.
6. according to a kind of diatom facial film described in claim 1 to 5, it is characterized in that: described thickening agent is hydroxy methocel or polyvinylpyrrolidone or 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers or polyacrylamide/C13-C14 isoparaffin/laureth-7.
7. according to a kind of diatom facial film described in claim 1 to 5, it is characterized in that: described Chinese medicine extract preparation method: above-mentioned Chinese medicine is cleaned and dries, pulverize, add 1-5 times of water soaking 2 hours, in 60-120 DEG C of soak by water 1-2 hour, filter to get filtrate, medicinal residues add 1-2 times of water, be 60-150 DEG C decoct 30-60 minute in temperature, filter to get filtrate, merging filtrate, filtrate is after adsorption bleaching, concentrated.
8. according to the preparation of a kind of diatom facial film described in claim 1 to 6, it is characterized in that: be added in reaction pot A by diatom shell, Chinese medicine extract, control temperature is 50 DEG C-80 DEG C, stir 30min-120min; The water of surplus is heated to 50 DEG C-80 DEG C in prewired pot B, then adds wetting agent, thickening agent and Mel successively and stir; Being transferred to by material in prewired pot B answers in pot A again, and Keep agitation 30min-120min, then cools to 20 DEG C-50 DEG C; Add antiseptic, anti-sensitizer and quintessence oil again, stir 10min-120min, cooling discharging obtains diatom facial film.
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Cited By (5)
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| CN104586696A (en) * | 2015-01-09 | 2015-05-06 | 青岛泉佳美硅藻泥科技有限公司 | Diatom facial cleanser and preparation method thereof |
| CN104771353A (en) * | 2015-05-08 | 2015-07-15 | 山东友励商贸有限责任公司 | Cream used for deep cleaning and caring of face skin |
| CN107648140A (en) * | 2017-10-28 | 2018-02-02 | 安徽孔氏奇医药科技有限公司 | A kind of salubrious anti-acne mud film and preparation method thereof |
| CN108403587A (en) * | 2018-04-20 | 2018-08-17 | 朱华伟 | A kind of diatom facial mask and preparation method thereof |
| CN112315822A (en) * | 2020-10-21 | 2021-02-05 | 杭州协合医疗用品有限公司 | Diatom mineral mud mask and preparation method thereof |
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| CN104586696A (en) * | 2015-01-09 | 2015-05-06 | 青岛泉佳美硅藻泥科技有限公司 | Diatom facial cleanser and preparation method thereof |
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| CN108403587A (en) * | 2018-04-20 | 2018-08-17 | 朱华伟 | A kind of diatom facial mask and preparation method thereof |
| CN112315822A (en) * | 2020-10-21 | 2021-02-05 | 杭州协合医疗用品有限公司 | Diatom mineral mud mask and preparation method thereof |
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Address after: Laoshan District, Qingdao three road 266000 Shandong city of Qingdao province No. 8 poly center 10 layer 1109 Applicant after: Qingdao Spring Gamay Diatom Ooze Technology Co., Ltd. Address before: 1305 room 182-6, Haier Road, Laoshan District, Shandong, Qingdao, 266000 Applicant before: Qingdao Spring Gamay Diatom Ooze Technology Co., Ltd. |
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