CN110638677A - Volcanic mud makeup removing lotion and preparation method thereof - Google Patents
Volcanic mud makeup removing lotion and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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Abstract
A volcanic mud makeup removing lotion and a preparation method thereof relate to a makeup removing lotion and a preparation method thereof. The invention aims to solve the problems that the existing makeup removing emulsion contains alcohol, emulsifier and other components, damages skin, has no skin care property and has poor makeup removing performance, and the problems that the effective components of the volcanic slime need to be extracted in the utilization process, the extracted slime cannot be utilized and the utilization rate of raw materials is low. The volcanic mud makeup removing cream is prepared from natural mineral water of Wudalianchi, volcanic mud extract of Wudalianchi, mixture of precipitate and oil phase liquid, mannitol, rhamnose, tea tree essential oil, aloe essential oil, rosemary essential oil, butanediol, centella asiatica extract, aloe extract, ginseng extract, raspberry extract, phenoxyethanol and preservative. The preparation method comprises the following steps: firstly, weighing at one time; secondly, preparing a mud phase alcohol extract; thirdly, preparing a mud-phase water extract; fourthly, preparing oil phase liquid; fifthly, homogenizing; sixthly, weighing for the second time; and seventhly, mixing.
Description
Technical Field
The invention relates to makeup removing lotion and a preparation method thereof.
Background
Skin cleaning is an indispensable link for skin care, the cleansing milk has strong cleansing power, can be used for removing dirt on the skin, especially residues of cosmetics, but the existing cleansing milk contains components such as alcohol, emulsifier and the like, damages the skin, has no skin care property and has poor cleansing performance.
Volcanic slime is formed by long-term soaking of mineral water in particulate substances generated by volcanic eruption, migration, ion exchange, adsorption and enrichment under biochemical action and redox conditions, has proved to have very remarkable curative effect in the aspects of treating skin diseases, arthritis, alopecia and the like, and is widely applied in daily chemical industries such as beauty and skin care and the like, but the prior volcanic slime needs to extract effective components in the utilization process, the extracted slime cannot be utilized, and the utilization rate of raw materials is low.
Disclosure of Invention
The volcanic mud makeup removing cream and the preparation method thereof are provided by the invention for solving the problems that the existing makeup removing cream contains alcohol, emulsifier and other components, damages skin, has no skin care property and has poor makeup removing performance, and the problems that the effective components of volcanic mud need to be extracted in the utilization process, the extracted mud cannot be utilized and the utilization rate of raw materials is low in the utilization process of the existing volcanic mud.
A volcanic mud makeup removing emulsion is prepared by 20 to 25 portions of Wudalianchi natural mineral water, 20 to 25 portions of Wudalianchi volcanic mud extract and mixture of sediment and oil phase liquid, 0.1 to 0.5 portion of mannitol, 0.1 to 0.5 portion of rhamnose, 0.01 to 0.1 portion of tea tree essential oil, 0.01 to 0.1 portion of aloe essential oil, 0.01 to 0.1 portion of rosemary essential oil, 0.1 to 0.5 portion of butanediol, 0.1 to 1 portion of centella asiatica extract, 0.1 to 1 portion of aloe extract, 0.1 to 1 portion of ginseng extract, 0.1 to 1 portion of raspberry extract, 0.01 to 0.5 portion of phenoxyethanol and 0.05 to 0.1 portion of preservative according to the mass portions;
the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
the mixture of the volcanic mud extract of the Wudalianchi and the sediment and the oil phase liquid is prepared by the following steps:
firstly, weighing:
weighing 30-40 parts of Wudalianchi volcanic slime, 2-5 parts of olive oil, 2-5 parts of linseed oil, 2-5 parts of wheat germ oil, 2-5 parts of sweet almond oil, 2-3 parts of jojoba oil and 2-3 parts of coconut oil according to parts by mass;
secondly, preparing a mud phase alcohol extract:
firstly, 30 to 40 parts of the Wudalianchi volcanic slime is frozen and dried at the temperature of minus 50 to minus 35 ℃, then ground at the temperature of 20 to 30 ℃ until the granularity is 2 to 5 mu m, and the Wudalianchi volcanic slime micro powder is obtained;
secondly, adding 85-95% of ethanol by mass percent into the Wudalianchi volcanic mud micro powder, and extracting for 1.5-2 h at constant temperature under the condition of 40-50 ℃ to obtain supernatant extracted by an alcohol phase and precipitate extracted by the alcohol phase at one time;
the volume ratio of the Wudalianchi volcanic mud micro powder to 85-95% of ethanol in percentage by mass is 1 (3-5);
thirdly, repeating the precipitate after the primary alcohol phase extraction for three times according to the second step, and combining the supernatant liquid of the alcohol phase extraction to obtain an alcohol extraction liquid and the precipitate after the alcohol phase extraction;
fourthly, concentrating the alcohol extract under reduced pressure to 10 to 30 percent of the original volume to obtain a mud-phase alcohol extract;
thirdly, preparing a mud-phase water extract:
adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in a Wudalianchi pool, and extracting at a constant temperature of 60-75 ℃ for 60-90 min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction;
the volume ratio of the precipitate after alcohol phase extraction to the Wudalianchi natural mineral water is 1 (3-5); the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
secondly, repeating the precipitate obtained after the primary water phase extraction for three times according to the third step, and combining the supernatant obtained after the water phase extraction to obtain a water extracting solution and the precipitate obtained after the water phase extraction;
thirdly, decompressing and concentrating the water extract to 10-30% of the original volume to obtain a mud-phase water extract;
fourthly, preparing oil phase liquid:
mixing 2 to 5 parts of olive oil, 2 to 5 parts of linseed oil, 2 to 5 parts of wheat germ oil, 2 to 5 parts of sweet almond oil, 2 to 3 parts of jojoba oil and 2 to 3 parts of coconut oil to obtain an oil phase, heating the oil phase to the temperature of between 70 and 85 ℃, and uniformly stirring to obtain an oil phase liquid;
fifthly, homogenizing:
and (3) uniformly mixing the mud-phase alcohol extract obtained in the second step, the mud-phase water extract obtained in the third step and the oil-phase liquid obtained in the fourth step, adding the precipitate obtained in the third step after water-phase extraction, homogenizing for 0.5-1 h by using a high-speed homogenizer at the rotation speed of 8000-10000 r/min, repeating the homogenization process for three times, and cooling to room temperature to obtain the volcanic sludge extract of the Wudalianchi pool and the mixture of the precipitate and the oil-phase liquid.
The preparation method of the volcanic mud cleansing milk comprises the following steps:
firstly, weighing at one time:
weighing 30-40 parts of Wudalianchi volcanic slime, 2-5 parts of olive oil, 2-5 parts of linseed oil, 2-5 parts of wheat germ oil, 2-5 parts of sweet almond oil, 2-3 parts of jojoba oil and 2-3 parts of coconut oil according to parts by mass;
secondly, preparing a mud phase alcohol extract:
firstly, 30 to 40 parts of the Wudalianchi volcanic slime is frozen and dried at the temperature of minus 50 to minus 35 ℃, then ground at the temperature of 20 to 30 ℃ until the granularity is 2 to 5 mu m, and the Wudalianchi volcanic slime micro powder is obtained;
secondly, adding 85-95% of ethanol by mass percent into the Wudalianchi volcanic mud micro powder, and extracting for 1.5-2 h at constant temperature under the condition of 40-50 ℃ to obtain supernatant extracted by an alcohol phase and precipitate extracted by the alcohol phase at one time;
the volume ratio of the Wudalianchi volcanic mud micro powder to 85-95% of ethanol in percentage by mass is 1 (3-5);
thirdly, repeating the precipitate after the primary alcohol phase extraction for three times according to the second step, and combining the supernatant liquid of the alcohol phase extraction to obtain an alcohol extraction liquid and the precipitate after the alcohol phase extraction;
fourthly, concentrating the alcohol extract under reduced pressure to 10 to 30 percent of the original volume to obtain a mud-phase alcohol extract;
thirdly, preparing a mud-phase water extract:
adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in a Wudalianchi pool, and extracting at a constant temperature of 60-75 ℃ for 60-90 min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction;
the volume ratio of the precipitate after alcohol phase extraction to the Wudalianchi natural mineral water is 1 (3-5); the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
secondly, repeating the precipitate obtained after the primary water phase extraction for three times according to the third step, and combining the supernatant obtained after the water phase extraction to obtain a water extracting solution and the precipitate obtained after the water phase extraction;
thirdly, decompressing and concentrating the water extract to 10-30% of the original volume to obtain a mud-phase water extract;
fourthly, preparing oil phase liquid:
mixing 2 to 5 parts of olive oil, 2 to 5 parts of linseed oil, 2 to 5 parts of wheat germ oil, 2 to 5 parts of sweet almond oil, 2 to 3 parts of jojoba oil and 2 to 3 parts of coconut oil to obtain an oil phase, heating the oil phase to the temperature of between 70 and 85 ℃, and uniformly stirring to obtain an oil phase liquid;
fifthly, homogenizing:
uniformly mixing the mud-phase alcohol extract obtained in the second step, the mud-phase water extract obtained in the third step and the oil-phase liquid obtained in the fourth step, adding the precipitate obtained in the third step after water-phase extraction, homogenizing for 0.5-1 h by using a high-speed homogenizer at the rotating speed of 8000-10000 r/min, repeating the homogenization process for three times, and cooling to room temperature to obtain a mixture of the volcanic mud extract and the precipitate with the oil-phase liquid in the Wudalianchi pool;
sixthly, weighing for the second time:
weighing 20 to 25 parts of natural mineral water of the Wudalianchi, 20 to 25 parts of volcanic mud extract of the Wudalianchi, 0.1 to 0.5 part of mannitol, 0.1 to 0.5 part of rhamnose, 0.01 to 0.1 part of tea tree essential oil, 0.01 to 0.1 part of aloe essential oil, 0.01 to 0.1 part of rosemary essential oil, 0.1 to 0.5 part of butanediol, 0.1 to 1 part of centella asiatica extract, 0.1 to 1 part of aloe extract, 0.1 to 1 part of ginseng extract, 0.1 to 1 part of raspberry extract, 0.01 to 0.5 part of phenoxyethanol and 0.05 to 0.1 part of preservative according to the mass parts;
the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
seventhly, mixing:
weighing 20 to 25 parts of the volcanic mud extract of the Wudalianchi and the mixture of the sediment and the oil phase liquid, 20 to 25 parts of the natural mineral water of the Wudalianchi, 0.1 to 0.5 part of mannitol, 0.1 to 0.5 part of rhamnose, 0.01 to 0.1 part of tea tree essential oil, 0.01 to 0.1 part of aloe essential oil, 0.01 to 0.1 part of rosemary essential oil, 0.1 to 0.5 part of butanediol, 0.1 to 1 part of centella asiatica extract, 0.1 to 1 part of aloe extract, 0.1 to 1 part of ginseng extract, 0.1 to 1 part of raspberry extract, 0.01 to 0.5 part of phenoxyethanol and 0.05 to 0.1 part of preservative, and uniformly mixing to obtain the volcanic mud makeup removing milk.
The invention has the beneficial effects that:
1. the invention simplifies the extraction process of the skin care active ingredients of the Wudalianchi volcanic mud, combines alcohol extraction and water extraction, and improves the utilization rate of raw materials because the extracted precipitate is also applied to makeup removing milk.
2. The volcanic mud cleansing milk of the invention well retains the effective skin care ingredients in the volcanic mud of WudalianchiIs (Ca)2+，Mg2+，K+，Na+，Zn2+，SiO3 2-，HCO3 -And various mineral ions) and has better makeup removing effect, wherein the moisture content of the skin before makeup removing is 22%, the oil content is 26%, the moisture content after use is 54%, and the oil content is 12%.
3. The volcanic mud is used as a special clay, has a unique porous structure, has very strong adsorption capacity, can effectively adsorb grease and clean pores, and is a very ideal natural makeup removing material. According to the invention, no emulsifier is added, the volcanic mud is prepared into particles (2-5 μm) with the optimal size, a stable emulsion system is achieved by utilizing the self-emulsifying capacity of the volcanic mud, the addition of the emulsifier is avoided, and the extracted precipitate is used as the emulsifier, so that the formula is more refreshing, and the burden on the skin is less.
4. The volcanic mud makeup removing lotion can achieve the effects of makeup removal and facial mask at the same time, simplifies the process of skin care, and can introduce skin care ingredients in mineral spring and slime products into skin during makeup removal due to the softness and naturalness of the formula.
5. The raw materials of the invention can achieve better synergistic effect, and achieve the best makeup removing and skin care effects.
Detailed Description
The first embodiment is as follows: the volcanic mud makeup removing milk is prepared from, by mass, 20-25 parts of Wudalianchi natural mineral water, 20-25 parts of Wudalianchi volcanic mud extract, a mixture of precipitate and oil phase liquid, 0.1-0.5 part of mannitol, 0.1-0.5 part of rhamnose, 0.01-0.1 part of tea tree essential oil, 0.01-0.1 part of aloe essential oil, 0.01-0.1 part of rosemary essential oil, 0.1-0.5 part of butanediol, 0.1-1 part of centella asiatica extract, 0.1-1 part of aloe extract, 0.1-1 part of ginseng extract, 0.1-1 part of raspberry extract, 0.01-0.5 part of phenoxyethanol and 0.05-0.1 part of preservative;
the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
the mixture of the volcanic mud extract of the Wudalianchi and the sediment and the oil phase liquid is prepared by the following steps:
firstly, weighing:
weighing 30-40 parts of Wudalianchi volcanic slime, 2-5 parts of olive oil, 2-5 parts of linseed oil, 2-5 parts of wheat germ oil, 2-5 parts of sweet almond oil, 2-3 parts of jojoba oil and 2-3 parts of coconut oil according to parts by mass;
secondly, preparing a mud phase alcohol extract:
firstly, 30 to 40 parts of the Wudalianchi volcanic slime is frozen and dried at the temperature of minus 50 to minus 35 ℃, then ground at the temperature of 20 to 30 ℃ until the granularity is 2 to 5 mu m, and the Wudalianchi volcanic slime micro powder is obtained;
secondly, adding 85-95% of ethanol by mass percent into the Wudalianchi volcanic mud micro powder, and extracting for 1.5-2 h at constant temperature under the condition of 40-50 ℃ to obtain supernatant extracted by an alcohol phase and precipitate extracted by the alcohol phase at one time;
the volume ratio of the Wudalianchi volcanic mud micro powder to 85-95% of ethanol in percentage by mass is 1 (3-5);
thirdly, repeating the precipitate after the primary alcohol phase extraction for three times according to the second step, and combining the supernatant liquid of the alcohol phase extraction to obtain an alcohol extraction liquid and the precipitate after the alcohol phase extraction;
fourthly, concentrating the alcohol extract under reduced pressure to 10 to 30 percent of the original volume to obtain a mud-phase alcohol extract;
thirdly, preparing a mud-phase water extract:
adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in a Wudalianchi pool, and extracting at a constant temperature of 60-75 ℃ for 60-90 min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction;
the volume ratio of the precipitate after alcohol phase extraction to the Wudalianchi natural mineral water is 1 (3-5); the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
secondly, repeating the precipitate obtained after the primary water phase extraction for three times according to the third step, and combining the supernatant obtained after the water phase extraction to obtain a water extracting solution and the precipitate obtained after the water phase extraction;
thirdly, decompressing and concentrating the water extract to 10-30% of the original volume to obtain a mud-phase water extract;
fourthly, preparing oil phase liquid:
mixing 2 to 5 parts of olive oil, 2 to 5 parts of linseed oil, 2 to 5 parts of wheat germ oil, 2 to 5 parts of sweet almond oil, 2 to 3 parts of jojoba oil and 2 to 3 parts of coconut oil to obtain an oil phase, heating the oil phase to the temperature of between 70 and 85 ℃, and uniformly stirring to obtain an oil phase liquid;
fifthly, homogenizing:
and (3) uniformly mixing the mud-phase alcohol extract obtained in the second step, the mud-phase water extract obtained in the third step and the oil-phase liquid obtained in the fourth step, adding the precipitate obtained in the third step after water-phase extraction, homogenizing for 0.5-1 h by using a high-speed homogenizer at the rotation speed of 8000-10000 r/min, repeating the homogenization process for three times, and cooling to room temperature to obtain the volcanic sludge extract of the Wudalianchi pool and the mixture of the precipitate and the oil-phase liquid.
The beneficial effects of the embodiment are as follows: 1. the embodiment simplifies the extraction process of the skin care active ingredients of the Wudalianchi volcanic mud, combines alcohol extraction and water extraction, and improves the utilization rate of raw materials because the extracted precipitate is also applied to the makeup removing milk.
2. The volcanic mud cleansing milk of the embodiment well retains the effective skin care ingredients (Ca) in the volcanic mud of Wudalianchi2+，Mg2+，K+，Na+，Zn2+，SiO3 2-，HCO3 -And various mineral ions) and has better makeup removing effect, wherein the moisture content of the skin before makeup removing is 22%, the oil content is 26%, the moisture content after use is 54%, and the oil content is 12%.
3. The volcanic mud is used as a special clay, has a unique porous structure, has very strong adsorption capacity, can effectively adsorb grease and clean pores, and is a very ideal natural makeup removing material. In the embodiment, no emulsifier is added, the volcanic mud is made into particles (2-5 μm) with the optimal size, a stable emulsion system is achieved by utilizing the self-emulsifying capacity of the volcanic mud, the addition of the emulsifier is avoided, and the extracted precipitate is used as the emulsifier, so that the formula is more refreshing, and the burden on the skin is less.
4. The volcanic mud makeup removing lotion can achieve the effects of makeup removal and facial mask at the same time, simplifies the process of skin care, and can introduce skin care ingredients in mineral spring and slime products into skin during makeup removal due to softness and naturalness of the formula.
5. The raw materials of the embodiment can achieve better synergistic effect, and achieve the best makeup removing and skin care effects.
The second embodiment is as follows: the first difference between the present embodiment and the specific embodiment is: the volcanic slime of the Wudalianchi is collected in a slime layer of 80-150 cm below the surface of the mineral slime zone of the Wudalianchi Yaquan wetland in the step one. The rest is the same as the first embodiment.
The volcanic mud in Wudalianchi according to the embodiment is mainly composed of dark grey to black viscous mud with volcanic glass as a main component, and contains various abundant mineral elements and various rare earth elements with biological activity effect.
The third concrete implementation mode: this embodiment is different from the first or second embodiment in that: the preservative is methyl chloroisothiazolinone or methyl isothiazolinone. The other is the same as in the first or second embodiment.
The fourth concrete implementation mode: the difference between this embodiment mode and one of the first to third embodiment modes is: secondly, adding 95 percent ethanol in percentage by mass into the Wudalianchi volcanic mud micro powder, and extracting for 2 hours at constant temperature under the condition of 45-50 ℃ to obtain supernatant extracted by an alcohol phase and precipitate extracted by the primary alcohol phase; and in the second step, the volume ratio of the Wudalianchi volcanic mud micro powder to 95 percent ethanol in percentage by mass is 1: 3. The others are the same as the first to third embodiments.
The fifth concrete implementation mode: the difference between this embodiment and one of the first to fourth embodiments is: adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in the Wudalianchi pool, and extracting at a constant temperature of 75 ℃ for 60min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction; and the volume ratio of the precipitate obtained after the alcohol phase extraction in the third step to the Wudalianchi natural mineral water is 1: 3. The rest is the same as the first to fourth embodiments.
The sixth specific implementation mode: the preparation method of the volcanic mud cleansing milk provided by the embodiment is carried out according to the following steps:
firstly, weighing at one time:
weighing 30-40 parts of Wudalianchi volcanic slime, 2-5 parts of olive oil, 2-5 parts of linseed oil, 2-5 parts of wheat germ oil, 2-5 parts of sweet almond oil, 2-3 parts of jojoba oil and 2-3 parts of coconut oil according to parts by mass;
secondly, preparing a mud phase alcohol extract:
firstly, 30 to 40 parts of the Wudalianchi volcanic slime is frozen and dried at the temperature of minus 50 to minus 35 ℃, then ground at the temperature of 20 to 30 ℃ until the granularity is 2 to 5 mu m, and the Wudalianchi volcanic slime micro powder is obtained;
secondly, adding 85-95% of ethanol by mass percent into the Wudalianchi volcanic mud micro powder, and extracting for 1.5-2 h at constant temperature under the condition of 40-50 ℃ to obtain supernatant extracted by an alcohol phase and precipitate extracted by the alcohol phase at one time;
the volume ratio of the Wudalianchi volcanic mud micro powder to 85-95% of ethanol in percentage by mass is 1 (3-5);
thirdly, repeating the precipitate after the primary alcohol phase extraction for three times according to the second step, and combining the supernatant liquid of the alcohol phase extraction to obtain an alcohol extraction liquid and the precipitate after the alcohol phase extraction;
fourthly, concentrating the alcohol extract under reduced pressure to 10 to 30 percent of the original volume to obtain a mud-phase alcohol extract;
thirdly, preparing a mud-phase water extract:
adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in a Wudalianchi pool, and extracting at a constant temperature of 60-75 ℃ for 60-90 min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction;
the volume ratio of the precipitate after alcohol phase extraction to the Wudalianchi natural mineral water is 1 (3-5); the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
secondly, repeating the precipitate obtained after the primary water phase extraction for three times according to the third step, and combining the supernatant obtained after the water phase extraction to obtain a water extracting solution and the precipitate obtained after the water phase extraction;
thirdly, decompressing and concentrating the water extract to 10-30% of the original volume to obtain a mud-phase water extract;
fourthly, preparing oil phase liquid:
mixing 2 to 5 parts of olive oil, 2 to 5 parts of linseed oil, 2 to 5 parts of wheat germ oil, 2 to 5 parts of sweet almond oil, 2 to 3 parts of jojoba oil and 2 to 3 parts of coconut oil to obtain an oil phase, heating the oil phase to the temperature of between 70 and 85 ℃, and uniformly stirring to obtain an oil phase liquid;
fifthly, homogenizing:
uniformly mixing the mud-phase alcohol extract obtained in the second step, the mud-phase water extract obtained in the third step and the oil-phase liquid obtained in the fourth step, adding the precipitate obtained in the third step after water-phase extraction, homogenizing for 0.5-1 h by using a high-speed homogenizer at the rotating speed of 8000-10000 r/min, repeating the homogenization process for three times, and cooling to room temperature to obtain a mixture of the volcanic mud extract and the precipitate with the oil-phase liquid in the Wudalianchi pool;
sixthly, weighing for the second time:
weighing 20 to 25 parts of natural mineral water of the Wudalianchi, 20 to 25 parts of volcanic mud extract of the Wudalianchi, 0.1 to 0.5 part of mannitol, 0.1 to 0.5 part of rhamnose, 0.01 to 0.1 part of tea tree essential oil, 0.01 to 0.1 part of aloe essential oil, 0.01 to 0.1 part of rosemary essential oil, 0.1 to 0.5 part of butanediol, 0.1 to 1 part of centella asiatica extract, 0.1 to 1 part of aloe extract, 0.1 to 1 part of ginseng extract, 0.1 to 1 part of raspberry extract, 0.01 to 0.5 part of phenoxyethanol and 0.05 to 0.1 part of preservative according to the mass parts;
the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
seventhly, mixing:
weighing 20 to 25 parts of the volcanic mud extract of the Wudalianchi and the mixture of the sediment and the oil phase liquid, 20 to 25 parts of the natural mineral water of the Wudalianchi, 0.1 to 0.5 part of mannitol, 0.1 to 0.5 part of rhamnose, 0.01 to 0.1 part of tea tree essential oil, 0.01 to 0.1 part of aloe essential oil, 0.01 to 0.1 part of rosemary essential oil, 0.1 to 0.5 part of butanediol, 0.1 to 1 part of centella asiatica extract, 0.1 to 1 part of aloe extract, 0.1 to 1 part of ginseng extract, 0.1 to 1 part of raspberry extract, 0.01 to 0.5 part of phenoxyethanol and 0.05 to 0.1 part of preservative, and uniformly mixing to obtain the volcanic mud makeup removing milk.
The seventh embodiment: the sixth embodiment is different from the sixth embodiment in that: the volcanic slime of the Wudalianchi is collected in a slime layer of 80-150 cm below the surface of the mineral slime zone of the Wudalianchi Yaquan wetland in the step one. The rest is the same as the sixth embodiment.
The specific implementation mode is eight: the present embodiment differs from one of the sixth or seventh embodiments in that: and sixthly, the preservative is methyl chloroisothiazolinone or methyl isothiazolinone. The others are the same as the sixth or seventh embodiments.
The specific implementation method nine: this embodiment differs from one of the sixth to eighth embodiments in that: secondly, adding 95 percent ethanol in percentage by mass into the Wudalianchi volcanic mud micro powder, and extracting for 2 hours at constant temperature under the condition of 45-50 ℃ to obtain supernatant extracted by an alcohol phase and precipitate extracted by the primary alcohol phase; and in the second step, the volume ratio of the Wudalianchi volcanic mud micro powder to 95 percent ethanol in percentage by mass is 1: 3. The others are the same as the embodiments six to eight.
The detailed implementation mode is ten: the present embodiment differs from one of the sixth to ninth embodiments in that: adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in the Wudalianchi pool, and extracting at a constant temperature of 75 ℃ for 60min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction; and the volume ratio of the precipitate obtained after the alcohol phase extraction in the third step to the Wudalianchi natural mineral water is 1: 3. The others are the same as in the sixth to ninth embodiments.
The following examples were used to demonstrate the beneficial effects of the present invention:
the first embodiment is as follows:
the preparation method of the volcanic mud cleansing milk comprises the following steps:
firstly, weighing at one time:
weighing 30 parts of Wudalianchi volcanic slime, 5 parts of olive oil, 5 parts of linseed oil, 5 parts of wheat germ oil, 5 parts of sweet almond oil, 3 parts of jojoba oil and 2 parts of coconut oil according to parts by mass;
secondly, preparing a mud phase alcohol extract:
firstly, 30 parts of the Wudalianchi volcanic slime is frozen and dried at the temperature of minus 40 ℃, then ground at the temperature of 25 ℃ until the granularity is 2-5 mu m, and the Wudalianchi volcanic slime micro powder is obtained;
secondly, adding 95 percent ethanol in percentage by mass into the Wudalianchi volcanic mud micro powder, and extracting for 2 hours at a constant temperature at 45 ℃ to obtain supernatant of alcohol phase extraction and precipitate after primary alcohol phase extraction;
the volume ratio of the Wudalianchi volcanic mud micro powder to 95 percent ethanol in percentage by mass is 1: 3;
thirdly, repeating the precipitate after the primary alcohol phase extraction for three times according to the second step, and combining the supernatant liquid of the alcohol phase extraction to obtain an alcohol extraction liquid and the precipitate after the alcohol phase extraction;
fourthly, concentrating the alcohol extract under reduced pressure to 15 percent of the original volume to obtain a mud-phase alcohol extract;
thirdly, preparing a mud-phase water extract:
adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in the Wudalianchi pool, and extracting at a constant temperature of 75 ℃ for 60min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction;
the volume ratio of the precipitate after alcohol phase extraction to the Wudalianchi natural mineral water is 1: 3; the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1: 1.5;
secondly, repeating the precipitate obtained after the primary water phase extraction for three times according to the third step, and combining the supernatant obtained after the water phase extraction to obtain a water extracting solution and the precipitate obtained after the water phase extraction;
thirdly, decompressing and concentrating the water extract to 15 percent of the original volume to obtain a mud-phase water extract;
fourthly, preparing oil phase liquid:
mixing 5 parts of olive oil, 5 parts of linseed oil, 5 parts of wheat germ oil, 5 parts of sweet almond oil, 3 parts of jojoba oil and 2 parts of coconut oil to obtain an oil phase, heating the oil phase to 75 ℃, and uniformly stirring to obtain an oil phase liquid;
fifthly, homogenizing:
uniformly mixing the mud-phase alcohol extract obtained in the second step, the mud-phase water extract obtained in the third step and the oil-phase liquid obtained in the fourth step, adding the precipitate obtained in the third step after water-phase extraction, homogenizing for 0.5h by using a high-speed homogenizer at the rotation speed of 10000r/min, repeating the homogenization process for three times, and cooling to room temperature to obtain a volcanic mud extract of the quinquepetary pond and a mixture of the precipitate and the oil-phase liquid;
sixthly, weighing for the second time:
weighing 25 parts of natural Wudalianchi mineral water, 25 parts of Wudalianchi volcanic mud extract, a mixture of a precipitate and an oil phase liquid, 0.2 part of mannitol, 0.2 part of rhamnose, 0.02 part of tea tree essential oil, 0.02 part of aloe essential oil, 0.01 part of rosemary essential oil, 0.2 part of butanediol, 0.2 part of centella asiatica extract, 0.2 part of aloe extract, 0.2 part of ginseng extract, 0.2 part of raspberry extract, 0.1 part of phenoxyethanol and 0.05 part of preservative according to the mass parts;
the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1: 1.5;
seventhly, mixing:
uniformly mixing 25 parts of the weighed volcanic mud extract of the Wudalianchi, 25 parts of the natural mineral water of the Wudalianchi, 0.2 part of mannitol, 0.2 part of rhamnose, 0.02 part of tea tree essential oil, 0.02 part of aloe essential oil, 0.01 part of rosemary essential oil, 0.2 part of butanediol, 0.2 part of centella extract, 0.2 part of aloe extract, 0.2 part of ginseng extract, 0.2 part of raspberry extract, 0.1 part of phenoxyethanol and 0.05 part of preservative to obtain the volcanic mud makeup removing milk.
The volcanic slime of the Wudalianchi is collected in a slime layer of 80-150 cm below the surface of the mineral slime zone of the Wudalianchi Yaquan wetland in the step one.
And sixthly, the preservative is methyl chloroisothiazolinone.
Cleaning and skin care performance test:
100 volunteers were recruited, all women who made up daily, using method: after shaking uniformly, a proper amount of the face cream is applied to the palm or the cosmetic cotton, the face cream is wiped on the face, the thick and heavy part of the color cosmetics is increased, and after dirt of the color cosmetics is dissolved out, the daily skin cleaning link is carried out. It is administered once daily for 4 weeks.
The volunteers were tested for oil control (skin tester) and moisture retention (stratum corneum moisture tester), and the average values of the test results are shown in table 1.
TABLE 1 oil control and moisture retention test results
| Oil control | Moisture retention | |
| Before makeup removal | Oil content: 26 percent of | Water content: 22 percent |
| After the volcanic mud makeup removing cream is removed | Oil content: 12 percent of | Water content: 54 percent |
TABLE 2 survey of skin-care and makeup cleansing in use
| Allergic conditions (example) | Refreshing property (example) | Elasticity (example) | Cleaning property (example) | |
| Is very good | 95 | 99 | 96 | 99 |
| Good taste | 5 | 1 | 4 | 1 |
| Is preferably used | 0 | 0 | 3 | 0 |
| In general | 0 | 0 | 0 | 0 |
| Difference (D) | 0 | 0 | 0 | 0 |
The results of the investigation on the skin-care and makeup cleansing effects of the volunteers were respectively shown in table 2, and it can be seen from the table that the volcanic mud makeup remover prepared in the first example has good skin-care and makeup cleansing effects.
Inorganic element detection was performed on the volcanic mud makeup remover by ICP-MS method, and SiO was performed on the volcanic mud makeup remover as shown in Table 33 2Detection of the content of SiO3 2-The content of (A) is 18.3mg/kg, so that the volcanic mud cleansing milk prepared in the example I better retains the effective skin care ingredient (Ca) in the volcanic mud of Wudalianchi2+，Mg2+，K+，Na+，Zn2+，SiO3 2-And various mineral ions) and contains moderate trace elements and organic acids, and is mild and easy to absorb.
TABLE 3 inorganic elements and contents (μ g/g) of the volcanic mud makeup remover prepared in example one
In this example, the pH value of Wudalianchi natural mineral water (20-25 parts) is close to that of skin, and the pH value is 5.5.
In the embodiment, no emulsifier is added, and a stable emulsion system is achieved by only preparing the Wudalianchi volcanic slime into particles with the optimal size (the particle size is 2-5 mu m in the second step), and utilizing the self-emulsifying capacity of the Wudalianchi volcanic slime.
Emulsion stability test
The prepared volcanic mud makeup removing cream is diluted by 100 times after being placed for different time, the stability of the volcanic mud makeup removing cream is represented by particle size analysis, and the particle size of liquid drops is determined by a dynamic light scattering method: diluting the volcanic mud makeup removing lotion by 100 times, carrying out ultrasonic uniform measurement, wherein the measurement times are 10 times, the measurement temperature is 25 ℃, and the average particle size is automatically calculated and generated by software.
TABLE 4 droplet size
| Time (minutes) | 5 | 10 | 30 | 60 |
| Effective particle size (nm) | 278.6 | 288.1 | 314.9 | 317.1 |
As can be seen from the table, the effective particle size of the droplets changed very little and no delamination or demulsification was observed. It was confirmed that the emulsifying effect was stable.
Claims (10)
1. A volcanic mud makeup removing milk is characterized in that the volcanic mud makeup removing milk is prepared by 20-25 parts of Wudalianchi natural mineral water, 20-25 parts of Wudalianchi volcanic mud extract, a mixture of precipitate and oil phase liquid, 0.1-0.5 part of mannitol, 0.1-0.5 part of rhamnose, 0.01-0.1 part of tea tree essential oil, 0.01-0.1 part of aloe essential oil, 0.01-0.1 part of rosemary essential oil, 0.1-0.5 part of butanediol, 0.1-1 part of centella asiatica extract, 0.1-1 part of aloe extract, 0.1-1 part of ginseng extract, 0.1-1 part of raspberry extract, 0.01-0.5 part of phenoxyethanol and 0.05-0.1 part of preservative by mass;
the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
the mixture of the volcanic mud extract of the Wudalianchi and the sediment and the oil phase liquid is prepared by the following steps:
firstly, weighing:
weighing 30-40 parts of Wudalianchi volcanic slime, 2-5 parts of olive oil, 2-5 parts of linseed oil, 2-5 parts of wheat germ oil, 2-5 parts of sweet almond oil, 2-3 parts of jojoba oil and 2-3 parts of coconut oil according to parts by mass;
secondly, preparing a mud phase alcohol extract:
firstly, 30 to 40 parts of the Wudalianchi volcanic slime is frozen and dried at the temperature of minus 50 to minus 35 ℃, then ground at the temperature of 20 to 30 ℃ until the granularity is 2 to 5 mu m, and the Wudalianchi volcanic slime micro powder is obtained;
secondly, adding 85-95% of ethanol by mass percent into the Wudalianchi volcanic mud micro powder, and extracting for 1.5-2 h at constant temperature under the condition of 40-50 ℃ to obtain supernatant extracted by an alcohol phase and precipitate extracted by the alcohol phase at one time;
the volume ratio of the Wudalianchi volcanic mud micro powder to 85-95% of ethanol in percentage by mass is 1 (3-5);
thirdly, repeating the precipitate after the primary alcohol phase extraction for three times according to the second step, and combining the supernatant liquid of the alcohol phase extraction to obtain an alcohol extraction liquid and the precipitate after the alcohol phase extraction;
fourthly, concentrating the alcohol extract under reduced pressure to 10 to 30 percent of the original volume to obtain a mud-phase alcohol extract;
thirdly, preparing a mud-phase water extract:
adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in a Wudalianchi pool, and extracting at a constant temperature of 60-75 ℃ for 60-90 min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction;
the volume ratio of the precipitate after alcohol phase extraction to the Wudalianchi natural mineral water is 1 (3-5); the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
secondly, repeating the precipitate obtained after the primary water phase extraction for three times according to the third step, and combining the supernatant obtained after the water phase extraction to obtain a water extracting solution and the precipitate obtained after the water phase extraction;
thirdly, decompressing and concentrating the water extract to 10-30% of the original volume to obtain a mud-phase water extract;
fourthly, preparing oil phase liquid:
mixing 2 to 5 parts of olive oil, 2 to 5 parts of linseed oil, 2 to 5 parts of wheat germ oil, 2 to 5 parts of sweet almond oil, 2 to 3 parts of jojoba oil and 2 to 3 parts of coconut oil to obtain an oil phase, heating the oil phase to the temperature of between 70 and 85 ℃, and uniformly stirring to obtain an oil phase liquid;
fifthly, homogenizing:
and uniformly mixing the mud-phase alcohol extract, the mud-phase water extract and the oil-phase liquid, then adding the precipitate obtained after the water-phase extraction, homogenizing for 0.5-1 h by using a high-speed homogenizer at the rotating speed of 8000-10000 r/min, repeating the homogenization process for three times, and cooling to room temperature to obtain the volcanic mud extract of the quintuplerian pool and the mixture of the precipitate and the oil-phase liquid.
2. The volcanic mud makeup removing cream as claimed in claim 1, wherein said volcanic mud of Wudalianchi in step one is collected from 80-150 cm of mud layer under the surface of the mineral mud zone of Wudalianchi Yaquan wetland.
3. The volcanic mud makeup removing lotion according to claim 1, wherein said preservative is methylchloroisothiazolinone or methylisothiazolinone.
4. The volcanic mud makeup removing cream as claimed in claim 1, characterized in that in the second step, 95% by mass of ethanol is added into the volcanic mud micropowder of Wudalianchi, and the mixture is extracted at a constant temperature of 45-50 ℃ for 2 hours to obtain supernatant of alcohol phase extraction and precipitate after primary alcohol phase extraction; and in the second step, the volume ratio of the Wudalianchi volcanic mud micro powder to 95 percent ethanol in percentage by mass is 1: 3.
5. The volcanic mud makeup removing lotion as claimed in claim 1, wherein in step three, the alcohol phase extracted precipitate obtained in step two is added into natural mineral water in Wudalianchi, and extraction is carried out at a constant temperature of 75 ℃ for 60min to obtain supernatant of aqueous phase extraction and precipitate of primary aqueous phase extraction; and the volume ratio of the precipitate obtained after the alcohol phase extraction in the third step to the Wudalianchi natural mineral water is 1: 3.
6. The preparation method of the volcanic mud makeup removing lotion as claimed in claim 1, wherein the preparation method of the volcanic mud makeup removing lotion is carried out according to the following steps:
firstly, weighing at one time:
weighing 30-40 parts of Wudalianchi volcanic slime, 2-5 parts of olive oil, 2-5 parts of linseed oil, 2-5 parts of wheat germ oil, 2-5 parts of sweet almond oil, 2-3 parts of jojoba oil and 2-3 parts of coconut oil according to parts by mass;
secondly, preparing a mud phase alcohol extract:
firstly, 30 to 40 parts of the Wudalianchi volcanic slime is frozen and dried at the temperature of minus 50 to minus 35 ℃, then ground at the temperature of 20 to 30 ℃ until the granularity is 2 to 5 mu m, and the Wudalianchi volcanic slime micro powder is obtained;
secondly, adding 85-95% of ethanol by mass percent into the Wudalianchi volcanic mud micro powder, and extracting for 1.5-2 h at constant temperature under the condition of 40-50 ℃ to obtain supernatant extracted by an alcohol phase and precipitate extracted by the alcohol phase at one time;
the volume ratio of the Wudalianchi volcanic mud micro powder to 85-95% of ethanol in percentage by mass is 1 (3-5);
thirdly, repeating the precipitate after the primary alcohol phase extraction for three times according to the second step, and combining the supernatant liquid of the alcohol phase extraction to obtain an alcohol extraction liquid and the precipitate after the alcohol phase extraction;
fourthly, concentrating the alcohol extract under reduced pressure to 10 to 30 percent of the original volume to obtain a mud-phase alcohol extract;
thirdly, preparing a mud-phase water extract:
adding the precipitate obtained in the second step after alcohol phase extraction into natural mineral water in a Wudalianchi pool, and extracting at a constant temperature of 60-75 ℃ for 60-90 min to obtain supernatant obtained by water phase extraction and precipitate obtained by primary water phase extraction;
the volume ratio of the precipitate after alcohol phase extraction to the Wudalianchi natural mineral water is 1 (3-5); the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
secondly, repeating the precipitate obtained after the primary water phase extraction for three times according to the third step, and combining the supernatant obtained after the water phase extraction to obtain a water extracting solution and the precipitate obtained after the water phase extraction;
thirdly, decompressing and concentrating the water extract to 10-30% of the original volume to obtain a mud-phase water extract;
fourthly, preparing oil phase liquid:
mixing 2 to 5 parts of olive oil, 2 to 5 parts of linseed oil, 2 to 5 parts of wheat germ oil, 2 to 5 parts of sweet almond oil, 2 to 3 parts of jojoba oil and 2 to 3 parts of coconut oil to obtain an oil phase, heating the oil phase to the temperature of between 70 and 85 ℃, and uniformly stirring to obtain an oil phase liquid;
fifthly, homogenizing:
uniformly mixing the mud-phase alcohol extract obtained in the second step, the mud-phase water extract obtained in the third step and the oil-phase liquid obtained in the fourth step, adding the precipitate obtained in the third step after water-phase extraction, homogenizing for 0.5-1 h by using a high-speed homogenizer at the rotating speed of 8000-10000 r/min, repeating the homogenization process for three times, and cooling to room temperature to obtain a mixture of the volcanic mud extract and the precipitate with the oil-phase liquid in the Wudalianchi pool;
sixthly, weighing for the second time:
weighing 20 to 25 parts of natural mineral water of the Wudalianchi, 20 to 25 parts of volcanic mud extract of the Wudalianchi, 0.1 to 0.5 part of mannitol, 0.1 to 0.5 part of rhamnose, 0.01 to 0.1 part of tea tree essential oil, 0.01 to 0.1 part of aloe essential oil, 0.01 to 0.1 part of rosemary essential oil, 0.1 to 0.5 part of butanediol, 0.1 to 1 part of centella asiatica extract, 0.1 to 1 part of aloe extract, 0.1 to 1 part of ginseng extract, 0.1 to 1 part of raspberry extract, 0.01 to 0.5 part of phenoxyethanol and 0.05 to 0.1 part of preservative according to the mass parts;
the natural Wudalianchi mineral water is prepared by mixing Wudalianchi bicarbonate mineral water and Wudalianchi metasilicic acid mineral water, wherein the volume ratio of the Wudalianchi bicarbonate mineral water to the Wudalianchi metasilicic acid mineral water is 1 (1-2);
seventhly, mixing:
weighing 20 to 25 parts of the volcanic mud extract of the Wudalianchi and the mixture of the sediment and the oil phase liquid, 20 to 25 parts of the natural mineral water of the Wudalianchi, 0.1 to 0.5 part of mannitol, 0.1 to 0.5 part of rhamnose, 0.01 to 0.1 part of tea tree essential oil, 0.01 to 0.1 part of aloe essential oil, 0.01 to 0.1 part of rosemary essential oil, 0.1 to 0.5 part of butanediol, 0.1 to 1 part of centella asiatica extract, 0.1 to 1 part of aloe extract, 0.1 to 1 part of ginseng extract, 0.1 to 1 part of raspberry extract, 0.01 to 0.5 part of phenoxyethanol and 0.05 to 0.1 part of preservative, and uniformly mixing to obtain the volcanic mud makeup removing milk.
7. The preparation method of the volcanic mud makeup removing lotion as claimed in claim 6, wherein said volcanic mud of Wudalianchi in step one is collected from a 80-150 cm layer of ore mud under the surface of the mineral mud zone of Wudalianchi Yaquan wetland.
8. The method for preparing the volcanic mud makeup removing lotion according to claim 6, wherein the preservative in the sixth step is methylchloroisothiazolinone or methylisothiazolinone.
9. The preparation method of the volcanic mud makeup removing cream as claimed in claim 6, characterized in that in the second step, 95% by mass of ethanol is added into the volcanic mud micropowder of Wudalianchi, and the mixture is extracted at a constant temperature of 45-50 ℃ for 2 hours to obtain supernatant of alcohol phase extraction and precipitate of primary alcohol phase extraction; and in the second step, the volume ratio of the Wudalianchi volcanic mud micro powder to 95 percent ethanol in percentage by mass is 1: 3.
10. The preparation method of volcanic mud makeup removing lotion as claimed in claim 6, wherein in step three, the alcohol phase extracted precipitate obtained in step two is added into natural mineral water in Wudalianchi, and extraction is carried out at a constant temperature of 75 ℃ for 60min to obtain a supernatant of aqueous phase extraction and a precipitate of primary aqueous phase extraction; and the volume ratio of the precipitate obtained after the alcohol phase extraction in the third step to the Wudalianchi natural mineral water is 1: 3.
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