CN110151628A - A kind of rose lipstick and preparation method thereof - Google Patents
A kind of rose lipstick and preparation method thereof Download PDFInfo
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- CN110151628A CN110151628A CN201910541694.2A CN201910541694A CN110151628A CN 110151628 A CN110151628 A CN 110151628A CN 201910541694 A CN201910541694 A CN 201910541694A CN 110151628 A CN110151628 A CN 110151628A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention provides a kind of rose lipsticks and preparation method thereof, belong to cosmetic field.Rose lipstick of the present invention includes following components in percentage by weight: Tujue's rose floral wax of 0.5-4%, the jojoba seed oil of 25-40%, the olive oil of 25-40%, the tocopherol of 0.1-0.5% and the Flos Rosae Rugosae extract of 0.1-3%, pass through Tujue's rose floral wax, jojoba seed oil, olive oil, cooperateing with crease-resistant effect and there is excellent anti-wrinkle effect between tocopherol and Flos Rosae Rugosae extract, energy deep layer moistens lip, slow down lip roughness and cheilogramma depth, and it is not required to additionally add essence, pigment, preservative, just there is pleasant fragrance, strong color and good anti-corrosion ability, natural and safety, furthermore, the preparation method simple process of rose lipstick of the present invention, it is easy to industrialized production.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to a kind of rose lipstick and preparation method thereof.
Background technique
Lip drying is very universal phenomenon, especially autumn and winter, in order to prevent with alleviate drying, people often apply lip
Cream.But currently marketed lipstick has the following problems more:
(1) raw material is chemical synthesis substance, is easy intake in vivo after being applied to lip, generates risk；
(2) mostly using the synthesis material of petroleum resources and to stick lipstick skin sense greasy, cause user experience poor；
(3) close membrane is formed in lip, block cell breathes and breathes freely, and cannot form natural skin care barrier, no deep layer
The effect of moisturizing, full lips；
(4) pigment, essence or preservative containing synthesis, have certain irritation；
(5) the conceptual addition of both effectiveness ingredient, additive amount is few, and lipstick is caused to have no actual effect.
Therefore, it is necessary in view of the above-mentioned problems, develop a natural safety, not stick greasy and effective lipstick.
Summary of the invention
It is an object of the invention to overcome drawbacks described above in the prior art, a kind of rose lipstick and its preparation side are provided
Method.
To achieve the above object, the technical solution adopted by the present invention are as follows:
In a first aspect, it includes following components in percentage by weight: 0.5-4% the present invention provides a kind of rose lipstick
Tujue's rose floral wax, the jojoba seed oil of 25-40%, the olive oil of 25-40%, 0.1-0.5% tocopherol and
The Flos Rosae Rugosae extract of 0.1-3%；Preferably, it includes 2% Tujue's rose floral wax, 32% jojoba seed oil, 33.7%
Olive oil, 0.3% tocopherol and 2% Flos Rosae Rugosae extract.Tujue's rose floral wax has inhibition to elastoser
Effect has skin softening and anti-wrinkle effect, in addition, also having rose fragrance, good smell；Jojoba seed oil is not easy to be oxidized,
Viscosity variation is small under high temperature and pressure, has excellent tactile and ductility, is easily absorbed by the skin, and is outstanding in cosmetics
Finish, moisturizing agent and moisturizer；Olive oil is food-grade Extra Virgin, contains a large amount of monounsaturated fatty acids
With the antioxidant such as vitamin, while deep layer nourishes, repairs lip, moreover it is possible to slow down the aging of lip skin；Tocopherol,
Free radical can not only be removed, protect intracellular lipoprotein and unsaturated fatty acid, moreover it is possible to for skin provide long-acting hair conditioning with
Moisture retention；Flos Rosae Rugosae extract not only assigns lipstick strong exterior beauty, also has effects that crease-resistant, moisturizing, antibacterial anti-inflammatory.
Applicant has found after study, when rose lipstick contains Tujue's rose floral wax, the 25- that weight percent is respectively 0.5-4%
40% jojoba seed oil, the olive oil of 25-40%, the tocopherol of 0.1-0.5% and 0.1-3% Flos Rosae Rugosae extract
When, under the synergistic effect of Tujue's rose floral wax, jojoba seed oil, olive oil, tocopherol and Flos Rosae Rugosae extract, lipstick
Energy deep layer moistens lip, has good anti-wrinkle effect, especially when lipstick contains Tujue rose that weight percent is respectively 2%
When floral wax, 32% jojoba seed oil, 33.7% olive oil, 0.3% tocopherol and 2% Flos Rosae Rugosae extract,
It is more preferable to the moist of lip, anti-wrinkle effect.
Preferably, the Flos Rosae Rugosae extract by fresh roseleaf successively through extraction, filtering, concentration preparation and
At；The extraction is using the ethanol solution of the 50-90% of pH=1-4 as solvent, solid-liquid ratio 1g:4-8mL, Extracting temperature 40-
80 DEG C, extraction time is 1-4 times, extracts 20-50min every time；The mass concentration of the Flos Rosae Rugosae extract is 70-90%.
It is further preferred that described extract using 70% ethanol solution of pH=2.5 as solvent, solid-liquid ratio 1g:
6mL, Extracting temperature are 60 DEG C, and extraction time is 2 times, and each extraction time is 30min；The quality of the Flos Rosae Rugosae extract is dense
Degree is 87%.Thus obtained Flos Rosae Rugosae extract functional component content is higher, both effectiveness more preferable.
Preferably, the rose lipstick also includes Butyrospermum parkii fruit rouge, and Butyrospermum parkii fruit rouge accounts for the rose lipstick weight
10-18%.Butyrospermum parkii fruit rouge is a kind of food grade materials in pure plant source, contains non-saponified ingredient abundant,
It is easily absorbed by the body, the season cracking of skin can not only be prevented, moreover it is possible to further restore and keep the natural elasticity of skin, have
There is deep layer that can also play antiinflammation while moistening effect.
Preferably, the rose lipstick also includes thickener, and the thickener includes to account for the rose lipstick weight 10-
18% candelila wax.Candelila wax is a kind of natural plants wax, has efficient thickening power, can assign lipstick rod-like morphology.
Preferably, the rose lipstick also includes emulsifier, and the emulsifier includes to account for the rose lipstick weight 1-3%
Sucrose oleate.Sucrose oleate is a kind of tasteless nontoxic food grade emulsifier, has splendid biological degradability, can be
System forming liquid crystal structure has very strong emulsifying capacity and emulsion stability.
Preferably, the rose lipstick includes following components in percentage by weight: 2% Tujue's rose floral wax, 32%
Jojoba seed oil, 33.7% olive oil, 0.3% tocopherol, 2% Flos Rosae Rugosae extract, 14% Butyrospermum parkii
Fruit rouge, 14% candelila wax and 2% sucrose oleate.The lipstick is applied to that lip is salubrious, it is greasy not stick.
Second aspect, the present invention provides a kind of preparation methods of rose lipstick comprising following steps:
(1) candelila wax and Tujue's rose floral wax are mixed, is heated to 80-85 DEG C, open stirring, setting revolving speed is 400-
500r/min, stirring obtain A phase materials to being uniformly mixed；
(2) Butyrospermum parkii fruit rouge, jojoba seed oil, olive oil and sucrose oleate are added in the A phase materials,
Under the conditions of 80-85 DEG C after mixing evenly, 10-20min is kept the temperature, is cooled to 65-70 DEG C later, tocopherol is added and rose mentions
Object is taken, is stirred evenly, is discharged up to the rose lipstick.
It preferably, further include step (a) before the step (1), the step (a) is by fresh roseleaf
It is extracted 1-4 times at 40-80 DEG C in pH=1-4, the ethanol solution that volumetric concentration is 50-90%, extracts 20-50min every time,
Combined extract, filtering, being concentrated into mass concentration is 70-90% up to the Flos Rosae Rugosae extract, wherein extracts the material of use
Liquor ratio is 1g:4-8mL；It is further preferred that the step (a) is that fresh roseleaf is dense in pH=2.5%, volume
Degree extracts 30-40min, combined extract, filtering is concentrated into matter to extract 2 times at 60 DEG C in 70% ethanol solution every time
Measuring concentration is 87% to get the Flos Rosae Rugosae extract, wherein extracts the solid-liquid ratio used as 1g:6mL.
Compared with prior art, the present invention has the following advantages and beneficial effects:
(1) rose lipstick of the present invention is by by Tujue's rose floral wax, jojoba seed oil, olive oil, tocopherol and rose
Rare flower extract is rationally used in compounding and has good anti-wrinkle effect, and energy deep layer moistens lip, slows down lip roughness and lip
Line depth.
(2) raw material sources of rose lipstick of the present invention are natural, good with skin affinity, and mild safety is not required to additionally add
Essence, pigment, preservative just have pleasant fragrance, strong color and good anti-corrosion ability.
(3) rose lipstick of the present invention is salubrious, it is greasy not stick, and user is enabled to have good usage experience.
(4) the preparation method simple process of rose lipstick of the present invention, condition is controllable, easy to industrialized production.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1-7
Embodiment 1-7 is a kind of embodiment of rose lipstick of the present invention, and the composition of these rose lipsticks is as shown in table 1,
Wherein Tujue rose floral wax is the Rose Wax purchased from Appalachian Valley Natural Products company.
Composition/% of rose lipstick in 1 embodiment 1-7 of table
Rose lipstick in embodiment 1-7 is prepared by following steps:
(1) candelila wax and Tujue's rose floral wax are mixed, is heated to 80-85 DEG C, open stirring, setting revolving speed is 400-
500r/min, stirring obtain A phase materials to being uniformly mixed；
(2) Butyrospermum parkii fruit rouge, jojoba seed oil, olive oil and sucrose oleate are added in the A phase materials,
Under the conditions of 80-85 DEG C after mixing evenly, 10-20min is kept the temperature, is cooled to 65-70 DEG C later, tocopherol is added and rose mentions
Object is taken, is stirred evenly, is discharged up to the rose lipstick.
Wherein, the Flos Rosae Rugosae extract in embodiment 1 is prepared by the following method: by fresh roseleaf in pH
=1, after extracting 20min at 40 DEG C in the ethanol solution that volumetric concentration is 50%, filtering, being concentrated into mass concentration is 70%,
Up to the Flos Rosae Rugosae extract, wherein extract the solid-liquid ratio used as 1g:4mL；
Flos Rosae Rugosae extract in embodiment 2 is prepared by the following method: by fresh roseleaf in pH=
2.5%, it is extracted 2 times at 60 DEG C in the ethanol solution that volumetric concentration is 70%, extracts 30-40min every time, combined extract,
Filtering, being concentrated into mass concentration is 87% to get the Flos Rosae Rugosae extract, wherein extracts the solid-liquid ratio used as 1g:6mL；
Flos Rosae Rugosae extract in embodiment 3 is prepared by the following method: by fresh roseleaf pH=4,
It is extracted 4 times at 80 DEG C in the ethanol solution that volumetric concentration is 90%, extracts 50min every time, combined extract filters, concentration
It is 90% to get the Flos Rosae Rugosae extract to mass concentration, wherein extract the solid-liquid ratio used as 1g:8mL；
Flos Rosae Rugosae extract preparation method in embodiment 4-7 is identical as in embodiment 2.
Comparative example 1
Comparative example 1 is a kind of lipstick, and the lipstick is by candelila wax, Butyrospermum parkii fruit rouge, jojoba seed oil, olea europaea fruit
Oil, sucrose oleate, tocopherol and Flos Rosae Rugosae extract are prepared, wherein candelila wax, Butyrospermum parkii fruit rouge and sucrose oil
The content of acid esters is same as Example 2, and jojoba seed oil, olive oil, the ratio of tocopherol and Flos Rosae Rugosae extract are closed
System is also same as Example 2, and the preparation method of Flos Rosae Rugosae extract is same as Example 2.
Comparative example 2
Comparative example 2 is a kind of lipstick, and the lipstick is by candelila wax, Tujue's rose floral wax, Butyrospermum parkii fruit rouge, olea europaea fruit
Oil, sucrose oleate, tocopherol and Flos Rosae Rugosae extract are prepared, wherein candelila wax, Butyrospermum parkii fruit rouge and sucrose oil
The content of acid esters is same as Example 2, Tujue's rose floral wax, olive oil, the ratio of tocopherol and Flos Rosae Rugosae extract
Relationship is also same as Example 2, and the preparation method of Flos Rosae Rugosae extract is same as Example 2.
Comparative example 3
Comparative example 3 is a kind of lipstick, and the lipstick is by candelila wax, Tujue's rose floral wax, Butyrospermum parkii fruit rouge, Jojoba seed
Oil, sucrose oleate, tocopherol and Flos Rosae Rugosae extract are prepared, wherein candelila wax, Butyrospermum parkii fruit rouge and sucrose oil
The content of acid esters is same as Example 2, Tujue's rose floral wax, jojoba seed oil, the ratio of tocopherol and Flos Rosae Rugosae extract
Relationship is also same as Example 2, and the preparation method of Flos Rosae Rugosae extract is same as Example 2.
Comparative example 4
Comparative example 4 is a kind of lipstick, and the lipstick is by candelila wax, Tujue's rose floral wax, Butyrospermum parkii fruit rouge, Jojoba seed
Oil, olive oil, sucrose oleate and Flos Rosae Rugosae extract are prepared, wherein candelila wax, Butyrospermum parkii fruit rouge and sugarcane
The content of sugar and oil acid esters is same as Example 2, and Tujue's rose floral wax, jojoba seed oil, olive oil and rose are extracted
The proportionate relationship of object is also same as Example 2, and the preparation method of Flos Rosae Rugosae extract is same as Example 2.
Comparative example 5
Comparative example 5 is a kind of lipstick, and the lipstick is by candelila wax, Tujue's rose floral wax, Butyrospermum parkii fruit rouge, Jojoba seed
Oil, olive oil, sucrose oleate and tocopherol are prepared, wherein candelila wax, Butyrospermum parkii fruit rouge and sucrose oleic acid
The content of ester is same as Example 2, Tujue's rose floral wax, jojoba seed oil, the proportionate relationship of olive oil and tocopherol
Also same as Example 2.
The female subjects that 60 ages are 45-50 years old are divided into 6 groups by applicant, and every group of subject is using test specimens
Before product, lip roughness and cheilogramma depth are close, specific as shown in table 2.Every group of subject uses a kind of test sample, continuously makes
With 4 weeks, the 0th week (i.e. before use), the 1st week, the 2nd are being used using MicroSkinII Multi-functional skin mirror image analysis system
Roughness and cheilogramma depth on the right side of week, week 3 and Week 4 test each group subject lower lips, test sample is 2 He of embodiment
Lipstick in comparative example 1-5, test result are shown in Table 3, and related calculation formula is as follows:
Certain lipstick using n-th week lip roughness changing value=(using the lipstick after n-th week lip roughness-use this
Lip roughness before lipstick)/use lip roughness × 100% before the lipstick；
Certain lipstick uses the sum of this group of lip roughness changing value of n-th week lip roughness average change value=the n-th week ÷
5；
Certain lipstick using n-th week cheilogramma change in depth value=(using the lipstick after n-th week cheilogramma depth-use the lipstick
Preceding cheilogramma depth)/use cheilogramma depth × 100% before the lipstick；
Certain lipstick uses the sum of this group of cheilogramma change in depth value of n-th week cheilogramma depth-averaged changing value=the n-th week ÷ 5.
Table 2 uses lip mean roughness and cheilogramma mean depth before sample
| Group | Lip mean roughness | Cheilogramma mean depth |
| Embodiment 2 | 9.432 | 35.589 |
| Comparative example 1 | 9.569 | 36.421 |
| Comparative example 2 | 9.489 | 36.022 |
| Comparative example 3 | 9.665 | 35.944 |
| Comparative example 4 | 9.443 | 36.510 |
| Comparative example 5 | 9.589 | 36.020 |
3 lip test result of table
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should
Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention
And range.
Claims (10)
1. a kind of rose lipstick, it is characterised in that: the rose lipstick includes following components in percentage by weight: 0.5-4%'s
Tujue's rose floral wax, the jojoba seed oil of 25-40%, the olive oil of 25-40%, 0.1-0.5% tocopherol and 0.1-
3% Flos Rosae Rugosae extract.
2. rose lipstick according to claim 1, it is characterised in that: the rose lipstick includes following weight percent
Component: 2% Tujue's rose floral wax, 32% jojoba seed oil, 33.7% olive oil, 0.3% tocopherol and 2%
Flos Rosae Rugosae extract.
3. rose lipstick according to claim 1 or 2, it is characterised in that: the Flos Rosae Rugosae extract is by fresh rose
Petal is successively prepared by extracting, filtering, be concentrated；The extraction is molten with the ethanol solution of the 50-90% of pH=1-4
Matchmaker, solid-liquid ratio 1g:4-8mL, Extracting temperature are 40-80 DEG C, and extraction time is 1-4 times, extract 20-50min every time；The rose
The mass concentration of rare flower extract is 70-90%.
4. rose lipstick according to claim 1 or 2, it is characterised in that: the Flos Rosae Rugosae extract is by fresh rose
Petal is successively prepared by extracting, filtering, be concentrated；The extraction is using 70% ethanol solution of pH=2.5 as solvent, material
Liquor ratio is 1g:6mL, and Extracting temperature is 60 DEG C, and extraction time is 2 times, extracts 30min every time；The matter of the Flos Rosae Rugosae extract
Measuring concentration is 87%.
5. rose lipstick according to claim 1 or 2, it is characterised in that: the rose lipstick also includes Butyrospermum parkii fruit
Rouge, Butyrospermum parkii fruit rouge account for the 10-18% of the rose lipstick weight.
6. rose lipstick according to claim 1 or 2, it is characterised in that: the rose lipstick also includes thickener, described
Thickener includes the candelila wax for accounting for the rose lipstick weight 10-18%.
7. rose lipstick according to claim 1 or 2, it is characterised in that: the rose lipstick also includes emulsifier, described
Emulsifier includes the sucrose oleate for accounting for the rose lipstick weight 1-3%.
8. rose lipstick according to claim 1 or 2, it is characterised in that: the rose lipstick includes following weight percent
The component of ratio: 2% Tujue's rose floral wax, 32% jojoba seed oil, 33.7% olive oil, 0.3% tocopherol,
2% Flos Rosae Rugosae extract, 14% Butyrospermum parkii fruit rouge, 14% candelila wax and 2% sucrose oleate.
9. a kind of preparation method of rose lipstick, it is characterised in that: the preparation method comprises the following steps:
(1) candelila wax and Tujue's rose floral wax are mixed, is heated to 80-85 DEG C, open stirring, setting revolving speed is 400-
500r/min, stirring obtain A phase materials to being uniformly mixed；
(2) Butyrospermum parkii fruit rouge, jojoba seed oil, olive oil and sucrose oleate are added in the A phase materials,
Under the conditions of 80-85 DEG C after mixing evenly, 10-20min is kept the temperature, is cooled to 65-70 DEG C later, tocopherol is added and rose is extracted
Object stirs evenly, and discharges up to the rose lipstick.
10. preparation method according to claim 9, it is characterised in that: further include step before the step (1)
(a), the step (a) be by fresh roseleaf in the ethanol solution that pH=1-4, volumetric concentration are 50-90% in 40-
Extracted 1-4 times at 80 DEG C, extract 20-50min every time, combined extract, filtering, be concentrated into mass concentration be 70-90% to obtain the final product
The Flos Rosae Rugosae extract, wherein extract the solid-liquid ratio used as 1g:4-8mL；Preferably, the step (a) be will be fresh
Roseleaf extracts 2 times at 60 DEG C in pH=2.5%, the ethanol solution that volumetric concentration is 70%, extracts 30- every time
40min, combined extract, filtering, being concentrated into mass concentration is 87% up to the Flos Rosae Rugosae extract, wherein extraction uses
Solid-liquid ratio be 1g:6mL.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910541694.2A CN110151628B (en) | 2019-06-20 | 2019-06-20 | Rose lipstick and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910541694.2A CN110151628B (en) | 2019-06-20 | 2019-06-20 | Rose lipstick and preparation method thereof |
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Cited By (1)
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| CN113440442A (en) * | 2020-08-04 | 2021-09-28 | 长沙黛西生物科技有限公司 | Composition and cosmetic composition for resisting wrinkle, resisting inflammation and keeping moisture of skin, lipstick and preparation method thereof |
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| CN107811891A (en) * | 2017-10-31 | 2018-03-20 | 苏州安特化妆品股份有限公司 | Natural plants nourish lipstick and preparation method thereof |
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| CN107811891A (en) * | 2017-10-31 | 2018-03-20 | 苏州安特化妆品股份有限公司 | Natural plants nourish lipstick and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113440442A (en) * | 2020-08-04 | 2021-09-28 | 长沙黛西生物科技有限公司 | Composition and cosmetic composition for resisting wrinkle, resisting inflammation and keeping moisture of skin, lipstick and preparation method thereof |
| CN113440442B (en) * | 2020-08-04 | 2022-09-20 | 长沙黛西生物科技有限公司 | Composition and cosmetic composition for resisting wrinkle, resisting inflammation and keeping moisture of skin, lipstick and preparation method thereof |
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