CN111494252A - Preparation method of high-adsorption facial mask loaded with modified volcanic cold slime - Google Patents
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract
The invention discloses a preparation method of a high-adsorption facial mask loaded with modified volcanic cold slime, which relates to the field of facial masks and aims to solve the problems that the existing volcanic facial mask has poor skin improvement effect and particularly has poor heavy metal adsorption effect on skin. The mask disclosed by the invention can form a fit state in a short time, the stratum corneum is softened by closely contacting with the stratum corneum, the strong adsorption effect is achieved, meanwhile, the mask is attached to pores, the effects of removing heavy metals, removing grease and dust particles can be achieved by the effects of ion exchange, electrostatic adsorption and the like, and the mask has a strong effect on relieving dark pigment spots and the like. The invention is applied to the field of volcanic mud masks.
Description
Technical Field
The invention relates to the field of masks, and particularly relates to a preparation method of a high-adsorption mask loaded with modified volcanic cold slime.
Background
Consumers who use the cosmetics have the problems that the side effect of the efficacy type cosmetics is obvious, lead and mercury in the cosmetics are deposited, heavy metal residues are left on the face after long-term use, and even if the makeup removing products are used, the heavy metal is deeply deposited by the skin, and common cleaning products cannot be removed; pigmentation is severe over time, resulting in dull skin.
In addition, with the development of society and the improvement of living standard, automobiles are more and more, solid pollutants are added to the air by automobile combustion residues on the air on the street, and the PM2.5 index is higher. When human skin is placed in the air, solid pollutants are adsorbed in pores by the direct contact of the skin, electrostatic adsorption and the like, and the solid pollutants are not easy to clean. Although the volcanic slime facial mask has related products, the facial masks in the market can not effectively play the role of the volcanic slime, have poor skin improvement effect, and particularly have poor heavy metal adsorption effect on the skin.
Disclosure of Invention
The invention aims to solve the problems that the existing volcano mask has poor skin improvement effect, especially poor heavy metal adsorption effect on skin, and provides a preparation method of a high adsorption mask loaded with modified volcano cold slime.
The invention discloses a preparation method of a high-adsorption mask loaded with modified volcanic cold slime, which comprises the following steps of:
firstly, volcanic mud pretreatment:
selecting Wudalianchi volcanic mud with plant roots and stems, freeze-drying at-35-40 ℃, grinding into powder by a grinder, and sieving by a 100-mesh sieve to obtain fine mud powder for later use;
secondly, volcanic mud modification:
mixing 5% hydrochloric acid and 3% sulfuric acid in equal proportion to prepare mixed acid, weighing the slurry powder obtained in the first step, adding the slurry powder into a reaction kettle, adding the mixed acid, reacting for 3-5h at room temperature under the condition of continuous stirring, and washing with deionized water to be neutral; wherein the mass volume ratio of the ore mud powder to the mixed acid is 1: 2-3;
thirdly, preparing the high-adsorption slime mask:
1) dispersing hyaluronic acid, single water-based fruit acid and a preservative in a humectant, adding sodium citrate, sodium chloride and deionized water, heating to 85-90 ℃ in a water phase pot, and stirring the solution uniformly;
2) adding an emulsifier, an antioxidant and tea polyphenol into an emulsifying pot, heating to 80-90 ℃, and dissolving uniformly;
3) mixing an adsorbent, vitamin E and an acid-base regulator, and uniformly stirring the mixture with the substances prepared in the steps 1) and 2) to obtain the load modified volcanic cold slime high adsorption facial mask;
wherein, the adsorbent is the mixture of the volcanic slime, the active carbon and the montmorillonite modified in the second step; the high-adsorption facial mask is prepared from 60-65% of an adsorbent, 8% of a humectant, 5% of an antioxidant, 2% of tea polyphenol, 3% of hyaluronic acid, 2% of vitamin E, 3-5% of single water-based tartaric acid, 1% of an acid-base regulator, 1-3% of an emulsifier, 1% of a preservative and the balance of deionized water in percentage by mass.
The Wudalianchi cold mineral spring mud has rich trace elements and minerals, has certain adsorption performance according to the microstructure characteristics, and has obvious effect in cleaning products. Therefore, the invention develops a high-heavy metal mud adsorption mask product while maintaining the excellent performance of the cold mineral mud.
The Wudalianchi volcanic slime is the result of long-time soaking interaction of volcanic ash and mineral water, so that the Wudalianchi volcanic slime has abundant and various trace elements which are beneficial to skin care, such as lithium, strontium, zinc, iron, manganese, copper, fluorine, selenium, iodine, silicon, tin and mineral components.
The mask disclosed by the invention can form a fit state in a short time, the stratum corneum is softened by closely contacting with the stratum corneum, the strong adsorption effect is achieved, meanwhile, the mask is attached to pores, the effects of removing heavy metals, removing grease and dust particles can be achieved by the effects of ion exchange, electrostatic adsorption and the like, and the mask has a strong effect on relieving dark pigment spots and the like.
Detailed Description
The first embodiment is as follows: the preparation method of the high-adsorption facial mask loaded with the modified volcanic cold slime is carried out according to the following steps:
firstly, volcanic mud pretreatment:
selecting Wudalianchi volcanic mud with plant roots and stems, freeze-drying at-35-40 ℃, grinding into powder by a grinder, and sieving by a 100-mesh sieve to obtain fine mud powder for later use;
secondly, volcanic mud modification:
mixing 5% hydrochloric acid and 3% sulfuric acid in equal proportion to prepare mixed acid, weighing the slurry powder obtained in the first step, adding the slurry powder into a reaction kettle, adding the mixed acid, reacting for 3-5h at room temperature under the condition of continuous stirring, and washing with deionized water to be neutral; wherein the mass volume ratio of the ore mud powder to the mixed acid is 1: 2-3;
thirdly, preparing the high-adsorption slime mask:
1) dispersing hyaluronic acid, single water-based fruit acid and a preservative in a humectant, adding sodium citrate, sodium chloride and deionized water, heating to 85-90 ℃ in a water phase pot, and stirring the solution uniformly;
2) adding an emulsifier, an antioxidant and tea polyphenol into an emulsifying pot, heating to 80-90 ℃, and dissolving uniformly;
3) mixing an adsorbent, vitamin E and an acid-base regulator, and uniformly stirring the mixture with the substances prepared in the steps 1) and 2) to obtain the load modified volcanic cold slime high adsorption facial mask;
wherein, the adsorbent is the mixture of the volcanic slime, the active carbon and the montmorillonite modified in the second step; the high-adsorption facial mask is prepared from 60-65% of an adsorbent, 8% of a humectant, 5% of an antioxidant, 2% of tea polyphenol, 3% of hyaluronic acid, 2% of vitamin E, 3-5% of single water-based tartaric acid, 1% of an acid-base regulator, 1-3% of an emulsifier, 1% of a preservative and the balance of deionized water in percentage by mass.
The second embodiment is as follows: the first difference between the present embodiment and the specific embodiment is: the antioxidant is squalane. The rest is the same as the first embodiment.
The third concrete implementation mode: the first difference between the present embodiment and the specific embodiment is: the humectant is glycerin. The other is the same as the first embodiment.
The fourth concrete implementation mode: the first difference between the present embodiment and the specific embodiment is: the single water-based fruit acid is glycolic acid. The rest is the same as the first embodiment.
The fifth concrete implementation mode: the first difference between the present embodiment and the specific embodiment is: the emulsifier is long carbon chain alcohol. The rest is the same as the first embodiment.
The sixth specific implementation mode: the first difference between the present embodiment and the specific embodiment is: the long carbon chain alcohol is one or more of lauryl alcohol, arachidyl alcohol, stearyl alcohol, cetyl alcohol and palmityl alcohol. The rest is the same as the first embodiment.
The seventh embodiment: the first difference between the present embodiment and the specific embodiment is: the preservative comprises, by weight, 10-15 parts of rosemary extract, 5-10 parts of licorice extract, 2-5 parts of tea extract, 1-5 parts of sophora flavescens extract, 1-5 parts of calendula extract and 20-60 parts of butanediol. The rest is the same as the first embodiment.
The specific implementation mode is eight: the first difference between the present embodiment and the specific embodiment is: the acidity and alkalinity regulator comprises acidity regulator and alkalinity regulator, wherein the acidity regulator is citric acid, and the alkalinity regulator is triethanolamine. The rest is the same as the first specific embodiment.
The beneficial effects of the present invention are demonstrated by the following examples:
example 1
The preparation method of the high-adsorption facial mask loaded with the modified volcanic cold slime is carried out according to the following steps:
firstly, volcanic mud pretreatment:
selecting Wudalianchi volcanic mud with plant roots and stems, freeze-drying at-35 ℃, grinding into powder by a grinding machine, and sieving by a 100-mesh sieve to obtain fine mud powder for later use;
secondly, volcanic mud modification:
mixing 5% hydrochloric acid and 3% sulfuric acid in equal proportion to prepare mixed acid, weighing the slurry powder obtained in the step one, adding the slurry powder into a reaction kettle, adding the mixed acid, reacting for 4 hours at room temperature under the condition of continuous stirring, and washing to be neutral by deionized water; wherein the mass volume ratio of the ore mud powder to the mixed acid is 1: 2;
thirdly, preparing the high-adsorption slime mask:
1) dispersing hyaluronic acid, glycolic acid and antiseptic in glycerol, adding sodium citrate, sodium chloride and deionized water, heating to 85 deg.C in water phase pot, and stirring the solution;
2) adding mixture of palmityl alcohol and lauryl alcohol in equal proportion, squalane and tea polyphenol into an emulsifying pot, heating to 90 ℃, and dissolving uniformly;
3) mixing an adsorbent, vitamin E and an acid-base regulator, and uniformly stirring the mixture with the substances prepared in the steps 1) and 2) to obtain the load modified volcanic cold slime high adsorption facial mask;
wherein, the adsorbent is the mixture of the volcanic slime, the active carbon and the montmorillonite modified in the second step; the high-adsorption facial mask is prepared from 60% of adsorbent, 8% of humectant, 5% of squalane, 2% of tea polyphenol, 3% of hyaluronic acid, 2% of vitamin E, 5% of glycolic acid, 1% of acid-base regulator, 2% of mixture of palm alcohol and lauryl alcohol in equal proportion, 1% of preservative and the balance of deionized water in percentage by mass; the preservative is composed of 10g of rosemary extract, 7g of liquorice extract, 4g of tea extract, 2g of sophora flavescens extract, 2g of calendula extract and 45g of butanediol; the acidity and alkalinity regulator comprises an acidity regulator and an alkalinity regulator, wherein the acidity regulator is citric acid, and the alkalinity regulator is triethanolamine.
Example 2
This example is a comparative example, and is different from example 1 in that: and (3) omitting the modification operation of the Wudalianchi volcanic mud in the first step and the second step, and adding no modified Wudalianchi volcanic mud in the film preparation in the third step. The rest is the same as in example 1.
Example 3
This example is a comparative example, and is different from example 1 in that: the three-side film preparation step is omitted, and the tea polyphenol, the hyaluronic acid and the glycolic acid are prepared. The rest is the same as in example 1.
Example 4
This example is a comparative example, and is different from example 1 in that: the facial mask is prepared by directly using the Wudalianchi fire ore mud containing the plant rootstocks without carrying out the improvement treatment of the first step and the second step. The rest is the same as in example 1.
Example 5
This example is a comparative example, and is different from example 1 in that: selecting Wudalianchi fire-top slime without plant rhizome to prepare the facial mask. The rest is the same as in example 1.
Carrying out heavy metal adsorption verification on the facial mask prepared in the embodiment:
the masks prepared in examples 1 to 3 were subjected to adsorption experiments with equal mass of 10 mmol/L of lead nitrate, equal mass of 10 mmol/L of mercury nitrate and equal mass of 10 mmol/L of cadmium nitrate, respectively, and tested for adsorption capacity at 15min, 30min, 60min, as shown in the following table:
TABLE 1 adsorption Capacity results
As can be seen from table 1, by adopting the scheme of example 1, the adsorption capacity of the modified slime containing the quintuple pith for heavy metals of lead, mercury and cadmium is obviously better than that of the mask containing the modified slime containing the quintuple pith in example 2, and the mask containing the modified slime containing the quintuple pith in example 3 omits tea polyphenol, hyaluronic acid and glycolic acid substances, and the adsorption capacity for heavy metals is reduced compared with that of example 1. Example 4, the non-modified quinquefolia fire-feeding slime containing the plant rhizome is adopted, the absorption effect is obviously reduced, and the modification and the non-modification have great influence on the heavy metal absorption, which shows that the modification technology of the invention has great influence on the heavy metal absorption. Example 5 the adsorption effect of the modified treatment with slime containing no plant roots was less desirable than that of the slime containing plant roots. Therefore, the technical scheme of the invention has a remarkable heavy metal adsorption effect.
The mask of examples 1 to 5 was subjected to subject evaluation analysis. People who are often exposed outdoors, especially in the vicinity of driveways, are selected to develop symptoms such as facial allergies, red blood streaks, etc.
The above-mentioned persons were subjected to a grouping experiment of 15 persons each. The mask of examples 1 to 5 was used 1 time a day for 1 month without any other skin care treatment.
And testing heavy metals by adopting a clinical quality evaluation standard. The results are shown in Table 2
TABLE 2
After the above tests, the test of example 1 emphasizes that the metal removal effect is significant, and the treatment effect is obviously improved compared with the treatment effects of the comparative examples (examples 2 to 5).
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
The present invention is not limited to the above description of the embodiments, and those skilled in the art who have the benefit of this disclosure will appreciate that many modifications and variations of the present invention are possible within the scope of the present invention without departing from the inventive concepts herein.
Claims (8)
1. A preparation method of a high-adsorption mask loaded with modified volcanic cold slime is characterized by comprising the following steps:
firstly, volcanic mud pretreatment:
selecting Wudalianchi volcanic mud with plant roots and stems, freeze-drying at-35-40 ℃, grinding into powder by a grinder, and sieving by a 100-mesh sieve to obtain fine mud powder for later use;
secondly, volcanic mud modification:
mixing 5% hydrochloric acid and 3% sulfuric acid in equal proportion to prepare mixed acid, weighing the slurry powder obtained in the step one, adding the slurry powder into a reaction kettle, adding the mixed acid, reacting for 3-5h at room temperature under the condition of continuous stirring, and washing with deionized water to be neutral; wherein the mass volume ratio of the ore mud powder to the mixed acid is 1: 2-3;
thirdly, preparing the high-adsorption slime mask:
1) dispersing hyaluronic acid, single water-based fruit acid and a preservative in a humectant, adding sodium citrate, sodium chloride and deionized water, heating to 85-90 ℃ in a water phase pot, and stirring the solution uniformly;
2) adding an emulsifier, an antioxidant and tea polyphenol into an emulsifying pot, heating to 80-90 ℃, and dissolving uniformly;
3) mixing an adsorbent, vitamin E and an acid-base regulator, and uniformly stirring the mixture with the substances prepared in the steps 1) and 2) to obtain the load modified volcanic cold slime high adsorption mask;
wherein, the adsorbent is the mixture of the volcanic slime, the active carbon and the montmorillonite modified in the second step; the high-adsorption facial mask is prepared from 60-65% of an adsorbent, 8% of a humectant, 5% of an antioxidant, 2% of tea polyphenol, 3% of hyaluronic acid, 2% of vitamin E, 3-5% of single water-based tartaric acid, 1% of an acid-base regulator, 1-3% of an emulsifier, 1% of a preservative and the balance of deionized water in percentage by mass.
2. The preparation method of the mask with high adsorption capacity loaded with the modified volcanic cold slime as claimed in claim 1, wherein the antioxidant is squalane.
3. The preparation method of the mask loaded with the modified volcanic cold mud high adsorption material as claimed in claim 1, wherein the humectant is glycerin.
4. The preparation method of the high-adsorption mask loaded with the modified volcanic cold slime as claimed in claim 1, wherein the single water-based fruit acid is glycolic acid.
5. The preparation method of the mask with high adsorption capacity loaded with the modified volcanic cold slime as claimed in claim 1, wherein the emulsifier is long-carbon-chain alcohol.
6. The preparation method of the mask as claimed in claim 5, wherein the long carbon chain alcohol is one or more of lauryl alcohol, arachidyl alcohol, stearyl alcohol, cetyl alcohol, and palmityl alcohol.
7. The preparation method of the mask with high adsorption capacity loaded with the modified volcanic cold slime as claimed in claim 1, wherein the preservative comprises, by weight, 10-15 parts of rosemary extract, 5-10 parts of licorice extract, 2-5 parts of tea extract, 1-5 parts of sophora flavescens extract, 1-5 parts of calendula extract and 20-60 parts of butanediol.
8. The preparation method of the mask as claimed in claim 1, wherein the acidity regulator comprises citric acid and alkalinity regulator comprises triethanolamine.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112494359A (en) * | 2020-12-15 | 2021-03-16 | 广州市尚梓化工科技有限公司 | Preparation method of seaweed oligosaccharide and application of seaweed oligosaccharide in anti-aging cosmetics |
| WO2023135170A1 (en) * | 2022-01-13 | 2023-07-20 | Givaudan Sa | Composition |
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