CN106176328A - A kind of mask composition containing natural volcanic mud and preparation method thereof - Google Patents
A kind of mask composition containing natural volcanic mud and preparation method thereof Download PDFInfo
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- CN106176328A CN106176328A CN201610556774.1A CN201610556774A CN106176328A CN 106176328 A CN106176328 A CN 106176328A CN 201610556774 A CN201610556774 A CN 201610556774A CN 106176328 A CN106176328 A CN 106176328A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
nullThe invention discloses a kind of mask composition containing natural volcanic mud，It is made up of each raw material components of following percentage by weight: glycerol 2.0%～6.0%、The medicinal sludge in Wudalianchi 20.0%～50.0%、Stearyl alcohol 1.0%～4.0%、Glyceryl stearate 0.5%～1.8%、1，3 propylene glycol 0.5%～3.0%，Stearic acid 2.0%～4.0%、Hydroxyethyl cellulose 0.1%～1.0%、Polyvinyl alcohol 0.5%～2.0%、Isopropyl palmitate 2.0%～8.0%、Vitamin C 0.1%～0.5%、Polydimethylsiloxane 1.0%～6.0%、Polysorbate 20 0.3%～1.2%、Hyaluronate sodium 0.01%～0.05%、Prunus dulcis oil 1.0%～5.0%、Ethyl hydroxybenzoate 0.05%～0.1%、Essence 0.01%～0.1%，Surplus is wudalianchi minerals.The present invention uses the produce (Volcano Mineral Spring Water and medicinal sludge) of Wudalianchi to combine, similar mud film product on market to be far superior in increase skin elasticity, glossiness, safety, antibacterial performance.
Description
Technical field
The present invention relates to a kind of mask composition, belong to cosmetic technical field, particularly relate to a kind of containing Wudalianchi
Mineral spring and sludge, there is treatment dermatosis, the volcanic mineral mud film of skin energy can be excited again simultaneously.
Background technology
In we, although medical science and beauty culture all achieve many new breakthroughs, but we have found that those use in epoch
Natural material, as spring water, Sargassum, mud, clay etc. do the method treated but in recovery.It is clearly people and re-recognizes that
A little the Nature give our benefit having medicative element, this be also a kind of confirmation to nature and ancestors' wisdom with
Returning, especially in terms of the medicinal sliming cosmetic of exploitation natural green, medicinal sludge, as primary raw material therein, has not
Alternative effect.
There is long history Wudalianchi, and it is formed five connected volcano dammings by slag blocking river course, the Baihe
Lake is therefore named, is one of famous scenic spot of China, is again the maximum cold spring convalescence area of China.Mineral element is human body generation
Thanking to indispensable key factor, a lot of trace element are the cores of cellular enzymes, participate in the metabolism of enzyme, increase cell enzyme activity, right
The founction metabolism generation effect of human body, accelerates blood circulation, thus promotes the circulation of Skin Cell life.Simultaneously as directly
Act on skin surface, the element balance of adjustable local skin, be highly suitable to be applied in all kinds of facial film and skin-protection product.
Wudalianchi Volcanic mineral water: be one of big cold spring in the world three, the China and foreign countries that make a name enjoy " Castalia ", the U.S. of " holy water "
Reputation, the long-term water temperature stability of spring water, at 2-4 DEG C, belongs to ferrum siliceous heavy carbonic magnesium calcium calcareous type mineral water.Natural, pure, health, does not has dirt
Dye, containing the trace element of multiple needed by human, can cure, can drink, can bathe, and is precious mineral resource.Have through medical certificate
Expansion blood capillary, the effect of excited peripheral nerve, can promote the blood circulation of tip, and beneficially tip, skin is isocellular
Pathological changes is recovered, and can treat peripheral circulation disorders disease and multiple dermatosis, enhance metabolism.
The medicinal sludge in Wudalianchi is by the volcanic eruption of Earth, through the natural action of tens thousand of with mineral water years, by
Stone becomes soft sludge, and multiple element dissociates out from crystal and becomes ionic state.Due to this deposition sludge have special
The origin cause of formation, thus there is the highest medicinal, health care its cosmetic values, can the multiple disease such as hair growth, allergic dermatitis, rheumatism
Suffer from, the most obvious beauty care effect.Effective ingredient in sludge all exists with ionic state form, and it can help blood
Circulation, thus promote the renewal of Skin Cell, contribute to purifying blood, enhance metabolism, increase the required trace in blood
Element, can treat various skin problem.
At present, the most do not occur using compounding to Wudalianchi Volcanic mineral water and the medicinal sludge in Wudalianchi, more simultaneously
It is not added simultaneously to facial treatment mask product obtains the application example of good using effect.
Summary of the invention
For the application on facial film of the current sludge, it is an object of the invention to provide a kind of face containing natural volcanic mud
Film, the characteristic of the two of Wudalianchi kinds of characteristic raw materials (natural Volcano Mineral Spring Water and medicinal sludge) is dissolved into and is protected by well
In skin product, form a kind of mineral energy facial film shown unique characteristics, give the more effect of mask product and concept.
Another object of the present invention is to provide the preparation method of the above-mentioned mask composition containing natural volcanic mud.
The object of the invention to solve the technical problems realizes by the following technical solutions.Propose according to the present invention
A kind of mask composition containing natural volcanic mud, be made up of each raw material components of following percentage by weight:
Emulsifying agent 0.1%-5.0%；Emollient 10%-30%；Wudalianchi medicinal sludge 20%-50%；Wetting agent
0.1%-10.0%；Whitening agent 0.1%-3.0%；Thickening agent 0.1%-5.0%；Odorant 0.01%-0.2%；Film former
0.5%-5.0%；Preservative 0.05%-0.5%；Wudalianchi minerals surplus.
A kind of mask composition containing natural volcanic mud, is made up of each raw material components of following percentage by weight:
Emulsifying agent 0.5%-1.8%；Emollient 10%-20%；Wudalianchi medicinal sludge 20%-50%；Wetting agent
0.6%-3.5%；Whitening agent 0.1%-0.5%；Thickening agent 0.1%-1.0%；Odorant 0.01%-0.08%；Film former
0.5%-2.0%；Preservative 0.05%-0.1%；Wudalianchi minerals surplus.
The medicinal sludge in described Wudalianchi is prepared by following technique:
Extract fresh sludge from unpolluted stratum, stir (the weight portion of mud and water with Volcano Mineral Spring Water
Proportioning example is l:3), at room temperature sieve (filter screens of 700 mesh), centrifugal 4000r/min, 10min, collects wet mud, high temperature (120
DEG C) be dried 3 hours, pulverize and 1000 mesh that sieve through high pressure draught, to obtain final product.
Described emulsifying agent is selected from glyceryl stearate, polysorbate-20, sorbitan sesquioleate, olein, gathers
One or more mixing of glycerol-3 polyricinoleate；
Described emollient is in stearyl alcohol, stearic acid, isopropyl palmitate, polydimethylsiloxane, Prunus dulcis oil
Mixing that any one or both are above；
Described wetting agent is selected from any one in glycerol, hyaluronate sodium, 1,3-PD, pantothenylol or both above mixing
Close；
Described thickening agent is selected from hydroxyethyl cellulose, polyvinyl alcohol, HANSHENGJIAO, Magnesiumaluminumsilicate, acrylic acid (ester) class/C10-
30 alkylol acrylamide acid esters cross linked polymers, pectin, one or more mixing of carbomer；
Any one in ethyl hydroxybenzoate, phenoxyethanol of described preservative.
It addition, a kind of mask composition containing natural volcanic mud, it is made up of each raw material components of following percentage by weight:
Glycerol 2.0%～6.0%, the medicinal sludge in Wudalianchi 20.0%～50.0%, stearyl alcohol 1.0%～4.0%, sweet
Oleostearin acid esters 0.5%～1.8%, 1,3-PD 0.5%～3.0%, stearic acid 2.0%～4.0%, hydroxyethyl cellulose
0.1%～1.0%, polyvinyl alcohol 0.5%～2.0%, isopropyl palmitate 2.0%～8.0%, vitamin C 0.1%～
0.5%, polydimethylsiloxane 1.0%～6.0%, polysorbate-20 0.3%～1.2%, hyaluronate sodium 0.01%～
0.05%, Prunus dulcis oil 1.0%～5.0%, ethyl hydroxybenzoate 0.05%～0.1%, essence 0.01%～0.1%, surplus is five
Pond, Dalian mineral water.
It addition, the present invention also proposes the preparation method of a kind of mask composition containing natural volcanic mud, comprise the following steps:
Described mask composition is made up of the raw material components of following percentage by weight:
Component A: glyceryl stearate 0.5-1.8%, stearyl alcohol 1.0-4.0%, stearic acid 20-4.0%, Palmic acid isopropyl
Ester 2.0-8.0%, polydimethylsiloxane 1.0-6.0%, Prunus dulcis oil 1.0-5.0%, ethyl hydroxybenzoate 0.05-0.1%；
B component: glycerol 2.0-6.0%, hydroxyethyl cellulose 0.1-5.0%, hyaluronate sodium 0.01-0.05%, 1,3-
Propylene glycol 0.5-3.0%, polysorbate-20 0.3-1.2%, wudalianchi minerals 10.0-60.0%；
C phase: Wu Da Lian chi sludge 20-50%, polyvinyl alcohol 0.5-2.0%；
D phase: phenoxyethanol 0.3-0.5%, vitamin C 0.1-0.5%, 0.1-0.6%, essence 0.01-0.08%；
1) the oil phase raw material in component A is sequentially added in oil phase pot, open stirring 30 revs/min, be warming up to 80 DEG C～
85 DEG C, it is incubated 5～10 minutes；
2) wudalianchi minerals of B component is added in emulsifying pot, with glycerol hydroxyethyl cellulose and hyaluronic acid
Sodium moistening, is uniformly mixed, and adds in emulsifying pot, is subsequently adding other B phase raw material, and is warming up to 85 DEG C～90 DEG C；
3) by other raw materials of component A slowly suction emulsifying pot, high speed homogenization 10 minutes；
4) add sludge and the polyvinyl alcohol of C phase, be incubated 10 minutes, high speed homogenization 20 minutes, start cooling；
5) when emulsifying pot drops to 45 DEG C, then D is added in emulsifying pot, stirs, be incubated 10 minutes；
6) discharging when 38 DEG C it is down to.The pH value range of discharging product controls 5.0～6.5.
By technique scheme, the invention have the advantages that and Advantageous Effects:
1, the present invention uses the comminution by gas stream ore deposit sludge treatment technology of advanced person, obtains in terms of the fineness and stability of product
Further optimize, due to the trace element contained in product and radioelement, it can go deep into and penetrate play suppress or
Kill the effect of pathogenic bacteria, it is possible to reduce the addition of preservative so that product is more gentle.
2, the present invention adds mineral spring natural, containing abundant mineral element and medicinal sludge to traditional face pack prescription
In, impart the more effect of mask product, widened the range of application of facial film, substantially increase the market extra price of product
Value, the formula technique of this combination is different from commercially available common mud film, has obvious performance advantage and innovation concept, will
Liking of more and more consumer can be obtained.
Detailed description of the invention
It it is below the function introduction of primary raw material of the present invention.
1, Wudalianchi Volcanic Mineral Water Components composition:
Mainly containing potassium, calcium, sodium, magnesium in mineral water, wherein iron content is 30～40mg/L, manganese 6～7mg/L, inclined silicon
Acid is 60～70mg/L, and the trace element of the needed by human such as macroelement and zinc, copper, lithium, strontium, cobalt, nickel.Its water quality is steady
Fixed, organoleptic indicator, physical and chemical index, contamination index meet country's GB 8537-1995 natural mineral water standard.
Product efficacy: due to be volcano mineral spring be low temperature mineral spring, wherein contain substantial amounts of carbon dioxide, have expansion hair
Thin blood vessel, the effect of excited peripheral nerve, thus promote the blood circulation of tip, increase the infiltration of various ions in mineral water and make
With, the beneficially histiocytic pathological changes such as tip, skin is recovered, therefore can treat peripheral circulation disorders disease and various skin
Sick.Confirm that full bath or hair washing, foot bath all have the effect of blood pressure lowering through clinic.Wudalianchi minerals passes through ion
Osmosis, the ion of intraor extracellular can reach balance, skin beauty water content and metabolic function will recover normal, and skin is grown
Moisten, delicacy is glossy, flexible, reappears life.
2, the medicinal sludge in Wudalianchi becomes to be grouped into:
Main by basaltic tephre, quartz, pyroxene, illite, chlorite, kaolinite and quartzy, a small amount of Anhydrite etc.
Multiple clay mineral forms.Wu Da Lian chi sludge, is natural aging sludge, in sludge containing various trace elements, mineral and
Organic acid, is referred to as " cell activator " and " cell detergent ", has the longest applicating history.
Reparation technology: the present invention uses and extracts fresh sludge from unpolluted stratum, uses Volcano Mineral Spring Water
Stir (mud is l:3 with the ratio of water), and at room temperature sieve (filter screens of 700 mesh), and centrifugal 4000r/min, 10min receive
Collect wet mud, high temperature (120 DEG C) is dried 3 hours, high pressure draught is pulverized, sieve 1000 mesh.This method obtains water content < 0.5%
Medicinal sludge, compared with the sludge that it processes with Traditional Method, particle diameter is thinner, surface is rounder and more smooth, and performance is more stable.
Product efficacy: scientific experiments proves, the active ingredient contained by sludge can make local skin produce analogued histamine material,
Expansible local vascular, acceleration blood circulation, promote skin metabolism, keep moisture of skin, increase skin-nourishing, make skin
Keep moist, flexible.The elements such as silicon in sludge, manganese, trivalent chromium can add volcanic slurry microgranule with vessel softening and skin
The characteristic of porous so that it is have stronger adsorptivity, makes sludge remove the dead cell of skin epidermis by rubbing, accelerates skin
Metabolism, cytoactive strengthens, and keeps skin elasticity, makes coarse skin reappear smooth.Metasilicic acid ion cluster also can be with
Dirt in pore combines, and removes dirt so that it is shrinking pore.
The present invention uses produce (Volcano Mineral Spring Water and the medicinal sludge) compositions of Wudalianchi, and clinical experiment is demonstrate,proved
Bright, containing this compositions mud film, is increasing city to be far superior in skin elasticity, glossiness, safety, antibacterial performance
Similar mud film product on field, demonstrates the high technology content of comparison and good application performance.
Compliance test result test example is combined to further illustrate the mask composition of the present invention below by way of concrete preferred embodiment
Thing, but the present invention is not limited in below example.
Table 1 embodiment 1-3 and reference examples 1 raw material components composition
The process for making of above-mentioned mineral mud film, comprises the steps:
1) the oil phase raw material in component A is sequentially added in oil phase pot, open stirring 30 revs/min, be warming up to 80 DEG C～
85 DEG C, it is incubated 5～10 minutes.
2) wudalianchi minerals of B component is added in emulsifying pot, with glycerol hydroxyethyl cellulose and hyaluronic acid
Sodium moistening, is uniformly mixed, and adds in emulsifying pot, is subsequently adding other B phase raw material, and is warming up to 85 DEG C～90 DEG C.
3) by other raw materials of component A slowly suction emulsifying pot, high speed homogenization 10 minutes；
4) add sludge and the polyvinyl alcohol of C phase, be incubated 10 minutes, high speed homogenization 20 minutes；Start cooling.
5) when emulsifying pot drops to 45 DEG C, then D is added in emulsifying pot, stirs, be incubated 10 minutes；
6) being down to discharging when 38 DEG C, pH value range controls 5.0～6.5.
Compliance test result test example
Test example 1
One, beauty and skin care (glossiness, elasticity) effect assessment
Test sample: embodiment 3 and commercially available famous brand name mud film
Test purpose: used mud film by adult female volunteer the most continuously, assesses this product in beauty treatment
Effect in terms of skin protection.
Volunteer: 30 people, 25～40 years old, sex: women.
Volunteer's face skin quality: blee is obscure, matt, have obvious pox to print.
Product uses frequency: after cleaning and using astringent, takes out facial film and is uniformly applied to face and cervical region, and deposited 10-15 divides
Clock, rinses well with clear water.Once a day, left face is embodiment 3 sample, and right face is commercially available famous brand name mud film, uses product
After surrounding, (Day28) and use product are after eight weeks (Day56).
Test event: skin shine, the elastic effect of skin.
Appraisal procedure: use the mode of questionnaire survey, after using product 4 weeks and 8 weeks, experimenter is to skin after product use
Skin glossiness, elastic improvement situation.
Judging quota is divided into: DeGrain, effect are general, more apparent, clearly.
1) after using product surrounding, (Day 28) skin shine experimental result see table shown in 2.
Using effect after table 2 embodiment 3 and commercially available prod surrounding
2) use product after eight weeks (Day 56) skin shine experimental result see table shown in 3.
Using effect after table 3 embodiment 3 and commercially available prod surrounding
By the result of above-mentioned table 2 and 3 it can be seen that use the mud film (embodiment 3) of the present invention after 28 days, there are about 73.3%
Volunteer feel that skin shine has obvious improvement effect.After 56 days, the volunteer that there are about 86.7% feels skin
Glossiness has obvious improvement effect.The effect improving skin shine to be substantially better than by the mud film of the present invention commercially available to be known
Name brand mud film.
3) use product after eight weeks (Day 56) skin elasticity experimental result see table shown in 4.
Using effect after table 4 embodiment 3 and commercially available prod surrounding
4) after using product surrounding, (Day28) skin elasticity experimental result see table shown in 5.
Using effect after table 5 embodiment 3 and commercially available prod surrounding
Conclusion: using the mud film (embodiment 3) of this patent after 28 days, the volunteer that there are about 63.3% feels that skin elasticity has
Obvious improvement effect.After 56 days, the volunteer that there are about 86% feels that skin elasticity has obvious improvement effect.This
The mud film of patent to be substantially better than commercially available famous brand name mud film to the effect improving skin elasticity.
Test example 2
Two, Product Safety assessment (human skin patch result)
Evaluation methodology:
1) tested material: embodiment
2) negative control: reference examples
3) experimenter: totally 30 people, male 10 people, female 20 people, age 18～40 years old, meet experimenter and volunteer inclusion criteria.
4) speckle method for testing: select qualified speckle examination device, with closed patch test method, by tested material about 0.02ml～
0.025ml is applied in speckle examination device, and external special adhesive tape is pasted on experimenter's forearm song side, removes tested material, in going after 24 hours
Except 30min after tested material speckle examination device, after impression disappears, observe dermoreaction, by " cosmetics health specification " (version in 2007)
Dermoreaction grade scale records its result.
5) evaluation of result: record reaction result by table 6 (skin adverse reaction grade scale).
Table 6 dermoreaction result
6) result of the test:
Cosmetics human skin patch result see table shown in 7:
Table 7 embodiment 1-3 and the human skin patch of reference examples product
Human skin patch result shows:
In A, embodiment 1,2,3 (this patent formula), 30 the most negative (grading systems: 0 of subjects skin
Level).According to " cosmetics health specification " (version in 2007) human body skin class patch test criterion, sample is to human body without skin not
Good reaction.
B, reference examples (commercially available famous brand name mud film) have 2 experimenters to occur, and 1 order reaction and 1 experimenter occur 2 grades instead
Should.
Be we can see that by the experimental result of table 7: the mildness of the formula of the present invention is the highest, be completely suitable for all kinds of
The crowd of skin quality.
Test example 3
Three, antibiotic effect evaluation
Preservative efficacy is tested: test basis and the method for analysis (Standard and Methods): by EU criteria
USP51, BP2002 XVI C EFFICAIY OF ANTIMICROBIAL PRESERVATION measures cosmetics opposing microorganism
The ability polluted performs.
Sample ID: the preservative efficacy test result of embodiment 3 see table shown in 8.
The preservative efficacy test of table 8 embodiment 3
Conclusion criterion (the Standard of conclusion) result of embodiment 3 see table shown in 9.
The conclusion criterion of table 9 embodiment 3
Experimental result: the protective system of this product (embodiment 3) is tested by challenge, and this protective system is reasonable to microorganism
Effect is killed in pressing down of thinking, product is less susceptible to be polluted by microorganism when producing, storing and use.
Sample ID: the product test result of reference examples see table shown in 10.
The test result of table 10 embodiment 3
Conclusion criterion (Standard of conclusion) see table shown in 11.
The conclusion criterion of table 11 embodiment 3
Experimental result: the protective system of this product (reference examples) is not over challenge test, and this protective system is to microorganism
Pressing down that to kill effect undesirable, product is highly susceptible to the pollution of microorganism when producing, storing and use.
Contrast conclusion: by above-mentioned parallel laboratory test it can be seen that in the case of formula is identical, select Wudalianchi mineral spring
Being better than the most commercially available mineral spring of use and the facial film of sludge with the anti-microbe ability of the facial film of sludge, experimental result can be with table
Bright: Wudalianchi mineral spring and sludge have good anti-microbial property.
Compared with existing mud membrane technology, the Wudalianchi mud film of the present invention has a big feature in following 6:
1, with the addition of and derive from volcano mineral spring and the facial film of medicinal sludge in source, sky, Wudalianchi, they are rich in lot of trace
Element and mineral, have the epidermal tissue being penetrated into and passing human body by pore, can stimulate the tissue in deep and cell
Activity, increases regeneration capacity, excites the energy of skin.
2, the present invention applies the medicinal sludge of Wudalianchi, and it is polished into light through high pressure draught pulverization process, surface
Sliding, the spheroid of uniform particle sizes, is possible not only to provide good and smears skinfeel, with after skin can be allowed more added with exquisiteness, be rich in light
Pool.
3, by organic collocation of two kinds of compositions (Volcano Mineral Spring Water and medicinal sludge), due to the symbiotic co-existence between them
Environment, has the effect of Synergistic between their active component, compared with single volcano mineral spring or single sludge, it
Beauty effect become apparent from.
4, the strong magnetic field circumstance residing for Wudalianchi, Volcano Mineral Spring Water and medicinal sludge through the magnetization of 10000000 year,
Their characteristic there occurs change, and its effect is compared with common sludge and mineral water, and it is higher with the affinity of skin, inhales
Attached performance is more preferably.
5, this formula is without dioxane, without mineral oil, heavy metal without artificial color and other amount of having, in sludge
Trace element and radioelement play suppression or kill the effect of antibacterial, it is possible to reduce the addition of preservative in formula, produce
The safety of product is higher, goes for all kinds of skin quality and various people.
6, Wu Da Lian chi sludge is different with other sludge, and it contains Natural Proportioning and the ratio of human body needs of various ion
Example is almost consistent, and these ions or the interaction of ion cluster can produce powerful osmotic pressure, and ion channel is by penetration cell
Film, enters cell interior, and by ion osmosis, the ion of intraor extracellular can reach balance so that skin moisturizing, delicacy have
Gloss, flexible.
The above, be only presently preferred embodiments of the present invention, and the present invention not makees any pro forma restriction, therefore
Every without departing from technical solution of the present invention content, any simply repaiied according to what above example made by the technical spirit of the present invention
Change, equivalent variations and modification, all still fall within the range of technical solution of the present invention.
Claims (7)
1. the mask composition containing natural volcanic mud, it is characterised in that be by each raw material components of following percentage by weight
Composition:
Emulsifying agent 0.1%-5.0%；
Emollient 10%-30%；
Wudalianchi medicinal sludge 20%-50%；
Wetting agent 0.1%-10.0%；
Whitening agent 0.1%-3.0%；
Thickening agent 0.1%-5.0%；
Odorant 0.01%-0.2%；
Film former 0.5%-5.0%；
Preservative 0.05%-0.5%；
Wudalianchi minerals surplus.
Mask composition containing natural volcanic mud the most according to claim 1, it is characterised in that: it is by following weight percent
Each raw material components composition of ratio:
Emulsifying agent 0.5%-1.8%；
Emollient 10%-20%；
Wudalianchi medicinal sludge 20%-50%；
Wetting agent 0.6%-3.5%；
Whitening agent 0.1%-0.5%；
Thickening agent 0.1%-1.0%；
Odorant 0.01%-0.08%；
Film former 0.5%-2.0%；
Preservative 0.05%-0.1%；
Wudalianchi minerals surplus.
Mask composition containing natural volcanic mud the most according to claim 1 and 2, it is characterised in that: described Wudalianchi
Medicinal sludge is prepared by following technique:
Extract fresh sludge from unpolluted stratum, stir (the weight of mud and water with Volcano Mineral Spring Water
Example is l:3), at room temperature sieve (filter screens of 700 mesh), centrifugal 4000r/min, 10min, collects wet mud, high temperature (120 DEG C) is done
Dry 3 hours, pulverize and 1000 mesh that sieve through high pressure draught, to obtain final product.
Mask composition containing natural volcanic mud the most according to claim 1 and 2, it is characterised in that:
Described emulsifying agent is selected from glyceryl stearate, polysorbate-20, sorbitan sesquioleate, olein, poly-sweet
One or more mixing of oil-3 polyricinoleates；
It is arbitrary that described emollient is selected from stearyl alcohol, stearic acid, isopropyl palmitate, polydimethylsiloxane, Prunus dulcis oil
Kind or mixing that both are above；
Any one in glycerol, hyaluronate sodium, 1,3-PD, pantothenylol of described wetting agent or the mixing more than both；
Described thickening agent is selected from hydroxyethyl cellulose, polyvinyl alcohol, HANSHENGJIAO, Magnesiumaluminumsilicate, acrylic acid (ester) class/C10-30 alkane
Alcohol acrylate crosspolymers, pectin, one or more mixing of carbomer；
Any one in ethyl hydroxybenzoate, phenoxyethanol of described preservative.
Mask composition containing natural volcanic mud the most according to claim 1, it is characterised in that be by following weight percent
Each raw material components composition of ratio:
Glycerol 2.0%～6.0%, the medicinal sludge in Wudalianchi 20.0%～50.0%, stearyl alcohol 1.0%～4.0%, glycerol are hard
Fat acid ester 0.5%～1.8%, 1,3-PD 0.5%～3.0%, stearic acid 2.0%～4.0%, hydroxyethyl cellulose
0.1%～1.0%, polyvinyl alcohol 0.5%～2.0%, isopropyl palmitate 2.0%～8.0%, vitamin C 0.1%～
0.5%, polydimethylsiloxane 1.0%～6.0%, polysorbate-20 0.3%～1.2%, hyaluronate sodium 0.01%～
0.05%, Prunus dulcis oil 1.0%～5.0%, ethyl hydroxybenzoate 0.05%～0.1%, essence 0.01%～0.1%, surplus is five
Pond, Dalian mineral water.
6. the preparation method of the mask composition containing natural volcanic mud, it is characterised in that comprise the following steps:
Described mask composition is made up of the raw material components of following percentage by weight:
Component A: glyceryl stearate 0.5-1.8%, stearyl alcohol 1.0-4.0%, stearic acid 20-4.0%, isopropyl palmitate
2.0-8.0%, polydimethylsiloxane 1.0-6.0%, Prunus dulcis oil 1.0-5.0%, ethyl hydroxybenzoate 0.05-0.1%；
B component: glycerol 2.0-6.0%, hydroxyethyl cellulose 0.1-5.0%, hyaluronate sodium 0.01-0.05%, 1,3-the third two
Alcohol 0.5-3.0%, polysorbate-20 0.3-1.2%, wudalianchi minerals 10.0-60.0%；
C phase: Wu Da Lian chi sludge 20-50%, polyvinyl alcohol 0.5-2.0%；
D phase: phenoxyethanol 0.3-0.5%, vitamin C 0.1-0.5%, 0.1-0.6%, essence 0.01-0.08%；
1) the oil phase raw material in component A is sequentially added in oil phase pot, opens stirring 30 revs/min, be warming up to 80 DEG C～85 DEG C,
It is incubated 5～10 minutes；
2) wudalianchi minerals of B component is added in emulsifying pot, with glycerol, hydroxyethyl cellulose and hyaluronate sodium are moistened
Wet, it is uniformly mixed, adds in emulsifying pot, be subsequently adding other B phase raw material, and be warming up to 85 DEG C～90 DEG C；
3) by the raw material of component A slowly suction emulsifying pot, high speed homogenization 10 minutes；
4) add sludge and the polyvinyl alcohol of C phase, be incubated 10 minutes, high speed homogenization 20 minutes, start cooling；
5) when emulsifying pot drops to 45 DEG C, then D is added in emulsifying pot, stirs, be incubated 10 minutes；
6) discharging when 38 DEG C it is down to.
7. the mask composition containing natural volcanic mud stated according to claim 6, it is characterised in that: step 6) discharging product
PH value range controls 5.0～6.5.
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| CN106806177A (en) * | 2017-03-23 | 2017-06-09 | 广州市帝臣日化科技有限公司 | A kind of volcano clay mask and preparation method thereof |
| CN109223626A (en) * | 2018-11-23 | 2019-01-18 | 黑龙江省科学院火山与矿泉研究所 | Wudalianchi cold spring mouth and nose nursing spray and preparation method thereof |
| CN110123696A (en) * | 2019-06-10 | 2019-08-16 | 黑龙江省科学院火山与矿泉研究所 | Preparation method of composite preservative for natural volcanic mud mask |
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| CN111494252A (en) * | 2020-04-22 | 2020-08-07 | 黑龙江省科学院火山与矿泉研究所 | Preparation method of high-adsorption facial mask loaded with modified volcanic cold slime |
| CN113081908A (en) * | 2021-04-23 | 2021-07-09 | 黑龙江省科学院自然与生态研究所 | Artificial growth-promoting volcanic mud and preparation method and application thereof |
| CN114028243A (en) * | 2021-10-21 | 2022-02-11 | 科玛化妆品(无锡)有限公司 | Mud membrane composition and preparation method and application thereof |
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| CN106806177A (en) * | 2017-03-23 | 2017-06-09 | 广州市帝臣日化科技有限公司 | A kind of volcano clay mask and preparation method thereof |
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| CN110478282A (en) * | 2019-09-11 | 2019-11-22 | 黑龙江省科学院火山与矿泉研究所 | A kind of multi-functional volcanic slurry cleaning mud film and preparation method thereof and application method |
| CN111494252A (en) * | 2020-04-22 | 2020-08-07 | 黑龙江省科学院火山与矿泉研究所 | Preparation method of high-adsorption facial mask loaded with modified volcanic cold slime |
| CN111494252B (en) * | 2020-04-22 | 2022-09-20 | 黑龙江省科学院火山与矿泉研究所 | Preparation method of modified volcanic cold mineral mud loaded adsorption mask |
| CN113081908A (en) * | 2021-04-23 | 2021-07-09 | 黑龙江省科学院自然与生态研究所 | Artificial growth-promoting volcanic mud and preparation method and application thereof |
| CN114028243A (en) * | 2021-10-21 | 2022-02-11 | 科玛化妆品(无锡)有限公司 | Mud membrane composition and preparation method and application thereof |
| CN114028243B (en) * | 2021-10-21 | 2023-11-17 | 科玛化妆品(无锡)有限公司 | Mud film composition and preparation method and application thereof |
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Application publication date: 20161207 |