CN105232369A - Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof - Google Patents
Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof Download PDFInfo
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- CN105232369A CN105232369A CN201510627755.9A CN201510627755A CN105232369A CN 105232369 A CN105232369 A CN 105232369A CN 201510627755 A CN201510627755 A CN 201510627755A CN 105232369 A CN105232369 A CN 105232369A
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- auricularia
- wudalianchi
- fructus hippophae
- facial film
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- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 235000003145 Hippophae rhamnoides Nutrition 0.000 title abstract 5
- 240000000950 Hippophae rhamnoides Species 0.000 title 1
- 241000229143 Hippophae Species 0.000 claims abstract description 87
- 230000001815 facial effect Effects 0.000 claims abstract description 66
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 31
- 239000011707 mineral Substances 0.000 claims abstract description 31
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 241000221377 Auricularia Species 0.000 claims description 89
- 235000003935 Hippophae Nutrition 0.000 claims description 83
- 239000010802 sludge Substances 0.000 claims description 83
- 239000003643 water by type Substances 0.000 claims description 21
- 230000001954 sterilising effect Effects 0.000 claims description 12
- 238000004659 sterilization and disinfection Methods 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 239000000839 emulsion Substances 0.000 claims description 4
- 229930003944 flavone Natural products 0.000 claims description 4
- 235000011949 flavones Nutrition 0.000 claims description 4
- 238000004108 freeze drying Methods 0.000 claims description 4
- 238000004806 packaging method and process Methods 0.000 claims description 4
- 238000010008 shearing Methods 0.000 claims description 4
- 239000011550 stock solution Substances 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 4
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 claims description 3
- 150000002212 flavone derivatives Chemical class 0.000 claims description 3
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 15
- 230000003020 moisturizing effect Effects 0.000 abstract description 11
- 239000002994 raw material Substances 0.000 abstract description 9
- 230000003078 antioxidant effect Effects 0.000 abstract description 5
- 241000233866 Fungi Species 0.000 abstract description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 21
- 235000010755 mineral Nutrition 0.000 description 20
- 239000000047 product Substances 0.000 description 9
- 241000863032 Trieres Species 0.000 description 8
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 8
- 230000003064 anti-oxidating effect Effects 0.000 description 5
- 230000009286 beneficial effect Effects 0.000 description 4
- 230000002500 effect on skin Effects 0.000 description 4
- 230000035807 sensation Effects 0.000 description 4
- 238000002835 absorbance Methods 0.000 description 3
- 239000002390 adhesive tape Substances 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 206010020751 Hypersensitivity Diseases 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- 208000026935 allergic disease Diseases 0.000 description 2
- 230000007815 allergy Effects 0.000 description 2
- 235000020682 bottled natural mineral water Nutrition 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 241000221454 Auriculariaceae Species 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical class [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000172 allergic effect Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 230000009693 chronic damage Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
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- 239000003381 stabilizer Substances 0.000 description 1
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- 239000000758 substrate Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
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- Cosmetics (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
Disclosed is a Wudalianchi volcanic slime and sea buckthorn edible fungus additive-free facial mask and a preparation method thereof, relating to the Wudalianchi volcanic slime and sea buckthorn edible fungus additive-free facial mask and the preparation method thereof. The invention aims to solve the problems that the existing mask products need to be added with industrial raw materials, potential harm is generated to the skin and the body of a consumer, and the skin care effect of the product without the industrial raw materials is not good. It comprises sea buckthorn agaric gel extract, Wudalianchi volcanic slime and Wudalianchi metasilicic acid mineral water. The mask disclosed by the invention is a mask product without any industrial raw material and with good moisturizing and antioxidant effects, so that people can feel more confident and safely enjoy the natural skin care effects of the natural volcanic mineral mud in the five great continuous ponds and the sea buckthorn edible fungi.
Description
Technical field
The present invention relates to Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without adding facial film and preparation method thereof.
Background technology
The formula of facial treatment mask product has the raw material of industry to add, as wetting agent, and emulsifying agent, stabilizing agent, mineral oil, artificial oils and fats, antiseptic, quintessence oil etc.And the skin of these additives to people has potential hazard, long-time use can cause the chronic injury of skin profound level.And the product skin effect not adding these raw materials of industry is undesirable, in order to address this problem, the present invention with natural Wudalianchi Volcanic sludge and mineral water for base material, be aided with the Fructus Hippophae Auricularia gel extract having good moisturizing and anti-oxidation efficacy, be developed into Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without adding facial film, namely solve the potential hazard of the raw material of industry to skin, have again good skin effect.
Fructus Hippophae Auricularia is the edible fungus of Auriculariaceae, Auricularia.Recent study finds, containing abundant polysaccharide and collagen protein in Auricularia, there are good moisturizing and antioxidation isoreactivity, Fructus Hippophae Auricularia is also containing a large amount of flavone, better antioxidation is had than other kind Auricularias, the skin care effects such as uvioresistant, these effects of Fructus Hippophae Auricularia have good skin-protection and health-care effect, the present invention by with Auricularia and have the natural base material of same skin care effect " Wudalianchi Volcanic sludge ", " Wudalianchi natural mineral water " be developed into Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without adding facial film.Pure natural can better play natural Wu Da Lian chi sludge, the skin care effect of mineral resource and Fructus Hippophae Auricularia without interpolation.
Summary of the invention
The object of the invention is all to need to add the raw material of industry to solve existing mask product, all potential hazard is produced to consumer skin and health, and the problem that the product skin effect not adding the raw material of industry is bad, and provide Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without adding facial film and preparation method thereof.
Wudalianchi Volcanic sludge of the present invention and Fructus Hippophae Auricularia are without adding facial film, and its active component to be mass fraction be Fructus Hippophae Auricularia gel extract, the mass fraction of 5 ~ 20 parts the be Wudalianchi Volcanic sludge of 20 ~ 60 parts and mass fraction are 30 ~ 80 portions of Wudalianchi metasilicic acid mineral waters.
Wudalianchi Volcanic sludge of the present invention and Fructus Hippophae Auricularia are without the preparation method of adding facial film, and it carries out according to following steps:
One, get Fructus Hippophae Auricularia to clean, naturally dry in the shade, then 200 orders are crushed to, mix with the ratio of deionized water in solid-to-liquid ratio 50:1,10h is extracted again under 80 DEG C of conditions, then centrifugal under the centrifugal condition of 4000 revs/min, get that supernatant is evaporated to stock solution 1/5, last lyophilization, obtains Fructus Hippophae Auricularia gel extract;
Two, get Wudalianchi Volcanic sludge, be crushed to 800 orders, obtain Wudalianchi Volcanic sludge powder;
Three, the Fructus Hippophae Auricularia gel extract of 5 ~ 20 parts, the Wudalianchi Volcanic sludge of 20 ~ 60 parts and 30 ~ 80 portions of Wudalianchi metasilicic acid mineral waters are got by weight, be placed in emulsion tank to shear, wherein, shear temperature is 70 DEG C, shear time is 20min, shearing rotating speed is 4000 revs/min, obtains Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without adding facial film;
Four, the facial film that step 3 obtains is loaded in high temperature resistant sterilization packaging, carry out high pressure steam sterilization, sterilising conditions is: 121.3 DEG C, 20min, aseptically encapsulate, namely complete described Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without the preparation adding facial film.
The present invention comprises following beneficial effect:
The present invention's Wudalianchi Volcanic sludge, Wudalianchi natural mineral water, be developed into namely without adding any raw material of industry with Fructus Hippophae Auricularia gel extract, there are again the Wudalianchi Volcanic sludge of good moisturizing and antioxidant effect and Fructus Hippophae Auricularia without adding mask product, make people more relieved, the enjoyment natural Wudalianchi Volcanic mineral spring sludge of safety and the natural skin effect of Fructus Hippophae Auricularia.
The moistening effect of facial film of the present invention in 1 hour is better than 10% glycerol, and the moistening effect of facial film is better.Facial film is to the clearance rate of DPPH all more than 50%, and facial film has good antioxidant activity.
Detailed description of the invention
Detailed description of the invention one: the Wudalianchi Volcanic sludge of present embodiment and Fructus Hippophae Auricularia are without adding facial film, and its active component to be mass fraction be Fructus Hippophae Auricularia gel extract, the mass fraction of 5 ~ 20 parts the be Wudalianchi Volcanic sludge of 20 ~ 60 parts and mass fraction are 30 ~ 80 portions of Wudalianchi metasilicic acid mineral waters.
Detailed description of the invention two: present embodiment and detailed description of the invention one unlike: Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia are without adding facial film, and its active component to be mass fraction be Fructus Hippophae Auricularia gel extract, the mass fraction of 8 ~ 16 parts the be Wudalianchi Volcanic sludge of 25 ~ 55 parts and mass fraction are 35 ~ 65 portions of Wudalianchi metasilicic acid mineral waters.Other is identical with detailed description of the invention one.
Detailed description of the invention three: present embodiment and detailed description of the invention one unlike: Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia are without adding facial film, and its active component to be mass fraction be Fructus Hippophae Auricularia gel extract, the mass fraction of 10 ~ 15 parts the be Wudalianchi Volcanic sludge of 28 ~ 50 parts and mass fraction are 40 ~ 60 portions of Wudalianchi metasilicic acid mineral waters.Other is identical with detailed description of the invention one.
Detailed description of the invention four: present embodiment and detailed description of the invention one unlike: Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia are without adding facial film, and its active component to be mass fraction be Fructus Hippophae Auricularia gel extract, the mass fraction of 11 ~ 14 parts the be Wudalianchi Volcanic sludge of 30 ~ 45 parts and mass fraction are 45 ~ 55 portions of Wudalianchi metasilicic acid mineral waters.Other is identical with detailed description of the invention one.
Detailed description of the invention five: present embodiment and detailed description of the invention one unlike: Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia are without adding facial film, and its active component to be mass fraction be Fructus Hippophae Auricularia gel extract, the mass fraction of 12 ~ 13 parts the be Wudalianchi Volcanic sludge of 35 ~ 40 parts and mass fraction are 45 ~ 50 portions of Wudalianchi metasilicic acid mineral waters.Other is identical with detailed description of the invention one.
Detailed description of the invention six: present embodiment and detailed description of the invention one unlike: described Wudalianchi Volcanic sludge is the sludge taking from Wudalianchi Yaoquanshan sludge band, the trace element containing multiple beneficial skins such as potassium, sodium, calcium, magnesium, zinc, strontiums and multiple organic acid and fatty acid composition.Other is identical with detailed description of the invention one.
Detailed description of the invention seven: present embodiment and detailed description of the invention one unlike: described Wudalianchi metasilicic acid mineral water is the mineral water taking from two dragon's fountains, the trace element containing multiple beneficial skins such as metasilicic acid, potassium, sodium, calcium, magnesium, strontiums.Other is identical with detailed description of the invention one.
Detailed description of the invention eight: present embodiment and detailed description of the invention one unlike: described Fructus Hippophae Auricularia is the Auricularia being enriched with Fructus Hippophae flavone, containing abundant flavones ingredient in Auricularia, can play good natural anti-oxidation skin care activity.Other is identical with detailed description of the invention one.
Detailed description of the invention nine: the Wudalianchi Volcanic sludge of present embodiment and Fructus Hippophae Auricularia are without the preparation method of adding facial film, and it carries out according to following steps:
One, get Fructus Hippophae Auricularia to clean, naturally dry in the shade, then 200 orders are crushed to, mix with the ratio of deionized water in solid-to-liquid ratio 50:1,10h is extracted again under 80 DEG C of conditions, then centrifugal under the centrifugal condition of 4000 revs/min, get that supernatant is evaporated to stock solution 1/5, last lyophilization, obtains Fructus Hippophae Auricularia gel extract;
Two, get Wudalianchi Volcanic sludge, be crushed to 800 orders, Wudalianchi Volcanic sludge powder;
Three, the Fructus Hippophae Auricularia gel extract of 5 ~ 20 parts, the Wudalianchi Volcanic sludge of 20 ~ 60 parts and 30 ~ 80 portions of Wudalianchi metasilicic acid mineral waters are got by weight, be placed in emulsion tank to shear, wherein, shear temperature is 70 DEG C, shear time is 20min, shearing rotating speed is 4000 revs/min, obtains Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without adding facial film;
Four, the facial film that step 3 obtains is loaded in high temperature resistant sterilization packaging, carry out high pressure steam sterilization, sterilising conditions is: 121.3 DEG C, 20min, aseptically encapsulate, namely complete described Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without the preparation adding facial film.
Detailed description of the invention ten: present embodiment and detailed description of the invention nine are the Wudalianchi Volcanic sludge of 25 ~ 55 parts and mass fraction unlike: Fructus Hippophae Auricularia gel extract, the mass fraction of getting 8 ~ 16 parts by weight described in step 3 is 35 ~ 65 portions of Wudalianchi metasilicic acid mineral waters.Other is identical with detailed description of the invention nine.
Detailed description of the invention 11: present embodiment and detailed description of the invention nine are the Wudalianchi Volcanic sludge of 28 ~ 50 parts and mass fraction unlike: Fructus Hippophae Auricularia gel extract, the mass fraction of getting 10 ~ 15 parts by weight described in step 3 is 40 ~ 60 portions of Wudalianchi metasilicic acid mineral waters.Other is identical with detailed description of the invention nine.
Detailed description of the invention 12: present embodiment and detailed description of the invention nine are the Wudalianchi Volcanic sludge of 30 ~ 45 parts and mass fraction unlike: Fructus Hippophae Auricularia gel extract, the mass fraction of getting 11 ~ 14 parts by weight described in step 3 is 45 ~ 55 portions of Wudalianchi metasilicic acid mineral waters.Other is identical with detailed description of the invention nine.
Detailed description of the invention 13: present embodiment and detailed description of the invention nine are the Wudalianchi Volcanic sludge of 35 ~ 40 parts and mass fraction unlike: Fructus Hippophae Auricularia gel extract, the mass fraction of getting 12 ~ 13 parts by weight described in step 3 is 45 ~ 50 portions of Wudalianchi metasilicic acid mineral waters.Other is identical with detailed description of the invention nine.
Content of the present invention is not limited only to the content of the respective embodiments described above, and the combination of one of them or several detailed description of the invention equally also can realize the object of inventing.
Beneficial effect of the present invention is verified by following examples:
The Wudalianchi Volcanic sludge that following embodiment adopts and Fructus Hippophae Auricularia to be Fructus Hippophae Auricularia gel extract, the mass fraction of 12 parts without to add its active component of facial film be mass fraction the be Wudalianchi Volcanic sludge of 39 parts and mass fraction are 49 portions of Wudalianchi metasilicic acid mineral waters.
This Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia as follows without the preparation method of adding facial film:
One, get Fructus Hippophae Auricularia to clean, naturally dry in the shade, then 200 orders are crushed to, mix with the ratio of deionized water in solid-to-liquid ratio 50:1,10h is extracted again under 80 DEG C of conditions, then centrifugal under the centrifugal condition of 4000 revs/min, get that supernatant is evaporated to stock solution 1/5, last lyophilization, obtains Fructus Hippophae Auricularia gel extract;
Two, get Wudalianchi Volcanic sludge, be crushed to 800 orders, Wudalianchi Volcanic sludge powder;
Three, the Fructus Hippophae Auricularia gel extract of 12 parts, the Wudalianchi Volcanic sludge of 39 parts and 49 portions of Wudalianchi metasilicic acid mineral waters are got by weight, be placed in emulsion tank to shear, wherein, shear temperature is 70 DEG C, shear time is 20min, shearing rotating speed is 4000 revs/min, obtains Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without adding facial film;
Four, the facial film that step 3 obtains is loaded in high temperature resistant sterilization packaging, carry out high pressure steam sterilization, sterilising conditions is: 121.3 DEG C, 20min, aseptically encapsulate, namely complete described Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without the preparation adding facial film.
Embodiment 1
Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia are without the moisturizing experimentation of adding facial film
Choose clean glass plate one piece, paste the medical air-permeable adhesive tape of one deck 1.0cm × 5.0cm size above, accurate facial film use amount, to 0.25g, spreads upon medical air-permeable adhesive tape surface uniformly, and being equivalent to applying amount is 50mg/cm
2, close with actual use amount.Select in exsiccator and place that saturated calcium chloride is molten and to control room temperature be that 20 degrees Celsius of liquid make moisture stable in exsiccator 27%.The medical air-permeable adhesive tape scribbling facial film is placed on respectively at 0.5 hour in exsiccator, 1 hour, 1.5 hours, within 2 hours, measures its moisturizing rate.And with 10% glycerol with do not add the mask matrix of Auricularia gel product measuring method is the same in contrast.Measurement result is shown in Table 1.
Moisturizing rate=M
t÷ M
0× 100% (M in formula
tfor the quality of sample after the placement t time, M
0for placing the quality of front sample)
The external moisturizing experimental measurements of table 1
Because the service time of facial film is at 0.5 hours, thus the facial film of this experiment measuring, mask matrix, the 10% glycerol moistening effect of 0 to 2 hours.Moisturizing rate forms downward trend along with the increase of time, the decrease speed of substrate in two hours is obviously greater than the glycerol of facial film and 10%, the moisturizing rate decrease speed of facial film and the speed of 10% glycerol are relatively, can prove that the Wudalianchi Volcanic sludge adopted is close with 10% glycerol without the moistening effect adding facial film with Fructus Hippophae Auricularia, as shown in Table 1, the moistening effect of facial film in 1 hour is better than 10% glycerol, according to document (Du little Hao, 2000) known, the moistening effect of facial film is better.
Embodiment 2
Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia are tested the removing of DPPH without adding facial film
For verifying the antioxidant activity of this facial film, the present embodiment is studied for the scavenging action of this facial film to DPPH.The DPPH solution of the 20mg/L of sample thief 1mg facial film and 5mL adds in same test tube, shake up, place 30 minutes in the dark, measuring absorbance with ultraviolet spectrophotometer at 517nm is A sample, measuring absorbance at 517nm after removing the ionized water 1mL method process same with sample is ADPPH contrast, the ethanol solution of sample thief 1mg facial film and 5mL adds in same test tube and shakes up, and dark place placement 30 minutes, measuring absorbance with ultraviolet spectrophotometer at 517nm was A sample blank.Calculate DPPH clearance rate as follows:
DPPH clearance rate=[1-(A sample-A sample blank)/ADPPH contrasts] × 100% repeats to do 5 groups of experiments, and experimental result is in table 2.By experimental result known each group experiment facial film to the clearance rate of DPPH all more than 50% DPPH clearance rate meansigma methods be 52.78%, visible facial film has good antioxidant activity.
Table 2DPPH removes experimental measurements
The Wudalianchi Volcanic sludge prepared for understanding the present invention and Fructus Hippophae Auricularia are without the result of use of adding facial film, with the form of questionnaire survey, the Wudalianchi Volcanic sludge of preparation and Fructus Hippophae Auricularia are carried out to try out widely to have been investigated (as shown in table 3) without adding facial film, trier 100 people, wherein male 45 people, women 55 people, the oldest 53 years old, minimum 18 years old, about 32 years old mean age, trier has the symptom such as drying, peeling in various degree in Wudalianchi Volcanic sludge on probation and Fructus Hippophae Auricularia without skin before adding facial film.Regain effective questionnaire 95 parts altogether after on probation, 95 triers use this product after 4 weeks to smearing sensation, skin improves, stimulate the result of use of the indices of allergy, the result of self evaluation is as follows:
Table 3 product beta test statistical effect table
As shown in Table 3:
1, shower sensation: the trier of 53.68% takes a shower and feels good, the trier of 25.26% takes a shower sensation better;
2, skin condition: the trier of 51.57% has moderate to improve, and the trier of 21.05% has clear improvement;
3, allergy is stimulated: non-stimulated irritated example.
As can be seen from the result of the self assessment of trier, Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia have well smear sensation without adding facial film, have good improvement result, do not find that product produces stimulation allergic phenomena to trier to the skin condition of user.Show according to survey result: Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia have higher moisturizing and anti-oxidation efficacy without the effective ingredient and Wudalianchi Volcanic sludge powder, metasilicic acid mineral water effective ingredient adding facial film effective land productivity Fructus Hippophae Auricularia gel, effectively can improve skin condition, recover skin natural health.
Claims (10)
1. Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia are without adding facial film, it is characterized in that its active component to be mass fraction be the Fructus Hippophae Auricularia gel extract of 5 ~ 20 parts, mass fraction is the Wudalianchi Volcanic sludge of 20 ~ 60 parts and mass fraction is 30 ~ 80 portions of Wudalianchi metasilicic acid mineral waters.
2. Wudalianchi Volcanic sludge according to claim 1 and Fructus Hippophae Auricularia are without adding facial film, it is characterized in that its active component to be mass fraction be the Fructus Hippophae Auricularia gel extract of 8 ~ 16 parts, mass fraction is the Wudalianchi Volcanic sludge of 25 ~ 55 parts and mass fraction is 35 ~ 65 portions of Wudalianchi metasilicic acid mineral waters.
3. Wudalianchi Volcanic sludge according to claim 2 and Fructus Hippophae Auricularia are without adding facial film, it is characterized in that its active component to be mass fraction be the Fructus Hippophae Auricularia gel extract of 10 ~ 15 parts, mass fraction is the Wudalianchi Volcanic sludge of 28 ~ 50 parts and mass fraction is 40 ~ 60 portions of Wudalianchi metasilicic acid mineral waters.
4. Wudalianchi Volcanic sludge according to claim 3 and Fructus Hippophae Auricularia are without adding facial film, it is characterized in that its active component to be mass fraction be the Fructus Hippophae Auricularia gel extract of 11 ~ 14 parts, mass fraction is the Wudalianchi Volcanic sludge of 30 ~ 45 parts and mass fraction is 45 ~ 55 portions of Wudalianchi metasilicic acid mineral waters.
5. Wudalianchi Volcanic sludge according to claim 1 and Fructus Hippophae Auricularia are without adding facial film, it is characterized in that described Wudalianchi Volcanic sludge is the sludge taking from Wudalianchi Yaoquanshan sludge band.
6. Wudalianchi Volcanic sludge according to claim 1 and Fructus Hippophae Auricularia are without adding facial film, it is characterized in that described Wudalianchi metasilicic acid mineral water is the mineral water taking from two dragon's fountains.
7. Wudalianchi Volcanic sludge according to claim 1 and Fructus Hippophae Auricularia are without adding facial film, and its special type is that described Fructus Hippophae Auricularia is the Auricularia being enriched with Fructus Hippophae flavone.
8. preparation Wudalianchi Volcanic sludge according to claim 1 and Fructus Hippophae Auricularia are without the method for adding facial film, it is characterized in that it carries out according to following steps:
One, get Fructus Hippophae Auricularia to clean, naturally dry in the shade, then 200 orders are crushed to, mix with the ratio of deionized water in solid-to-liquid ratio 50:1,10h is extracted again under 80 DEG C of conditions, then centrifugal under the centrifugal condition of 4000 revs/min, get that supernatant is evaporated to stock solution 1/5, last lyophilization, obtains Fructus Hippophae Auricularia gel extract;
Two, get Wudalianchi Volcanic sludge, be crushed to 800 orders, Wudalianchi Volcanic sludge powder;
Three, the Fructus Hippophae Auricularia gel extract of 5 ~ 20 parts, the Wudalianchi Volcanic sludge of 20 ~ 60 parts and 30 ~ 80 portions of Wudalianchi metasilicic acid mineral waters are got by weight, be placed in emulsion tank to shear, wherein, shear temperature is 70 DEG C, shear time is 20min, shearing rotating speed is 4000 revs/min, obtains Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without adding facial film;
Four, the facial film that step 3 obtains is loaded in high temperature resistant sterilization packaging, carry out high pressure steam sterilization, sterilising conditions is: 121.3 DEG C, 20min, aseptically encapsulate, namely complete described Wudalianchi Volcanic sludge and Fructus Hippophae Auricularia without the preparation adding facial film.
9. Wudalianchi Volcanic sludge according to claim 8 and Fructus Hippophae Auricularia are without the preparation method of adding facial film, it is characterized in that getting the Fructus Hippophae Auricularia gel extract of 8 ~ 16 parts, the Wudalianchi Volcanic sludge of 25 ~ 55 parts and 35 ~ 65 portions of Wudalianchi metasilicic acid mineral waters by weight described in step 3.
10. Wudalianchi Volcanic sludge according to claim 8 and Fructus Hippophae Auricularia are without the preparation method of adding facial film, it is characterized in that getting the Fructus Hippophae Auricularia gel extract of 10 ~ 15 parts, the Wudalianchi Volcanic sludge of 28 ~ 50 parts and 40 ~ 60 portions of Wudalianchi metasilicic acid mineral waters by weight described in step 3.
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| WO2018145446A1 (en) * | 2017-02-08 | 2018-08-16 | 广州无添加主义化妆品有限公司 | Aseptic facial mask filling device and mask preparation method therefor |
| CN113081908A (en) * | 2021-04-23 | 2021-07-09 | 黑龙江省科学院自然与生态研究所 | Artificial growth-promoting volcanic mud and preparation method and application thereof |
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