CN105232369B - Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof - Google Patents
Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof Download PDFInfo
- Publication number
- CN105232369B CN105232369B CN201510627755.9A CN201510627755A CN105232369B CN 105232369 B CN105232369 B CN 105232369B CN 201510627755 A CN201510627755 A CN 201510627755A CN 105232369 B CN105232369 B CN 105232369B
- Authority
- CN
- China
- Prior art keywords
- agaric
- wudalianchi
- buckthorn
- sea
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000003145 Hippophae rhamnoides Nutrition 0.000 title claims abstract description 84
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 240000000950 Hippophae rhamnoides Species 0.000 title 1
- 241000229143 Hippophae Species 0.000 claims abstract description 83
- 230000001815 facial effect Effects 0.000 claims abstract description 63
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 31
- 239000011707 mineral Substances 0.000 claims abstract description 31
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000010802 sludge Substances 0.000 claims description 72
- 239000003643 water by type Substances 0.000 claims description 20
- 230000001954 sterilising effect Effects 0.000 claims description 12
- 239000000470 constituent Substances 0.000 claims description 11
- 238000004659 sterilization and disinfection Methods 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 7
- 239000002002 slurry Substances 0.000 claims description 7
- 238000010008 shearing Methods 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 239000000839 emulsion Substances 0.000 claims description 4
- 229930003944 flavone Natural products 0.000 claims description 4
- 235000011949 flavones Nutrition 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 238000004806 packaging method and process Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 claims description 2
- 150000002212 flavone derivatives Chemical class 0.000 claims description 2
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 16
- 230000003020 moisturizing effect Effects 0.000 abstract description 11
- 239000002994 raw material Substances 0.000 abstract description 9
- 230000003078 antioxidant effect Effects 0.000 abstract description 7
- 241000233866 Fungi Species 0.000 abstract description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 12
- 239000000047 product Substances 0.000 description 9
- 241000863032 Trieres Species 0.000 description 8
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 8
- 235000011187 glycerol Nutrition 0.000 description 6
- 238000012360 testing method Methods 0.000 description 5
- 230000002500 effect on skin Effects 0.000 description 4
- 206010020751 Hypersensitivity Diseases 0.000 description 3
- 238000002835 absorbance Methods 0.000 description 3
- 239000002390 adhesive tape Substances 0.000 description 3
- 208000026935 allergic disease Diseases 0.000 description 3
- 230000007815 allergy Effects 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000011835 investigation Methods 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 238000003825 pressing Methods 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 235000006708 antioxidants Nutrition 0.000 description 2
- 235000020682 bottled natural mineral water Nutrition 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 150000002213 flavones Chemical class 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000011591 potassium Substances 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 229910052712 strontium Inorganic materials 0.000 description 2
- CIOAGBVUUVVLOB-UHFFFAOYSA-N strontium atom Chemical compound [Sr] CIOAGBVUUVVLOB-UHFFFAOYSA-N 0.000 description 2
- 241000221377 Auricularia Species 0.000 description 1
- 241000221454 Auriculariaceae Species 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000172 allergic effect Effects 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 230000009693 chronic damage Effects 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
Disclosed is a Wudalianchi volcanic slime and sea buckthorn edible fungus additive-free facial mask and a preparation method thereof, relating to the Wudalianchi volcanic slime and sea buckthorn edible fungus additive-free facial mask and the preparation method thereof. The invention aims to solve the problems that the existing mask products need to be added with industrial raw materials, potential harm is generated to the skin and the body of a consumer, and the skin care effect of the product without the industrial raw materials is not good. It comprises sea buckthorn agaric gel extract, Wudalianchi volcanic slime and Wudalianchi metasilicic acid mineral water. The mask disclosed by the invention is a mask product without any industrial raw material and with good moisturizing and antioxidant effects, so that people can feel more confident and safely enjoy the natural skin care effects of the natural volcanic mineral mud in the five great continuous ponds and the sea buckthorn edible fungi.
Description
Technical field
The present invention relates to Wudalianchi Volcanic sludges and the no added facial mask of sea-buckthorn agaric and preparation method thereof.
Background technology
The formula of facial treatment mask product has a raw material of industry addition, such as moisturizer, emulsifier, stabilizer, mineral oil, manually
Grease, preservative, essential oil etc..And these additives have potential hazard to the skin of people, for a long time using skin can be caused
Profound chronic injury.Product skin effect without adding these raw materials of industry is again undesirable, in order to solve this problem,
The present invention is aided with the sand for having good moisturizing and anti-oxidation efficacy using natural Wudalianchi Volcanic sludge and mineral water as base-material
Spine agaric gel extract is developed into Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric, that is, solves the raw material of industry
To the potential hazard of skin, and there is good skin effect.
Sea-buckthorn agaric is Auriculariaceae, the edible fungus of Auricularia.Recent study is found, relatively rich sugar is contained in agaric
And collagen, there are good moisturizing and anti-oxidant isoreactivity, sea-buckthorn agaric also contains a large amount of flavones, than other kind agarics
There are better anti-oxidant, the skin care effects such as uvioresistant, these effects of sea-buckthorn agaric to there is good skin-protection and health-care to act on, this hair
It is bright to be ground with natural base-material " Wudalianchi Volcanic sludge ", " the Wudalianchi natural mineral water " for having same skin care effect with agaric
Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric is made.It is pure natural no added preferably to play natural Wudalianchi
Sludge, the skin care effect of mineral resource and sea-buckthorn agaric.
Invention content
The purpose of the present invention is to solve existing mask products all to need the addition raw material of industry, to consumer skin and body
Body all generates potential hazard, without adding the product skin effect of the raw material of industry and bad problem, and provides Wudalianchi
Volcanic slurry and the no added facial mask of sea-buckthorn agaric and preparation method thereof.
The Wudalianchi Volcanic sludge of the present invention and the no added facial mask of sea-buckthorn agaric, its active constituent is that mass fraction is
5~20 parts of sea-buckthorn agaric gel extract, the Wudalianchi Volcanic sludge that mass fraction is 20~60 parts and mass fraction are
30~80 portions of Wudalianchi metasilicic acid mineral waters.
The preparation method of the Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric of the present invention, it is according to following step
Suddenly it carries out：
One, it takes sea-buckthorn agaric to clean, dries in the shade naturally, be then crushed to 200 mesh, solid-to-liquid ratio 50 is pressed with deionized water:1 ratio
Example mixing, then 10h is extracted under the conditions of 80 DEG C, it is then centrifuged under 4000 revs/min of centrifugal condition, supernatant is taken to be concentrated under reduced pressure
It to the 1/5 of stoste, is finally freeze-dried, obtains sea-buckthorn agaric gel extract；
Two, Wudalianchi Volcanic sludge is taken, 800 mesh are crushed to, obtains Wudalianchi Volcanic sludge powder；
Three, 5~20 parts of sea-buckthorn agaric gel extract, 20~60 parts of Wudalianchi Volcanic sludge are taken in parts by weight
It with 30~80 portions of Wudalianchi metasilicic acid mineral waters, is placed in emulsion tank and is sheared, wherein shear temperature is 70 DEG C, shearing
Time is 20min, and shearing rotating speed is 4000 revs/min, obtains Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric；
Four, the facial mask that step 3 obtains is fitted into high temperature resistant sterilization packaging, carries out high pressure steam sterilization, sterilising conditions
For：121.3 DEG C, 20min is aseptically packaged, that is, completes the Wudalianchi Volcanic sludge and sea-buckthorn agaric
The preparation of no added facial mask.
The present invention includes following advantageous effect：
Present invention Wudalianchi Volcanic sludge, Wudalianchi natural mineral water and sea-buckthorn agaric gel extract development
At i.e. no added any raw material of industry, and there are the Wudalianchi Volcanic sludge of good moisturizing and antioxidant effect and sea-buckthorn agaric
No added mask product, allows people more to trust, the day of safe enjoyment natural Wudalianchi Volcanic mineral spring sludge and sea-buckthorn agaric
Right skin effect.
Moistening effect of the facial mask of the present invention in 1 hour is got well than 10% glycerine, and the moistening effect of facial mask is preferable.Facial mask
To the clearance rate of DPPH 50% or more, facial mask has preferable antioxidant activity.
Specific implementation mode
Specific implementation mode one：The Wudalianchi Volcanic sludge of present embodiment and the no added facial mask of sea-buckthorn agaric, it
Active constituent is the sea-buckthorn agaric gel extract that mass fraction is 5~20 parts, the Wudalianchi that mass fraction is 20~60 parts
Volcanic slurry and mass fraction are 30~80 portions of Wudalianchi metasilicic acid mineral waters.
Specific implementation mode two：The present embodiment is different from the first embodiment in that：Wudalianchi Volcanic sludge with
The no added facial mask of sea-buckthorn agaric, its active constituent are the sea-buckthorn agaric gel extract that mass fraction is 8~16 parts, mass parts
Number is 35~65 portions of Wudalianchi metasilicic acid mineral waters for 25~55 parts of Wudalianchi Volcanic sludge and mass fraction.It is other with
Specific implementation mode one is identical.
Specific implementation mode three：The present embodiment is different from the first embodiment in that：Wudalianchi Volcanic sludge with
The no added facial mask of sea-buckthorn agaric, its active constituent are the sea-buckthorn agaric gel extract that mass fraction is 10~15 parts, quality
The Wudalianchi Volcanic sludge and mass fraction that number is 28~50 parts are 40~60 portions of Wudalianchi metasilicic acid mineral waters.It is other
It is same as the specific embodiment one.
Specific implementation mode four：The present embodiment is different from the first embodiment in that：Wudalianchi Volcanic sludge with
The no added facial mask of sea-buckthorn agaric, its active constituent are the sea-buckthorn agaric gel extract that mass fraction is 11~14 parts, quality
The Wudalianchi Volcanic sludge and mass fraction that number is 30~45 parts are 45~55 portions of Wudalianchi metasilicic acid mineral waters.It is other
It is same as the specific embodiment one.
Specific implementation mode five：The present embodiment is different from the first embodiment in that：Wudalianchi Volcanic sludge with
The no added facial mask of sea-buckthorn agaric, its active constituent are the sea-buckthorn agaric gel extract that mass fraction is 12~13 parts, quality
The Wudalianchi Volcanic sludge and mass fraction that number is 35~40 parts are 45~50 portions of Wudalianchi metasilicic acid mineral waters.It is other
It is same as the specific embodiment one.
Specific implementation mode six：The present embodiment is different from the first embodiment in that：The Wudalianchi Volcanic
Sludge is the sludge for being derived from Wudalianchi Yaoquanshan sludge band, contains the micro- of the multiple beneficials skin such as potassium, sodium, calcium, magnesium, zinc, strontium
Secondary element and a variety of organic acids and fatty acid ingredient.It is other same as the specific embodiment one.
Specific implementation mode seven：The present embodiment is different from the first embodiment in that：The inclined silicon in the Wudalianchi
Sour mineral water is taken from the mineral water of two dragon's fountains, the micro member containing the multiple beneficials skin such as metasilicic acid, potassium, sodium, calcium, magnesium, strontium
Element.It is other same as the specific embodiment one.
Specific implementation mode eight：The present embodiment is different from the first embodiment in that：The sea-buckthorn agaric is richness
Collection has the agaric of Hippophate flavone, contains abundant flavones ingredient in agaric, can play good natural anti-oxidation skin care and live
Property.It is other same as the specific embodiment one.
Specific implementation mode nine：The preparation of the Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric of present embodiment
Method, it is followed the steps below：
One, it takes sea-buckthorn agaric to clean, dries in the shade naturally, be then crushed to 200 mesh, solid-to-liquid ratio 50 is pressed with deionized water:1 ratio
Example mixing, then 10h is extracted under the conditions of 80 DEG C, it is then centrifuged under 4000 revs/min of centrifugal condition, supernatant is taken to be concentrated under reduced pressure
It to the 1/5 of stoste, is finally freeze-dried, obtains sea-buckthorn agaric gel extract；
Two, take Wudalianchi Volcanic sludge, be crushed to 800 mesh, Wudalianchi Volcanic sludge powder；
Three, 5~20 parts of sea-buckthorn agaric gel extract, 20~60 parts of Wudalianchi Volcanic sludge are taken in parts by weight
It with 30~80 portions of Wudalianchi metasilicic acid mineral waters, is placed in emulsion tank and is sheared, wherein shear temperature is 70 DEG C, shearing
Time is 20min, and shearing rotating speed is 4000 revs/min, obtains Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric；
Four, the facial mask that step 3 obtains is fitted into high temperature resistant sterilization packaging, carries out high pressure steam sterilization, sterilising conditions
For：121.3 DEG C, 20min is aseptically packaged, that is, completes the Wudalianchi Volcanic sludge and sea-buckthorn agaric
The preparation of no added facial mask.
Specific implementation mode ten：Present embodiment is unlike specific implementation mode nine：Weight is pressed described in step 3
Amount number takes 8~16 parts of sea-buckthorn agaric gel extract, the Wudalianchi Volcanic sludge that mass fraction is 25~55 parts and matter
Amount number is 35~65 portions of Wudalianchi metasilicic acid mineral waters.It is other identical as specific implementation mode nine.
Specific implementation mode 11：Present embodiment is unlike specific implementation mode nine：Pressing described in step 3
Parts by weight take 10~15 parts sea-buckthorn agaric gel extract, mass fraction be 28~50 parts Wudalianchi Volcanic sludge and
Mass fraction is 40~60 portions of Wudalianchi metasilicic acid mineral waters.It is other identical as specific implementation mode nine.
Specific implementation mode 12：Present embodiment is unlike specific implementation mode nine：Pressing described in step 3
Parts by weight take 11~14 parts sea-buckthorn agaric gel extract, mass fraction be 30~45 parts Wudalianchi Volcanic sludge and
Mass fraction is 45~55 portions of Wudalianchi metasilicic acid mineral waters.It is other identical as specific implementation mode nine.
Specific implementation mode 13：Present embodiment is unlike specific implementation mode nine：Pressing described in step 3
Parts by weight take 12~13 parts sea-buckthorn agaric gel extract, mass fraction be 35~40 parts Wudalianchi Volcanic sludge and
Mass fraction is 45~50 portions of Wudalianchi metasilicic acid mineral waters.It is other identical as specific implementation mode nine.
The content of present invention is not limited only to the content of the respective embodiments described above, the group of one of them or several specific implementation modes
Contract sample can also realize the purpose of invention.
Beneficial effects of the present invention are verified by following embodiment：
Wudalianchi Volcanic sludge that following embodiments use is with the no added facial mask of sea-buckthorn agaric its active constituent for matter
Measuring sea-buckthorn agaric gel extract, the Wudalianchi Volcanic sludge that mass fraction is 39 parts and mass fraction that number is 12 parts is
49 portions of Wudalianchi metasilicic acid mineral waters.
The preparation method of the Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric is as follows：
One, it takes sea-buckthorn agaric to clean, dries in the shade naturally, be then crushed to 200 mesh, solid-to-liquid ratio 50 is pressed with deionized water:1 ratio
Example mixing, then 10h is extracted under the conditions of 80 DEG C, it is then centrifuged under 4000 revs/min of centrifugal condition, supernatant is taken to be concentrated under reduced pressure
It to the 1/5 of stoste, is finally freeze-dried, obtains sea-buckthorn agaric gel extract；
Two, take Wudalianchi Volcanic sludge, be crushed to 800 mesh, Wudalianchi Volcanic sludge powder；
Three, 12 parts of sea-buckthorn agaric gel extract, 39 parts of Wudalianchi Volcanic sludge and 49 parts are taken in parts by weight
Wudalianchi metasilicic acid mineral water, is placed in emulsion tank and is sheared, wherein shear temperature is 70 DEG C, and shear time is
20min, shearing rotating speed are 4000 revs/min, obtain Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric；
Four, the facial mask that step 3 obtains is fitted into high temperature resistant sterilization packaging, carries out high pressure steam sterilization, sterilising conditions
For：121.3 DEG C, 20min is aseptically packaged, that is, completes the Wudalianchi Volcanic sludge and sea-buckthorn agaric
The preparation of no added facial mask.
Embodiment 1
The moisturizing experimental study of Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric
One piece clean of glass plate is chosen, in the medical air-permeable adhesive tape of one layer of 1.0cm × 5.0cm size of upper face paste, accurately
Facial mask usage amount is uniformly applied to medical air-permeable adhesive tape surface to 0.25g, and it is 50mg/cm to be equivalent to applying amount2, with reality
Usage amount is close.Select drier in place saturation calcium chloride it is molten and control room temperature be 20 degrees Celsius of liquid make it is wet in drier
Degree is stablized 27%.The medical air-permeable adhesive tape for being coated with facial mask is placed in drier respectively at 0.5 hour, 1 hour, 1.5 is small
When, measure within 2 hours its moisturizing rate.And with 10% glycerine and it is added without the mask matrix of agaric gel product measurement method as a contrast
Ibid.Measurement result is shown in Table 1.
Moisturizing rate=Mt÷M0× 100% (M in formulatFor the quality of sample after the placement t times, M0For the matter of sample before placement
Amount)
1 external moisturizing experimental measurements of table
Since the usage time of facial mask was at 0.5 hour or so, so the facial mask, mask matrix, 10% sweet that this experiment measures
0 to 2 hours moistening effects of oil.Moisturizing rate decreases as time increases, lower reduction of speed of the matrix in two hours
Degree is significantly greater than facial mask and 10% glycerine, and the moisturizing rate decrease speed of facial mask and the speed of 10% glycerine relatively, can be with
Prove that the Wudalianchi Volcanic sludge used and the moistening effect of the no added facial mask of sea-buckthorn agaric are close with 10% glycerine, by table 1
It is found that moistening effect of the facial mask in 1 hour is got well than 10% glycerine, according to document (Du little Hao, 2000) it is found that the guarantor of facial mask
Wet effect is preferable.
Embodiment 2
Wudalianchi Volcanic sludge tests the removing of DPPH with the no added facial mask of sea-buckthorn agaric
To verify the antioxidant activity of this facial mask, the present embodiment studies the scavenging effect of DPPH for the facial mask.
It takes the DPPH solution of sample 1mg facial masks and the 20mg/L of 5mL to be added in same test tube, shakes up, place 30 minutes in the dark, use
It is A samples that ultraviolet specrophotometer measures absorbance in 517nm, remove after same with the sample methods of ionized water 1mL are handled
517nm measures absorbance and is compareed for ADPPH, takes the ethanol solution of sample 1mg facial masks and 5mL to be added in same test tube and shakes
It is even, it is placed 30 minutes at dark, it is A sample blanks to measure absorbance in 517nm with ultraviolet specrophotometer.As follows
Calculate DPPH clearance rates：
DPPH clearance rates=[1- (A sample-A sample blanks)/ADPPH controls] × 100% repeats to do 5 groups of experiments, tests
It the results are shown in Table 2.Each group experiment facial mask is averaged to the clearance rate of DPPH in 50% or more DPPH clearance rates known to experimental result
Value is 52.78%, it is seen that facial mask has preferable antioxidant activity.
Table 2DPPH removes experimental measurements
。
To understand the using effect of Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric prepared by the present invention, to ask
The form for rolling up investigation has carried out extensive investigation on probation to the Wudalianchi Volcanic sludge of preparation with the no added facial mask of sea-buckthorn agaric
(as shown in table 3), 100 people of trier, wherein 45 people of male, 55 people of women is the oldest 53 years old, 18 years old minimum, average age
32 years old or so, trier's skin before Wudalianchi Volcanic sludge on probation and the no added facial mask of sea-buckthorn agaric had in various degree
The symptoms such as drying, peeling.Withdraw 95 parts of effective questionnaire after on probation altogether, 95 triers using this product after 4 weeks to smear feel,
Skin improves, stimulates the using effect of the indices of allergy, and the result of self-assessment is as follows：
3 product beta test effect statistical form of table
As shown in Table 3：
1, it takes a shower and feels：53.68% trier takes a shower and feels good, and 25.26% trier, which takes a shower, feels preferable；
2, skin condition：51.57% trier has moderate improvement, 21.05% trier to have clear improvement；
3, allergy is stimulated：Non-stimulated allergy example.
Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric are can be seen that from the result of the self-assessment of trier
Have to smear well and feel there is good improvement result to the skin condition of user, does not find that product generates trier
Stimulate allergic phenomena.It is shown according to investigation result：Wudalianchi Volcanic sludge and the effective land productivity of the no added facial mask of sea-buckthorn agaric are husky
Active ingredient and Wudalianchi Volcanic sludge powder, the metasilicic acid mineral water active ingredient of spine agaric gel have higher moisturizing and resist
Oxidation efficiency can be effectively improved skin condition, restore skin natural health.
Claims (7)
1. Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric, it is characterised in that its active constituent is that mass fraction is
5~20 parts of sea-buckthorn agaric gel extract, the Wudalianchi Volcanic sludge that mass fraction is 20~60 parts and mass fraction are
30~80 portions of Wudalianchi metasilicic acid mineral waters；The Wudalianchi Volcanic sludge is to be derived from Wudalianchi Yaoquanshan sludge band
Sludge；The Wudalianchi metasilicic acid mineral water is taken from the mineral water of two dragon's fountains；The sea-buckthorn agaric is to be enriched with
The agaric of Hippophate flavone；The sea-buckthorn agaric gel extract preparation method is as follows：It takes sea-buckthorn agaric to clean, dries in the shade naturally,
Then 200 mesh are crushed to, solid-to-liquid ratio 50 is pressed with deionized water:1 ratio mixing, then 10h is extracted under the conditions of 80 DEG C, then exist
It is centrifuged under 4000 revs/min of centrifugal condition, takes supernatant to be concentrated under reduced pressure into the 1/5 of stoste, be finally freeze-dried, obtain sea-buckthorn agaric
Gel extract.
2. Wudalianchi Volcanic sludge according to claim 1 and the no added facial mask of sea-buckthorn agaric, it is characterised in that it
Active constituent is the sea-buckthorn agaric gel extract that mass fraction is 8~16 parts, the Wudalianchi that mass fraction is 25~55 parts
Volcanic slurry and mass fraction are 35~65 portions of Wudalianchi metasilicic acid mineral waters.
3. Wudalianchi Volcanic sludge according to claim 2 and the no added facial mask of sea-buckthorn agaric, it is characterised in that it
Active constituent is the sea-buckthorn agaric gel extract that mass fraction is 10~15 parts, the Wudalianchi that mass fraction is 28~50 parts
Volcanic slurry and mass fraction are 40~60 portions of Wudalianchi metasilicic acid mineral waters.
4. Wudalianchi Volcanic sludge according to claim 3 and the no added facial mask of sea-buckthorn agaric, it is characterised in that it
Active constituent is the sea-buckthorn agaric gel extract that mass fraction is 11~14 parts, the Wudalianchi that mass fraction is 30~45 parts
Volcanic slurry and mass fraction are 45~55 portions of Wudalianchi metasilicic acid mineral waters.
5. the method for preparing Wudalianchi Volcanic sludge described in claim 1 and the no added facial mask of sea-buckthorn agaric, feature exist
It is followed the steps below in it：
One, it takes sea-buckthorn agaric to clean, dries in the shade naturally, be then crushed to 200 mesh, solid-to-liquid ratio 50 is pressed with deionized water:1 ratio is mixed
It closes, then 10h is extracted under the conditions of 80 DEG C, then centrifuged under 4000 revs/min of centrifugal condition, supernatant is taken to be concentrated under reduced pressure into original
The 1/5 of liquid, is finally freeze-dried, and obtains sea-buckthorn agaric gel extract；
Two, take Wudalianchi Volcanic sludge, be crushed to 800 mesh, Wudalianchi Volcanic sludge powder；
Three, 5~20 parts of sea-buckthorn agaric gel extract, 20~60 parts of Wudalianchi Volcanic sludge and 30 are taken in parts by weight
~80 portions of Wudalianchi metasilicic acid mineral waters, are placed in emulsion tank and are sheared, wherein shear temperature is 70 DEG C, shear time
For 20min, shearing rotating speed is 4000 revs/min, obtains Wudalianchi Volcanic sludge and the no added facial mask of sea-buckthorn agaric；
Four, the facial mask that step 3 obtains is fitted into high temperature resistant sterilization packaging, carries out high pressure steam sterilization, sterilising conditions are：
121.3 DEG C, 20min is aseptically packaged, that is, completes the Wudalianchi Volcanic sludge and sea-buckthorn agaric without adding
Add the preparation of facial mask.
6. the preparation method of Wudalianchi Volcanic sludge according to claim 5 and the no added facial mask of sea-buckthorn agaric, special
Sign is to take 8~16 parts of sea-buckthorn agaric gel extract, 25~55 parts of five Dalian in parts by weight described in step 3
Pond volcanic slurry and 35~65 portions of Wudalianchi metasilicic acid mineral waters.
7. the preparation method of Wudalianchi Volcanic sludge according to claim 5 and the no added facial mask of sea-buckthorn agaric, special
Sign is to take 10~15 parts of sea-buckthorn agaric gel extract, 28~50 parts of five Dalian in parts by weight described in step 3
Pond volcanic slurry and 40~60 portions of Wudalianchi metasilicic acid mineral waters.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510627755.9A CN105232369B (en) | 2015-09-28 | 2015-09-28 | Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510627755.9A CN105232369B (en) | 2015-09-28 | 2015-09-28 | Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105232369A CN105232369A (en) | 2016-01-13 |
| CN105232369B true CN105232369B (en) | 2018-09-28 |
Family
ID=55030379
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510627755.9A Expired - Fee Related CN105232369B (en) | 2015-09-28 | 2015-09-28 | Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105232369B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176328A (en) * | 2016-07-12 | 2016-12-07 | 广州聚泽生物科技有限公司 | A kind of mask composition containing natural volcanic mud and preparation method thereof |
| CN106829000B (en) * | 2017-02-08 | 2018-03-16 | 广州无添加主义化妆品有限公司 | The equipment and its sterilization filling method of sterilization filling facial mask |
| CN113081908B (en) * | 2021-04-23 | 2023-04-28 | 黑龙江省科学院自然与生态研究所 | Artificial fire mountain-promoting mineral mud and preparation method and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1891197A (en) * | 2005-07-04 | 2007-01-10 | 宋长昕 | Nano volcanic slurry beauty skin powder and its preparing method |
| CN101023912A (en) * | 2006-02-22 | 2007-08-29 | 王振宇 | Black agaric collagen mask and preparing method |
| CN101112357A (en) * | 2007-08-07 | 2008-01-30 | 李强 | Black fungus face pack powder for skin whitening |
| CN103142425A (en) * | 2013-04-02 | 2013-06-12 | 黑龙江省科学院火山与矿泉研究所 | Mineral mud nutritional emulsion and preparation method thereof |
| CN104905994A (en) * | 2015-05-15 | 2015-09-16 | 黑龙江省科学院火山与矿泉研究所 | Method for preparing Wudalianchi volcanic mud freeze-dried powder |
-
2015
- 2015-09-28 CN CN201510627755.9A patent/CN105232369B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1891197A (en) * | 2005-07-04 | 2007-01-10 | 宋长昕 | Nano volcanic slurry beauty skin powder and its preparing method |
| CN101023912A (en) * | 2006-02-22 | 2007-08-29 | 王振宇 | Black agaric collagen mask and preparing method |
| CN101112357A (en) * | 2007-08-07 | 2008-01-30 | 李强 | Black fungus face pack powder for skin whitening |
| CN103142425A (en) * | 2013-04-02 | 2013-06-12 | 黑龙江省科学院火山与矿泉研究所 | Mineral mud nutritional emulsion and preparation method thereof |
| CN104905994A (en) * | 2015-05-15 | 2015-09-16 | 黑龙江省科学院火山与矿泉研究所 | Method for preparing Wudalianchi volcanic mud freeze-dried powder |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105232369A (en) | 2016-01-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR101562560B1 (en) | Natural extract fermentation-maturity composition for preventing skin aging and improving skin wrinkle, Natural cosmetics containing that and Manufacturing method thereof | |
| CN103520053B (en) | Hair and body bathing powder | |
| CN106880551A (en) | A kind of body lotion for the moist soft and smooth skin that compacts and preparation method thereof | |
| CN105106660B (en) | A kind of kibe ointment and preparation method thereof of the easypro trace of skin care | |
| CN105232369B (en) | Wudalianchi volcanic mud and sea buckthorn agaric additive-free mask and preparation method thereof | |
| CN104398435A (en) | Mild cutin removing mask and preparation method thereof | |
| CN113332181A (en) | Essential oil capable of repairing damaged sebum membrane and cuticle and preparation method thereof | |
| KR100854017B1 (en) | Method of massaging skin having enhanced convenience | |
| CN105456124A (en) | Grape seed whitening mask | |
| CN104644535A (en) | Hair and body wash powder | |
| CN106176481A (en) | A kind of edible cosmetic composition and preparation method thereof | |
| CN105342865A (en) | Natural skin whitening and tendering mask | |
| CN114028282B (en) | Oil-control skin-cleaning composition and preparation method and application thereof | |
| CN113318025B (en) | Preparation method of Artocarpus heterophyllus extract and moisturizing and repairing composition | |
| CN104739715A (en) | Facial mask liquid containing flaxseed gum extracting solution and preparation method thereof | |
| CN108703918A (en) | It is a kind of to have effects that anti-dandruff shampoo and preparation method thereof | |
| CN107456567A (en) | Moist heel cream and preparation method thereof is repaired in a kind of anticracking detumescence | |
| CN112438935A (en) | Hemerocallis fulva leaf extracting solution and preparation method and application thereof | |
| CN108524342A (en) | A kind of hand pine needle face cream and preparation method thereof | |
| CN110013462A (en) | A kind of wormwood mud cream and preparation method thereof for whitening and skin-protecting | |
| CN105030585A (en) | Pure natural facial cream used for removing wrinkles | |
| CN108392456A (en) | A kind of natural skin-care dendrobium candidum surfactant and preparation method thereof | |
| CN105287977B (en) | A kind of sweet basil, aloe composition, preparation and its preparation method and application | |
| CN110151628A (en) | A kind of rose lipstick and preparation method thereof | |
| CN117771127B (en) | Colored microcapsule oil bead composition, soothing essence and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180928 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |