CN104983609B - A kind of aerosol type facial mask and preparation method thereof - Google Patents
A kind of aerosol type facial mask and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to a kind of aerosol type facial mask, it is characterised in that：Including the PPG 12/SMDI copolymers, the tamarind seed glue that mass ratio is 1 ~ 3%, the glycerin polyether 26 that mass ratio is 0.5 ~ 3% Wen Quinces seed extract, mass ratio is 4 ~ 10% that mass ratio is 3 ~ 6%.The advantage of the invention is that：Viscosity can increase with the rise of temperature, at less than 27 DEG C, low viscosity working fluid shape is presented, common atomizing pump can be used to be sprayed；Temperature rises to 30 DEG C ~ 45 DEG C, then retrogradation, which is presented, does not flow gel shape, user-friendly, and cationic salts of the product without monovalence or divalence, safe and environment-friendly, corrosion-free to production equipment.
Description
Technical field
The present invention relates to technical field of cosmetic preparation, more particularly to a kind of aerosol type facial mask and preparation method thereof.
Background technology
Facial mask class product in cosmetics, is mainly covered in face, moisture is penetrated into the cuticula of skin epidermis, skin
Become soft, high resilience.Facial mask class product has the effect of strengthening skin light, making skin that aerobic color be presented.Spraying facial mask
It is a kind of by atomizing pump, the bottled mask product that product spray is used on the facial skin.If normal pressure in bottle, then
Using mechanical force caused by finger pressure atomizing pump, extrude product and sprayed by spray nozzle；It is if empty for compression in bottle
Internal pressure caused by the solvent flashing such as gas or the third butane, then extrude product using internal pressure and sprayed by spray nozzle
Mist.If necessary to realize good fine and smooth uniform spraying, then require that in spraying, the flow fluid of low viscosity is presented in product content thing
Body shape.
Although spraying facial mask has the characteristics of easy to use, there is also some defects, such as the viscosity of spraying facial mask
It is relatively low, easily flowed down from the face, cause other inconvenience to consumer, be easier to make clothing dirty.In the prior art, facial mask is overcome
The scheme of flowing is that facial mask directly made into gel or gel shape, for example, Chinese patent CN 1669550A " comprising gellan gum or its
The cosmetic composition of derivative, solid chemical compound and monovalent salt, use the method for this composition and its application ", China is specially
Sharp CN 102836089A " spray skin-care cosmetic composition and its application ".The technical scheme proposed in above-mentioned patent document is
Gel spray is formed by gellan gum, PEG-240/HDI copolymers pair-ether of decyl tetradecyl alcohol polyethers -20 and monovalent cation salt
Mist product.
The technical scheme that above-mentioned patent uses is required to add the cationic salts of monovalence or divalence in the product to help
Gel is formed, salt is to production equipment and the atomizing pump containing metal parts has corrosiveness, is made troubles to production and use.Separately
Outside, gel facial mask needs the atomizing pump of particular design, realizes gel shear shinning using thixotropy principle and sprays.For spraying
Unsuitable too high, the too high then more difficult ejection of the gel viscosity of mist, or increase packaging material cost.After gel facial mask sprays, particle ratio
It is relatively thick, typically exhibit linear, do not reach the effect of spraying, the uneven technical problem of spraying effect be present.In the prior art
Have and for good spray effect, be prepared into the relatively low liquid facial mask of viscosity, but this liquid facial mask is ejected into after face
Easily flow, inconvenience is brought to user.Existing facial mask can not solve to need low viscosity, cover skin during spraying
After need highly viscous technical problem.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of aerosol type facial mask, and the viscosity of the facial mask can be with the liter of temperature
It is high and increase, presentation low viscosity working fluid shape at less than 27 DEG C, it common atomizing pump can be used to be sprayed, without particular design
Shower nozzle；Temperature rises to 30 DEG C -45 DEG C, then retrogradation, which is presented, does not flow gel shape, user-friendly, and product is free of one
The cationic salts of valency or divalence, it is safe and environment-friendly, it is corrosion-free to production equipment.
In order to solve the above technical problems, the present invention uses following technical scheme：A kind of aerosol type facial mask, it is characterised in that：
It is 0.5 ~ 3% including PPG-12/SMDI copolymers, the tamarind seed glue that mass ratio is 1 ~ 3%, mass ratio that mass ratio is 3 ~ 6%
Wen Quince seed extract, the glycerin polyether -26 that mass ratio is 4 ~ 10%.
Surplus be deionized water or deionized water with NMF, essence, preservative, there is moisturizing or whitening or crease-resistant work(
The mixed liquor of the active component of effect.NMF, essence, preservative, there is moisturizing or the active component of whitening or crease-resistant effect
Addition is conventional addition, no particular/special requirement.
Cationic salts of the technical solution of the present invention without monovalence or divalence.
The present invention also provides the preparation method of above-mentioned aerosol type facial mask, it is characterised in that：Comprise the following steps：
A, PPG-12/SMDI copolymers, tamarind seed Jiao, Wen Quinces seed extract are weighed in mass ratio, glycerin polyether -26, are gone
Ionized water, NMF, essence, preservative, there is moisturizing or the active component of whitening or crease-resistant effect；
B, by PPG-12/SMDI copolymers, tamarind seed Jiao, Wen Quinces seed extract, glycerin polyether -26 in rustless steel container
In be well mixed, be heated to 52 ~ 55 DEG C, be maintained at the temperature, stand 24 hours, then using three Kun grinding mills, mill to be formed
Slurry；
C, slurry obtained by step B is mixed with 5 ~ 20 DEG C of deionized water, stirs, obtain transparent flow liquid；
D, by NMF, essence, preservative, there is moisturizing or the active component of whitening or crease-resistant effect to add step C institutes
Transparent flow liquid is obtained, 5 ~ 20 DEG C is maintained at and stirs, be then returned to 20 ~ 25 DEG C, produce a kind of aerosol type facial mask.
PPG-12/SMDI copolymers of the present invention, CAS No.:9042-82-4, its feature are PPG-12/SMDI
The hydrophobic micro-structural of temperature-sensitive containing self aggregation in copolymer, the hydrophobic micro-structural meeting conglomerate of temperature-sensitive, makes viscosity when temperature raises
Increase with the rise of temperature.PPG-12/SMDI copolymers can select the commodity of A＆E CONNOCK companies production, trade name
Referred to as AEC PPG-12/SMDI Copolymer,
Tamarind seed glue of the present invention, CAS No.:84961-62-6, is a kind of water soluble polymer polysaccharide, Ke Yixuan
Food and the commodity of chemical company production are assisted with Japan five, trade name is GLYLOID 6C.
This invention Suo Shu Wen Quince seed extracts, CAS No.:85117-13-1, it is a kind of water soluble polymer polysaccharide,
The commodity of Japanese KOEI companies production can be selected, trade name is Quince Seed BG.
Glycerin polyether -26 of the present invention is solvent, CAS No.:31694-55-0, Switzerland CLARIANT can be selected
The commodity of company's production, trade name is Genapol G260.
Aerosol type facial mask prepared by the present invention, when temperature is below 27 DEG C, low viscosity working fluid shape is rendered as, can be used
Common atomizing pump is sprayed；When the thing temperature of aerosol type facial mask rises to 30 DEG C -45 DEG C, viscosity then increases retrogradation, presents
Gel shape is not flowed.Aerosol type facial mask prepared by the present invention, viscosity can vary with temperature, and without monovalence or divalent salts from
Son adds, safe and environment-friendly, corrosion-free to production equipment.
Aerosol type facial mask prepared by the present invention have spraying effect it is good, spraying uniformly, easily spray, with after skin contact with temperature
The rise viscosity of degree quickly raises, the advantages that being not susceptible to flow.
The using effect evaluation experimental of aerosol type facial mask
By changing the proportioning of PPG-12/SMDI copolymers, tamarind seed Jiao, Wen Quinces seed extracts and glycerin polyether -26,
Different spraying facial masks is prepared, by measuring spray area size, 25 DEG C and drop weight at 35 DEG C and viscosity up to maximum
Temperature during value evaluates the using effect of prepared spraying facial mask, and solvent is deionized water.
Spray area measuring method：A black plate is put vertically, is being sprayed at the cm of black plate 10 using the pressing of identical strength
Mist bottle, black plate level is placed immediately, draw the area shared by circle calculating lotion, spray area is bigger, illustrates that spray effect is got over
It is good；
Drop weight measuring method：A length of 10cm square temperature controllable constant temperature iron plate is set aside vertically, is set respectively
Iron plate temperature is 25 DEG C and 35 DEG C, puts an empty plate below.Sprayed at the cm of temperature-constant plate 10 using the pressing of identical strength
The weight that the facial mask liquid in following empty plate is flow down and dropped onto from constant temperature iron plate is collected and weighs after mist bottle 3 times, 5 minutes
Amount, the drop weight under the conditions of 25 DEG C and 35 DEG C is measured respectively.
Thermometry during ultimate viscosity number：Spray to preparation is surveyed using Brookfield companies DV-III rheometers
Cloudy surface membrane sample carries out viscosity with temperature change curve test, and record viscosity reaches temperature during maximum.Experimental result, such as table 1
It is shown：
The service condition evaluation table of the prepared aerosol type facial mask of the heterogeneity of table 1 composition
As shown in Table 1, sample 1 lacks PPG-12/SMDI copolymers, sample 2 lacks tamarind seed glue, the extraction of the Que Shao Wen Quinces seed of sample 3
Thing, sample 4 lack glycerin polyether -26, and sample 1, sample 2, sample 3, the spraying facial mask spray area of the formulated in combination of sample 4 are smaller, and 25 DEG C and
35 DEG C of drop weight is larger, and temperature rise drop weight is basically unchanged, and viscosity with temperature change unobvious, illustrates temperature sensitive combination
Four kinds of compositions of thing are indispensable, and other any three kinds compositions can not meet the preparation purpose of the present invention.
Sample 5, sample 6, sample 7, the PPG-12/SMDI copolymers in the composition of sample 8, tamarind seed Jiao, Wen Quinces seed extracts and sweet
Within the scope of the invention, significant changes are presented in viscosity with temperature change to the oily addition of polyethers -26, temperature during viscosity maxima
Close to 37 DEG C or so of skin temperature；Addition in sample 9, sample 10, sample 11, sample 12 exceedes the content range of the present invention, and viscosity is most
Temperature during big value just not in the range of 30 ~ 37 DEG C, illustrate PPG-12/SMDI copolymers, tamarind seed Jiao, Wen Quinces seed extract,
The addition of glycerin polyether -26 only present invention provide that in the range of effectively, any one of which material exceeds defined scope
The preparation purpose of the present invention can not be met.
PPG-12/SMDI copolymers, tamarind seed Jiao, Wen Quinces seed extracts and glycerin polyether in sample 13, the composition of sample 14-
26 addition exceeds the scope of the invention, and the spraying facial mask properties of preparation can not meet the preparation purpose of the present invention.
Test result indicates that four kinds of component PPG-12/SMDI copolymers, tamarind seed Jiao, Wen Quinces seed extracts and glycerine gather
Ether -26 must add simultaneously, and addition, in proper range, the spraying facial mask prepared just meets the object of the invention, can
Enough when below 27 DEG C, low viscosity working fluid shape is rendered as, common atomizing pump can be used to be sprayed；When aerosol type facial mask
Thing temperature when rising to 30 DEG C ~ 45 DEG C, viscosity then increases retrogradation, and gel shape is not flowed in presentation.
The viscosity with temperature variation tendency of prepared spraying facial mask
Surveyed using Brookfield companies DV-III rheometers to embodiment one, embodiment two, embodiment three, embodiment
4th, spraying film sample prepared by embodiment five carries out the test of viscosity with temperature change curve, and sample is placed in into institute during test
The min of water-bath inside holding 10 of test temperature, is then measured, experimental result such as Fig. 1（Viscosity versus temperature change curve）
It is shown, learnt by the change curve of viscosity with temperature, the viscosity of the spraying facial mask prepared by above-mentioned 5 embodiments is at 5 ~ 20 DEG C
When it is relatively low, increased dramatically with the rise viscosity of temperature, 37 DEG C nearby reach maximum after slowly decline.It is prepared by the present invention
Spraying mask product, be at normal temperatures the relatively low flow regime of viscosity, be easy to spray, and glued after being ejected on skin with body temperature
Degree is significantly improved, and forms not runny gel shape, and one layer of protection can be formed in face rapidly again by neither influenceing smearing use feeling
Film.
Spray profile membrane preparation method provided by the invention, processing step is simple, and gained aerosol type facial mask is below 27 DEG C
When, low viscosity working fluid shape is presented, common atomizing pump can be used to be sprayed；Temperature rises to 30 DEG C ~ 45 DEG C, then retrogradation is in
Gel shape is not flowed now.Human facial skin's temperature is generally between 30 ~ 37 DEG C, therefore this spraying facial mask is injected on skin,
Presented with body temperature meeting retrogradation at once and do not flow gel shape, rested on skin and play a role.
In summary, the advantage of the invention is that：Viscosity can increase with the rise of temperature, at less than 27 DEG C, present low
Viscosity flow is liquid, common atomizing pump can be used to be sprayed；Temperature rises to 30 DEG C ~ 45 DEG C, then retrogradation is presented and do not flowed
Gel shape, it is user-friendly, and cationic salts of the product without monovalence or divalence, it is safe and environment-friendly, to production equipment without
Corrosion.
Brief description of the drawings
Fig. 1 is viscosity versus temperature change curve.
Embodiment
Embodiment one：
A kind of preparation method of mist type facial mask, comprises the following steps：
A. 3g PPG-12/SMDI copolymers (AEC PPG-12/SMDI Copolymer), 1g tamarinds are weighed in proportion
Seed glue (GLYLOID 6C), 0.5g Wen Quinces seed extract (Quince Seed BG), (Genapol of 4g glycerin polyethers -26
G260), it is well mixed in rustless steel container, is heated to 52 DEG C, is maintained at the temperature and soaks 24 hours, then using EXAKT
Three Kun grinding mills, mill to form slurry；
B. 8.5g slurries and 5 DEG C of 85g deionized water mixing are weighed, stirs, obtains transparent flow liquid；
C. add and be pre-mixed uniform 3.1g butanediols, 0.6g 1,2- hexylene glycols and 0.6g parahydroxyacet-ophenones；So
The 0.05g essence and 0.15g PEG-40 rilanit specials being pre-mixed are added afterwards；Then the extraction of 1g fur pines algae is added
Thing, 1g alcohol, it is maintained at 5 DEG C and stirs, produces a kind of aerosol type facial mask with moisture-keeping efficacy.
In aerosol type facial mask manufactured in the present embodiment, PPG-12/SMDI copolymers (AEC PPG-12/SMDI
Copolymer) content be 3.0%, tamarind seed glue (GLYLOID 6C) content be 1.0%, Wen Quinces seed extract (Quince Seed
BG) content is that 0.5%, glycerin polyether -26 (Genapol G260) content is 4.0%.At 27 DEG C, viscosity is aerosol type facial mask
1000cps, in liquid, at 30 DEG C, viscosity 4000cps, gel shape being presented, 33.4 DEG C of viscosity reach peak,
25000cps, high-viscosity gel shape is presented, 37 DEG C of viscosity are 9000cps, and gel shape is presented, and 38 DEG C of viscosity are 2800cps, are presented
It is liquid.In 30 DEG C of -37 DEG C of sections, in high viscosity gel shape.
Embodiment two：
A kind of preparation method of mist type facial mask, comprises the following steps：
A. 4g PPG-12/SMDI copolymers (AEC PPG-12/SMDI Copolymer), 2.5g acid are weighed in proportion
Beans seed glue (GLYLOID 6C), 1g Wen Quinces seed extract (Quince Seed BG), (Genapol of 5g glycerin polyethers -26
G260), it is well mixed in rustless steel container, is heated to 55 DEG C, is maintained at the temperature and soaks 24 hours, then using EXAKT
Three Kun grinding mills, mill to form slurry；
B. 12.5g slurries and 15 DEG C of 75g deionized water mixing are weighed, stirs, obtains transparent flow liquid；
C. add and be pre-mixed uniform 3.1g butanediols, 0.6g 1,2- hexylene glycols and 0.6g parahydroxyacet-ophenones；So
The 0.05g essence and 0.15g PEG-40 rilanit specials being pre-mixed are added afterwards；Then 2g trehaloses, 1g cigarettes are added
Acid amides, 1g palm leaf tree extracts, 1.5g PEG/PPG-17/6 copolymers, 2.5g propane diols, is maintained at 15 DEG C and stirs,
Produce a kind of aerosol type facial mask with white-skinned face function.
In aerosol type facial mask manufactured in the present embodiment, PPG-12/SMDI copolymers (AEC PPG-12/SMDI
Copolymer) content be 4.0%, tamarind seed glue (GLYLOID 6C) content be 2.5%, Wen Quinces seed extract (Quince Seed
BG) content is that 1.0%, glycerin polyether -26 (Genapol G260) content is 5.0%.At 27 DEG C, viscosity is aerosol type facial mask
1500cps, in liquid, at 30 DEG C, viscosity 5000cps is presented gel shape, and 33 DEG C of viscosity reach peak, 28000cps,
High-viscosity gel shape is presented, 37 DEG C of viscosity are 8000cps, and gel shape is presented, and 38 DEG C of viscosity are 2300cps, are presented liquid.
30 DEG C of -37 DEG C of sections, in high viscosity gel shape.
Embodiment three：
A kind of preparation method of mist type facial mask, comprises the following steps：
A. 5g PPG-12/SMDI copolymers (AEC PPG-12/SMDI Copolymer), 1.5g acid are weighed in proportion
Beans seed glue (GLYLOID 6C), 2g Wen Quinces seed extract (Quince Seed BG), (Genapol of 6g glycerin polyethers -26
G260), it is well mixed in rustless steel container, is heated to 53 DEG C, is maintained at the temperature and soaks 24 hours, then using EXAKT
Three Kun grinding mills, mill to form slurry；
B. 14.5g slurries and 20 DEG C of 72.5g deionized water mixing are weighed, stirs, obtains transparent flow liquid；
C. add and be pre-mixed uniform 3.1g butanediols, 0.6g 1,2- hexylene glycols and 0.6g parahydroxyacet-ophenones；So
The 0.05g essence and 0.15g PEG-40 rilanit specials being pre-mixed are added afterwards；Then the fan algae extraction of 2g powder balls is added
Thing, 2g polyethylene glycol -32,1.5g methyl gluceth -20,1g sorbierites, 2g alcohol, it is equal to be maintained at 20 DEG C of stirrings
It is even, produce a kind of aerosol type facial mask with crease-resistant effect.
In aerosol type facial mask manufactured in the present embodiment, PPG-12/SMDI copolymers (AEC PPG-12/SMDI
Copolymer) content be 5.0%, tamarind seed glue (GLYLOID 6C) content be 1.5%, Wen Quinces seed extract (Quince Seed
BG) content is that 2.0%, glycerin polyether -26 (Genapol G260) content is 6.0%.At 27 DEG C, viscosity is aerosol type facial mask
900cps, in liquid, at 30 DEG C, viscosity 4500cps is presented gel shape, and 33 DEG C of viscosity reach peak, 33000cps,
High-viscosity gel shape is presented, 37 DEG C of viscosity are 9800cps, and gel shape is presented, and 38 DEG C of viscosity are 2100cps, are presented liquid.
30 DEG C of -37 DEG C of sections, in high viscosity gel shape.
Example IV：
A kind of preparation method of mist type facial mask, comprises the following steps：
A. 5.5g PPG-12/SMDI copolymers (AEC PPG-12/SMDI Copolymer), 2g acid are weighed in proportion
Beans seed glue (GLYLOID 6C), 1.5g Wen Quinces seed extract (Quince Seed BG), (Genapol of 8g glycerin polyethers -26
G260), it is well mixed in rustless steel container, is heated to 54 DEG C, is maintained at the temperature and soaks 24 hours, then using EXAKT
Three Kun grinding mills, mill to form slurry；
B. 17g slurries and 8 DEG C of 68g deionized water mixing are weighed, stirs, obtains transparent flow liquid；
C. add and be pre-mixed uniform 3.1g butanediols, 0.6g 1,2- hexylene glycols and 0.6g parahydroxyacet-ophenones；So
The 0.05g essence and 0.15g PEG-40 rilanit specials being pre-mixed are added afterwards；Then the extraction of 2g sugar sea-tangle is added
Thing, 5g glycerine, 1.5g propane diols, 2g alcohol, it is maintained at 8 DEG C and stirs, produces a kind of aerosol type with oil-control effect
Facial mask.
In aerosol type facial mask manufactured in the present embodiment, PPG-12/SMDI copolymers (AEC PPG-12/SMDI
Copolymer) content be 5.50%, tamarind seed glue (GLYLOID 6C) content be 2.0%, Wen Quince seed extracts (Quince
Seed BG) content is that 1.50%, glycerin polyether -26 (Genapol G260) content is 8.0%.Aerosol type facial mask at 27 DEG C,
Viscosity is 1100cps, in liquid, at 30 DEG C, viscosity 4800cps, gel shape is presented, and 33 DEG C of viscosity reach peak,
29000cps, high-viscosity gel shape is presented, 37 DEG C of viscosity are 7500cps, and gel shape is presented, and 38 DEG C of viscosity are 2500cps, are presented
It is liquid.In 30 DEG C of -37 DEG C of sections, in high viscosity gel shape.
Embodiment five：
A kind of preparation method of mist type facial mask, comprises the following steps：
A. 6g PPG-12/SMDI copolymers (AEC PPG-12/SMDI Copolymer), 3g tamarinds are weighed in proportion
Seed glue (GLYLOID 6C), 3g Wen Quinces seed extract (Quince Seed BG), (Genapol of 10g glycerin polyethers -26
G260), it is well mixed in rustless steel container, is heated to 55 DEG C, is maintained at the temperature and soaks 24 hours, then using EXAKT
Three Kun grinding mills, mill to form slurry；
B. 22g slurries and 17 DEG C of 66g deionized water mixing are weighed, stirs, obtains transparent flow liquid；
C. add and be pre-mixed uniform 3.1g butanediols, 0.6g 1,2- hexylene glycols and 0.6g parahydroxyacet-ophenones；So
The 0.05g essence and 0.15g PEG-40 rilanit specials being pre-mixed are added afterwards；Then 2g glycerine, 1g cottonseeds are added
Sugar, 1g gorgonian extracts, 1.5g beta glucans, 2g alcohol, it is maintained at 17 DEG C and stirs, producing one kind has anti-acne work(
The aerosol type facial mask of effect.
In aerosol type facial mask manufactured in the present embodiment, PPG-12/SMDI copolymers (AEC PPG-12/SMDI
Copolymer) content be 6.0%, tamarind seed glue (GLYLOID 6C) content be 3.0%, Wen Quinces seed extract (Quince Seed
BG) content is that 3.0%, glycerin polyether -26 (Genapol G260) content is 10.0%.Aerosol type facial mask is at 27 DEG C, viscosity
For 800cps, in liquid, at 30 DEG C, viscosity 4200cps, gel shape being presented, 33 DEG C of viscosity reach peak,
46000cps, high-viscosity gel shape is presented, 37 DEG C of viscosity are 7800cps, and gel shape is presented, and 38 DEG C of viscosity are 2300cps, are presented
It is liquid.In 30 DEG C of -37 DEG C of sections, in high viscosity gel shape.
Embodiments of the invention are the foregoing is only, are not intended to limit the scope of the invention, it is every to utilize this hair
The equivalent structure or equivalent flow conversion that bright description is done, or directly or indirectly it is used in other related technology necks
Domain, it is included within the scope of the present invention.
Claims (3)
- A kind of 1. aerosol type facial mask, it is characterised in that：Including mass ratio be 3 ~ 6% PPG-12/SMDI copolymers, mass ratio be 1 ~ 3% tamarind seed glue, the glycerin polyether -26 that mass ratio is 0.5 ~ 3% Wen Quinces seed extract, mass ratio is 4 ~ 10%；Do not contain Monovalence or divalent cation salt.
- 2. aerosol type facial mask according to claim 1, it is characterised in that：Surplus is deionized water or deionized water and guarantor Humectant, essence, preservative, the mixed liquor with moisturizing or the active component of whitening or crease-resistant effect.
- 3. the preparation method of aerosol type facial mask described in claim 2, it is characterised in that：Comprise the following steps：A, PPG-12/SMDI copolymers, tamarind seed Jiao, Wen Quinces seed extract, glycerin polyether -26, deionization are weighed in mass ratio Water, NMF, essence, preservative, there is moisturizing or the active component of whitening or crease-resistant effect；B, PPG-12/SMDI copolymers, tamarind seed Jiao, Wen Quinces seed extract, glycerin polyether -26 are mixed in rustless steel container Close uniformly, be heated to 52 ~ 55 DEG C, be maintained at the temperature, stand 24 hours, then using three Kun grinding mills, mill to form pulpous state Thing；C, slurry obtained by step B is mixed with 5 ~ 20 DEG C of deionized water, stirs, obtain transparent flow liquid；D, by NMF, essence, preservative, there is moisturizing or the active component of whitening or crease-resistant effect to add obtained by step C thoroughly Bright working fluid, it is maintained at 5 ~ 20 DEG C and stirs, be then returned to 20 ~ 25 DEG C, produces a kind of aerosol type facial mask.
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| CN105769587A (en) * | 2016-03-28 | 2016-07-20 | 王振武 | Spray type mask |
| CN106727136B (en) * | 2016-12-27 | 2020-05-22 | 广东芭薇生物科技股份有限公司 | Composition containing seed extract and preparation method thereof |
| CN108451831A (en) * | 2018-05-19 | 2018-08-28 | 山东朱氏药业集团有限公司 | Pregnant woman's moisturizing and nourishing smoothing toner and preparation method thereof |
| CN110772466A (en) * | 2019-08-29 | 2020-02-11 | 罗莹 | Preparation method of convenient traditional Chinese medicine mask |
| CN113384491A (en) * | 2021-06-24 | 2021-09-14 | 国药医养化妆品研发(杭州)有限公司 | Aqueous cosmetic mixture with protection and slow release functions and preparation method thereof |
| CN114306165B (en) * | 2022-01-11 | 2023-12-15 | 泉后(广州)生物科技研究院有限公司 | Moisturizing composition and preparation method thereof |
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| CN102836089A (en) * | 2012-09-20 | 2012-12-26 | 上海进瑞实业有限公司 | Spraying skin-protecting cosmetic composition and application thereof |
| CN104666128A (en) * | 2015-03-16 | 2015-06-03 | 黑龙江省科学院火山与矿泉研究所 | Volcanic mud essence spray mask and preparation method thereof |
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| CN104983609A (en) | 2015-10-21 |
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