CN111821239A - A hair blackening shampoo containing herba Gynostemmatis extract and its preparation method - Google Patents

A hair blackening shampoo containing herba Gynostemmatis extract and its preparation method Download PDF

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CN111821239A
CN111821239A CN202010805700.3A CN202010805700A CN111821239A CN 111821239 A CN111821239 A CN 111821239A CN 202010805700 A CN202010805700 A CN 202010805700A CN 111821239 A CN111821239 A CN 111821239A
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gynostemma pentaphylla
extract
hair blackening
hair
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彭涛
查春英
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Sichuan Bikang Biotechnology Co ltd
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Sichuan Bikang Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners

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  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
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  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a preparation method of hair blackening shampoo containing gynostemma pentaphylla extract and hair blackening shampoo prepared by the same, aiming at solving the problems that some common shampoo in the current market has low efficiency and rebound effect on human hair blackening, and the method comprises the steps of killing out, drying, crushing, extracting saponin, carrying out multi-substance-component compatibility and post-treatment and the like on gynostemma pentaphylla; the method is simple and convenient, easy to operate, short in production period and stable in product quality; the prepared hair blackening shampoo has the functions of moisturizing scalp and hair, blackening hair, protecting health and the like, has great significance for the sustainable development of the production of the hair blackening shampoo, and the technology of the invention reaches the international leading level.

Description

A hair blackening shampoo containing herba Gynostemmatis extract and its preparation method
Technical Field
The invention relates to the technical field of bioengineering and cosmetics, in particular to a preparation method of a hair blackening shampoo containing a gynostemma pentaphylla extract and a hair blackening shampoo prepared by the same.
Background
After the 20 th century and 90 s, along with the rapid economic growth and the rapid development of scientific technology, people have higher and higher demands on material life, stronger and stronger hopes of improving the life quality, keeping healthy and long life, protecting and beautifying skin and the like, and the requirements and hopes of improving the scientific proportion of the nutritional ingredients of the product for protecting and beautifying skin, resisting wrinkles and moisturizing skin and smoothing and tendering skin are increased synchronously. With the rapid development of molecular biology, quantum biology, medical treatment and health care comprehensive disciplines, people expect and select health care products and cosmetics widely and strictly. Therefore, a great deal of economy, technology, manpower and material resources are put into various countries in the world to comprehensively research high-quality and high-technology nutritional cosmetics.
Gynostemma pentaphylla is a precious traditional Chinese medicine, has high pharmacological, medicinal and medical values, but falls asleep for thousands of years in China. The study and application of gynostemma pentaphylla was earlier in japan abroad, and the study and application was started in 80 s of the 20 th century. China draws attention in the beginning of the 21 st century, and the gynostemma pentaphylla cosmetics are gradually developed in about 2010.
According to research and product practice, the gynostemma pentaphylla is a perennial herb climbing vine plant of the genus gynostemma of the family cucurbitaceae, also called fiveleaf gynostemma herb, groundsel and rootage, and the like, and contains rich gypenoside, brass, polysaccharide, amino acid and various trace elements. The anti-wrinkle skin care product and shampoo produced by gynostemma pentaphylla is an excellent cosmetic, and has the functions of resisting aging, resisting fatigue, promoting cell metabolism, moistening skin, beautifying, treating white hair, resisting cancer and the like.
However, although gynostemma pentaphylla skin care products exist in the market at present, the gynostemma pentaphylla skin care products are basically produced by adopting chemical means and methods. High chemical component content and low use effect, thus causing consumer dissatisfaction. The anti-wrinkle skin care product prepared by taking gynostemma pentaphylla as a main component is a product expected by consumers, and at present, the product is rarely reported in domestic and foreign markets.
Disclosure of Invention
In order to solve the technical problems, the invention aims to provide a preparation method of a hair blackening shampoo containing a gynostemma pentaphylla extract and the hair blackening shampoo prepared by the preparation method.
The technical scheme adopted by the invention is as follows: a method for preparing hair blackening shampoo containing herba Gynostemmatis extract comprises the following steps: a. putting 1-5 parts of gynostemma pentaphylla extract, 11-13.5 parts of saponin, 13-15 parts of sucrose fatty acid ester, 25.5-31.5 parts of trehalose, 10-19 parts of hyaluronic acid, 5-6 parts of xanthan gum, 17-19 parts of sodium alginate, 20-22.5 parts of potassium sorbate, 50-75 parts of glycerol, 30-60 parts of ethanol, 555-675 parts of water and 0.1-1 part of tyrosine into a reaction pot, mixing and heating to 75-80 ℃, and then cooling to 40-50 ℃ and adjusting the pH to 5.5-6.5 by using citric acid to obtain the hair blackening shampoo containing the gynostemma pentaphylla extract.
Further, the preparation method of the gynostemma pentaphylla extract comprises the following steps: (1) and when the gynostemma pentaphylla is mature in the late 9 th and the middle 10 th months, cutting off the gynostemma pentaphylla grass 5 cm away from the ground, removing weeds and rotten leaves, cutting into sections of 5-10 cm, cleaning, putting on a spreading cooling rack, and airing until the water content is 15-20%. The gynostemma pentaphylla harvested at this stage has the highest content of effective components. (2) The gynostemma pentaphylla that will dry is put into double helix squeezer and is squeezed, can constantly add material, and each item parameter when squeezing is: oil pressure: 35-40 MPa, the aperture of the screen mesh is 80 meshes, and the rotating speed of the screw is 6-12 r/min. Rotating the gynostemma pentaphylla material along with the double helix in the opposite direction, separating juice and residues, collecting the gynostemma pentaphylla juice, performing centrifugal filtration by using a centrifugal machine, wherein the centrifugal parameter is 2500-2800 rpm and is 4-6 min, and collecting filtrate to obtain light brown clear liquid without chlorophyll; (3) putting the light brown clear liquid obtained in the step (2) into a freeze dryer for freeze drying, wherein the parameters during freeze drying are as follows: the flow rate is 2-5 mL/min, the drying temperature is-10 to-15 ℃, the rotation speed of a peristaltic pump is 10-15 r/min, the drying time is 2-4 h, after drying is finished, the dried powder is collected and is sieved by a 200-mesh sieve, and a powdery solid of gynostemma pentaphylla is obtained; (4) putting the freeze-dried gynostemma pentaphylla powder solid into a low-temperature plant cell wall breaking machine for wall breaking ultramicro, wherein the parameters during wall breaking ultramicro are as follows: the indoor temperature is 18-22 ℃, the humidity is 30-32%, the temperature of materials in the wall breaking pulverizer is-8 to-5 ℃, and the pulverizing time is 35-40 minutes; pulverizing into 1800 mesh powder to obtain herba Gynostemmatis extract.
The hair blackening shampoo prepared by the preparation method of the hair blackening shampoo containing the gynostemma pentaphylla extract.
Compared with the prior art, the invention has the following beneficial effects: a hair blackening shampoo containing herba Gynostemmatis extract is more natural and environment-friendly, and has effects of moistening scalp and hair, and blackening hair.
Detailed Description
The present invention is further illustrated with reference to the following specific examples, without limiting the scope of the invention to the following examples. The procedures, conditions, reagents and the like for carrying out the present invention are general knowledge and common general knowledge in the art except for the contents specifically mentioned below, and the present invention is not particularly limited.
Example 1
A method for preparing hair blackening shampoo containing herba Gynostemmatis extract comprises the following steps: a. putting 1 part of gynostemma pentaphylla extract, 11 parts of saponin, 13 parts of sucrose fatty acid ester, 25.5 parts of trehalose, 10 parts of hyaluronic acid, 5 parts of xanthan gum, 17 parts of sodium alginate, 20 parts of potassium sorbate, 50 parts of glycerol, 30 parts of ethanol, 555 parts of water and 0.1-1 part of tyrosine into a reaction pot according to the parts by weight, mixing and heating to 75 ℃, and then adjusting the pH to 5.5 by using citric acid when cooling to 40 ℃ to obtain the hair blackening shampoo containing the gynostemma pentaphylla extract.
Further, the preparation method of the gynostemma pentaphylla extract comprises the following steps: (1) and when the gynostemma pentaphylla is mature in late 9 months, cutting off gynostemma pentaphylla grass 5 cm away from the ground, removing weeds and rotten leaves, cutting into sections of 5 cm, cleaning, putting on a spreading cooling rack, and airing until the water content is 15%. The gynostemma pentaphylla harvested at this stage has the highest content of effective components. (2) The gynostemma pentaphylla that will dry is put into double helix squeezer and is squeezed, can constantly add material, and each item parameter when squeezing is: oil pressure: 35MPa, the aperture of the screen mesh is 80 meshes, and the rotating speed of the screw is 6 revolutions per minute. Rotating the Gynostemma pentaphyllum material along with the double helix in the opposite direction, separating out juice and residue, collecting the Gynostemma pentaphyllum juice, centrifuging and filtering by a centrifuge with the centrifugation parameter of 2500rpm for 4min, and collecting the filtrate to obtain light brown clear liquid without chlorophyll; (3) putting the light brown clear liquid obtained in the step (2) into a freeze dryer for freeze drying, wherein the parameters during freeze drying are as follows: the flow rate is 2mL/min, the drying temperature is-10 ℃, the rotation speed of a peristaltic pump is 10r/min, the drying time is 2 hours, after drying is finished, the dried powder is collected and is sieved by a 200-mesh sieve, and the powdery solid of the gynostemma pentaphylla is obtained; (4) putting the freeze-dried gynostemma pentaphylla powder solid into a low-temperature plant cell wall breaking machine for wall breaking ultramicro, wherein the parameters during wall breaking ultramicro are as follows: the indoor temperature is 18 ℃, the humidity is 30%, the temperature of materials in the wall breaking pulverizer is-8 ℃, and the pulverizing time is 35 minutes; pulverizing into 1800 mesh powder to obtain herba Gynostemmatis extract.
The hair blackening shampoo prepared by the preparation method of the hair blackening shampoo containing the gynostemma pentaphylla extract.
Example 2
A method for preparing hair blackening shampoo containing herba Gynostemmatis extract comprises the following steps: a. putting 3 parts of gynostemma pentaphylla extract, 12 parts of saponin, 14 parts of sucrose fatty acid ester, 29 parts of trehalose, 15 parts of hyaluronic acid, 5.5 parts of xanthan gum, 18 parts of sodium alginate, 21 parts of potassium sorbate, 60 parts of glycerol, 50 parts of ethanol, 650 parts of water and 0.1-1 part of tyrosine into a reaction pot according to the parts by weight, mixing and heating to 77 ℃, and then adjusting the pH to 5.8 by using citric acid when the temperature is reduced to 44 ℃ to obtain the hair blackening shampoo containing the gynostemma pentaphylla extract.
Further, the preparation method of the gynostemma pentaphylla extract comprises the following steps: (1) and when the gynostemma pentaphylla is mature in late 9 months, cutting off gynostemma pentaphylla grass 5 cm away from the ground, removing weeds and rotten leaves, cutting into sections of 7 cm, cleaning, putting on a spreading cooling rack, and airing until the water content is 18%. The gynostemma pentaphylla harvested at this stage has the highest content of effective components. (2) The gynostemma pentaphylla that will dry is put into double helix squeezer and is squeezed, can constantly add material, and each item parameter when squeezing is: oil pressure: 38MPa, the aperture of the screen mesh is 80 meshes, and the rotating speed of the screw is 8 r/min. Rotating the Gynostemma pentaphyllum material along with the double helix in the opposite direction, separating juice and residue, collecting the Gynostemma pentaphyllum juice, centrifuging and filtering by a centrifuge with the centrifugation parameter of 2600rpm for 5min, and collecting the filtrate to obtain light brown clear liquid without chlorophyll; (3) putting the light brown clear liquid obtained in the step (2) into a freeze dryer for freeze drying, wherein the parameters during freeze drying are as follows: the flow rate is 4mL/min, the drying temperature is-12 ℃, the rotation speed of a peristaltic pump is 11r/min, the drying time is 3h, after drying is finished, the dried powder is collected and is sieved by a 200-mesh sieve, and the powdery solid of the gynostemma pentaphylla is obtained; (4) putting the freeze-dried gynostemma pentaphylla powder solid into a low-temperature plant cell wall breaking machine for wall breaking ultramicro, wherein the parameters during wall breaking ultramicro are as follows: the indoor temperature is 20 ℃, the humidity is 31%, the temperature of materials in the wall breaking pulverizer is-6 ℃, and the pulverizing time is 38 minutes; pulverizing into 1800 mesh powder to obtain herba Gynostemmatis extract.
The hair blackening shampoo prepared by the preparation method of the hair blackening shampoo containing the gynostemma pentaphylla extract.
Example 3
A method for preparing hair blackening shampoo containing herba Gynostemmatis extract comprises the following steps: a. putting 5 parts of gynostemma pentaphylla extract, 13.5 parts of saponin, 15 parts of sucrose fatty acid ester, 31.5 parts of trehalose, 19 parts of hyaluronic acid, 6 parts of xanthan gum, 19 parts of sodium alginate, 22.5 parts of potassium sorbate, 75 parts of glycerol, 60 parts of ethanol, 675 parts of water and 0.1-1 part of tyrosine into a reaction pot according to parts by weight, mixing and heating to 80 ℃, and then adjusting the pH to 6.5 by using citric acid when the temperature is reduced to 50 ℃ to obtain the hair blackening shampoo containing the gynostemma pentaphylla extract.
Further, the preparation method of the gynostemma pentaphylla extract comprises the following steps: (1) and when the gynostemma pentaphylla is mature in the middle ten days of 10 months, cutting off gynostemma pentaphylla grass 5 cm away from the ground, removing weeds and rotten leaves, cutting into sections of 10 cm, cleaning, putting on a spreading cooling rack, and airing until the water content is 20%. The gynostemma pentaphylla harvested at this stage has the highest content of effective components. (2) The gynostemma pentaphylla that will dry is put into double helix squeezer and is squeezed, can constantly add material, and each item parameter when squeezing is: oil pressure: 40MPa, the aperture of the screen mesh is 80 meshes, and the rotating speed of the screw is 12 r/min. Rotating the Gynostemma pentaphyllum material along with the double helix in the opposite direction, separating out juice and residue, collecting the Gynostemma pentaphyllum juice, centrifuging and filtering by a centrifuge with the centrifugation parameter of 2800rpm for 6min, and collecting the filtrate to obtain light brown clear liquid without chlorophyll; (3) putting the light brown clear liquid obtained in the step (2) into a freeze dryer for freeze drying, wherein the parameters during freeze drying are as follows: the flow rate is 5mL/min, the drying temperature is-15 ℃, the rotation speed of a peristaltic pump is 15r/min, the drying time is 4h, after drying is finished, the dried powder is collected and is sieved by a 200-mesh sieve, and the powdery solid of the gynostemma pentaphylla is obtained; (4) putting the freeze-dried gynostemma pentaphylla powder solid into a low-temperature plant cell wall breaking machine for wall breaking ultramicro, wherein the parameters during wall breaking ultramicro are as follows: the indoor temperature is 22 ℃, the humidity is 32%, the temperature of materials in the wall breaking pulverizer is-5 ℃, and the pulverizing time is 40 minutes; pulverizing into 1800 mesh powder to obtain herba Gynostemmatis extract.
The hair blackening shampoo prepared by the preparation method of the hair blackening shampoo containing the gynostemma pentaphylla extract.
Example 4
A method for preparing hair blackening shampoo containing herba Gynostemmatis extract comprises the following steps: a. putting 3.5 parts of gynostemma pentaphylla extract, 11 parts of saponin, 13 parts of sucrose fatty acid ester, 25.5 parts of trehalose, 10 parts of hyaluronic acid, 5 parts of xanthan gum, 17 parts of sodium alginate, 20 parts of potassium sorbate, 50 parts of glycerol, 30 parts of ethanol, 555 parts of water and 0.1-1 part of tyrosine into a reaction pot according to the parts by weight, mixing and heating to 75 ℃, and then adjusting the pH to 5.5 by using citric acid when the temperature is reduced to 40 ℃ to obtain the hair blackening shampoo containing the gynostemma pentaphylla extract.
Further, (1) when the gynostemma pentaphylla matures in the middle ten days of 10 months, the gynostemma pentaphylla grass is cut off 5 cm above the ground, weeds and rotten leaves are removed, the gynostemma pentaphylla grass is cut into sections of 10 cm, and the sections are cleaned and put on a spreading cooling rack to be dried until the water content is 20%. The gynostemma pentaphylla harvested at this stage has the highest content of effective components. (2) The gynostemma pentaphylla that will dry is put into double helix squeezer and is squeezed, can constantly add material, and each item parameter when squeezing is: oil pressure: 40MPa, the aperture of the screen mesh is 80 meshes, and the rotating speed of the screw is 12 r/min. Rotating the Gynostemma pentaphyllum material along with the double helix in the opposite direction, separating out juice and residue, collecting the Gynostemma pentaphyllum juice, centrifuging and filtering by a centrifuge with the centrifugation parameter of 2800rpm for 6min, and collecting the filtrate to obtain light brown clear liquid without chlorophyll; (3) putting the light brown clear liquid obtained in the step (2) into a freeze dryer for freeze drying, wherein the parameters during freeze drying are as follows: the flow rate is 5mL/min, the drying temperature is-15 ℃, the rotation speed of a peristaltic pump is 15r/min, the drying time is 4h, after drying is finished, the dried powder is collected and is sieved by a 200-mesh sieve, and the powdery solid of the gynostemma pentaphylla is obtained; (4) putting the freeze-dried gynostemma pentaphylla powder solid into a low-temperature plant cell wall breaking machine for wall breaking ultramicro, wherein the parameters during wall breaking ultramicro are as follows: the indoor temperature is 22 ℃, the humidity is 32%, the temperature of materials in the wall breaking pulverizer is-5 ℃, and the pulverizing time is 40 minutes; pulverizing into 1800 mesh powder to obtain herba Gynostemmatis extract.
The hair blackening shampoo prepared by the preparation method of the hair blackening shampoo containing the gynostemma pentaphylla extract.
Example 5
A method for preparing hair blackening shampoo containing herba Gynostemmatis extract comprises the following steps: a. putting 4.5 parts of gynostemma pentaphylla extract, 11 parts of saponin, 13 parts of sucrose fatty acid ester, 25.5 parts of trehalose, 10 parts of hyaluronic acid, 5 parts of xanthan gum, 17 parts of sodium alginate, 20 parts of potassium sorbate, 50 parts of glycerol, 30 parts of ethanol, 555 parts of water and 0.1-1 part of tyrosine into a reaction pot according to the parts by weight, mixing and heating to 75 ℃, and then adjusting the pH to 5.5 by using citric acid when the temperature is reduced to 40 ℃ to obtain the hair blackening shampoo containing the gynostemma pentaphylla extract.
Further, (1) when the gynostemma pentaphylla matures in the middle ten days of 10 months, the gynostemma pentaphylla grass is cut off 5 cm above the ground, weeds and rotten leaves are removed, the gynostemma pentaphylla grass is cut into sections of 10 cm, and the sections are cleaned and put on a spreading cooling rack to be dried until the water content is 20%. The gynostemma pentaphylla harvested at this stage has the highest content of effective components. (2) The gynostemma pentaphylla that will dry is put into double helix squeezer and is squeezed, can constantly add material, and each item parameter when squeezing is: oil pressure: 40MPa, the aperture of the screen mesh is 80 meshes, and the rotating speed of the screw is 12 r/min. Rotating the Gynostemma pentaphyllum material along with the double helix in the opposite direction, separating out juice and residue, collecting the Gynostemma pentaphyllum juice, centrifuging and filtering by a centrifuge with the centrifugation parameter of 2800rpm for 6min, and collecting the filtrate to obtain light brown clear liquid without chlorophyll; (3) putting the light brown clear liquid obtained in the step (2) into a freeze dryer for freeze drying, wherein the parameters during freeze drying are as follows: the flow rate is 5mL/min, the drying temperature is-15 ℃, the rotation speed of a peristaltic pump is 15r/min, the drying time is 4h, after drying is finished, the dried powder is collected and is sieved by a 200-mesh sieve, and the powdery solid of the gynostemma pentaphylla is obtained; (4) putting the freeze-dried gynostemma pentaphylla powder solid into a low-temperature plant cell wall breaking machine for wall breaking ultramicro, wherein the parameters during wall breaking ultramicro are as follows: the indoor temperature is 22 ℃, the humidity is 32%, the temperature of materials in the wall breaking pulverizer is-5 ℃, and the pulverizing time is 40 minutes; pulverizing into 1800 mesh powder to obtain herba Gynostemmatis extract.
The hair blackening shampoo prepared by the preparation method of the hair blackening shampoo containing the gynostemma pentaphylla extract.

Claims (3)

1. A preparation method of hair blackening shampoo containing gynostemma pentaphylla extract is characterized by comprising the following steps: a. putting 1-5 parts of gynostemma pentaphylla extract, 11-13.5 parts of saponin, 13-15 parts of sucrose fatty acid ester, 25.5-31.5 parts of trehalose, 10-19 parts of hyaluronic acid, 5-6 parts of xanthan gum, 17-19 parts of sodium alginate, 20-22.5 parts of potassium sorbate, 50-75 parts of glycerol, 30-60 parts of ethanol, 555-675 parts of water and 0.1-1 part of tyrosine into a reaction pot, mixing and heating to 75-80 ℃, and then cooling to 40-50 ℃ and adjusting the pH to 5.5-6.5 by using citric acid to obtain the black hair shampoo containing the gynostemma pentaphylla extract.
2. The method of preparing a hair blackening shampoo containing an extract of gynostemma pentaphyllum as set forth in claim 1, wherein the extract of gynostemma pentaphyllum is prepared by the steps of: (1) and when the gynostemma pentaphylla is mature in the late 9 th and the middle 10 th months, cutting off the gynostemma pentaphylla grass 5 cm away from the ground, removing weeds and rotten leaves, cutting into sections of 5-10 cm, cleaning, putting on a spreading cooling rack, and airing until the water content is 15-20%. The gynostemma pentaphylla harvested at this stage has the highest content of effective components. (2) The gynostemma pentaphylla that will dry is put into double helix squeezer and is squeezed, can constantly add material, and each item parameter when squeezing is: oil pressure: 35-40 MPa, the aperture of the screen mesh is 80 meshes, and the rotating speed of the screw is 6-12 r/min. Rotating the gynostemma pentaphylla material along with the double helix in the opposite direction, separating juice and residues, collecting the gynostemma pentaphylla juice, performing centrifugal filtration by using a centrifugal machine, wherein the centrifugal parameter is 2500-2800 rpm and is 4-6 min, and collecting filtrate to obtain light brown clear liquid without chlorophyll; (3) putting the light brown clear liquid obtained in the step (2) into a freeze dryer for freeze drying, wherein the parameters during freeze drying are as follows: the flow rate is 2-5 mL/min, the drying temperature is-10 to-15 ℃, the rotation speed of a peristaltic pump is 10-15 r/min, the drying time is 2-4 h, after drying is finished, the dried powder is collected and is sieved by a 200-mesh sieve, and a powdery solid of gynostemma pentaphylla is obtained; (4) putting the freeze-dried gynostemma pentaphylla powder solid into a low-temperature plant cell wall breaking machine for wall breaking ultramicro, wherein the parameters during wall breaking ultramicro are as follows: the indoor temperature is 18-22 ℃, the humidity is 30-32%, the temperature of materials in the wall breaking pulverizer is-8 to-5 ℃, and the pulverizing time is 35-40 minutes; pulverizing into 1800 mesh powder to obtain herba Gynostemmatis extract.
3. The hair blackening shampoo prepared by the method for preparing the hair blackening shampoo containing the gynostemma pentaphyllum extract according to claim 1 or 2.
CN202010805700.3A 2020-08-12 2020-08-12 A hair blackening shampoo containing herba Gynostemmatis extract and its preparation method Pending CN111821239A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114848556A (en) * 2022-06-02 2022-08-05 安徽师范大学 Application of Gynostemma pentaphyllum extract and Eucommia ulmoides extract in preparation of hair shampoo for promoting black hair/preventing gray hair

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