KR102093543B1 - Composition for washing hair and scalp to prevent hair losing and to promote hair growth and method for preparing the same - Google Patents

Abstract

The present invention provides a composition for cleaning hair and scalp having excellent functionality for moisturizing scalp, preventing hair loss, and promoting hair growth, including extracts of natural medicinal plants and kopexil, and hydrolyzed sponges, which exhibit functional properties for preventing hair loss and preparing the same It's about how.

Description

A composition for cleaning hair and scalp having a function of preventing hair loss and promoting hair growth, and a manufacturing method thereof {COMPOSITION FOR WASHING HAIR AND SCALP TO PREVENT HAIR LOSING AND TO PROMOTE HAIR GROWTH AND METHOD FOR PREPARING THE SAME}

The present invention relates to a composition for cleaning hair and scalp having a function of preventing hair loss and promoting hair growth and a method for manufacturing the same.

Normally, the human hair plays a role of buffering against external shock and protecting the human body from external stimuli such as ultraviolet rays and cold wind, and arsenic (As), mercury (Hg) or zinc (Zn), etc. It also plays a role of absorbing and discharging unnecessary heavy metals into the body.

The average adult has about 100,000 to 150,000 hairs, and each hair undergoes growth and degeneration through a process including an anagen, a catagen, and a telogen, A single hair will maintain a lifespan of approximately 1,000 days, and thus, on average, 50 to 100 hairs will be removed per day, and new hairs will be generated in areas where the hairs are removed.

However, hair loss in which new hair does not occur in the area where hair is missing due to recent unbalanced diet, excessive drinking and smoking, drug use, lack of sleep, excessive stress, childbirth, menopausal disorder, frequent perm and staining, and hormone imbalance In order to prevent hair loss as described above, in order to prevent hair loss, a hair growth agent made of a natural extract that is not harmful to the human body, a skin external preparation for preventing or alleviating hair loss by washing wastes of scalp and supplying artificial nutrients , Natural detergents (shampoos) are being developed.

For example, Korean Registered Patent No. 10-1263181 is effective for extracting herbal medicines from a mixture of medicinal herbs containing certain ratios of sorghum, ginseng, pine needles, Angelica, Cheongung, medicinal mugwort, sujijihwang, county medicinal, side baekyeop, Sangbaekpi, Hannyeoncho, Goji and licorice. There has been disclosed a hair growth-promoting wool and a scalp care composition for preventing hair loss, which is characterized by being an ingredient.

As another example, Korean Registered Patent No. 10-0805692 discloses a shampoo for preventing hair loss comprising a herbal extract, which is a mixed hot water extract of Baekji, Cheoncho, Yeongneunghyang, Gamguk, Cheongung, Hannyeoncho, Sangbaekpi, Gosam, and Baekshou There is a bar.

However, most of the hair loss progresses to the androgen type due to the action of the male hormone, and the method of preventing hair loss by the hair loss gene is known to be the most effective method of inhibiting dihydrotestosterone (DHT), and is currently medical Proven DHT inhibitors are hair growth accelerators such as finasteride, dutasteride, and minoxidil, but the above natural-derived compositions can create a positive environment for maintaining hair health. There is a problem in that it is difficult to expect hair growth, and the hair growth promoters are known to cause various side effects, and research on a new composition or method capable of supplementing the hair growth is needed.

(Document 01) Korean Registered Patent No. 10-1263181 (Publication date: 2013.05.10) (Document 02) Korean Registered Patent No. 10-0805692 (Publication date: 2008.02.21)

The present invention has been devised to solve the problems of the prior art as described above, including the extract of the soft medicinal plant and kopexil (kopexil) as an active ingredient, there is no side effect, it is safe to use for a long time, and improves the scalp condition. It is intended to provide technical information regarding a composition for cleaning hair and scalp having excellent functionality for moisturizing scalp, preventing hair loss and promoting hair growth, and a method for manufacturing the same.

In order to achieve the technical problem as described above, the present invention, medicinal plant extract and 2,4-diaminopyrimidine-3-oxide (2,4-diamino pyrimidine-) extracted from medicinal plants containing Hannyeoncho, sewage and hinoki It provides a composition for washing hair and scalp containing 3-oxide, Kopexil) as an active ingredient.

According to an embodiment of the present invention, the composition for cleaning hair and scalp is 1 to 10 parts by weight of the medicinal plant extract and 0.1 to 10 parts by weight of the 2,4-diaminopyrimidine-3-oxide based on 100 parts by weight of the composition It may include parts by weight, and may further include 0.5 to 5 parts by weight of the hydrolyzed sponge powder.

According to an embodiment of the present invention, the composition for cleaning hair and scalp is herbal extract, mushroom extract, vitamins, moisturizer, surfactant, foaming agent, conditioning agent, pH adjusting agent, pearling agent, preservative, antibacterial agent, fragrance and viscosity control It may further include one or more additives selected from the group consisting of zero.

In addition, the present invention provides a method for preparing the composition for washing hair and scalp described above, (a) supplying a medicinal plant mixture and water containing medicinal plants, sorghum, and oleander to a vacuum low temperature extractor, and extracting under reduced pressure distillation method Preparing a medicinal plant extract by; (b) supplying purified water and polyquaternium-10 to the compounding tank and heating to a temperature of 60 to 80 ° C. to prepare a first mixture; (c) heating the first mixture to a temperature of 60 to 80 ° C. and disodium laureth sulfosuccinate, alkylpolyglycosides, sodium cocoyl amino acid fructose), cocoamidopropyl betaine, cocoyl monoethanolamine, respectively, to sequentially supply to prepare a second mixture; (d) preparing a third mixture by heating the second mixture to a temperature of 40 to 60 ° C. and feeding PEG-120 methyl glucose dioleate; (e) heating the third mixture to a temperature of 30 to 50 ° C., glycerin, panthenol, salicylic acid, ethylenediamine tetra acetic acid (EDTA) disodium salt ), Linoleamidopropyl PG-dimonium chloride phosphate and the medicinal plant extract is sequentially added to prepare a fourth mixture; And (f) preparing a composition for cleaning hair and scalp by sequentially mixing a grapefruit extract, sodium benzoate, and a fragrance in a fourth mixture to prepare a composition for cleaning hair and scalp. do.

Further, according to an embodiment of the present invention, in step (e), after preparing the fourth mixture, it may further include the step of supplying a hydrolyzed sponge to the fourth mixture.

The composition for cleaning hair and scalp according to the present invention contains medicinal plant extracts showing excellent anti-hair loss performance, such as Hannyeoncho, sewage, and cypress, which promote blood circulation and scalp regeneration, and Kopexil, which exhibits excellent hair growth promoting effects. It has excellent hair growth and hair loss prevention performance.

In addition, the composition according to the present invention further comprises a hydrolysed sponge (hydrolysed sponge) capable of penetrating the active ingredient to the deep region of the scalp, as well as exhibiting excellent moisturizing effect, further promoting hair growth and hair loss prevention performance Can be improved.

1 is a conceptual diagram schematically showing a high-speed vacuum low-temperature extraction system used for preparing a medicinal plant extract according to an embodiment of the present invention.
Figure 2 is a result of measuring the rate of moisture change in the scalp over 6 hours after washing the hair and scalp with a shampoo composition prepared by the method according to Example 1, Example 2 and Comparative Example 1.

Hereinafter, the present invention will be described in detail.

The present invention includes medicinal plant extract and 2,4-diaminopyrimidine-3-oxide (2,4-diamino pyrimidine-3-oxide, Kopexil) as an active ingredient extracted from medicinal plants containing Hannyeoncho, sewage and cypress It provides a composition for washing hair and scalp.

The medicinal plant extract may be used extracts obtained from medicinal plants containing Hannyeoncho, sewage, and cypress leaves to promote hair growth and prevent hair loss, and exhibits efficacy to prevent hair loss in addition to the above-mentioned medicinal plants. It may be configured to further include extracts extracted from various medicinal plants.

In addition, the medicinal plant extract is extracted using a mixture of medicinal plants, including medicinal plants, sorghum and oleander, in various ways, such as hot water extraction, ethanol extraction, reflux extraction, heating and pressure extraction, which are commonly used to prepare plant extracts. You can use

Preferably, the medicinal plant extract supplies the medicinal plant mixture to a high-speed vacuum low-temperature extraction device to which a circulating steam cooling method is applied and extracts it under reduced pressure by distillation at a low temperature to prevent the destruction of active ingredients and improve the active ingredients. A medicinal plant extract containing the content can be used.

Among the medicinal plants, Hannyeoncho ( Eclipta prostrata L. ) is an annual plant of the Chrysanthemum family, saponin, nicotine, tannin, vitamin A, vitamin A, ecliptine, and thiophene. thiophene), etc., contains a large amount of compounds, is cold and has a sweet taste, is suitable for hair loss due to upper fever in young people, lowers heat and has excellent hemostatic effect, and has antibacterial, anti-inflammatory, anti-fungal and immune-enhancing effects. Indicated, the foot is made black and has the effect of preventing hair loss and promoting hair growth.

The sewage ( Pleuropterus multiflorus Turcz ) is a perennial plant with round tuber roots and having tendrils, and the sewage is largely drowned ( Polygonum multiflorum Thunberg and Cynan chum wilfordii Hemsley ) is divided into two types, which are mainly grown in our country. The sewage contains a large amount of anthraquinone components, such as chrysophanol, emodin, rhein, and physcion, and lecithin, etc., to develop and assimilate growth in the body. It is known to promote and promote blood circulation and blood supply to the scalp, and make the hair healthy and moisturize the skin.

The thyroid leaf ( Thuja orientalis L. ) is a herbal medicine prepared by drying raw leaves obtained from the cypress tree, aromadendrin, quercetin, amenthoflavone, myricetin, and hinokiflavone ( It contains a large amount of flavonoids, such as hinokiflavone), promotes hair growth, and is known to show efficacy to make white hair black.

In addition, the composition for washing hair and scalp according to the present invention may include the medicinal plant extract in a proportion of 1 to 10 parts by weight based on 100 parts by weight of the composition, and prevent hair loss when the content of the medicinal plant extract is less than 1 part by weight The induction effect is insignificant, it is difficult to expect further physical property improvement to exceed 10 parts by weight, and the stability of the composition to be described below is lowered, and thus, a phase separation may be induced during long-term storage.

In particular, the medicinal plant extract is preferably configured to include the Hannyeoncho, the sewage, and the side baekrye each in a weight ratio of 2: 1: 1 to be used by mixing the content of the above range so that the pharmacological effect of the medicinal plant is in harmony with each other. good.

More preferably, the composition may be configured to include a ratio of 6 to 9 parts by weight of the medicinal plant extract extracted from the medicinal plant mixture containing a ratio of 2: 1: 1 of Hannyeoncho, sewage, and hinoki respectively.

In addition, the 2,4-diaminopyrimidine-3-oxide (2,4-diamino pyrimidine-3-oxide, Kopexil) contained in the composition for washing hair and scalp according to the present invention can prevent hair loss. As a derivative of minoxidil, which is a type of DHT inhibitor, it can not only promote hair growth, but also prevent hair loss by preventing blood loss by expanding blood vessels and inducing the hair cycle from the resting period to the growth phase. It has a healing effect.

In the composition according to the present invention, the 2,4-diaminopyrimidine-3-oxide is preferably configured to include 0.1 to 10 parts by weight, and the 2,4-diaminopyrimidine-3-oxide If the content is less than 0.1 parts by weight, it is difficult to expect a synergistic effect of blood flow due to vasodilation, it is difficult to realize the effect of promoting hair growth, and when the content exceeds 10 parts by weight, it is difficult to expect further improvement in physical properties and side effects may occur. , More preferably, the composition may include 2,4-diaminopyrimidine-3-oxide in a proportion of 1 part by weight.

On the other hand, the composition for cleaning hair and scalp according to the present invention may be configured to further include 0.5 to 5 parts by weight of a hydrolyzed sponge (spicule) powder.

The hydrolyzed sponge is a bone fragment tissue extracted from the surface of the sea, and a large amount of fine-sized pins are formed on the surface. Various active ingredients included in the medicinal plant extract and 2,4-diaminopyrimidine-3-oxide, etc. Absorbs and helps to absorb the absorbed active ingredients into the deep areas of the scalp, promotes blood circulation, collagen production, and exfoliates keratin formed on the scalp, and at the same time removes unnecessary skin fat to promote regeneration of scalp cells. In addition to the effect, it can also exhibit an effect of increasing moisture.

In particular, the hydrolyzed sponge is generally prepared by a chemical purification process using an acid or base, but the hydrolyzed sponge added to the composition according to the present invention is preferably protease M (protease M) in sponge powder. ), Protease A (protease A), protamex (protamex), neutrases (neutrase), flavozyme (flavourzyme), protease obtained by adding proteolytic enzymes such as alcalase can be used have.

Specifically, the hydrolyzed sponge is prepared by mixing a sponge powder obtained by drying and pulverizing sponge animals with distilled water to prepare a sponge mixture, and protease M and protease A in the prepared sponge mixture. Proteolytic enzymes such as protamex, neutrase, flavozyme, and alcalase are added to decompose the protein, followed by heating to inactivate the proteolytic enzyme, followed by mixing. What was obtained by drying can be used.

In addition, the hydrolyzed sponge may use a powder having an average particle size of 0.01 to 2.0 mm, preferably, a powder pulverized to have a size of 0.1 to 0.5 mm, and the hydrolyzed sponge When the average particle size of the sponge is less than 0.1 mm, the scalp irritation effect is negligible and the amount of impregnation of the active ingredient is small, and when the average particle size of the hydrolyzed sponge exceeds 0.5 mm, there is a fear that the scalp is excessively irritated. More preferably, powder particles having a size of 0.1 to 0.2 mm can be used.

In addition, the hydrolyzed sponge may be included in a proportion of 0.5 to 5 parts by weight based on the total weight of the composition, when the content of the hydrolyzed sponge is less than 0.5 parts by weight, the scalp irritation effect is negligible, 5 parts by weight If exceeded, it is difficult to completely remove the spicule when washing, and it is difficult to expect further improvement in physical properties. More preferably, the composition may include a hydrolyzed sponge in a proportion of 1 part by weight.

Furthermore, the composition for cleaning hair and scalp according to the present invention includes herbal extracts, mushroom extracts, vitamins, moisturizers, surfactants, foaming agents, conditioning agents, pH adjusting agents, pearling agents, preservatives, antibacterial agents, fragrances, viscosity modifiers or mixtures thereof It may be configured to further include a hair and scalp cleaning purposes.

The herbal extract is not only excellent in improving the scalp disease such as hair loss, seborrheic dermatitis, dandruff, but also contains natural herbal extracts as an active ingredient, so it has an excellent skin soothing effect, and provides a peculiar scent to give the body and body aromatherapy effect. It can help relieve stress and can serve as a fragrance, so it can be used as a fragrance.

The herbal extracts include mint extract, lavender extract, basil extract, marshmallow extract, chamomile extract, tea tree extract, fennel extract, or mixtures thereof.

Preferably, the composition according to the present invention may be mixed with the herb extract or fragrance at a ratio of preferably 0.1 to 5 parts by weight, and when mixed with less than 0.1 parts by weight, it is difficult to impart sufficient odor, and exceeds 5 parts by weight If done, too strong odor can be imparted.

The mushroom extract may be used that contains a large amount of vegetable vitamin D, such as ergosterol (ergosterol), which may serve to supply a large amount of vitamin D to the composition.

Particularly, the mushroom extract is prepared by subjecting the mushroom raw material to ultraviolet light before performing the extraction process, thereby preparing a mushroom processed product having significantly increased the content of vitamin D contained in the mushroom, and mixing the prepared mushroom processed product with ethanol and citric acid. To extract ethanol using a solvent, a mushroom extract obtained by extracting vitamin D with high yield may be used.

In one example, the mushroom extract is powdered dry shiitake mushrooms prepared by drying shiitake mushrooms in a condition irradiated with ultraviolet rays, and concentrated vitamin D 10 by extracting shiitake mushroom powder extracted by an extraction process such as ethanol. Mushroom extract may be used to contain a high concentration of 30 mg / L, and it may be configured to prepare a composition in which the content of vitamin D is significantly increased using such a mushroom extract. The mushroom extract may be preferably included in the composition at a ratio of 0.5 to 5 parts by weight, and more preferably, vitamin D may be supplied to the scalp to be included at a rate of 1 part by weight to impart anti-hair loss efficacy.

In addition, the composition according to the present invention may be configured to further include panthenol, glycerol, etc. as a moisturizing agent in order to additionally provide moisturizing power.

In particular, the panthenol is a precursor material that is converted to vitamin B5, and can penetrate deeply into the scalp and hair, and can serve as a transporter that effectively delivers various active ingredients, has excellent ability to combine with moisture, and pantothe in the scalp and hair. It can be converted into a nitric acid, which can play a role in producing vitamin B5.

Therefore, the panthenol as described above can effectively penetrate the scalp and effectively induce hair loss prevention and vasodilation, and also exhibits strong binding properties with moisture, so that it penetrates into the hair shaft and hair roots, thereby providing strong moisturizing power to the scalp. It can serve as a grant.

The panthenol is preferably configured to be mixed at a ratio of 0.5 to 2 parts by weight, and when the content of the panthenol is less than 0.5 parts by weight, it is difficult to expect a sufficient effect, and when it exceeds 2 parts by weight, an additional physical property improvement is expected. Hard. More preferably, the panthenol may be configured to include in a proportion of 1 part by weight, and it is preferable to use D-panthenol.

The surfactant and the foaming agent serve to accelerate the formation of air bubbles in the composition and impart additional cleaning power, and may include anionic surfactants, amphoteric surfactants or mixtures thereof, and surfactants obtained from natural materials and Foaming agents can be preferably used.

In particular, the foaming agent is disodium laureth sulfosuccinate, alkylpolyglycosides, sodium cocoyl amino acid fructose, cocoamidopropyl betaine , Cocoyl monoethanolamine and the like.

The composition according to the present invention may be configured to include the foaming agent in a proportion of preferably 50 to 90 parts by weight, more preferably, the disodium laureth sulfo succinate, alkyl polyglycoside, sodium cocoyl amino acid -Fructose, cocoamidopropyl betaine, and cocoyl monoethanolamine can be used in a proportion of 80 parts by weight.

In addition, the viscosity modifier may serve to control the viscosity of the composition, for example, PEG-120 methyl glucose dioleate (PEG-120 methyl glucose dioleate).

In addition, the water softener serves to inactivate by reacting with various metal ions present in the scalp or hair, and ethylenediamine tetra acetic acid (EDTA) disodium salt is a typical example. Ethylenediaminetetraacetic acid disodium salt may be mixed in a proportion of 0.05 to 5 parts by weight, preferably 0.1 parts by weight.

The conditioning agent provides adhesion to the hair to enable styling and setting, and as the conditioning agent, linoleamidopropyl sebum-dimonium chloride phosphate and polyquaternium-10 Is a representative example.

In particular, the linoleamidopropyl sebum-dimonium chloride phosphate may serve as an emulsifier, hair conditioning agent, antistatic agent, and preferably, may be mixed at a ratio of 0.1 to 10 parts by weight based on the total weight of the composition, , More preferably, it can be mixed in a proportion of 0.5 parts by weight.

In addition, the polyquaternium-10 is a cationic polymer obtained by adding diglycidyl trimethylammonium chloride or 3-chloro-2-hydroxypropyl trimethylammonium chloride to hydroxyethyl cellulose, a hair dressing agent, a film forming agent, It may serve as an antistatic agent, etc., and may preferably be mixed at a ratio of 0.1 to 5 parts by weight, and more preferably at a ratio of 0.5 parts by weight.

The antibacterial agent not only imparts antibacterial properties to the hair and scalp, but also serves to contribute to the long-term stability of the composition, and grapefruit extract, sodium benzoate, and the like.

Preferably, the antimicrobial agent may be mixed in a proportion of 0.1 to 5 parts by weight, more preferably, a mixture of the grapefruit extract and sodium benzoate in a weight ratio of 1: 1 may be included in a proportion of 0.4 parts by weight. have.

The composition for cleaning hair and scalp according to the present invention as described above includes medicinal plant extracts showing excellent anti-hair loss performance, such as Hannyeoncho, sewage, and lateral leaves, which promote blood circulation and scalp regeneration, and copexil (Kopexil) showing excellent hair growth promoting effect ) As an active ingredient, and can penetrate the active ingredient deep into the scalp, and includes a hydrolyzed sponge that gives an excellent moisturizing effect, so it has excellent moisturizing, hair growth and hair loss prevention performance.

According to a preferred embodiment of the present invention, the composition for washing hair and scalp according to the present invention was prepared by extracting a mixture containing the above-mentioned Hannyeoncho, sewage, and side lobes in a weight ratio of 2: 1: 1 by a low-temperature vacuum extraction method. Medicinal plant extracts, hydrolyzed sponges pre-treated with proteolytic enzymes and shiitake mushroom extracts with a high content of vitamin D can be used to prepare compositions with shampoo formulations for washing hair and scalp.

Specifically, the composition for washing the hair and scalp is 7 parts by weight of medicinal plant extract prepared by the above method, 2,4-diamino pyrimidine-3-oxide, Kopexil ) 1 part by weight, 2 parts by weight of a hydrolyzed sponge, 1 part by weight of shiitake extract, 1 part by weight of panthenol, 35 parts by weight of disodium laureth sulfosuccinate, 10 parts by weight of alkylpolyglycosides, 10 parts by weight of sodium cocoyl amino acid fructose, 20 parts by weight of cocoamidoproply betaine, cocoyl monoethanolamine 5 parts by weight, PEG-120 methyl glucose dioleate 1 part by weight, 0.5 parts by weight of polyquaternium-10, 1 part by weight of glycerin, salicylic acid ) 0.1 parts by weight, ethyl 0.1 parts by weight of ethylenediamine tetra acetic acid (EDTA) disodium salt, 0.5 parts by weight of linoleamidopropyl PG-dimonium chloride phosphate, 0.2 parts by weight of grapefruit extract, sodium It may be configured to prepare a composition having a shampoo formulation by mixing 0.2 parts by weight of benzoate, 0.5 parts by weight of fragrance, and the remaining purified water, respectively.

The shampoo composition prepared by the above method has excellent hair loss prevention and hair growth promotion functions, has efficacy such as cleaning power and moisturization, and has excellent formulation stability, and thus can be easily utilized for a long period of time for the purpose of washing hair and scalp. .

On the other hand, the present invention provides a method for preparing a composition for cleaning hair and scalp as described above.

The method for preparing a composition for cleaning hair and scalp according to the present invention provides (a) a medicinal plant mixture including Hannyeoncho, sewage, and oleander leaves and water in a vacuum low temperature extractor, and extracts by distillation under reduced pressure to produce a medicinal plant extract. To do; (b) supplying purified water and polyquaternium-10 to the compounding tank and heating to a temperature of 60 to 80 ° C. to prepare a first mixture; (c) heating the first mixture to a temperature of 60 to 80 ° C. and disodium laureth sulfosuccinate, alkylpolyglycosides, sodium cocoyl amino acid fructose), cocoamidopropyl betaine, cocoyl monoethanolamine, respectively, to sequentially supply to prepare a second mixture; (d) preparing a third mixture by heating the second mixture to a temperature of 40 to 60 ° C. and feeding PEG-120 methyl glucose dioleate; (e) heating the third mixture to a temperature of 30 to 50 ° C., glycerin, panthenol, salicylic acid, ethylenediamine tetra acetic acid (EDTA) disodium salt ), Linoleamidopropyl PG-dimonium chloride phosphate and the medicinal plant extract is sequentially added to prepare a fourth mixture; And (f) preparing a composition for washing hair and scalp by sequentially mixing a grapefruit extract, sodium benzoate, and a fragrance in a fourth mixture, wherein each raw material is described in the aforementioned composition. The composition for washing hair and scalp may be prepared by utilizing the composition as described above.

In the step (a), a medicinal plant mixture including Hannyeoncho, sewage, and cypress leaves is supplied to a vacuum low-temperature extractor and extracted by distillation under reduced pressure to prepare a medicinal plant extract.

The medicinal plant extract may be prepared using a variety of conventional methods for preparing extracts from plants, such as hot water extraction, ethanol extraction, reflux extraction, etc., but preferably, a short time using a vacuum low temperature extraction method employing a circulating steam cooling method. While preventing the destruction of the active ingredient, it can be configured to produce a medicinal plant extract containing the active ingredient in a high yield.

To this end, the vacuum low-temperature extraction method, by using a high-speed vacuum low-temperature extraction system as shown below, to prepare a medicinal plant extract through a reduced pressure distillation method to shorten the extraction time and minimize the destruction of active ingredients.

1 is a conceptual diagram showing a high-speed vacuum cryogenic extraction system 10 used to manufacture a medicinal plant extract according to the present invention.

Referring to Figure 1, the high-speed vacuum low-temperature extraction system 10, a receiving space for supporting medicinal plants and water is formed, a heating means 110 is provided on the lower side to heat the mixture of the medicinal plants and water, , A vacuum tank 100 equipped with a first outlet 150 for discharging steam formed by heating by providing a steam outlet 130 on one side of the upper side and a medicinal plant extract formed on the other side of the lower side ), Is connected to the steam outlet 130 formed on the upper side of the vacuum tank 100 to cool the steam generated in the vacuum tank 100, a second discharge unit 210 for discharging the cooled steam It is provided, the first cooler 200 having a third discharge unit 230 for discharging condensed water formed from the cooled steam, is connected to the first cooler 200 via the first cooler 200 It receives the steam and cools it by water cooling, and a circulation pump 310 is provided to cool it. A second cooler 300 for transferring one steam to the first cooler 200, an accommodating space for supporting distilled water is formed therein, and the first cooler 200 is connected to the third discharge unit 230 Recovering the condensed water generated in the distilled water storage tank 400 provided with a fourth discharge unit 410 for discharging the distilled water, the distilled water storage tank 400 is connected to one side of the distilled water storage tank 400 and the agent 1 Vacuum pump 430 equipped with a hydrolysis filter 420 for forming a vacuum inside the receiving space of the vacuum tank 100 connected to the cooler 200 and discharging water flowing from the distilled water storage tank 400, and It is connected to the first discharge unit 150 and the fourth discharge unit 410 and includes an extract storage tank 500 for storing the medicinal plant extract and distilled water discharged from the vacuum chamber 100 and the distilled water storage tank 400 It has a structure.

The vacuum low-temperature extractor as described above can produce a medicinal plant extract by distillation under reduced pressure, thereby shortening the extraction time and minimizing the destruction of active ingredients.

More specifically, the vacuum tank 100 is formed with a receiving space therein to accommodate the medicinal plants and water, and can seal the receiving space to form a space for vacuum decompression, and a heating means on the lower side. (110) is provided to prepare a medicinal plant extract by heating the mixture of the medicinal plant and water. A steam outlet portion 130 is formed on one side of the upper portion of the vacuum chamber 100 to discharge the vapor generated when preparing the medicinal plant extract through heating to the first cooler 200, and the generated medicinal portion on the other side of the bottom. A first discharge unit 150 for discharging the plant extract is provided to discharge the medicinal plant extract into the extract storage tank 500 to be described later. In addition, the vacuum tank 100 may be provided with a discharge means 170 for discharging the steam generated therein to the outside.

The first cooler 200 may be connected to a steam outlet 130 to receive and cool the steam discharged from the vacuum tank 100, and one side may be connected to the distilled water storage tank 400 to be described later. The condensed water formed by the condensation of steam inside the cooler 200 may be configured to be recovered by the distilled water storage tank 400, thereby forming a structure for recovering the active ingredients contained in the steam, thereby effectively containing the medicinal plants. The extraction yield of ingredients can be maximized. In addition, the other side of the first cooler 200 may be connected to the second cooler 300 to transfer the primary cooled steam from the first cooler 200 to the second cooler to cool again, and the second cooler Recirculating structure for cooling the hot air supplied from the vacuum tank 100 may be formed by receiving the steam cooled again at 300. To this end, the first cooler 200 may be provided with a cooling compressor or a cooling fan to form a structure for cooling steam in the vacuum chamber 100.

The second cooler 300 is connected to the first cooler 200 to receive the steam passing through the first cooler 200 to cool the steam again by water cooling, and a circulation pump 310 is provided to provide the second cooler A structure capable of cooling the steam discharged from the vacuum chamber 100 may be formed by passing the steam passing through the 300 to the first cooler 200. In addition, the second cooler 300 is provided with a cooling core 320 through which steam flows, and a cooling fan 330 is provided on the outside to cool the water cooled by the second cooler 300 again. Can be configured.

In addition, the distilled water storage tank 400 connected to the other side of the first cooler 200 is formed with a receiving space for supporting distilled water therein, and is connected to the first cooler 200 to cool in the first cooler 200 It is possible to form a structure for recovering the condensed water formed by the steam, thereby, it is possible to form a structure for recovering the active ingredient contained in the steam. In addition, a third discharge unit 410 for discharging the distilled water carrying the active ingredient is provided to form a structure for discharging the distilled water carrying the active ingredient to the extract storage tank 500 to be described later.

In particular, a vacuum pump 430 equipped with a hydrolysis filter 420 for discharging water flowing from the distilled water storage tank 400 is connected to one side of the distilled water storage tank 400 to depressurize the distilled water storage tank 400. A vacuum environment is formed, and the vacuum chamber 100 connected to the first cooler 200 may also be depressurized.

In addition, the extract storage tank 500 is connected to the first discharge unit 150 and the third discharge unit 410 to store the medicinal plant extract and distilled water discharged from the vacuum tank 100 and the distilled water storage tank 400 May be provided with a fourth discharge portion 510 on one side to form a structure for discharging the medicinal plant extracts supported therein.

Furthermore, the vacuum tank 100, the first cooler 200, the second cooler 300, the distilled water storage tank 400 and the extract storage tank 500 are respectively connected by a connection pipe, and the connection pipe is provided with a valve. It can form a structure to control the flow of steam, extract, distilled water.

The high-speed vacuum low-temperature extraction system 10 as described above drives the heating means mounted under the vacuum tank 100 in a state in which the vacuum pressure is continuously applied to extract hot water from a mixture of medicinal plants and water. The steam generated in the extraction process is cooled by the first cooler 200 and the second cooler 300 to form a structure for recovering active ingredients.

The step (b) is a step of preparing a first mixture by mixing purified water and polyquaternium 10 in a compounding tank, wherein the purified water and polyquaternium 10 are heated to a temperature of 60 to 80 ° C. to completely dissolve the first mixture. It can be prepared, preferably, by mixing the purified water and polyquaternium 10 and heated to a temperature of 70 ℃ to prepare a first mixture.

In step (c), disodium laureth sulfolaxinate, alkylpolyglycoside, sodium cocoylamino acid-fructose, cocoamidopropyl betaine, and cocoyl monoethanolamine are sequentially supplied to the first mixture, respectively. The second mixture may be prepared by mixing while heated to a temperature of 60 to 80 ° C, and preferably, the second mixture may be prepared by heating to a temperature of 70 ° C.

In the step (d), the third mixture may be prepared by heating the second mixture to a temperature of 40 to 60 ° C. and feeding PEG-120 methyl glucose dioleate, preferably at a temperature of 50 ° C. By heating, a third mixture can be prepared.

In the step (e), the third mixture is heated to a temperature of 30 to 50 ° C. and glycerin, panthenol, salicylic acid, ethylenediaminetetraacetic acid disodium salt, linoleamidopropyl sebum-dimonium chloride phosphate and the medicinal plant extract It may be sequentially introduced to prepare a fourth mixture, preferably, heated to a temperature of 40 ℃ to prepare a fourth mixture.

In addition, in this step, after preparing the fourth mixture, it may be configured to further include the step of supplying a hydrolyzed sponge to the fourth mixture, and supplying the hydrolyzed sponge to the fourth mixture After reacting for a sufficient time, it can be configured to absorb the active ingredient.

In the step (f), a composition for washing hair and scalp may be prepared by sequentially mixing a grapefruit extract, sodium benzoate, and a fragrance in a fourth mixture, and preferably, heating the composition at a temperature of 40 ° C. Can be produced.

According to the method of preparing a composition for cleaning hair and scalp according to the present invention as described above, it is configured to mix medicinal plant extracts and various additives at a specific temperature condition, thereby producing a stable composition without phase separation even during long-term use. The composition can be utilized in various formulations, such as shampoos, conditioners, etc., for cleaning hair and scalp.

Hereinafter, the present invention will be described in more detail with reference to examples.

The examples presented are only specific examples of the invention and are not intended to limit the scope of the invention.

<Production Example> Preparation of medicinal plant extract

Commercially available Hannyeoncho (Daejeon-dong, Yeongcheon-si, Gyeongbuk), Hasuo (Donggwanghanjae, Sojeo-ro, Yeongju-si, Gyeongbuk), and Baekbaek-yeop (medicinal herb house, Soje, Bongdam-eup, Hwaseong-si, Gyeonggi-do) were purchased.

 After supplying 500 g of Hannyeoncho, 250 g of sewage, and 250 g of side ferns at a weight ratio of 2: 1: 1 to a high-speed vacuum low-temperature extractor to which a circulating steam cooling method has been applied, 10 L of water is supplied to deposit the herbal mixture. , Was maintained at room temperature for about 12 hours to soften the herbal medicine mixture.

Thereafter, an extraction process was performed by performing an extraction process using a vacuum low-temperature extraction method using a vacuum low-temperature extractor as shown in FIG. 1 to introduce a medicinal plant extract. An extract was prepared.

<Example 1>

Medicinal plant extract prepared by the method according to the manufacturing example was used, grapefruit extract, fragrance, disodium laureth sulfosuccinate (LES / Miwon Corporation), alkyl polyglycosides (alkylpolyglycosides, APG / LG life) Health), sodium cocoyl amino acid fructose (Oliveoel fruttoside / Kalichem italia, italy), cocoamidoproply betaine, Mitaine CA / cocoyl monoethanolamine, CME / Miwon Corporation), PEG-120 methyl glucose dioleate, DOE120 / Lubrizol, diaminopyrimidine oxide, Kopexil / Kumar, polyquaternium-10 10, Miwon Corporation), glycerin, panthenol, salicylic acid, ethylenediamine tetra acetic acid (EDTA) disodium salt, linoleami Linoleamidopropyl PG-dimonium chloride phosphate, sodium benzoate, protein hydrolysis treatment, 1 part by weight of a hydrolyzed sponge with an average particle size of 200 μm, shiitake mushroom extract ( 20 mg / L) was mixed with the composition as shown in Table 1 below to prepare a shampoo composition.

Specifically, purified water and polyquaternium 10 were supplied to the compounding batch, and heated to 70 ° C. and stirred sufficiently until completely dissolved. Then, disodium laureth sulfolaxinate, alkyl polyglycoside, sodium cocoyl amino acid-fructose, cocoamidopropyl betaine, and cocoyl monoethanolamine were sequentially supplied and completely dissolved, followed by diaminopyrimidine oxide. And completely dissolved to prepare a mixture.

Subsequently, methyl glucose dioleate was supplied to the mixture and dissolved in a state where the heating temperature was lowered to 50 ° C., and the heating temperature was lowered to 40 ° C., followed by glycerin, panthenol, salicylic acid, ethylenediaminetetraacetic acid, and linoleamidopropyl sebum -Dimonium chloride phosphate, medicinal plant extracts prepared by the method according to the manufacturing example, and shiitake extracts were sequentially supplied and mixed, and then, a hydrolyzed sponge having an average particle size of 200 μm was mixed. Then, the grapefruit extract, sodium benzoate, and fragrance were finally supplied to prepare a shampoo composition.

<Example 2>

A shampoo composition was prepared in the same manner as in Example 1, except that 4.9 parts by weight of a hydrolyzed sponge instead of purified water was mixed.

<Example 3>

A shampoo composition was prepared in the same manner as in Example 1, except that 4.9 parts by weight of shiitake mushroom extract was mixed instead of purified water.

<Comparative Example 1>

A shampoo composition was prepared in the same manner as in Example, except that purified water was added instead of the hydrolyzed sponge.

<Comparative Example 2>

A shampoo composition was prepared in the same manner as in Example except that 4.9 parts by weight of purified water was added instead of shiitake mushroom extract.

<Experimental Example 1> Anti-hair loss efficacy analysis

In order to confirm the anti-hair loss effect of the prepared shampoo composition, the compositions according to Examples and Comparative Examples 1 to 4 were washed once a day for 30 men with alopecia for hair and scalp, and the usage period was 2 months. By measuring the degree of anti-hair loss effect, the results were shown as an average value, and the results are shown in Table 1 below (however, in Table 1 below, 5 points when the effect of reducing the amount of hair loss was remarkable after 2 months of washing, 4 points for excellent, 3 points for normal, 2 points for invariant, 1 point for severe hair loss symptoms).

As shown in Table 2, the compositions according to Examples 1 to 3 were able to confirm that the hair loss prevention effect was superior to Comparative Examples 1 and 2, and in particular, hair loss of the shampoo composition without using a hydrolyzed sponge. Since it was confirmed that the prevention efficacy was the lowest, it was confirmed that the effect of preventing hair loss was significantly increased due to the addition of the hydrolyzed sponge.

In addition, in the case of Comparative Example 2 in which no mushroom extract was used, it was confirmed that the hair loss prevention effect was inferior to Examples 1 to 3 in which the mushroom extract was mixed, so that the hair loss prevention effect was due to the introduction of vitamin D contained in the mushroom extract. It was confirmed that it increased.

<Experimental Example 2> Moisturizing effect analysis

In order to analyze the moisturizing effect of the prepared composition, 30 males were washed with hair and scalp for 2 months with the compositions of Examples 1 to 3 and Comparative Example 1, and finally washed after 2 months had passed. Then, the moisture change rate was measured for 1 to 6 hours, and the results are shown in FIG. 2 below.

As shown in Figure 2, compared to the shampoo composition according to Comparative Example 1, it was confirmed that the moisture level was excellent in the scalp of men washed with the shampoo compositions of Examples 1 and 2, and the moisturizing effect was excellent. , Through this fact, it was confirmed that the moisturizing effect was increased by the hydrolyzed sponge.

<Experiment 3> Analysis of dandruff removal effect

Thirty males in their thirties who were judged to have a lot of dandruff were selected, divided into three groups, and the dandruff accumulated for two days was collected with a vacuum suction device and the weight of the collected dandruff was measured. Thereafter, for each formulation for each group, the hair and scalp cleaning compositions were washed once a day for 2 months, and the weights of dandruff accumulated at intervals of 2 days were compared, and as shown in Equation 1 below, The dandruff reduction rate was calculated by comparing the weight of dandruff before washing with the composition and the weight of dandruff after 2 months of using the composition, and the results are shown in Table 3 below.

[Equation 1]

As shown in Table 3, while the composition prepared by the method according to Examples 1 to 3 was able to confirm that the anti-dandruff effect is also excellent, in the case of the composition of Comparative Example 1 that does not contain a hydrolyzed sponge , It was confirmed that the anti-dandruff effect was the worst.

<Experimental Example 4> Formulation stability analysis

In order to analyze the formulation stability of the shampoo compositions prepared by the methods according to Examples 1 to 3, the prepared shampoo compositions were respectively left at high temperature (40 ° C), low temperature (3 ° C), and room temperature (20 ° C) conditions. Then, the change over time was carefully observed for approximately 3 months, and in particular, the high temperature condition was observed, and the change in color, odor, etc. was confirmed in comparison with the low temperature condition.

Lastly, the prepared shampoo composition is stored for 12 hours at frozen conditions (-20 ° C), thawed at room temperature for 12 hours, and then stored again under frozen conditions for 10 times, and the liquid phase change of the prepared shampoo composition ( Freeze-thaw test was performed to observe layer separation, precipitation, etc.).

As a result, it was confirmed that phase separation did not occur in the shampoo composition in all cases, and it was confirmed that the shampoo composition with excellent formulation stability can be prepared by dissolving each material at a specific temperature.

Claims (6)

Medicinal plant extracts, 2,4-diamino pyrimidine-3-oxide, Kopexil and hydrolysed sponges extracted from medicinal plants including Hannyeoncho, sewage, and cypress sponge) as a composition comprising a powder as an active ingredient,
1 to 10 parts by weight of the medicinal plant extract based on 100 parts by weight of the composition, 0.1 to 10 parts by weight of the 2,4-diaminopyrimidine-3-oxide and 0.5 to 5 parts by weight of a hydrolysed sponge powder Composition for cleaning hair and scalp, characterized in that it contains a part. delete delete According to claim 1,
Herbal extracts, mushroom extracts, vitamins, moisturizers, surfactants, foaming agents, conditioning agents, pH adjusting agents, pearling agents, preservatives, antibacterial agents, flavoring agents and viscosity control agents further comprising at least one additive selected from the group consisting of Composition for cleaning hair and scalp. According to claim 1,
(A) supplying a mixture of medicinal plants and water containing medicinal plants including Hannyeoncho, sageo, baekryeop in a vacuum low temperature extractor, and extracting by distillation under reduced pressure to prepare a medicinal plant extract;
(b) supplying purified water and polyquaternium-10 to the compounding tank and heating to a temperature of 60 to 80 ° C. to prepare a first mixture;
(c) heating the first mixture to a temperature of 60 to 80 ° C. and disodium laureth sulfosuccinate, alkylpolyglycosides, sodium cocoyl amino acid fructose), cocoamidopropyl betaine, cocoyl monoethanolamine, respectively, to sequentially supply to prepare a second mixture;
(d) preparing the third mixture by heating the second mixture to a temperature of 40 to 60 ° C. and supplying PEG-120 methyl glucose dioleate;
(e) heating the third mixture to a temperature of 30 to 50 ° C., glycerin, panthenol, salicylic acid, ethylenediamine tetra acetic acid (EDTA) disodium salt ), Linoleamidopropyl PG-dimonium chloride phosphate and the medicinal plant extract is sequentially added to prepare a fourth mixture;
f) to the fourth mixture
In step (e), after preparing the fourth mixture, preparing a fifth mixture by supplying a hydrolyzed sponge to the fourth mixture;
(g) preparing a sixth mixture by sequentially mixing a grapefruit extract, sodium benzoate, and a fragrance in the fifth mixture; And
h) A method of preparing a composition for washing hair and scalp, comprising mixing 2,4-diaminopyrimidine-3-oxide in the sixth mixture.
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