CN108125869A - Dried orange peel general flavone and its application in cosmetics are extracted from dried orange peel using ultrasonic wave auxiliary law - Google Patents
Dried orange peel general flavone and its application in cosmetics are extracted from dried orange peel using ultrasonic wave auxiliary law Download PDFInfo
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- CN108125869A CN108125869A CN201810103219.2A CN201810103219A CN108125869A CN 108125869 A CN108125869 A CN 108125869A CN 201810103219 A CN201810103219 A CN 201810103219A CN 108125869 A CN108125869 A CN 108125869A
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- orange peel
- dried orange
- ultrasonic wave
- cosmetics
- extraction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Abstract
The invention discloses the methods that dried orange peel flavones is extracted from dried orange peel using ultrasonic wave auxiliary law, include the following steps：1) dried orange peel of drying is crushed, it is spare；2) in dried orange peel after being pulverized, after adding in the infiltration of organic solution extractant, using ultrasonic wave extraction；3) it filters, centrifuge filtrate, it is dried orange peel flavone extractive to take supernatant liquor.The present invention extracts dried orange peel flavones using ultrasonic wave auxiliary law from dried orange peel, and the extracting method is simple to operation, extraction efficiency is high, low energy consumption；The dried orange peel flavones of extraction has excellent sun-proof ability, and scientific basis and theoretical foundation are provided for the deep level development of dried orange peel resource and popularization to the research of dried orange peel sun-screening function.
Description
Technical field
The invention belongs to the technical fields of dried orange peel comprehensive utilization, and in particular to be extracted from dried orange peel using ultrasonic wave auxiliary law
Dried orange peel flavones and its application in cosmetics, more particularly relate to dried orange peel flavones as sun-prevention component in cosmetics should
With.
Background technology
With the continuous development of society with progress and the increasing living standard of people, cosmetics have been increasingly becoming existing
An indispensable part in living for life.Requirement of the people for the quality of cosmetics is also higher and higher.Exploitation is beneficial to people
It body health and takes into account the green cosmetics of beauty and health care functions and has a vast market prospect, environmentally protective is modern cosmetics
Eternal topic.The cosmetics of pure natural active ingredient are added due to small irritation, stronger permeability and higher-security
Physicochemical property and physiological activity, and in skin care item have diversified application, such as anti-oxidant, anti-aging, sun-proof whitening
And convergence moisturizing etc., therefore have wide market and application prospect in emerging cosmetic field.Plant cosmetics have
Good application foundation.In ancient Chinese, people are had a finger in every pie using the juice of plant come beauty and skin care, such as with balsamine
It is first-class.It was handled, just directly used, active ingredient is indefinite, and efficiency is low by simple physical with fruit or branches and leaves in the past.And show
Some plant extracts deposit technique and mostly start with from the active ingredient of plant, carry out the monomer separation of active ingredient, every time only separation one
Kind ingredient, causes extraction cost to rise, wastage of material, it is difficult to universal.In fact, inside a kind of plant, active ingredient is more
Kind is various, if can be extracted and directly used, for cosmetic industry, not only improves extraction efficiency, but also
Reduce extraction cost.Cheap and safe raw material can be widely used at once.Flavonoids is plant in cosmetics
One of effective constituents.As a kind of skin-protecting factor, Flavonoid substances have anti-oxidant, sun-proof, radioresistance, antibacterial and other effects.
Dried orange peel is rutaceae orange and its dry mature skin of variety, containing abundant flavonoid substance, is had
Multiple biological activities[1-2], in addition, the country mainly concentrates the research of dried orange peel its application in terms of pharmacology at present, such as anti-swollen
Knurl, antiallergy, it is anti-inflammatory and anti-oxidant the effects that[3-6], but for its application in cosmetics, do not find also targetedly to grind
Study carefully.Also, it mainly to the orange peel of Xinhui citrus reticulata, pulp processing and utilization, and gives it up to mandarin orange seed, causes certain wasting of resources.
Therefore, to dried orange peel extracts, the research of performance used for cosmetic provides section for the deep level development of dried orange peel resource and popularization
Learn foundation and theoretical foundation.
Invention content
It is yellow the object of the present invention is to provide dried orange peel is extracted in a kind of slave dried orange peel easy to operate, extraction efficiency is high and low energy consumption
The method of ketone, and study application of the dried orange peel extracts in cosmetics.
The technical solution adopted by the present invention is：The method for extracting dried orange peel flavones from dried orange peel using ultrasonic wave auxiliary law, packet
Include following steps：
1) dried orange peel of drying is crushed, it is spare；
2) in dried orange peel after being pulverized, after adding in the infiltration of organic solution extractant, using ultrasonic wave extraction；
3) it filters, centrifuge filtrate, it is dried orange peel flavone extractive to take supernatant liquor.
Preferably, in step 2), the organic solution extractant is absolute ethyl alcohol or 1,2-PD.It is furthermore preferred that institute
It is 1,2- propylene glycol to state organic solution extractant.
Preferably, in step 2), the solid-liquid ratio of dried orange peel and organic solution extractant is 0.02-0.4g:20mL.More preferably
, in step 2), the solid-liquid ratio of dried orange peel and organic solution extractant is 0.09-0.4g:20mL；It is further preferred that step 2)
In, the solid-liquid ratio of dried orange peel and organic solution extractant is 0.09-0.32g:20mL；It is furthermore preferred that dried orange peel is extracted with organic solution
The solid-liquid ratio of agent is 0.32g:20mL.
Preferably, in step 2), the condition control of ultrasonic wave extraction is：Extracting temperature is 28-35 DEG C, and extraction time is
20-120min.It is furthermore preferred that in step 2), the condition control of ultrasonic wave extraction is：Extracting temperature is 30 DEG C, and extraction time is
80min。
It is furthermore preferred that in step 3), the UVC of dried orange peel flavone extractive be 0.019-0.325, UVB be 0.097-0.391 and
UVA is 0.044-0.913.
The present invention provides application of the dried orange peel flavones in cosmetics, and the dried orange peel flavones is added as active components of plants
It is added in cosmetics.It is furthermore preferred that the dried orange peel flavones is made an addition to as sun-prevention component in cosmetics.
Preferably, the dosage form of the cosmetics is solution, gel, lotion or cream shape.
Preferably, the cosmetics further include common cosmetic.It is further preferred that the cosmetic is
Antioxidant, preservative, fragrance, surfactant, moisturizer, thickener, pH adjusting agent, fragrance, pigment and skin penetrant
In it is one or more.
A kind of facial mask liquid, by the percent by weight of raw material, the facial mask liquid includes the dried orange peel extracting flavonoids of 10-20%
Liquid.
A kind of anti-aging whitening emulsion includes the component of following weight percent：Dried orange peel flavone extractive 20-30% plants
Object essential oil 8-15%, Hydrolyzed Collagen 3-5%, surplus is deionized water.
A kind of Essence includes the component of following weight percent：Trehalose 3-8%, preservative 0.2-0.8%, surplus
For dried orange peel flavone extractive.
A kind of lotion includes the component of following weight percent：18-25% panthenols 5.0,1-5% Hydrolyzed Collagens,
20-40% dried orange peel flavone extractives, 0.2-0.8% preservatives, surplus are deionized water.
The beneficial effects of the invention are as follows：The present invention extracts sun-prevention component dried orange peel Huang using ultrasonic wave auxiliary law from dried orange peel
Ketone, the extracting method is simple to operation, extraction efficiency is high, low energy consumption；The dried orange peel flavones of extraction have excellent sun-proof ability and
Stability provides scientific basis and theoretical base to the research of dried orange peel sun-screening function for the deep level development of dried orange peel resource and popularization
Plinth.
Description of the drawings
Fig. 1 shows dried orange peel and influence of the organic solution extractant type to the sunscreen actives of dried orange peel flavone extractive；
Fig. 2 shows the solid-liquid ratio of dried orange peel and organic solution extractant to the shadow of the sunscreen actives of dried orange peel flavone extractive
It rings.
Specific embodiment
Embodiment 1
This investigates extractant and the relationship of dried orange peel flavone extractive absorbance.
Accurate 4 parts of dried orange peel sample for weighing 80-100 mesh is divided into two groups, and first group is two parts of 20mg dried orange peels, and second group is
Two parts of 90mg dried orange peels, are separately added into 1,2-PD in first group and second group and 2 kinds of different solvents of absolute ethyl alcohol are each
20mL is filtered after infiltration in 30 DEG C of ultrasonic wave extraction 20min, and filtrate centrifuges 15min under 4000r/min, takes 2ml supernatants,
Its ultra-violet absorption spectrum between 200-400nm is surveyed, and calculates the mean absorbance values of its UVC, UVB and UVA.
Using dried orange peel flavone extractive to ultraviolet spectra trap as evaluation criteria, solvent type is to ultrasonic extracting process
Influence see Fig. 1 and table 1.As shown in Figure 1,1,2-PD is better than ethyl alcohol as extracting solution, extraction effect.
Influence of the 1 organic solution extractant of table to the sunscreen actives of dried orange peel flavone extractive
Embodiment 2
This investigates dried orange peel and the solid-liquid ratio of organic solution extractant and the relationship of dried orange peel flavone extractive absorbance.
Accurate 8 parts of dried orange peel sample for weighing 80-100 mesh, every part be 90mg, 110mg, 150mg, 220mg, 280mg,
320mg, 380mg, 390mg are separately added into 1,2-PD 20mL, are filtered after infiltration in 30 DEG C of ultrasonic wave extraction 20min, filtrate
15min is centrifuged under 4000r/min, takes 2ml supernatants, ultra-violet absorption spectrum measures same as Example 1.
Using dried orange peel flavone extractive to ultraviolet spectra trap as evaluation criteria, the material of dried orange peel and organic solution extractant
Influence of the liquor ratio to dried orange peel flavone extractive sunscreen actives is as shown in Figure 2.As shown in Figure 2, with the increase of solid-liquid ratio, dried orange peel carries
The sunscreen actives of flavone extractive are also increasing, in 0.09-0.32:When 20 (g/mL), reach maximum value.But with solid-liquid ratio
Continue increase, the sunscreen actives of dried orange peel extracts are reduced instead.Reason may be that sun-prevention component is molten in the case that raw material is certain
Extracting rate is certain, and when solid-liquid ratio is excessive, dried orange peel is not extracted fully, in addition excessively increases the body of Extraction solvent 1,2-PD
Product, also brings burden for subsequent recovery operation.Therefore, best solid-liquid ratio is 0.32:20(g/mL).
Embodiment 3
This investigates ultrasonic extraction time and the relationship of dried orange peel flavone extractive absorbance.
Accurate 4 parts of dried orange peel sample for weighing 80-100 mesh, every part is 320mg, is separately added into 1,2-PD 20mL, is infiltrated
Afterwards in 30 DEG C of ultrasonic wave extractions, extraction time is respectively 20min, and 40min, 60min, 80min, 100min, 120min filtering are filtered
Liquid centrifuges 15min under 4000r/min, takes 2ml supernatants, and ultra-violet absorption spectrum measures same as Example 1.
Using dried orange peel flavone extractive to ultraviolet spectra trap as evaluation criteria, the ultrasonic extraction time carries dried orange peel flavones
The influence for taking liquid sunscreen actives is as shown in table 2.As shown in Table 2, upon extracting between in 20-80min, dried orange peel extracts it is sun-proof
Activity increases with the extension of extraction time, and after 80min, recovery rate is not further added by or increases very slow.It is this is because super
Extraction time is long under the conditions of sound, it is possible to sun-prevention component can be caused in dried orange peel by certain loss, accordingly, it is determined that best
Extraction time is 80min.
Influence of the 2 ultrasonic extraction time of table to the sunscreen actives of dried orange peel flavone extractive
Test case 1
This investigates influence of the storage temperature to the stability of dried orange peel flavone extractive.
The dried orange peel flavone extractive of preparation is divided into 4 parts, every part of 10mL respectively, respectively at -10 DEG C, 0 DEG C, 30 DEG C and 40 DEG C
After lower heat preservation 4h, its UV Absorption degree is measured, acquired results are shown in Table 3.
Influence of 3 storage temperature of table to the stability of dried orange peel flavone extractive
As shown in Table 3, dried orange peel flavone extractive after different Temperature Treatments, protect by UVA, UVB, UVC mean absorbance values
It stays rate variation little, illustrates that temperature is smaller to the stability influence of dried orange peel flavone extractive.Therefore, dried orange peel flavone extractive has
Preferable thermal stability.
Test case 2
This investigates influence of the ultraviolet light to the stability of dried orange peel flavone extractive.
The dried orange peel flavone extractive of preparation is divided into 3 parts, every part of 100mL respectively, is irradiated 10 days, 20 days and 30 days respectively,
Its UV Absorption degree is measured, acquired results are shown in Table 4.
Influence of 4 ultraviolet light of table to the sun-proof stability of dried orange peel flavone extractive
As shown in Table 4, after different Temperature Treatments, UVA, UVB, UVC mean absorbance values become dried orange peel flavone extractive
Change less, illustrate that ultraviolet light is smaller to the sun-proof stability influence of dried orange peel flavone extractive.Therefore, dried orange peel extracts have
Preferable ultraviolet light stability.
Embodiment 4
A kind of anti-aging whitening emulsion includes the component of following weight percent：
Embodiment 5
A kind of Essence includes the component of following weight percent：
Trehalose 5%,
Preservative 0.2%,
Surplus is dried orange peel flavone extractive.
Embodiment 6
A kind of lotion includes the component of following weight percent：
Skin care item prepared by embodiment 4-6 play the role of skin anti-oxidant and anti-aging, and mildness is good, natural nothing
Poison contributes to skin to restore elasticity and gloss.
Bibliography：
[1] Liao Su fawns the isolating and purifying of dried orange peel polysaccharide, structural characterization and its free-radical scavenging activity research [D] Guangzhou：
Guangdong Pharmaceutical University, 2009
[2] high bud citrus chachiensis hortorums flavone compound and volatile oil component and its activity research [D] Wuhan：Central China agricultural is big
It learns, 2011.
The orange peels such as [3] Wan Lixiu, Xiao Gengsheng, Xu Yujuan flavones before purification after inoxidizability comparative studies [J] food
Science, 2011 (32), 87-91.
[4] research [J] the Inner Mongol that chromocor compound in equality tangerine peels removes free radical is tieed up in Li Shumei, Song Gangya, field
Agriculture university's journal, 2004 (25), 89-91.
[5] Li Keke, suitable progress [J] food research and developments into Flavonoids from Dried Orange Peel, 2017,
38 (17), 221-224.
[6] antioxidant activity research [J] the Heilungkiang medicine of Mia Audina dried orange peel extracts, 2014,27 (2), 306-
309.
Claims (10)
1. the method that dried orange peel flavones is extracted from dried orange peel using ultrasonic wave auxiliary law, which is characterized in that include the following steps：
1) dried orange peel of drying is crushed, it is spare；
2) in dried orange peel after being pulverized, after adding in the infiltration of organic solution extractant, using ultrasonic wave extraction；
3) it filters, centrifuge filtrate, it is dried orange peel flavone extractive to take supernatant liquor.
2. according to the method described in claim 1, it is characterized in that, in step 2), the organic solution extractant is anhydrous second
Alcohol or 1,2- propylene glycol；In step 2), the solid-liquid ratio of dried orange peel and organic solution extractant is 0.02-0.4g:20mL.
3. according to the method described in claim 1, it is characterized in that, in step 2), the condition control of ultrasonic wave extraction is：Extraction
Temperature is 28-35 DEG C, extraction time 20-120min；In step 3), the condition control of centrifugation is：Centrifugal rotational speed is 2000-
6000r/min, centrifugation time 5-30min.
4. according to the method described in claim 1, it is characterized in that, in step 3), the UVC of dried orange peel flavone extractive is 0.019-
0.325th, UVB is 0.097-0.391 and UVA is 0.044-0.913.
5. application of the dried orange peel flavones in cosmetics, is characterized in that, the dried orange peel flavones makes an addition to cosmetics as sun-prevention component
In.
6. application according to claim 5, is characterized in that, the dosage form of the cosmetics is solution, gel, lotion or cream
Shape.
7. a kind of facial mask liquid, which is characterized in that by the percent by weight of raw material, the facial mask liquid includes the right of 10-20%
It is required that the dried orange peel flavone extractive described in 1.
8. a kind of anti-aging whitening emulsion, which is characterized in that include the component of following weight percent：It is described in claim 1
Dried orange peel flavone extractive 20-30%, plants essential oil 8-15%, Hydrolyzed Collagen 3-5%, surplus is deionized water.
9. a kind of Essence, which is characterized in that include the component of following weight percent：Trehalose 3-8%, preservative 0.2-
0.8%, surplus is dried orange peel flavone extractive described in claim 1.
10. a kind of lotion, which is characterized in that include the component of following weight percent：18-25% panthenols 5.0,1-5% water
Collagen is solved, 20-40% dried orange peel flavone extractives described in claim 1,0.2-0.8% preservatives, surplus is deionization
Water.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109077961A (en) * | 2018-09-17 | 2018-12-25 | 广州市藻谷生物科技有限公司 | A kind of sunscreen and preparation method thereof with antibacterial effect |
| CN109363981A (en) * | 2018-09-30 | 2019-02-22 | 江门职业技术学院 | A kind of plant amino acid shampoo |
| CN109370785A (en) * | 2018-09-30 | 2019-02-22 | 江门职业技术学院 | A kind of amino acid soap and preparation method thereof containing dried orange peel extracts |
| CN110251427A (en) * | 2019-06-10 | 2019-09-20 | 江门职业技术学院 | A kind of plant multiple-effect composition and its application |
| WO2020073368A1 (en) * | 2018-10-10 | 2020-04-16 | 温伟成 | Formulation and process for preparing body wash employing xinhui tangerine peels and blossom extract |
| CN115651090A (en) * | 2022-10-31 | 2023-01-31 | 五邑大学 | Preparation method and application of polysaccharide extract of pericarpium citri reticulatae enriched with lactobacillus |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109077961A (en) * | 2018-09-17 | 2018-12-25 | 广州市藻谷生物科技有限公司 | A kind of sunscreen and preparation method thereof with antibacterial effect |
| CN109363981A (en) * | 2018-09-30 | 2019-02-22 | 江门职业技术学院 | A kind of plant amino acid shampoo |
| CN109370785A (en) * | 2018-09-30 | 2019-02-22 | 江门职业技术学院 | A kind of amino acid soap and preparation method thereof containing dried orange peel extracts |
| CN109370785B (en) * | 2018-09-30 | 2021-02-05 | 江门职业技术学院 | Amino acid soap containing dried orange peel extract and preparation method thereof |
| WO2020073368A1 (en) * | 2018-10-10 | 2020-04-16 | 温伟成 | Formulation and process for preparing body wash employing xinhui tangerine peels and blossom extract |
| CN110251427A (en) * | 2019-06-10 | 2019-09-20 | 江门职业技术学院 | A kind of plant multiple-effect composition and its application |
| CN115651090A (en) * | 2022-10-31 | 2023-01-31 | 五邑大学 | Preparation method and application of polysaccharide extract of pericarpium citri reticulatae enriched with lactobacillus |
| CN115651090B (en) * | 2022-10-31 | 2024-04-26 | 广东新宝堂制药有限公司 | Preparation method and application of wide orange peel polysaccharide extract enriched with lactobacillus |
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