CN109355946A - 一种涤棉面料黑色染色用固色剂的制备方法 - Google Patents

一种涤棉面料黑色染色用固色剂的制备方法 Download PDF

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CN109355946A
CN109355946A CN201811075265.2A CN201811075265A CN109355946A CN 109355946 A CN109355946 A CN 109355946A CN 201811075265 A CN201811075265 A CN 201811075265A CN 109355946 A CN109355946 A CN 109355946A
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polyester
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盛婷婷
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Tongxiang Puyuan Woolen Knitting Technology Service Center
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    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
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Abstract

本发明涉及染色助剂技术领域，尤其是一种涤棉面料黑色染色用固色剂的制备方法，配制如下组分：聚氧乙烯二胺、环氧氯丙烷、三乙醇胺、过硫酸铵、1,5‑二羟基萘、酚醛树脂、浓硫酸、冰醋酸、25％氨水、乙二醇单丁醚、去离子水；将上述各组分放置在密闭容器内，在密闭容器内加压至1.5个大气压，然后升温至35‑45℃，搅拌并保温25‑30min，出料即可。本发明所得到的一种涤棉面料黑色染色用固色剂的制备方法，其得到的固色剂能有效提升涤棉面料的固色性能，尤其是黑色染色过程中，能确保面料不褪色等。

Description

一种涤棉面料黑色染色用固色剂的制备方法
技术领域
本发明涉及染色助剂技术领域，尤其是一种涤棉面料黑色染色用固色剂的制备方法。
背景技术
现有技术中，固色剂都是通用产品，在固色剂使用过程中对于不同面料而言其效果是不同的。尤其是对于涤棉混纺面料黑色染色过程中其固色性能相对较差，严重影响产品的染色性能。
发明内容
本发明的目的是为了解决上述技术的不足而提供一种能有效的提升固色性能的涤棉面料黑色染色用固色剂的制备方法。
为了达到上述目的，本发明所设计的一种涤棉面料黑色染色用固色剂的制备方法，配制如下组分：聚氧乙烯二胺、环氧氯丙烷、三乙醇胺、过硫酸铵、1,5-二羟基萘、酚醛树脂、浓硫酸、冰醋酸、25％氨水、乙二醇单丁醚、去离子水，其中各组分的质量份数为：聚氧乙烯二胺10-20份、环氧氯丙烷5-15份、三乙醇胺8-10份、过硫酸铵2-10份、1,5-二羟基萘3-6份、酚醛树脂3-5份、浓硫酸0.3-1份、冰醋酸2-4份、25％氨水2-5份、乙二醇单丁醚3-6份、去离子水260-300份；将上述各组分放置在密闭容器内，在密闭容器内加压至1.5个大气压，然后升温至35-45℃，搅拌并保温25-30min，出料即可。
作为优选，上述各组分的质量份数为：聚氧乙烯二胺15份、环氧氯丙烷12份、三乙醇胺9份、过硫酸铵8份、1,5-二羟基萘5份、酚醛树脂4份、浓硫酸0.8份、冰醋酸3份、25％氨水4份、乙二醇单丁醚5份、去离子水280份。
本发明所得到的一种涤棉面料黑色染色用固色剂的制备方法，其得到的固色剂能有效提升涤棉面料的固色性能，尤其是黑色染色过程中，能确保面料不褪色等。
具体实施方式
下面通过实施例对本发明作进一步的描述。
实施例1：
本实施例描述的一种涤棉面料黑色染色用固色剂的制备方法，配制如下组分：聚氧乙烯二胺、环氧氯丙烷、三乙醇胺、过硫酸铵、1,5-二羟基萘、酚醛树脂、浓硫酸、冰醋酸、25％氨水、乙二醇单丁醚、去离子水，其中各组分的质量份数为：聚氧乙烯二胺10-20份、环氧氯丙烷15份、三乙醇胺10份、过硫酸铵10份、1,5-二羟基萘6份、酚醛树脂5份、浓硫酸1份、冰醋酸4份、25％氨水5份、乙二醇单丁醚6份、去离子水300份；将上述各组分放置在密闭容器内，在密闭容器内加压至1.5个大气压，然后升温至35℃，搅拌并保温30min，出料即可。
实施例2：
本实施例描述的一种涤棉面料黑色染色用固色剂的制备方法，配制如下组分：聚氧乙烯二胺、环氧氯丙烷、三乙醇胺、过硫酸铵、1,5-二羟基萘、酚醛树脂、浓硫酸、冰醋酸、25％氨水、乙二醇单丁醚、去离子水，其中各组分的质量份数为：聚氧乙烯二胺10份、环氧氯丙烷5份、三乙醇胺8份、过硫酸铵2份、1,5-二羟基萘3份、酚醛树脂3份、浓硫酸0.3份、冰醋酸2份、25％氨水2份、乙二醇单丁醚3份、去离子水260份；将上述各组分放置在密闭容器内，在密闭容器内加压至1.5个大气压，然后升温至45℃，搅拌并保温25min，出料即可。
实施例3：
本实施例描述的一种涤棉面料黑色染色用固色剂的制备方法，配制如下组分：聚氧乙烯二胺、环氧氯丙烷、三乙醇胺、过硫酸铵、1,5-二羟基萘、酚醛树脂、浓硫酸、冰醋酸、25％氨水、乙二醇单丁醚、去离子水，其中各组分的质量份数为：聚氧乙烯二胺15份、环氧氯丙烷12份、三乙醇胺9份、过硫酸铵8份、1,5-二羟基萘5份、酚醛树脂4份、浓硫酸0.8份、冰醋酸3份、25％氨水4份、乙二醇单丁醚5份、去离子水280份；将上述各组分放置在密闭容器内，在密闭容器内加压至1.5个大气压，然后升温至40℃，搅拌并保温28min，出料即可。

Claims (2)

1.一种涤棉面料黑色染色用固色剂的制备方法，其特征是：配制如下组分：聚氧乙烯二胺、环氧氯丙烷、三乙醇胺、过硫酸铵、1,5-二羟基萘、酚醛树脂、浓硫酸、冰醋酸、25％氨水、乙二醇单丁醚、去离子水，其中各组分的质量份数为：聚氧乙烯二胺10-20份、环氧氯丙烷5-15份、三乙醇胺8-10份、过硫酸铵2-10份、1,5-二羟基萘3-6份、酚醛树脂3-5份、浓硫酸0.3-1份、冰醋酸2-4份、25％氨水2-5份、乙二醇单丁醚3-6份、去离子水260-300份；将上述各组分放置在密闭容器内，在密闭容器内加压至1.5个大气压，然后升温至35-45℃，搅拌并保温25-30min，出料即可。
2.根据权利要求1所述的一种涤棉面料黑色染色用固色剂的制备方法，其特征是：上述各组分的质量份数为：聚氧乙烯二胺15份、环氧氯丙烷12份、三乙醇胺9份、过硫酸铵8份、1,5-二羟基萘5份、酚醛树脂4份、浓硫酸0.8份、冰醋酸3份、25％氨水4份、乙二醇单丁醚5份、去离子水280份。
CN201811075265.2A 2018-09-14 2018-09-14 一种涤棉面料黑色染色用固色剂的制备方法 Pending CN109355946A (zh)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105332298A (zh) * 2015-12-10 2016-02-17 陈逸君 一种用于活性染料染色的固色剂
CN105386337A (zh) * 2015-12-14 2016-03-09 唐晓琦 一种改性粘胶纤维的酸性染料染色方法
CN105463889A (zh) * 2015-12-10 2016-04-06 陈逸君 一种用于活性染料染色的固色剂的制备方法
CN106917308A (zh) * 2017-04-10 2017-07-04 南通大学 一种涤棉混纺面料同浴染色专用固色剂
CN107100018A (zh) * 2017-04-28 2017-08-29 晋江市南星印染材料有限公司 一种酸性染料染色用固色剂及其制备方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105332298A (zh) * 2015-12-10 2016-02-17 陈逸君 一种用于活性染料染色的固色剂
CN105463889A (zh) * 2015-12-10 2016-04-06 陈逸君 一种用于活性染料染色的固色剂的制备方法
CN105386337A (zh) * 2015-12-14 2016-03-09 唐晓琦 一种改性粘胶纤维的酸性染料染色方法
CN106917308A (zh) * 2017-04-10 2017-07-04 南通大学 一种涤棉混纺面料同浴染色专用固色剂
CN107100018A (zh) * 2017-04-28 2017-08-29 晋江市南星印染材料有限公司 一种酸性染料染色用固色剂及其制备方法

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