CN109319815A - 一种纳米碳酸钙的制备方法 - Google Patents
一种纳米碳酸钙的制备方法 Download PDFInfo
- Publication number
- CN109319815A CN109319815A CN201811290679.7A CN201811290679A CN109319815A CN 109319815 A CN109319815 A CN 109319815A CN 201811290679 A CN201811290679 A CN 201811290679A CN 109319815 A CN109319815 A CN 109319815A
- Authority
- CN
- China
- Prior art keywords
- calcium
- calcium carbonate
- temperature
- preparation
- nanometer
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims abstract description 107
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims abstract description 54
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 238000006243 chemical reaction Methods 0.000 claims abstract description 41
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 36
- 238000005273 aeration Methods 0.000 claims abstract description 32
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 30
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 24
- 125000004122 cyclic group Chemical group 0.000 claims abstract description 22
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 21
- 239000011575 calcium Substances 0.000 claims abstract description 21
- 238000001914 filtration Methods 0.000 claims abstract description 19
- 239000012141 concentrate Substances 0.000 claims abstract description 18
- 238000004090 dissolution Methods 0.000 claims abstract description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 15
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 claims abstract description 15
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 15
- 229960000935 dehydrated alcohol Drugs 0.000 claims abstract description 15
- 239000001863 hydroxypropyl cellulose Substances 0.000 claims abstract description 15
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 159000000007 calcium salts Chemical class 0.000 claims abstract description 13
- 238000001704 evaporation Methods 0.000 claims abstract description 13
- 230000008020 evaporation Effects 0.000 claims abstract description 13
- 239000000725 suspension Substances 0.000 claims abstract description 13
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 11
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 11
- 238000010438 heat treatment Methods 0.000 claims abstract description 11
- 239000002244 precipitate Substances 0.000 claims abstract description 10
- 239000012153 distilled water Substances 0.000 claims abstract description 8
- 238000002604 ultrasonography Methods 0.000 claims abstract description 8
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 claims description 20
- 229910001424 calcium ion Inorganic materials 0.000 claims description 20
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 6
- 239000001110 calcium chloride Substances 0.000 claims description 6
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 6
- 229920002678 cellulose Polymers 0.000 claims description 2
- 239000001913 cellulose Substances 0.000 claims description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 2
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 2
- 229910002090 carbon oxide Inorganic materials 0.000 claims 1
- 238000005286 illumination Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000002207 thermal evaporation Methods 0.000 claims 1
- 239000000920 calcium hydroxide Substances 0.000 abstract description 14
- 229910001861 calcium hydroxide Inorganic materials 0.000 abstract description 14
- 238000001035 drying Methods 0.000 abstract description 12
- 230000009466 transformation Effects 0.000 abstract description 6
- 238000002425 crystallisation Methods 0.000 abstract description 5
- 230000008025 crystallization Effects 0.000 abstract description 5
- 239000002245 particle Substances 0.000 abstract description 4
- 238000000034 method Methods 0.000 description 10
- 239000007789 gas Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- 239000004033 plastic Substances 0.000 description 6
- 229920003023 plastic Polymers 0.000 description 6
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 239000000908 ammonium hydroxide Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000009514 concussion Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 239000013078 crystal Chemical group 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 230000005476 size effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
- -1 uses charring Chemical compound 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
- C01F11/182—Preparation of calcium carbonate by carbonation of aqueous solutions and characterised by an additive other than CaCO3-seeds
- C01F11/183—Preparation of calcium carbonate by carbonation of aqueous solutions and characterised by an additive other than CaCO3-seeds the additive being an organic compound
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
- C01F11/181—Preparation of calcium carbonate by carbonation of aqueous solutions and characterised by control of the carbonation conditions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Composite Materials (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Description
实施例1 | 实施例2 | 实施例3 | 对比例 | |
粒径 | 50nm | 25nm | 30nm | 90nm |
分布率 | 97% | 98% | 97% | 65% |
Claims (9)
Priority Applications (1)
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CN201811290679.7A CN109319815B (zh) | 2018-10-31 | 2018-10-31 | 一种纳米碳酸钙的制备方法 |
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CN201811290679.7A CN109319815B (zh) | 2018-10-31 | 2018-10-31 | 一种纳米碳酸钙的制备方法 |
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CN109319815A true CN109319815A (zh) | 2019-02-12 |
CN109319815B CN109319815B (zh) | 2020-11-20 |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110183873A (zh) * | 2019-06-14 | 2019-08-30 | 北京工商大学 | 一种基于碳酸钙的食用色淀的制备方法 |
CN112266005A (zh) * | 2020-11-10 | 2021-01-26 | 吴亚良 | 一种纳米碳酸钙的制备方法 |
CN112408447A (zh) * | 2020-11-10 | 2021-02-26 | 吴亚良 | 一种高纯度纳米碳酸钙的制备方法 |
CN112456532A (zh) * | 2020-12-08 | 2021-03-09 | 理光感热技术(无锡)有限公司 | 一种碳酸钙的制备方法 |
CN115448346A (zh) * | 2022-08-11 | 2022-12-09 | 中南大学 | 一种超细轻质碳酸钙的制备方法 |
Citations (6)
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WO2009081548A1 (ja) * | 2007-12-25 | 2009-07-02 | Nihon University | ナノサイズ炭酸カルシウムの製造法 |
PL212968B1 (pl) * | 2009-08-20 | 2012-12-31 | Inst Chemii Fizycznej Polskiej Akademii Nauk | Sposób wytwarzania nanocząsteczkowego, monodyspersyjnego węglanu wapnia |
CN103232051A (zh) * | 2013-04-24 | 2013-08-07 | 陕西科技大学 | 一种超细多孔碳酸钙微球的制备方法 |
PL420003A1 (pl) * | 2016-12-29 | 2018-07-02 | Wkg Spółka Z Ograniczoną Odpowiedzialnością Spółka Komandytowa | Sposób wytwarzania nanocząsteczkowego węglanu wapnia oraz układ do wytwarzania nanocząsteczkowego węglanu wapnia |
CN108291096A (zh) * | 2015-12-01 | 2018-07-17 | 欧米亚国际集团 | 用于生产包含经表面反应的碳酸钙的粒料的方法 |
CN108586969A (zh) * | 2017-12-26 | 2018-09-28 | 新疆兵团现代绿色氯碱化工工程研究中心(有限公司) | 一种聚氯乙烯/纳米碳酸钙复合树脂的悬浮聚合方法 |
-
2018
- 2018-10-31 CN CN201811290679.7A patent/CN109319815B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2009081548A1 (ja) * | 2007-12-25 | 2009-07-02 | Nihon University | ナノサイズ炭酸カルシウムの製造法 |
PL212968B1 (pl) * | 2009-08-20 | 2012-12-31 | Inst Chemii Fizycznej Polskiej Akademii Nauk | Sposób wytwarzania nanocząsteczkowego, monodyspersyjnego węglanu wapnia |
CN103232051A (zh) * | 2013-04-24 | 2013-08-07 | 陕西科技大学 | 一种超细多孔碳酸钙微球的制备方法 |
CN108291096A (zh) * | 2015-12-01 | 2018-07-17 | 欧米亚国际集团 | 用于生产包含经表面反应的碳酸钙的粒料的方法 |
PL420003A1 (pl) * | 2016-12-29 | 2018-07-02 | Wkg Spółka Z Ograniczoną Odpowiedzialnością Spółka Komandytowa | Sposób wytwarzania nanocząsteczkowego węglanu wapnia oraz układ do wytwarzania nanocząsteczkowego węglanu wapnia |
CN108586969A (zh) * | 2017-12-26 | 2018-09-28 | 新疆兵团现代绿色氯碱化工工程研究中心(有限公司) | 一种聚氯乙烯/纳米碳酸钙复合树脂的悬浮聚合方法 |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110183873A (zh) * | 2019-06-14 | 2019-08-30 | 北京工商大学 | 一种基于碳酸钙的食用色淀的制备方法 |
WO2020249092A1 (zh) * | 2019-06-14 | 2020-12-17 | 北京工商大学 | 一种基于碳酸钙的食用色淀的制备方法 |
CN112266005A (zh) * | 2020-11-10 | 2021-01-26 | 吴亚良 | 一种纳米碳酸钙的制备方法 |
CN112408447A (zh) * | 2020-11-10 | 2021-02-26 | 吴亚良 | 一种高纯度纳米碳酸钙的制备方法 |
CN112408447B (zh) * | 2020-11-10 | 2023-08-08 | 邯郸市裕耀建材科技有限公司 | 一种高纯度纳米碳酸钙的制备方法 |
CN112456532A (zh) * | 2020-12-08 | 2021-03-09 | 理光感热技术(无锡)有限公司 | 一种碳酸钙的制备方法 |
CN112456532B (zh) * | 2020-12-08 | 2023-10-24 | 理光感热技术(无锡)有限公司 | 一种碳酸钙的制备方法 |
CN115448346A (zh) * | 2022-08-11 | 2022-12-09 | 中南大学 | 一种超细轻质碳酸钙的制备方法 |
CN115448346B (zh) * | 2022-08-11 | 2024-03-12 | 中南大学 | 一种超细轻质碳酸钙的制备方法 |
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