CN109223632A - A kind of eye essence oil and preparation method thereof - Google Patents

A kind of eye essence oil and preparation method thereof Download PDF

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Publication number
CN109223632A
CN109223632A CN201810996871.1A CN201810996871A CN109223632A CN 109223632 A CN109223632 A CN 109223632A CN 201810996871 A CN201810996871 A CN 201810996871A CN 109223632 A CN109223632 A CN 109223632A
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phase
extract
seed
eye
oil
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宿果英
贾中华
董银卯
孟宏
何凡
何一凡
郑立波
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Huayantang (beijing) Biotechnology Co Ltd
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Huayantang (beijing) Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/342Alcohols having more than seven atoms in an unbroken chain
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/347Phenols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/496Triazoles or their condensed derivatives, e.g. benzotriazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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Abstract

The invention discloses a kind of eye essence oil and preparation method thereof.The eye essence oil includes following component: A phase, including the pure and mild isooctadecanol isostearate of pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamate), campesterol class/cetearyl alcohol;B phase, including bisabolol, phytosterol/octyl dodecanol lauroyl glutamate ester, tocopherol acetate, Ascorbyl Tetraisopalmitate, conditioner, functional additive, ring five dimethyl silicone polymer/cyclohexasiloxane and benzotriazole base dodecyl p- cresols;C phase, including essence;D phase, including caprylic/capric triglyceride.Eye essence oil of the invention includes plurality of active ingredients, good absorbing, not president's fat granule after, and moisturizing and anti-wrinkle effect are good, can significantly improve black eye and eye is swollen, also have preferable improvement to periocualr skin elasticity.The preparation method simple process of eye essence oil of the present invention, easily operated, Product Safety is good.

Description

A kind of eye essence oil and preparation method thereof
Technical field
The present invention relates to the applications of a kind of eye essence oil and preparation method thereof and eye essence oil, belong to makeup Product technical field.
Background technique
Eye skin is position the weakest in human skin, and the thickness summation of eye epidermis and corium is about 0.55mm, the only one third of face skin thickness to 1/5th, eye is subcutaneously almost without the distribution of sebaceous glands sweat gland, Yan The thin thin skin skin in state is very easy to drying, because moistening ability almost without automatic, the grease that can be supplied is considerably less, contained Collagen, elastin are less.
Also very frequently, under normal circumstances, people will blink 15 times or more per minute, that is to say, that people for the activity of eye skin Blink is more than 10,000 times daily.Further, since external factor etc. influences, for example, ultraviolet light and computer radiation, bad life habits, It pollutes and in makeup due to pullling the movement such as eyelid, so that eye skin is very easy to grow wrinkle, black eye and eye pouch And one grows and is difficult to disappear.
The formation of eye pouch, black eye and eyeprint is a kind of chain reaction, due to the growth at age, the epidermis group of eye part skin Knit drying it is thinning, collagen and elastin laminin are gradually lost, the dusting cover for having collagen and elastomer to be interwoven originally Reticular structure receives destruction, just will appear the different wrinkle of thickness;Eye sluggish metabolism, poor blood circulation, blood capillary Blockage causes inflammatory reaction and pigmentation, forms black eye;The further aging of eye skin, it is certain when being aged to Degree, just the fat of support incessantly siltation, causes eye skin plumpness prominent, eye pouch there have been.
Currently, eye product on the market is many kinds of, but in the presence of absorbing, bad, effect is unobvious, easy long fat mostly The problems such as grain and allergy.Therefore, it is badly in need of developing the good eye product of the new good absorbing of one kind, effect.
Summary of the invention
It is an object of the invention to according to problem of the existing technology, provide a kind of eye essence oil and its preparation side Method.Eye essence oil of the invention includes plurality of active ingredients, good absorbing, not president's fat granule, and moisturizing and anti-wrinkle after Effect is good, can significantly improve black eye and eye is swollen, also have preferable improvement to periocualr skin elasticity.Eye essence of the present invention The preparation method simple process of oil, easily operated, Product Safety is good.
According to an aspect of the invention, there is provided a kind of eye essence oil, including following component:
A phase, including pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamate), campesterol class/cetearyl alcohol are pure and mild Isooctadecanol isostearate;
B phase, including it is bisabolol, phytosterol/octyl dodecanol lauroyl glutamate ester, tocopherol acetate, anti-bad The different palmitate of hematic acid four, conditioner, functional additive, ring five dimethyl silicone polymer/cyclohexasiloxane and benzotriazole Base dodecyl p- cresols;
C phase, including essence;
D phase, including caprylic/capric triglyceride.
It according to some embodiments of the present invention, is the mass content of each phase component in terms of 100% by the quality of essential oils Are as follows: A phase 10.00-34.00%, B phase 2.00-65.00%, C phase 0.008-0.45%, surplus are D phase.
Preferred embodiment in accordance with the present invention is the mass content of each phase component in terms of 100% by the quality of essential oils Are as follows: A phase 11.00-32.00%, B phase 30.00-62.00%, C phase 0.01-0.40%, surplus are D phase.
It according to certain embodiments of the present invention, is the matter of each component in the A phase in terms of 100% by the quality of essential oils Measure content are as follows: pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamate) 0.005-2%, campesterol class/cetostearyl alcohol 0.05-2%, isooctadecanol isostearate 8-34%.
It according to the preferred embodiment of the present invention, is the matter of each component in the A phase in terms of 100% by the quality of essential oils Measure content are as follows: pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamate) 0.01-1%, campesterol class/cetostearyl alcohol 0.1-1%, isooctadecanol isostearate 10-32%.
It according to certain embodiments of the present invention, is the matter of each component in the B phase in terms of 100% by the quality of essential oils Measure content are as follows: bisabolol 0.05-2%, phytosterol/octyl dodecanol lauroyl glutamate ester 0.05-6%, tocopherol second Acid esters 0.1-8%, Ascorbyl Tetraisopalmitate 0.05-3%, conditioner 0.3-22%, functional additive 0.5- 22%, ring five dimethyl silicone polymer/cyclohexasiloxane 0.5-40%, benzotriazole base dodecyl p- cresols 0.01-2%.
It according to the preferred embodiment of the present invention, is the matter of each component in the B phase in terms of 100% by the quality of essential oils Measure content are as follows: bisabolol 0.01-1%, phytosterol/octyl dodecanol lauroyl glutamate ester 0.1-5%, tocopheryl acetate Ester 0.2-5%, Ascorbyl Tetraisopalmitate 0.1-1.5%, conditioner 0.5-20%, functional additive 1-20%, ring Five dimethyl silicone polymers/cyclohexasiloxane 1-40%, benzotriazole base dodecyl p- cresols 0.01-1%.
According to one embodiment of present invention, the conditioner include caprylic/capric triglyceride, it is sunflower seed oil, male Red seed oil, grape seed oil, Purple Perilla Seed Oil, isooctadecanol isostearate, tocopherol acetate, the different palmitinic acid of ascorbic acid four Ester, retinyl palmitate and Butylated Hydroxytoluene.
It is the quality of each component in the conditioner in terms of 100% by the quality of essential oils in some specific embodiments Content are as follows: caprylic/capric triglyceride 0.1447-5.788%, sunflower seed oil 0.1-4%, peony seed oil 0.1-4%, grape Seed oil 0.05-2%, Purple Perilla Seed Oil 0.05-2%, isooctadecanol isostearate 0.025-1%, tocopherol acetate 0.025- 1%, Ascorbyl Tetraisopalmitate 0.005-0.2%, retinyl palmitate 0.00005-0.002%, Butylated Hydroxytoluene 0.00025-0.01%.
Preferred embodiment in accordance with the present invention, the functional additive include caprylic/capric triglyceride, hydrogenation gather it is different Butylene, peony extract, purple common perilla seed, extractive of flax seed, buckwheat seed extract, fructus lycii berry extract, lotus seed extract Object, silybum marianum seed extract, licorice root extract and Butylated Hydroxytoluene.
It is each component in the energy property additive in terms of 100% by the quality of essential oils in some specific embodiments Mass content are as follows: caprylic/capric triglyceride 0.6995-13.99%, Parleam 0.05-1%, peony extract 0.05-1%, purple common perilla seed 0.03-0.6%, extractive of flax seed 0.03-0.6%, buckwheat seed extract 0.03- 0.6%, fructus lycii berry extract 0.02-0.4%, lotus seed extract 0.02-0.4%, silybum marianum seed extract 0.02-0.4%, Licorice root extract 0.05-1%, Butylated Hydroxytoluene 0.0005-0.01%.
According to another aspect of the present invention, a kind of preparation method of above-mentioned eye essence oil is provided, comprising:
1) raw material of A phase and D phase component is mixed, is warming up to 85-95 DEG C;
2) cooling processing is carried out to the material that step 1) obtains, when being cooled to 60 DEG C or less, the B being pre-mixed is added Phase component raw material, mixing;
3) cooling processing is carried out to the material that step 2) obtains, when being cooled to 40 DEG C or less, C phase component raw material is added, Mixing;
4) cooling processing is carried out to the material that step 3) obtains, when being cooled to 38 DEG C or less, filtering, discharging to get.
According to some embodiments of the present invention, the step 2) includes:
2A) by bisabolol, phytosterol/octyl dodecanol lauroyl glutamate ester, tocopherol acetate, ascorbic acid Four different palmitates, conditioner, functional additive, ring five dimethyl silicone polymer/cyclohexasiloxane and benzotriazole base ten The mixing of dialkyl group p- cresols, the B phase component raw material mixed;
Cooling processing 2B) is carried out to the material that step 1) obtains, when being cooled to 60 DEG C or less, what addition had been pre-mixed B phase component raw material, mixing.
Some preferred embodiments according to the present invention, the step 2A) include:
2A1) by caprylic/capric triglyceride, sunflower seed oil, peony seed oil, grape seed oil, Purple Perilla Seed Oil, different tristearin Alcohol isostearate, tocopherol acetate, Ascorbyl Tetraisopalmitate, retinyl palmitate and Butylated Hydroxytoluene mixing, Obtain conditioner;
2A2) caprylic/capric triglyceride, Parleam, peony extract, purple common perilla seed, linseed are mentioned Take object, buckwheat seed extract, fructus lycii berry extract, lotus seed extract, silybum marianum seed extract, licorice root extract and fourth hydroxyl first Benzene mixing, obtains functional additive;
2A3) by bisabolol, phytosterol/octyl dodecanol lauroyl glutamate ester, tocopherol acetate, Vitamin C Sour four different palmitates, step 2A1) obtained conditioner, step 2A2) obtained functional additive, five poly dimethyl silicon of ring Oxygen alkane/cyclohexasiloxane and the mixing of benzotriazole base dodecyl p- cresols, the B phase component raw material mixed.
According to another aspect of the present invention, above-mentioned essential oils are additionally provided in detumescence, improvement black eye, anti-wrinkle, moisturizing Or the application in moisturizing field.
Essential oils of the invention have stronger free radical scavenging ability, can remove the free radical of skin in time, inhibit oxygen Change;It is remarkably improved the moisture content of skin after use, there is preferable moisturizing and moisturizing ability;Skin bullet can be effectively improved Property, and there is the preferable ability for improving skin roughness and wrinkle;And melanin content can be effectively reduced, can effectively it change Kind black eye.It is highly suitable as daily eye skin-protection product.
Specific embodiment
Combined with specific embodiments below, the present invention is described in further details:
Embodiment 1-3
1) it stocks up according to parts by weight shown in table 1;
2) by caprylic/capric triglyceride, sunflower seed oil, peony seed oil, grape seed oil, Purple Perilla Seed Oil, isooctadecanol Isostearate, tocopherol acetate, Ascorbyl Tetraisopalmitate, retinyl palmitate and Butylated Hydroxytoluene mixing are equal It is even, obtain conditioner;
3) caprylic/capric triglyceride, Parleam, peony extract, purple common perilla seed, linseed are extracted Object, buckwheat seed extract, lycium barbarum berry extract, lotus seed extract, silybum marianum seed extract, licorice root extract and fourth hydroxyl Toluene is uniformly mixed, and obtains functional additive;
4) by bisabolol, phytosterol/octyl dodecanol lauroyl glutamate ester, tocopherol acetate, ascorbic acid Functional additive that conditioner that four different palmitates, step 2) obtain, step 3) obtain, ring five dimethyl silicone polymer/ Cyclohexasiloxane and the mixing of benzotriazole base dodecyl p- cresols, the B phase component raw material mixed;
5) cooling processing is carried out to the material that step 1) obtains, when being cooled to 60 DEG C or less, the B being pre-mixed is added Phase component raw material, is uniformly mixed;
6) cooling processing is carried out to the material that step 5) obtains, when being cooled to 40 DEG C or less, C phase component raw material is added, It is uniformly mixed;
4) cooling processing is carried out to the material that step 6) obtains, when being cooled to 38 DEG C or less, using the strainer pair of 400 mesh Material is filtered processing, and filtrate is essence oil product.
The experimental data of each embodiment sees table 1.
Comparative example 1-2
In addition to the dosage of each raw material is different, remaining is shown in Table 1 with embodiment 1, the experimental data of each comparative example.
Comparative example 3
Other than being added without peony extract in B phase, remaining is the same as embodiment 2.
Comparative example 4
Other than being added without extractive of perilla in B phase, remaining is the same as embodiment 2.
Comparative example 5
Other than being added without extractive of flax seed in B phase, remaining is the same as embodiment 2.
Comparative example 6
Other than being added without buckwheat seed extract in B phase, remaining is the same as embodiment 2.
Comparative example 7
Other than being added without lycium barbarum berry extract in B phase, remaining is the same as embodiment 2.
Comparative example 8
Other than being added without lotus seed extract in B phase, remaining is the same as embodiment 2.
Comparative example 9
Other than being added without silybum marianum seed extract in B phase, remaining is the same as embodiment 2.
Comparative example 10
Other than being added without licorice root extract in B phase, remaining is the same as embodiment 2.
Comparative example 11
1) it stocks up according to parts by weight shown in table 1;
2) B phase component raw material is added to together in container and is uniformly mixed, the B phase component raw material mixed;
3) cooling processing is carried out to the material that step 1) obtains, when being cooled to 60 DEG C or less, the B being pre-mixed is added Phase component raw material, is uniformly mixed;
4) cooling processing is carried out to the material that step 3) obtains, when being cooled to 40 DEG C or less, C phase component raw material is added, It is uniformly mixed;
5) cooling processing is carried out to the material that step 4) obtains, when being cooled to 38 DEG C or less, using the strainer pair of 400 mesh Material is filtered processing, and filtrate is essence oil product of the invention.
Table 1
Free radical scavenging activity measurement is carried out to essence oil product as follows:
Aging is a complicated process, and wherein free radical theory is exactly generally acknowledged one of anti-aging theory.And it removes ABTS free radical is a kind of usual manner for analyzing antioxidant.Indicate that tested material removes the energy of free radical with clearance rate in test Power, clearance rate are bigger, then it represents that its oxidation resistance is stronger.
Specific test method:
It takes 0.0192gABTS that 5.00mL deionized water dissolving is added, mixes, be prepared into 7mmolL-1ABTS stock solution. 0.1892g potassium peroxydisulfate is weighed, 5.000mL deionized water dissolving is added, mixes, is prepared into 140mmolL-1Stock solution.It will A certain amount of 7mmolL-1ABTS and 140mmolL-1Potassium peroxydisulfate mixing, be protected from light lower standings for a period of time in room temperature Afterwards, ABTS free radical stock solution is formed.A certain amount of ABTS free radical stock solution is taken, is diluted with 50% ethyl alcohol, makes final test Negative control light absorption value is 0.70 ± 0.02.
The tested embodiment 1-3 and comparative example 1-11 essence oil product prepared is configured to 50% ethanol solution 1.0% test fluid.Test fluid, ABTS free radical stock solution are sequentially added, is vortexed and mixes, be placed in microplate reader and be protected from light incubation, At interval of 20min, its light absorption value is measured at wavelength 734nm with microplate reader.ABTS free radical scavenging activity is calculated by formula (1).
In formula (1): A is OD value after test fluid is mixed with ABTS solution, and B is OD after 50% ethyl alcohol is mixed with ABTS solution Value, C are OD value after 50% ethyl alcohol is mixed with sample solution.
The free radical scavenging activity of the essence oil product of embodiment 1-3 and comparative example 1-11 preparation the results are shown in Table 2.
Normal individual trial evaluation experimental
It is divided into 14 at healthy women subject 140 of 30~50 one full year of life through professional's trained age before test Group, every group of 10 people.All subjects without skin or systemic disease history, and tested period do not smear it is any unrelated with experiment Drug or cosmetics.Test method is, after morning and evening face cleaning, every group takes appropriate embodiment 1-3 and comparative example 1-11 to prepare respectively Essence oil product be applied to recipient site.
(1) respectively the 0th, 4 week to subject smear essential oils position carry out moisture content detection, the 4th week to by The position that examination person smears essential oils carries out skin elasticity detection.Test site room temperature (25 ± 1) DEG C, relative humidity (40 ± 5) %, Subject starts to test after testing under environment the 30min that sits quietly.Moisture content inspection is carried out using Multi-functional skin moisture tester It surveys, skin elasticity detection is carried out using skin elasticity tester;3 data measured are made even in same test zone when test Mean value carries out t check analysis using SPSS statistical software.The water of the essence oil product of embodiment 1-3 and comparative example 1-11 preparation Point content and skin elasticity testing result are shown in Table 2.
(2) VisioScan VC98 image analyzer is used, test subject smeared the portion of essential oils respectively at the 0th, 4 week The scales of skin that peel off index of position skin, scaling of skin variational rate when being calculated the 4th week the results are shown in Table 2.
(3) black at the position of essential oils is smeared in the 0th, 4 week test subject respectively using dermal melanin tester Element value, the results are shown in Table 2.
Table 2
The essence oil product free radical scavenging activity of embodiment 1-3 is higher it can be seen from the data of table 2, it was demonstrated that the present invention Essential oils there is stronger free radical scavenging ability, can remove the free radical of skin in time, inhibit oxidation;After 4 weeks, it uses The skin moisture content of the subject of the essence oil product of embodiment 1-3 is higher, it was demonstrated that essential oils of the invention have better Moisturizing and moisturizing ability;After 4 weeks, the higher, skin using the skin elasticity value of the subject of the essence oil product of embodiment 1-3 It is elastic more preferable, it was demonstrated that essential oils of the invention can effectively improve skin elasticity;After 4 weeks, the essential oils of embodiment 1-3 are used The scaling of skin variational rate of the subject of product is smaller, illustrates that scaling of skin is less, skin is more smooth, it was demonstrated that of the invention Essential oils can make skin more smooth, have the preferable ability for improving skin roughness and wrinkle;After 4 weeks, embodiment is used The skin part melanin value variation of the subject of the essence oil product of 1-3 becomes apparent from, more effectively reduction melanin content, card Bright essential oils of the invention can be effectively improved black eye.
It should be noted that embodiment described above for explaining only the invention, is not constituted to of the invention any Limitation.By referring to exemplary embodiments, invention has been described, it should be appreciated that word used in it is descriptive With explanatory vocabulary, rather than limited vocabulary.The present invention can be made within the scope of the claims by regulation Modification, and the present invention is revised in without departing substantially from scope and spirit of the present invention.Although the present invention described in it relates to And specific method, material and embodiment, it is not intended that the present invention is limited to particular case disclosed in it, on the contrary, this hair It is bright to can be extended to other all methods and applications with the same function.

Claims (10)

1. a kind of eye essence oil, including following component:
A phase, including pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamate), campesterol class/cetearyl alcohol are pure and mild different hard Lipidol isostearate;
B phase, including bisabolol, phytosterol/octyl dodecanol lauroyl glutamate ester, tocopherol acetate, ascorbic acid Four different palmitates, conditioner, functional additive, ring five dimethyl silicone polymer/cyclohexasiloxane and benzotriazole base ten Dialkyl group p- cresols;
C phase, including essence;
D phase, including caprylic/capric triglyceride.
2. essential oils according to claim 1, which is characterized in that by the quality of essential oils be 100% in terms of, each phase group The mass content divided are as follows: A phase 10.00-34.00%, B phase 2.00-65.00%, C phase 0.008-0.45%, surplus are D phase;It is excellent Select the mass content of each phase component are as follows: A phase 11.00-32.00%, B phase 30.00-62.00%, C phase 0.01-0.40%, Surplus is D phase.
3. essential oils according to claim 1 or 2, which is characterized in that by the quality of essential oils be 100% in terms of, the A phase The mass content of middle each component are as follows: pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamate) 0.005-2%, campesterol Class/cetostearyl alcohol 0.05-2%, isooctadecanol isostearate 8-34%.
4. essential oils described in any one of -3 according to claim 1, which is characterized in that with the quality of essential oils for 100% It counts, the mass content of each component in the B phase are as follows: bisabolol 0.05-2%, phytosterol/octyl dodecanol lauroyl paddy ammonia Acid esters 0.05-6%, tocopherol acetate 0.1-8%, Ascorbyl Tetraisopalmitate 0.05-3%, conditioner 0.3-22%, Functional additive 0.5-22%, ring five dimethyl silicone polymer/cyclohexasiloxane 0.5-40%, benzotriazole base dodecyl P- cresols 0.01-2%.
5. essential oils described in any one of -4 according to claim 1, which is characterized in that the conditioner includes octanoic acid/last of the ten Heavenly stems Acid glycerol three ester, sunflower seed oil, peony seed oil, grape seed oil, Purple Perilla Seed Oil, isooctadecanol isostearate, tocopherol second Acid esters, Ascorbyl Tetraisopalmitate, retinyl palmitate and Butylated Hydroxytoluene;And/or with the quality of essential oils for 100% It counts, the mass content of each component in the conditioner are as follows: caprylic/capric triglyceride 0.1447-5.788%, sunflower seed oil 0.1-4%, peony seed oil 0.1-4%, grape seed oil 0.05-2%, Purple Perilla Seed Oil 0.05-2%, isooctadecanol isostearate 0.025-1%, tocopherol acetate 0.025-1%, Ascorbyl Tetraisopalmitate 0.005-0.2%, retinol palmitinic acid Ester 0.00005-0.002%, Butylated Hydroxytoluene 0.00025-0.01%.
6. essential oils described in any one of -5 according to claim 1, which is characterized in that the functional additive includes pungent Acid/Triglyceride DDD, Parleam, peony extract, purple common perilla seed, extractive of flax seed, buckwheat seed extract Object, fructus lycii berry extract, lotus seed extract, silybum marianum seed extract, licorice root extract and Butylated Hydroxytoluene;And/or with essence The quality of oil is 100% meter, the mass content of each component in the energy property additive are as follows: caprylic/capric triglyceride 0.6995- 13.99%, Parleam 0.05-1%, peony extract 0.05-1%, purple common perilla seed 0.03-0.6%, linseed Extract 0.03-0.6%, buckwheat seed extract 0.03-0.6%, fructus lycii berry extract 0.02-0.4%, lotus seed extract 0.02-0.4%, silybum marianum seed extract 0.02-0.4%, licorice root extract 0.05-1%, Butylated Hydroxytoluene 0.0005- 0.01%.
7. the preparation method of eye essence oil described in any one of claim 1-6, comprising:
1) raw material of A phase and D phase component is mixed, is warming up to 85-95 DEG C;
2) cooling processing is carried out to the material that step 1) obtains, when being cooled to 60 DEG C or less, the B phase group being pre-mixed is added Divide raw material, mixing;
3) cooling processing is carried out to the material that step 2) obtains, when being cooled to 40 DEG C or less, C phase component raw material, mixing is added;
4) cooling processing is carried out to the material that step 3) obtains, when being cooled to 38 DEG C or less, filtering, discharging to get.
8. preparation method according to claim 7, which is characterized in that the step 2) includes:
It is 2A) that bisabolol, phytosterol/octyl dodecanol lauroyl glutamate ester, tocopherol acetate, ascorbic acid four is different Palmitate, conditioner, functional additive, ring five dimethyl silicone polymer/cyclohexasiloxane and benzotriazole base dodecane The mixing of base p- cresols, the B phase component raw material mixed;
Cooling processing 2B) is carried out to the material that step 1) obtains, when being cooled to 60 DEG C or less, the B phase being pre-mixed is added Component raw material, mixing.
9. preparation method according to claim 7 or 8, which is characterized in that the step 2A) include:
It is 2A1) that caprylic/capric triglyceride, sunflower seed oil, peony seed oil, grape seed oil, Purple Perilla Seed Oil, isooctadecanol is different Stearate, tocopherol acetate, Ascorbyl Tetraisopalmitate, retinyl palmitate and Butylated Hydroxytoluene mixing, obtain Conditioner;
2A2) caprylic/capric triglyceride, Parleam, peony extract, purple common perilla seed, linseed are extracted Object, buckwheat seed extract, fructus lycii berry extract, lotus seed extract, silybum marianum seed extract, licorice root extract and Butylated Hydroxytoluene Mixing, obtains functional additive;
2A3) by bisabolol, phytosterol/octyl dodecanol lauroyl glutamate ester, tocopherol acetate, ascorbic acid four Different palmitate, step 2A1) obtained conditioner, step 2A2) obtained functional additive, five polydimethylsiloxanes of ring Alkane/cyclohexasiloxane and the mixing of benzotriazole base dodecyl p- cresols, the B phase component raw material mixed.
10. preparation method preparation described in any one of the oil of eye essence described in any one of claim or claim Eye essence oil in detumescence, improve black eye, anti-wrinkle, the application in moisturizing or moisturizing field.
CN201810996871.1A 2018-08-29 2018-08-29 A kind of eye essence oil and preparation method thereof Pending CN109223632A (en)

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CN110227051A (en) * 2019-05-28 2019-09-13 河南大学淮河医院 Have effects that the skin care item of whitening and moistening skin
CN110448486A (en) * 2019-08-14 2019-11-15 广州睿晞生化科技有限公司 It is a kind of to repair the impaired essential oils of sebum film
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CN110227051A (en) * 2019-05-28 2019-09-13 河南大学淮河医院 Have effects that the skin care item of whitening and moistening skin
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CN110448486A (en) * 2019-08-14 2019-11-15 广州睿晞生化科技有限公司 It is a kind of to repair the impaired essential oils of sebum film
CN110448486B (en) * 2019-08-14 2021-06-11 广州睿晞生化科技有限公司 Essential oil capable of repairing damaged sebum membrane
CN114917144A (en) * 2022-04-21 2022-08-19 蓓悠清(广东)健康科技有限公司 Night skin whitening and anti-wrinkle composition and application thereof
CN114917145A (en) * 2022-04-21 2022-08-19 蓓悠清(广东)健康科技有限公司 Whitening anti-wrinkle composition and application thereof
CN114917144B (en) * 2022-04-21 2023-08-04 蓓悠清(广东)健康科技有限公司 Night whitening and anti-wrinkle composition and application thereof
CN114917145B (en) * 2022-04-21 2024-07-09 蓓悠清(广东)健康科技有限公司 Whitening and anti-wrinkle composition and application thereof
CN115721581A (en) * 2022-11-23 2023-03-03 深圳市仙迪化妆品股份有限公司 Antioxidant composition and skin-moistening essence oil prepared from same

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