CN108969437A - A kind of dandruff control shampoo containing and preparation method thereof - Google Patents
A kind of dandruff control shampoo containing and preparation method thereof Download PDFInfo
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- CN108969437A CN108969437A CN201810961954.7A CN201810961954A CN108969437A CN 108969437 A CN108969437 A CN 108969437A CN 201810961954 A CN201810961954 A CN 201810961954A CN 108969437 A CN108969437 A CN 108969437A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/10—Antimycotics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
It the invention discloses a kind of dandruff control shampoo containing and preparation method thereof, is made of the raw material for including following parts by weight: being in terms of 1 part by the weight of plants essential oil, 3-15 part of rice, diligent 20-120 parts of the jade cactus root pocket extract of crow, 10-30 parts of ginseng extract, 10-20 parts of Folium Artemisiae Argyi extract, 1 part of plants essential oil, 1-20 parts of auxiliary agent and 100-150 parts of water.The dandruff control shampoo containing the preparation method is as follows: (1) by rice grind into powder, adds water and stirs uniformly, add ginseng extract and Folium Artemisiae Argyi extract be uniformly mixed, obtain mixture;(2) step (1) resulting mixture is heated to 50-65 DEG C, is cooled to 20-35 DEG C after keeping the temperature 30-60min;(3) the diligent beautiful cactus root pocket extract of crow, plants essential oil and auxiliary agent are added into step (2) treated mixture, is uniformly mixed.Dandruff control shampoo containing of the invention can efficiently remove dandruff, good combination property.
Description
Technical field
The present embodiments relate to technical field of daily necessities, and in particular to a kind of dandruff control shampoo containing and preparation method thereof.
Background technique
Dandruff is the horn cell that scalp falls off, and during dandruff formation, two kinds of substances have played important role: head
Skin secretion grease, and with grease be eat fungi.Under certain condition, fungi may can in scalp surface mass propagation,
Scalp cells are stimulated to secrete more many greases of sauce;A large amount of grease further expands for fungi again provides nutrient.Finally, originally normal
Scalp corneocyte metabolism become unstable, jejune horn cell is assembled one after another to fall off, and just produces dandruff.
Currently, head on the market is washed, protects that product category is more, but mainly by added in shampoo can be antipruritic change
Learn reagent and achieve the effect that anti-dandruff and itching-relieving, such as ketoconazole, zinc pyrithione, although these chemical substances can quick anti-dandruff,
But also there is a great harm for scalp, it should not be used for a long time.In recent years, begun one's study the shampoo containing Chinese medicine additive, but
There are the problems such as anti-dandruff ineffective, preparation process is complicated.
Summary of the invention
The embodiment of the present invention is designed to provide a kind of dandruff control shampoo containing and preparation method thereof, as made from this method
The advantages that dandruff control shampoo containing has bactericidal effect obvious, and anti-dandruff thoroughly chemical component is few, harmless.
To achieve the above object, the technical solution of the embodiment of the present invention is as follows:
In a first aspect, the embodiment of the present invention provides a kind of dandruff control shampoo containing, it is made of the raw material for including following parts by weight: with
The weight of plants essential oil is 1 part of meter, 3-15 parts of rice, diligent beautiful 20-120 parts of the cactus root pocket extract of crow, ginseng extract 10-
30 parts, 10-20 parts of Folium Artemisiae Argyi extract, 1 part of plants essential oil, 1-20 parts of auxiliary agent and 100-150 parts of water.
Preferably, the dandruff control shampoo containing is by including that the raw material of following parts by weight is made: with the weight of plants essential oil for 1 part
Diligent beautiful 50-80 parts of the cactus root pocket extract of meter, 10-15 parts of rice, crow, 10-20 parts of ginseng extract, Folium Artemisiae Argyi extract 10-
20 parts, 1 part of plants essential oil, 1-10 parts of auxiliary agent and 100-120 parts of water.
In the embodiment of the present invention, the plants essential oil is not particularly limited, it can be for in shampoo
Common plants essential oil.The preparation method of plants essential oil can be various preparation methods well known in the art.It commercially available can also be obtained
?.In order to make dandruff control shampoo containing obtained that there is preferably sterilization, anti-dandruff and harmless effect, it is preferable that the plant
Object essential oil includes at least one of tea tree ethereal oil, Rosa Damascana and Lavender.More preferably tea tree ethereal oil.
In the embodiment of the present invention, the rice includes at least one of polished rice, long-grained nonglutinous rice and glutinous rice.
The diligent beautiful cactus root pocket extract of crow originates in Mexico, and also known as black diligent beautiful plant puree meets water in shape or pureed is frozen
The mud that skin epidermis can be deposited connects root and sticks up, and also can stick up dandruff from root of hair portion.The diligent beautiful cactus root pocket extract of crow
In containing there are many antimicrobial component, the fungi and bacterium of scalp surface can be killed efficient, nontoxic, non-stimulatedly, play efficient removal
Dandruff and the effect for curing scalp.The extract can be commercially available, for example, being purchased from the crow of Guangzhou Obo Cosmetic Co., Ltd.
Diligent jade cactus root pocket extract.
Ginseng extract is to form from Hydrolysis kinetics in the root, cauline leaf of Araliaceae ginseng, while having enhancing human body
The effects of vigor of superficial cell, inhibition aging.The preparation method of ginseng extract can be various preparations well known in the art
Method.It can also be commercially available, for example, being purchased from Xi'an Jin Heng Chemical Co., Ltd..
Folium Artemisiae Argyi extract also has disinfection, is able to suppress the fungus breeding of skin surface, eliminates the inflammation of skin, energy
Enough scurfs for promoting removal to be deposited in skin surface.The preparation method of Folium Artemisiae Argyi extract can be various preparations well known in the art
Method.It can also be commercially available, for example, being purchased from Shaanxi Cheng Gan Biotechnology Co., Ltd.
It further include auxiliary agent in the shampoo composite in the embodiment of the present invention, the auxiliary agent can be normal for this field
The various auxiliary agents used are advised, the present invention is not particularly limited.In order to make dandruff control shampoo containing obtained have preferably sterilization,
Anti-dandruff and harmless effect, it is preferable that the auxiliary agent can be laureth sulfuric acid, dodecanamide propyl beet
Alkali, laruyl alcohol phosphate ester salt, lauroyl both sexes guanidine-acetic acid salt, lauryl trimethyl ammonium chloride, Cocoamidopropyl betaine, palm fibre
Palmitic acid acid dissident ester, EDTA- disodium, methylisothiazolinone, AES ammonium salt, narrow leaf cowberry berry extract, acrylic ester copolymerization
One of object, carbomer, triethanolamine, silicone emulsion and essence are a variety of.
Preferably, in some embodiments of the present invention, the auxiliary agent includes laureth sulfuric acid, lauramide
Propyl betaine, laruyl alcohol phosphate ester salt, lauroyl both sexes guanidine-acetic acid salt, lauryl trimethyl ammonium chloride, cocamidopropyl propyl amide
Glycine betaine, palmitinic acid dissident ester, EDTA- disodium, methylisothiazolinone, AES ammonium salt, narrow leaf cowberry berry extract, acrylic acid
One of lipin polymer, carbomer, triethanolamine, silicone emulsion and essence are a variety of.
Preferably, in some embodiments of the present invention, the auxiliary agent includes lauroyl both sexes guanidine-acetic acid salt, lauroyl two
Property guanidine-acetic acid salt, lauryl trimethyl ammonium chloride, narrow leaf cowberry berry extract, acrylic acid esters co-polymer, EDTA- disodium, AES
Ammonium salt, methylisothiazolinone, carbomer, triethanolamine and essence.
Second aspect, the embodiment of the present invention also provide a kind of preparation method of dandruff control shampoo containing, including following step
It is rapid:
(1) it by rice grind into powder, adds water and stirs uniformly, adds ginseng extract and Folium Artemisiae Argyi extract mixing is equal
It is even, obtain mixture;
(2) step (1) resulting mixture is heated to 50-65 DEG C, is cooled to 20-35 DEG C after keeping the temperature 30-60min;
(3) the diligent beautiful cactus root pocket extract of crow, plants essential oil are added into step (2) treated mixture and helps
Agent is uniformly mixed.
Method of the invention, which still further comprises, is filtered mixture obtained by step (3), and the filtering makes described wash
Shampoo preferably passes through the aperture of 150-280 mesh, obtains filtered fluid, obtains anti-dandruff shampoo aquatic products of the invention.
The embodiment of the present invention has the advantages that
Existing shampoo is anti-dandruff to be not thorough, and chemical component is too many, is harmful to the human body, and is regenerated quickly with rear dandruff,
And effective component is used as, it can be achieved that good collaboration is made using as above various plant component cooperations in dandruff control shampoo containing of the invention
With, efficient, nontoxic, non-stimulated sterilization can be carried out to scalp surface, play the role of efficiently removing dandruff and cure scalp, it is comprehensive
It is good to close performance.
Specific embodiment
The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention..
1 the present embodiment of embodiment is used to illustrate dandruff control shampoo containing and preparation method thereof
(1) by 10g polished rice grind into powder, 120g water is added to stir evenly, adds 20g ginseng extract and 20g folium artemisiae argyi
Extract is uniformly mixed, and obtains mixture;
(2) step (1) resulting mixture is heated to 50 DEG C, is cooled to 20 DEG C after keeping the temperature 60min;
(3) be added into step (2) treated mixture the diligent beautiful cactus root pocket extract of 50g crow, 1g tea tree ethereal oil,
2g laureth sulfuric acid, 1.6g lauroyl both sexes guanidine-acetic acid salt, 1.2g lauryl trimethyl ammonium chloride, 2g acrylate
Analog copolymer, 0.8g methylisothiazolinone, 0.5gEDTA- disodium, 0.8g carbomer, 2g triethanolamine, 3g essence and 1g cream
Mixture obtained by step (3) after mixing, then is obtained filtered fluid by the bore filter of 150 mesh, obtained anti-dandruff by SiClx oil
Shampoo product.
2 the present embodiment of embodiment is used to illustrate dandruff control shampoo containing and preparation method thereof
(1) by 15g glutinous rice grind into powder, 110g water is added to stir evenly, adds 20g ginseng extract and 10g folium artemisiae argyi
Extract is uniformly mixed, and obtains mixture;
(2) step (1) resulting mixture is heated to 55 DEG C, is cooled to 25 DEG C after keeping the temperature 40min;
(3) be added into step (2) treated mixture the diligent beautiful cactus root pocket extract of 80g crow, 1g tea tree ethereal oil,
0.8g lauroyl both sexes guanidine-acetic acid salt, 0.5g lauroyl both sexes guanidine-acetic acid salt, 0.7g lauryl trimethyl ammonium chloride, the narrow leaf of 1g are got over
Tangerine berry extract, 1g acrylic acid esters co-polymer, 0.6gEDTA- disodium, 2gAES ammonium salt, 1g methylisothiazolinone, 0.6g card
Wave nurse, 1g triethanolamine and 1.2g essence, after mixing, then the bore filter that mixture obtained by step (3) is passed through into 210 mesh
Filtered fluid is obtained, anti-dandruff shampoo aquatic products are obtained.
3 the present embodiment of embodiment is used to illustrate dandruff control shampoo containing and preparation method thereof
(1) by 15g glutinous rice grind into powder, 110g water is added to stir evenly, adds 20g ginseng extract and 10g folium artemisiae argyi
Extract is uniformly mixed, and obtains mixture;
(2) step (1) resulting mixture is heated to 55 DEG C, is cooled to 25 DEG C after keeping the temperature 40min;
(3) be added into step (2) treated mixture the diligent beautiful cactus root pocket extract of 80g crow, 1g tea tree ethereal oil,
0.6g laruyl alcohol phosphate ester salt, 0.8g lauroyl both sexes guanidine-acetic acid salt, 0.5g lauryl trimethyl ammonium chloride, the narrow leaf cowberry of 0.5g
Berry extract, 1g acrylic acid esters co-polymer, 0.4gEDTA- disodium, 0.8g methylisothiazolinone, 0.8g carbomer, 1g tri-
Mixture obtained by step (3) after mixing, then is obtained filtered fluid by the bore filter of 210 mesh by ethanol amine and 1g essence,
Obtain anti-dandruff shampoo aquatic products.
4 the present embodiment of embodiment is used to illustrate dandruff control shampoo containing and preparation method thereof
(1) by 3g glutinous rice grind into powder, 100g water is added to stir evenly, adds 30g ginseng extract and 12g folium artemisiae argyi mentions
It takes object to be uniformly mixed, obtains mixture;
(2) step (1) resulting mixture is heated to 60 DEG C, is cooled to 25 DEG C after keeping the temperature 30min;
(3) be added into step (2) treated mixture the diligent beautiful cactus root pocket extract of 20g crow, 1g Rosa Damascana,
1g lauroyl both sexes guanidine-acetic acid salt, 0.5g lauryl trimethyl ammonium chloride, the narrow leaf cowberry berry extract of 0.5g, 1.2g acrylate
Analog copolymer, 0.8gEDTA- disodium, 0.7gAES ammonium salt, 0.5g methylisothiazolinone, 0.5g Cocoamidopropyl betaine,
0.8g palmitinic acid dissident ester, 1g carbomer, 1g triethanolamine, 0.4g essence and 1g silicone emulsion, after mixing, then by step
(3) gained mixture obtains filtered fluid by the bore filter of 280 mesh, obtains anti-dandruff shampoo aquatic products.
5 the present embodiment of embodiment is used to illustrate dandruff control shampoo containing and preparation method thereof
(1) by 15g glutinous rice grind into powder, 100g water is added to stir evenly, adds 10g ginseng extract and 20g folium artemisiae argyi
Extract is uniformly mixed, and obtains mixture;
(2) step (1) resulting mixture is heated to 65 DEG C, is cooled to 25 DEG C after keeping the temperature 30min;
(3) the diligent beautiful cactus root pocket extract of 120g crow, 1g lavender essence are added into step (2) treated mixture
Oil, 0.9g lauroyl both sexes guanidine-acetic acid salt, 0.6g lauryl trimethyl ammonium chloride, the narrow leaf cowberry berry extract of 1g, 1g acrylic acid
Lipin polymer, 0.5gEDTA- disodium, 0.7gAES ammonium salt, 0.5g methylisothiazolinone, 1g laureth sulfuric acid,
0.8g palmitinic acid dissident ester and 0.4g carbomer, 1g triethanolamine, 0.8g essence, after mixing, then will be mixed obtained by step (3)
It closes object and filtered fluid is obtained by the bore filter of 240 mesh, obtain anti-dandruff shampoo aquatic products.
1 the present embodiment of comparative example is used to illustrate dandruff control shampoo containing and preparation method thereof
The diligent beautiful cactus root pocket extract of crow is replaced with into water, remaining condition is same as Example 2, obtains anti-dandruff shampoo
Aquatic products.
6 effect assessment of embodiment
The volunteer of 25-45 years old age bracket is chosen as object on probation, random to be grouped, every group of 10 people use embodiment respectively
Shampoo composite prepared by 1-5 and comparative example 1.It is washed hair using shampoo of the invention within average 3 days primary, is no longer made after washing
It the use of the time is 2 months with any conditioner.It is best result that every using effect total score, which is 5 points: five points, is indicated very satisfied;
4 points are fine;3 points are that can receive;3 points the following are bad, cannot receive, and the assessment time is the 3rd after volunteer's hair washing
Before the hair washing of it and next time.The following are every averages, the results are shown in Table 1:
Table 1
Project | Anti-dandruff | Itching of the scalp | Oil-control effect | Irritation |
Embodiment 1 | 5 | 5 | 5 | 5 |
Embodiment 2 | 5 | 5 | 5 | 5 |
Embodiment 3 | 5 | 5 | 5 | 5 |
Embodiment 4 | 5 | 5 | 5 | 5 |
Embodiment 5 | 5 | 5 | 4 | 5 |
Comparative example 1 | 2 | 3 | 3 | 3 |
, can be efficiently anti-dandruff by the above results it is found that dandruff control shampoo containing of the invention has apparent antibacterial effect, suppression
Itching of the scalp processed, and oil-control effect is good, good combination property nonirritant to scalp.
The anti-dandruff effect test of embodiment 7
The dandruff control shampoo containing for respectively preparing embodiment 1-5 and comparative example 1, is configured to the solution of 0.2g/mL, with horse traction color
Reference culture is experimental subjects, according to side disclosed in " foundation and application study of the anti-dandruff effect detection evaluation method of shampoo "
Method carries out inhibition zone diameter test to shampoo made from embodiment, evaluates anti-dandruff effect of shampoo product.According to
Document " foundation and application study of the anti-dandruff effect detection evaluation method of shampoo " (where, Wang Tan, Jia Zebao, Hong Xiaopeng, Peng
Sincerely, research and development department of Si Bao daily use chemicals Co., Ltd, household chemicals science, o. 11th in 2009) method, tested.Antibacterial ring size
Diameter is bigger, and anti-dandruff effect is better, and experimental result is as shown in table 2.
Table 2
By the above results it is found that dandruff control shampoo containing of the invention has apparent antibacterial effect, anti-dandruff effect is good.
Although above having used general explanation and specific embodiment, the present invention is described in detail, at this
On the basis of invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Therefore,
These modifications or improvements without departing from theon the basis of the spirit of the present invention are fallen within the scope of the claimed invention.
Claims (10)
1. a kind of dandruff control shampoo containing, which is characterized in that be made of the raw material for including following parts by weight: 3-15 parts of rice, Wu Ziyu
20-120 parts of cactus root pocket extract, 10-30 parts of ginseng extract, 10-20 parts of Folium Artemisiae Argyi extract, 1 part of plants essential oil, auxiliary agent
1-20 parts and water 100-150 parts.
2. dandruff control shampoo containing according to claim 1, which is characterized in that be made of the raw material for including following parts by weight: big
Diligent 50-80 parts of the jade cactus root pocket extract of 10-15 part of rice, crow, 10-20 parts of ginseng extract, 10-20 parts of Folium Artemisiae Argyi extract,
1 part of plants essential oil, 1-10 parts of auxiliary agent and 100-120 parts of water.
3. dandruff control shampoo containing according to claim 1 or 2, which is characterized in that the plants essential oil include tea tree ethereal oil,
At least one of Rosa Damascana and Lavender.
4. dandruff control shampoo containing according to claim 3, which is characterized in that the plants essential oil is tea tree ethereal oil.
5. dandruff control shampoo containing according to claim 1 or 2, which is characterized in that the rice includes polished rice, long-grained nonglutinous rice and glutinous
At least one of rice.
6. dandruff control shampoo containing according to claim 1 or 2, which is characterized in that the auxiliary agent includes laureth sulphur
Acid esters salt, lauroylamidopropyl betaine, laruyl alcohol phosphate ester salt, lauroyl both sexes guanidine-acetic acid salt, lauryl trimethyl chlorination
Ammonium, Cocoamidopropyl betaine, palmitinic acid dissident ester, EDTA- disodium, methylisothiazolinone, AES ammonium salt, narrow leaf cowberry
One of berry extract, acrylic acid esters co-polymer, carbomer, triethanolamine, silicone emulsion and essence are a variety of.
7. dandruff control shampoo containing according to claim 6, which is characterized in that the auxiliary agent includes lauroyl both sexes guanidine-acetic acid
Salt, lauroyl both sexes guanidine-acetic acid salt, lauryl trimethyl ammonium chloride, narrow leaf cowberry berry extract, acrylic acid esters co-polymer,
EDTA- disodium, AES ammonium salt, methylisothiazolinone, carbomer, triethanolamine and essence.
8. dandruff control shampoo containing according to claim 6, which is characterized in that the auxiliary agent include laruyl alcohol phosphate ester salt,
Lauroyl both sexes guanidine-acetic acid salt, lauryl trimethyl ammonium chloride, narrow leaf cowberry berry extract, acrylic acid esters co-polymer, EDTA-
Disodium, methylisothiazolinone, carbomer triethanolamine and essence.
9. the preparation method of dandruff control shampoo containing described in -6 any one according to claim 1, which is characterized in that including following step
It is rapid:
(1) it by rice grind into powder, adds water and stirs uniformly, adds ginseng extract and Folium Artemisiae Argyi extract is uniformly mixed, obtain
To mixture;
(2) step (1) resulting mixture is heated to 50-65 DEG C, is cooled to 20-35 DEG C after keeping the temperature 30-60min;
(3) the diligent beautiful cactus root pocket extract of crow, plants essential oil and auxiliary agent are added into step (2) treated mixture, mixes
It closes uniform.
10. the method according to the description of claim 7 is characterized in that this method further include: by mixture mistake obtained by step (3)
Filter.
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CN104248557A (en) * | 2013-06-28 | 2014-12-31 | 青岛康泰鑫环保科技有限公司 | High efficiency anti-dandruff shampoo |
CN104546655A (en) * | 2013-10-17 | 2015-04-29 | 李文金 | Novel exfoliating body wash |
CN107281050A (en) * | 2017-08-25 | 2017-10-24 | 安庆徽云博冠化妆品科技有限公司 | A kind of antibacterial hairdressing shampoo and preparation method thereof |
CN107753369A (en) * | 2017-10-27 | 2018-03-06 | 湖南中医药大学 | Profit shield shampoo and preparation method thereof |
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