CN106821807A - Hair-loss preventing and hair-restoring shampoo and preparation method thereof - Google Patents
Hair-loss preventing and hair-restoring shampoo and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The present invention relates to a kind of hair-loss preventing and hair-restoring shampoo, raw material components include Thuja extract, sodium chloride, essence, acrylic ester thickener, guar hydroxypropyltrimonium chloride, NaOH, preservative, water, cleaning agent and conditioner；Wherein, cleaning agent includes sodium lauroyl sarcosine and Cocoamidopropyl betaine；Conditioner includes dimethiconol and cetostearyl alcohol.The hair-loss preventing and hair-restoring shampoo of offer of the invention, prescription proportioning science, safe without toxic side effect with excellent anti-alopecia-stopping and grows new effect.The hair-loss preventing and hair-restoring shampoo that the present invention is provided can penetrate deep into scalp, activation atrophy, the hair follicle cell degenerated, it fully divided, bred, promote the absorption of skin histology nutrition and the excretion of waste material, the microcirculation improvement scalp for stimulating and improving blood is ecological；So that hair follicle is recovered, hair recovers normal growth cycle, reaches the purpose of hair-loss preventing and hair-restoring.
Description
Technical field
The present invention relates to cosmetic technical field, and in particular to a kind of hair-loss preventing and hair-restoring shampoo and preparation method thereof.
Background technology
It is well known that cosmetics refer to smear, spray or other similar approach, intersperse among human body surface position, such as
Skin, hair, refer to toenail, lips and teeth etc., to reach cleaning, maintenance, beauty, modification and change outward appearance or amendment human scent,
Chemical industrial product or fine chemical product for the purpose of maintaining a good state.Shampoo is used as people's aily life necessitys, one
As only have anti-dandruff, treat with oil and hair dyeing etc. function.
In recent years, as the increase of life stress, inherent cause, 3male hormone secretion are excessive, spiritual overstretched, mood
Unstable, sleep insufficiency, overfeeding high lipid food, slow poisoning, microelement deficiencies, stress ability are low, interior point of autoimmunity
Secrete functional disturbance, menstruation and postpartum recuperating be improper and middle aged kidney deficiency etc., can be different degrees of cause people occur alopecia or
Cause bald phenomenon because of alopecia.
Alopecia may be generally divided into two types：The permanent alopecia that causes is damaged and because the hair follicle short time is received due to hair follicle
The temporary alopecia that damage is caused, it is bald that the former is common male.Additionally, hair dyeing, electricity hair, hair-waving, blowing, strong daylight
Irradiation, radiation, environment and chemistry hair washing water pollution, air humidity be excessive or too small etc. that external factor will also result in or accelerate alopecia
Formation.
The means of current hair growth are a lot, mainly there is surgical operation therapy, chemotherapy, Chinese herbal treatment etc..
But the shortcomings of these treatment means exist or need special and professional care to operate inconvenience or side effect big.Based on this, need badly a kind of new
Safe without toxic side effect, and can effectively anti-alopecia-stopping, promote natural on-off cycles of hair growth product.
The content of the invention
For defect of the prior art, the present invention is intended to provide a kind of hair-loss preventing and hair-restoring shampoo and preparation method thereof.This
The hair-loss preventing and hair-restoring shampoo of the offer of invention, prescription proportioning science, safe without toxic side effect, with excellent anti-alopecia-stopping and length
Go out new effect.The hair-loss preventing and hair-restoring shampoo that the present invention is provided can penetrate deep into scalp, and activation atrophy, the hair follicle degenerated are thin
Born of the same parents, make it fully divide, breed, and promote the absorption of skin histology nutrition and the excretion of waste material, stimulate and improve blood
Microcirculation to improve scalp ecological；So that hair follicle is recovered, hair recovers normal growth cycle, reaches the mesh of hair-loss preventing and hair-restoring
's.
Therefore, the present invention provides following technical scheme：
In a first aspect, the present invention provides a kind of hair-loss preventing and hair-restoring shampoo, raw material components by weight, including：Arbor-vitae carries
Take thing 5-15 weight portions, sodium chloride 0.5-1.5 weight portions, essence 0.1-1.0 weight portions, acrylic ester thickener 0.1-0.5
Weight portion, guar hydroxypropyltrimonium chloride 0.1-0.8 weight portions, NaOH 0.01-0.10 weight portions, preservative
0.05-0.15 weight portions, water 55-75 weight portions, cleaning agent and conditioner；Wherein, cleaning agent includes sodium lauroyl sarcosine
10-20 weight portions and Cocoamidopropyl betaine 5-10 weight portions；Conditioner includes dimethiconol 1-3 weight
Part and cetostearyl alcohol 0.5-2 weight portions.It should be noted that the Thuja extract in the present invention can be selected from commercially available product
Product, it is also possible to according to the method self-control that the present invention is provided；Specifically, the preparation method of Thuja extract includes：Using quality hundred
Point concentration makees extractant for the ethanol water of 45%-65%, and arbor-vitae is extracted under conditions of being 55 DEG C -65 DEG C in temperature
30min-90min；Wherein, arbor-vitae and the mass ratio of the ethanol water that mass percentage concentration is 45%-65% are 1：(3-5).
It is the dimethiconol of 5000-20000cp (25 DEG C) from viscosity.
In further embodiment of the invention, acrylic ester thickener includes esters of acrylic acid/C10-30 alkanols
Acrylate crosspolymers.
In further embodiment of the invention, preservative includes magnesium nitrate, methylchloroisothiazandnone, the different thiophene of methyl
One or more in oxazoline ketone and magnesium chloride.
In further embodiment of the invention, Thuja extract is selected from the extract of cacumen biotae.
In further embodiment of the invention, including following raw material components：The weight portion of Thuja extract 6, lauroyl
The weight portion of sodium sarcosinate 18, the weight portion of Cocoamidopropyl betaine 6, the weight portion of dimethiconol 2, cetostearyl alcohol
1 weight portion, the weight portion of sodium chloride 0.7, the weight portion of essence 0.5, the weight portion of acrylic ester thickener 0.3, melon glue hydroxypropyl
The weight portion of trimethyl ammonium chloride 0.4, the weight portion of NaOH 0.06, the weight portion of magnesium nitrate 0.02, methylchloroisothiazandnone
0.0012 weight portion, the weight portion of methylisothiazolinone 0.0004, the weight portion of magnesium chloride 0.009 and the weight portion of water 64.94.
Each raw material components for preparing hair-loss preventing and hair-restoring shampoo of the present invention are that, as proportioning, can be pressed in production according to mass parts
According to corresponding ratio increase or reduce, such as large-scale production can by kilogram or in units of ton, small-scale production can also gram
It is unit, weight can increase or reduce, but raw material components quality proportioning between each composition is constant.
Second aspect, the present invention provides a kind of preparation method of hair-loss preventing and hair-restoring shampoo, comprises the following steps：S101：Will
Acrylic ester thickener and guar hydroxypropyltrimonium chloride stir after mixing with water；S102：Obtained in S101
Product in add cleaning agent, conditioner and water, then stir；S103：Hydroxide is added in the product that S102 is obtained
Sodium and the mixed solution of water, continue to stir；S104：Thuja extract, sodium chloride, perfume (or spice) are added in the product that S103 is obtained
Essence, preservative and water, stir, filtrate is filtered and collected afterwards.It should be noted that those skilled in the art can be with root
The amount of addition water in each step is adjusted according to actual conditions, each raw material components of principle guarantee can be completely dissolved and be well mixed
；Certainly, the water of the weight portion such as addition is also possible in S101, S102, S103 and S104.
In further embodiment of the invention, in S101, S103 and S104, the condition of stirring is：Rotating speed is
1500rpm-2000rpm, temperature is 50 DEG C -55 DEG C.Specifically, those skilled in the art can adjust according to actual conditions and stir
Time, it is ensured that each raw material components fully dissolve and well mixed, and 30min-90min is possible in principle.
In further embodiment of the invention, in S102, after adding cleaning agent, conditioner and water, rotating speed is
1500rpm-2000rpm, temperature is stirring at 75 DEG C -80 DEG C.
In further embodiment of the invention, after S103, before S104, also include：The product that S103 is obtained
It is cooled to 44 DEG C -46 DEG C.
Above-mentioned technical proposal of the invention has the following advantages that compared to existing technology：
(1) applicant has found by numerous studies：The hair-loss preventing and hair-restoring shampoo of offer of the invention, raw material components include day
Right active material, prescription proportioning science, safe without toxic side effect with excellent anti-alopecia-stopping and grows new effect.This
Inventing the hair-loss preventing and hair-restoring shampoo for providing can penetrate deep into scalp, and activation atrophy, the hair follicle cell degenerated make it fully divide
Split, breed, promote the absorption of skin histology nutrition and the excretion of waste material, the microcirculation for stimulating and improving blood improves head
Skin is ecological；So that hair follicle is recovered, hair recovers normal growth cycle, reaches the purpose of hair-loss preventing and hair-restoring.
(2) using the present invention provide preparation method, can in each raw material components are retained to greatest extent active component
While, the active ingredient in each raw material components can be fully discharged, so that the final hair-loss preventing and hair-restoring for preparing
Shampoo has excellent effect.Additionally, the preparation method that the present invention is provided is easy to operate, with low cost, be highly advantageous to industry
Change big production.
Additional aspect of the invention and advantage will be set forth in part in the description, and will partly become from the following description
Obtain substantially, or recognized by practice of the invention.
Specific embodiment
The embodiment of technical solution of the present invention will be described in detail below.Following examples are only used for clearer
Explanation technical scheme, therefore be only used as example, and can not be limited the scope of the invention with this.
Experimental technique in following embodiments, unless otherwise specified, is conventional method.
Test material used in following embodiments, unless otherwise specified, is what is be commercially available from conventional reagent shop.
Quantitative test in following examples, is respectively provided with three repetitions and tests, and data are three average values of repetition experiment
Or mean+SD.
Guar hydroxypropyltrimonium chloride, sodium lauroyl sarcosine and dimethiconol in the present invention is equal
Purchased from Jining Bai Chuan Chemical Co., Ltd.s；Wherein, guar hydroxypropyltrimonium chloride model C-14S；Lauroyl flesh ammonia
The model LS-30 of sour sodium, the model DC-1785 of dimethiconol.Cocoamidopropyl betaine is purchased from Suzhou
Ming Hua sugar alcohols Co., Ltd of city, model CAB-35；Cetostearyl alcohol is purchased from the Chemical Co., Ltd. of Shandong 100,000, model
1670；Esters of acrylic acid/C10-30 alkylol acrylamide acid esters cross-linked polymer is purchased from Guangzhou Hong Chang Chemical Co., Ltd.s, model
Carbopol Ultrez 20.Cacumen Platycladi extract is purchased from Xi'an Olympic Competition bio tech ltd.Certainly, from other companies
Mentioned reagent it is also possible.
The present invention provides a kind of hair-loss preventing and hair-restoring shampoo, raw material components by weight, including：Thuja extract 5-15 weights
Amount part, sodium chloride 0.5-1.5 weight portions, essence 0.1-1.0 weight portions, acrylic ester thickener 0.1-0.5 weight portions, melon
Glue hydroxypropyl-trimethyl ammonium chloride 0.1-0.8 weight portions, NaOH 0.01-0.10 weight portions, preservative 0.05-0.15 weight
Part, water 55-75 weight portions, cleaning agent and conditioner；Wherein, cleaning agent include sodium lauroyl sarcosine 10-20 weight portions with
And Cocoamidopropyl betaine 5-10 weight portions；Conditioner includes that dimethiconol 1-3 weight portions and spermaceti are hard
Lipidol 0.5-2 weight portions.Wherein, Thuja extract is selected from the extract of cacumen biotae；Acrylic ester thickener includes acrylic acid
Esters/C10-30 alkylol acrylamide acid esters cross-linked polymers；Preservative includes magnesium nitrate, methylchloroisothiazandnone, the different thiophene of methyl
One or more in oxazoline ketone and magnesium chloride.
Preferably, the preparation method of Thuja extract includes：Use mass percentage concentration water-soluble for the ethanol of 45%-65%
Liquid makees extractant, and 30min-90min is extracted to arbor-vitae under conditions of being 55 DEG C -65 DEG C in temperature；Wherein, arbor-vitae and quality percentage
Concentration is 1 for the mass ratio of the ethanol water of 45%-65%：(3-5).
In addition, being directed to hair-loss preventing and hair-restoring shampoo of the invention, the special preparation hair-loss preventing and hair-restoring of the present invention that devises of the present invention is washed
The method of lotion, comprises the following steps：
S101：Stirred after acrylic ester thickener and guar hydroxypropyltrimonium chloride are mixed with water.
S102：Cleaning agent, conditioner and water are added in the product that S101 is obtained, is then stirred.Wherein, add clear
After clean dose, conditioner and water, regulation whipping temp is 75 DEG C -80 DEG C until stirring.
S103：The mixed solution of NaOH and water is added in the product that S102 is obtained, continues to stir.
S104：Thuja extract, sodium chloride, essence, preservative and water are added in the product that S103 is obtained, stirring is equal
It is even, filtrate is filtered and collected afterwards.
Preferably, the condition of stirring is specially：Rotating speed is 1500rpm-2000rpm, and temperature is 50 DEG C -55 DEG C.
Preferably, after S103, before S104, also include：The product that S103 is obtained is cooled to 44 DEG C -46 DEG C.
Illustrated with reference to specific embodiment：
Embodiment one
The present invention provides a kind of hair-loss preventing and hair-restoring shampoo, is made up of following raw material components：The weight portion of Cacumen Platycladi extract 15,
The weight portion of sodium lauroyl sarcosine 10, the weight portion of Cocoamidopropyl betaine 5, viscosity are the polydimethylsiloxanes of 10000cp
The weight portion of alkanol 1, the weight portion of cetostearyl alcohol 2, the weight portion of sodium chloride 1.5, the weight portion of essence 1.0, esters of acrylic acid/C10-30
The weight portion of alkylol acrylamide acid esters cross-linked polymer 0.5, the weight portion of guar hydroxypropyltrimonium chloride 0.1, NaOH
0.10 weight portion, the weight portion of magnesium nitrate 0.01, the weight portion of methylchloroisothiazandnone 0.04 and the weight portion of water 75.
By above-mentioned raw materials component, the preparation method provided using the present invention, the hair-loss preventing and hair-restoring hair washing needed for preparing the present invention
Liquid：
S101：By esters of acrylic acid/C10-30 alkylol acrylamide acid esters cross-linked polymers and melon glue Hydroxyproyl Trimethyl chlorine
It is 1500rpm, temperature to stir 30min under conditions of 55 DEG C to change after ammonium mix with water in rotating speed.
S102：Sodium lauroyl sarcosine, Cocoamidopropyl betaine, poly dimethyl are added in the product that S101 is obtained
Silica alkanol, cetostearyl alcohol and water, then heat to 75 DEG C, and 50min is stirred under conditions of rotating speed is 1500rpm.
S103：The mixed solution of NaOH and water is added in the product that S102 is obtained, is 1500rpm, temperature in rotating speed
Spend to stir 30min under conditions of 55 DEG C.
S104：The product obtained in S103 is cooled to 45 DEG C, is subsequently adding Cacumen Platycladi extract, sodium chloride, essence, nitric acid
Magnesium, methylchloroisothiazandnone and water, rotating speed be 1500rpm, temperature be 55 DEG C under conditions of stir 30min, filter afterwards simultaneously
Collect filtrate.Wherein, the preparation method of Cacumen Platycladi extract includes：Mass percentage concentration is used to make for 65% ethanol water
Extractant, 90min is extracted under conditions of being 55 DEG C in temperature to cacumen biotae；Wherein, cacumen biotae and mass percentage concentration are 65%
Ethanol water mass ratio be 1：5.
Embodiment two
The present invention provides a kind of hair-loss preventing and hair-restoring shampoo, is made up of following raw material components：The weight portion of Cacumen Platycladi extract 6,
The weight portion of sodium lauroyl sarcosine 18, the weight portion of Cocoamidopropyl betaine 6, viscosity are the dimethyl silicone polymer of 5000cp
The weight portion of alcohol 2, the weight portion of cetostearyl alcohol 1, the weight portion of sodium chloride 0.7, the weight portion of essence 0.5, esters of acrylic acid/C10-30 alkane
The weight portion of alcohol acrylate crosspolymers 0.3, the weight portion of guar hydroxypropyltrimonium chloride 0.4, NaOH 0.06
Weight portion, the weight portion of magnesium nitrate 0.02, the weight portion of methylchloroisothiazandnone 0.0012, the weight of methylisothiazolinone 0.0004
Part, the weight portion of magnesium chloride 0.009 and the weight portion of water 64.94.
By above-mentioned raw materials component, the preparation method provided using the present invention, the hair-loss preventing and hair-restoring hair washing needed for preparing the present invention
Liquid：
S101：By esters of acrylic acid/C10-30 alkylol acrylamide acid esters cross-linked polymers and melon glue Hydroxyproyl Trimethyl chlorine
It is 2000rpm, temperature to stir 50min under conditions of 50 DEG C to change after ammonium mix with water in rotating speed.
S102：Sodium lauroyl sarcosine, Cocoamidopropyl betaine, poly dimethyl are added in the product that S101 is obtained
Silica alkanol, cetostearyl alcohol and water, then heat to 80 DEG C, and 50min is stirred under conditions of rotating speed is 2000rpm.
S103：The mixed solution of NaOH and water is added in the product that S102 is obtained, is 2000rpm, temperature in rotating speed
Spend to stir 50min under conditions of 50 DEG C.
S104：The product obtained in S103 is cooled to 46 DEG C, is subsequently adding Cacumen Platycladi extract, sodium chloride, essence, nitric acid
Magnesium, methylchloroisothiazandnone, methylisothiazolinone, magnesium chloride and water, rotating speed are 2000rpm, the condition that temperature is 50 DEG C
Lower stirring 50min, filters and collects filtrate afterwards.Wherein, the preparation method of Cacumen Platycladi extract includes：It is dense using quality percentage
The ethanol water spent for 45% makees extractant, and 60min is extracted to cacumen biotae under conditions of being 55 DEG C in temperature；Wherein, arbor-vitae
Leaf is 1 with the mass ratio of the ethanol water that mass percentage concentration is 45%：3.
Embodiment three
The present invention provides a kind of hair-loss preventing and hair-restoring shampoo, is made up of following raw material components：The weight portion of Cacumen Platycladi extract 5,
The weight portion of sodium lauroyl sarcosine 20, the weight portion of Cocoamidopropyl betaine 10, viscosity are the polydimethylsiloxanes of 20000cp
The weight portion of alkanol 3, the weight portion of cetostearyl alcohol 0.5, the weight portion of sodium chloride 0.5, the weight portion of essence 0.1, esters of acrylic acid/C10-
The weight portion of 30 alkylol acrylamide acid esters cross-linked polymer 0.1, the weight portion of guar hydroxypropyltrimonium chloride 0.8, NaOH
0.01 weight portion, the weight portion of methylchloroisothiazandnone 0.1, the weight portion of magnesium chloride 0.05 and the weight portion of water 55.
By above-mentioned raw materials component, the preparation method provided using the present invention, the hair-loss preventing and hair-restoring hair washing needed for preparing the present invention
Liquid：
S101：By esters of acrylic acid/C10-30 alkylol acrylamide acid esters cross-linked polymers and melon glue Hydroxyproyl Trimethyl chlorine
It is 1800rpm, temperature to stir 40min under conditions of 53 DEG C to change after ammonium mix with water in rotating speed.
S102：Sodium lauroyl sarcosine, Cocoamidopropyl betaine, poly dimethyl are added in the product that S101 is obtained
Silica alkanol, cetostearyl alcohol and water, then heat to 78 DEG C, and 40min is stirred under conditions of rotating speed is 1800rpm.
S103：The mixed solution of NaOH and water is added in the product that S102 is obtained, is 1800rpm, temperature in rotating speed
Spend to stir 40min under conditions of 53 DEG C.
S104：The product obtained in S103 is cooled to 44 DEG C, is subsequently adding Cacumen Platycladi extract, sodium chloride, essence, methyl
Chloroisothiazole quinoline ketone, magnesium chloride and water, rotating speed be 1800rpm, temperature be 53 DEG C under conditions of stir 40min, filter afterwards simultaneously
Collect filtrate.Wherein, the preparation method of Cacumen Platycladi extract includes：Mass percentage concentration is used to make for 55% ethanol water
Extractant, 30min is extracted under conditions of being 60 DEG C in temperature to cacumen biotae；Wherein, cacumen biotae and mass percentage concentration are 55%
Ethanol water mass ratio be 1：4.
Example IV
The present invention provides a kind of hair-loss preventing and hair-restoring shampoo, is made up of following raw material components：The weight portion of Cacumen Platycladi extract 6,
The weight portion of sodium lauroyl sarcosine 18, the weight portion of Cocoamidopropyl betaine 6, viscosity are the polydimethylsiloxanes of 10000cp
The weight portion of alkanol 2, the weight portion of cetostearyl alcohol 1, the weight portion of sodium chloride 0.7, the weight portion of essence 0.5, esters of acrylic acid/C10-30
The weight portion of alkylol acrylamide acid esters cross-linked polymer 0.3, the weight portion of guar hydroxypropyltrimonium chloride 0.4, NaOH
0.06 weight portion, the weight portion of magnesium nitrate 0.02, the weight portion of methylchloroisothiazandnone 0.0012, methylisothiazolinone 0.0004
Weight portion, the weight portion of magnesium chloride 0.009 and the weight portion of water 64.94.
By above-mentioned raw materials component, the preparation method provided using the present invention, the hair-loss preventing and hair-restoring hair washing needed for preparing the present invention
Liquid：
S101：By esters of acrylic acid/C10-30 alkylol acrylamide acid esters cross-linked polymers and melon glue Hydroxyproyl Trimethyl chlorine
It is 2000rpm, temperature to stir 50min under conditions of 50 DEG C to change after ammonium mix with water in rotating speed.
S102：Sodium lauroyl sarcosine, Cocoamidopropyl betaine, poly dimethyl are added in the product that S101 is obtained
Silica alkanol, cetostearyl alcohol and water, then heat to 80 DEG C, and 50min is stirred under conditions of rotating speed is 2000rpm.
S103：The mixed solution of NaOH and water is added in the product that S102 is obtained, is 2000rpm, temperature in rotating speed
Spend to stir 50min under conditions of 50 DEG C.
S104：The product obtained in S103 is cooled to 46 DEG C, is subsequently adding Cacumen Platycladi extract, sodium chloride, essence, nitric acid
Magnesium, methylchloroisothiazandnone, methylisothiazolinone, magnesium chloride and water, rotating speed are 2000rpm, the condition that temperature is 50 DEG C
Lower stirring 50min, filters and collects filtrate afterwards.Wherein, Cacumen Platycladi extract is selected from commercially available prod.
In addition, the effect in order to preferably evaluate each embodiment, carries out following experiment：
First, toxicity test
The small white mouse 120 (each 60 of male and female) for selecting body weight to be 18-22g, is divided into 4 groups, every group of each 15 of male and female, small white mouse
Back unhairing exposes exocuticle, unhairing scope 2cm × 2cm, and first group to the 4th group is smeared the embodiment of the present invention one to reality respectively
The hair-loss preventing and hair-restoring shampoo that example four is prepared is applied, dosage is 5g, successive administration 30 days.During administration and 1 week after drug withdrawal
When, observe white mouse growth conditions and activity and diet, identification hematology, blood biochemical analysis, organ tissue structure and routine urinalysis etc..
Result finds the health existence of all small white mouses, without any side effects；Anatomic observation blood picture, liver function, each organs and tissues shape
State, indifference is compared with normal small white mouse.It is demonstrated experimentally that the hair-loss preventing and hair-restoring shampoo that the present invention is provided is nontoxic, drug safety can
Lean on.
2nd, clinical test
Call-up age is the volunteer 400 with alopecia symptom of 30-50 Sui.Specifically, volunteer is divided into 4
Group, every group 100.First group to the 4th group is tried out respectively the hair-loss preventing and hair-restoring shampoo of the embodiment of the present invention one and example IV
30 days, once a day, each 3g, application method was similar with shampoo：Take hair-loss preventing and hair-restoring shampoo to be applied on hair root, gently
Forlement a moment；It is such as accidentally pleasing to the eye, rinsed with clear water.
Curative effect is observed when on probation 10th day and the 30th day, it is specific as shown in table 1.Outcome measure is：Cure：Alopecia
Phenomenon is seriously reduced, and hair becomes pitch-black glossy, and it is strong that hair is tough.Take a turn for the better：Depilation phenomenon has been reduced, and hair is glossy
Degree makes moderate progress.It is invalid：Depilation phenomenon is without any change, and hair remains unchanged intensely dark pool.
Additionally, detecting each embodiment shampoo foaminess in use, washing rear compliance, use stimulation degree, produce
Quality properties are set to 5 grades.8-10 points：By force；6-8 points：It is stronger；3-6 points：Typically；1-3 points：It is weak.Test result is such as
Shown in table 2.
The effect statistical form one of each embodiment hair-loss preventing and hair-restoring shampoo of table 1
The effect statistical form two of each embodiment hair-loss preventing and hair-restoring shampoo of table 2
Certainly, except the situation that embodiment one to example IV is enumerated, the species and percentage by weight of other raw material components,
Condition and parameter in preparation process etc. are also possible.
The hair-loss preventing and hair-restoring shampoo of offer of the invention, raw material components include natural active matter, prescription proportioning science, peace
Completely without toxic and side effect, with excellent anti-alopecia-stopping and new effect is grown.The hair-loss preventing and hair-restoring hair washing liquid energy that the present invention is provided
Deep enough infiltration scalp, activation atrophy, the hair follicle cell degenerated, makes it fully divide, breed, and promotes skin histology nutrition
Absorption and the excretion of waste material, stimulating and improve the microcirculation of blood improves scalp ecology；So that hair follicle is recovered, hair is extensive
Multiple normal growth cycle, reaches the purpose of hair-loss preventing and hair-restoring.
In the description of this specification, it is to be understood that reference term " one embodiment ", " some embodiments ", " show
The description of example ", " specific example " or " some examples " etc. mean to combine the specific features of the embodiment or example description, structure,
Material or feature are contained at least one embodiment of the invention or example.In this manual, above-mentioned term is shown
The statement of meaning property is necessarily directed to identical embodiment or example.And, the specific features of description, structure, material or spy
Point can in an appropriate manner be combined in any one or more embodiments or example.Additionally, in the case of not conflicting,
Those skilled in the art can be by the different embodiments or example described in this specification and different embodiment or example
Feature is combined and combines.
Although embodiments of the invention have been shown and described above, it is to be understood that above-described embodiment is example
Property, it is impossible to limitation of the present invention is interpreted as, one of ordinary skill in the art within the scope of the invention can be to above-mentioned
Embodiment is changed, changes, replacing and modification.
Claims (9)
1. a kind of hair-loss preventing and hair-restoring shampoo, it is characterised in that raw material components by weight, including：
Thuja extract 5-15 weight portions, sodium chloride 0.5-1.5 weight portions, essence 0.1-1.0 weight portions, esters of acrylic acid thickening
Agent 0.1-0.5 weight portions, guar hydroxypropyltrimonium chloride 0.1-0.8 weight portions, NaOH 0.01-0.10 weight
Part, preservative 0.05-0.15 weight portions, water 55-75 weight portions, cleaning agent and conditioner；
Wherein, the cleaning agent includes sodium lauroyl sarcosine 10-20 weight portions and Cocoamidopropyl betaine 5-10 weights
Amount part；The conditioner includes dimethiconol 1-3 weight portions and cetostearyl alcohol 0.5-2 weight portions.
2. hair-loss preventing and hair-restoring shampoo according to claim 1, it is characterised in that：
The acrylic ester thickener includes esters of acrylic acid/C10-30 alkylol acrylamide acid esters cross-linked polymers.
3. hair-loss preventing and hair-restoring shampoo according to claim 1, it is characterised in that：
The preservative includes the one kind or many in magnesium nitrate, methylchloroisothiazandnone, methylisothiazolinone and magnesium chloride
Kind.
4. hair-loss preventing and hair-restoring shampoo according to claim 1, it is characterised in that：
The Thuja extract is selected from the extract of cacumen biotae.
5. hair-loss preventing and hair-restoring shampoo according to claim 1, it is characterised in that including following raw material components：
The weight portion of Thuja extract 6, the weight portion of sodium lauroyl sarcosine 18, the weight portion of Cocoamidopropyl betaine 6, poly- diformazan
The weight portion of radical siloxane alcohol 2, the weight portion of cetostearyl alcohol 1, the weight portion of sodium chloride 0.7, the weight portion of essence 0.5, esters of acrylic acid
The weight portion of thickener 0.3, the weight portion of guar hydroxypropyltrimonium chloride 0.4, the weight portion of NaOH 0.06, magnesium nitrate
0.02 weight portion, the weight portion of methylchloroisothiazandnone 0.0012, the weight portion of methylisothiazolinone 0.0004, magnesium chloride
0.009 weight portion and the weight portion of water 64.94.
6. the preparation method of hair-loss preventing and hair-restoring shampoo described in any one of claim 1-5, it is characterised in that comprise the following steps：
S101：Stirred after acrylic ester thickener and guar hydroxypropyltrimonium chloride are mixed with water；
S102：Cleaning agent, conditioner and water are added in the product that the S101 is obtained, is then stirred；
S103：The mixed solution of NaOH and water is added in the product that the S102 is obtained, continues to stir；
S104：Thuja extract, sodium chloride, essence, preservative and water are added in the product that the S103 is obtained, stirring is equal
It is even, filtrate is filtered and collected afterwards.
7. the preparation method of hair-loss preventing and hair-restoring shampoo according to claim 6, it is characterised in that：
In the S101, the S103 and the S104, the condition of the stirring is：Rotating speed is 1500rpm-2000rpm, temperature
Spend is 50 DEG C -55 DEG C.
8. the preparation method of hair-loss preventing and hair-restoring shampoo according to claim 6, it is characterised in that：
It is 1500rpm-2000rpm in rotating speed after adding cleaning agent, conditioner and water in the S102, temperature is 75 DEG C -80
Stirred under conditions of DEG C.
9. the preparation method of hair-loss preventing and hair-restoring shampoo according to claim 6, it is characterised in that：
After the S103, before the S104, also include：The product that the S103 is obtained is cooled to 44 DEG C -46 DEG C.
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| CN107362104A (en) * | 2017-09-04 | 2017-11-21 | 上海张苍生物科技有限公司 | A kind of alopecia-stopping, the leaves shampoo of hair tonic |
| CN108294998A (en) * | 2018-04-12 | 2018-07-20 | 广东医科大学 | Anticreep shampoo and preparation method thereof |
| CN108771645A (en) * | 2018-08-21 | 2018-11-09 | 广东博然堂生物科技有限公司 | A kind of quinoa shampoo and its manufacturing method |
| CN110179731A (en) * | 2019-07-09 | 2019-08-30 | 许富明 | A kind of hair-loss preventing and hair-restoring shampoo and preparation method thereof |
| CN110403882A (en) * | 2019-09-02 | 2019-11-05 | 佛山科学技术学院 | A kind of shampoo with hair-growing and hair care effect |
| CN111419750A (en) * | 2020-04-23 | 2020-07-17 | 广州市白云区莱媚美容美发日用化妆品厂 | Plant shampoo formula capable of effectively promoting hair growth and preparation method thereof |
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| CN107362104A (en) * | 2017-09-04 | 2017-11-21 | 上海张苍生物科技有限公司 | A kind of alopecia-stopping, the leaves shampoo of hair tonic |
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| CN108771645A (en) * | 2018-08-21 | 2018-11-09 | 广东博然堂生物科技有限公司 | A kind of quinoa shampoo and its manufacturing method |
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| CN110403882A (en) * | 2019-09-02 | 2019-11-05 | 佛山科学技术学院 | A kind of shampoo with hair-growing and hair care effect |
| CN111419750A (en) * | 2020-04-23 | 2020-07-17 | 广州市白云区莱媚美容美发日用化妆品厂 | Plant shampoo formula capable of effectively promoting hair growth and preparation method thereof |
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Application publication date: 20170613 |