CN108938512A - A kind of skin whitening, moisturizing body lotion of the extract containing acacia - Google Patents

A kind of skin whitening, moisturizing body lotion of the extract containing acacia Download PDF

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Publication number
CN108938512A
CN108938512A CN201811253948.2A CN201811253948A CN108938512A CN 108938512 A CN108938512 A CN 108938512A CN 201811253948 A CN201811253948 A CN 201811253948A CN 108938512 A CN108938512 A CN 108938512A
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temperature
under conditions
skin
constant
acacia
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张腾飞
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Hanshan Beipen Biotechnology Co Ltd
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Hanshan Beipen Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients

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  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Mycology (AREA)
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  • Epidemiology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention belongs to technical field of skin care, the skin whitening, moisturizing body lotion of especially a kind of extract containing acacia, is made of raw material from the following weight: rice, semen sojae atricolor, gumbo, Grape Skin, konjac glucomannan, acacia extract, Chinese toon powder, ant powder, dried silkworm chrysalis meal, water;A variety of green natural raw materials are added and carry out processing mating reaction, it does not stimulate mildly, do not add chemical addition agent, it is natural pollution-free, effectively avoid the generation of heavy-metal residual phenomenon, any side effect will not be caused to human body, formula is scientific and reasonable, raw material utilization efficiency can be effectively improved, nutritional ingredient rich in, effectively nutrition needed for supplement skin, enhance skin metabolic capability, improve skin oxidation resistance, effectively inhibit the precipitating of melanin and promotes the decomposition of melanin, the water lock for enhancing skin protects ability, effectively avoid the generation of the dry and cracked husking phenomenon of skin, so that skin is smooth beautiful flexible, whitening effect goes to wrinkle, replenishing water and preserving moisture, improve skin sense, promote the differentiation of horn cell.

Description

A kind of skin whitening, moisturizing body lotion of the extract containing acacia
Technical field
The invention belongs to technical field of skin care, the skin whitening, moisturizing body lotion of especially a kind of extract containing acacia.
Background technique
With people's substance, the progress of the continuous improvement of the level of cultural life and society, skin care item have become people Beautify the various daily neces saries of life;For reform and opening-up over 30 years, China's skin care item market sales revenue is fast with average annual 23.8% speed Speed increases, and speedup is much higher than the growth rate of GDP;Wherein the moistening effect of skin care item plays decisive work to the quality of skin care item With, and why moisturizing becomes a very important beauty concept, is the very easy loss of moisture because of skin, and skin Water shortage can directly result in the abnormal and aging of skin metabolism, a series of skin problems of wrinkle and itch etc. occurs, in addition, people The drying of living environment easily causes the dry husking of people's whole body even the phenomenon that itch occur, seriously affects people's lives Quality, and whitening skin is also that people pursue always, but current skin-protection product can generally contain chemical addition agent, thorn Swash skin, also will cause Heavy Metal Pollution, a series of side effect can be generated to body;Therefore, it should invent a kind of whitening guarantor Wet body lotion.
Summary of the invention
In view of the above-mentioned problems, the present invention is intended to provide a kind of skin whitening, moisturizing body lotion of extract containing acacia.
The invention is realized by the following technical scheme:
A kind of skin whitening, moisturizing body lotion of the extract containing acacia, is made of raw material from the following weight: 36 ~ 38 parts of rice, semen sojae atricolor 20 ~ 22 parts, 11 ~ 12 parts of gumbo, 26 ~ 28 parts of Grape Skin, 1.9 ~ 2.1 parts of konjac glucomannan, 0.44 ~ 0.48 part of acacia extract, Chinese toon 0.26 ~ 0.28 part of powder, 0.14 ~ 0.16 part of ant powder, 0.31 ~ 0.33 part of dried silkworm chrysalis meal, 70 ~ 80 parts of water;
The acacia extract, is prepared according to the following steps:
(1) the fresh robiniae,flos of 23 ~ 25 parts by weight and the fresh acacia leaf co-grinding of 14 ~ 16 parts by weight are beaten, merging temperature is Constant refrigeration handles 21 ~ 25min under conditions of 1.1 ~ 1.5 DEG C, takes out, and magnetizes under conditions of magnetic field strength is 360 ~ 380mT 10 ~ 12min is handled, constant refrigeration handles 46 ~ 50min under conditions of merging temperature is 3.3 ~ 3.5 DEG C, takes out, in magnetic field strength For 16 ~ 18min of magnetization treatment under conditions of 620 ~ 640mT, activation slurry must be refrigerated;
(2) cellulase of 0.24 ~ 0.28 parts by weight and the bromelain of 0.11 ~ 0.13 parts by weight is added into refrigeration activation slurry Enzyme stirs evenly, and merging temperature is 230 ~ 270min of enzymolysis processing under conditions of 32 ~ 34 DEG C, 65 ~ 75 parts by weight is added, temperature is 49 ~ 51 DEG C of water stirs evenly, and continues 40 ~ 50min of mild fire infusion after being boiled by slow fire, and filtering obtains infusion liquid and filter residue;
(3) 34 ~ 38 parts by weight, mass fraction are added into filter residue to stir evenly for 51% ~ 55% ethanol solution, are in power 265 ~ 275W, frequency are ultrasonically treated 15 ~ 17min, 40 ~ 50min of refluxing extraction after ebuillition of heated under conditions of being 119 ~ 125kHz, Filtering, takes filtrate, obtains reflux extracting liquid;
(4) merge infusion liquid and reflux extracting liquid, continue 14 ~ 18min of mild fire infusion after being boiled by slow fire, be -30 ~ -26 in temperature Vacuum freeze drying under conditions of DEG C obtains acacia extract.
As invention further embodiment: the Chinese toon powder is prepared according to the following steps: by Chinese toon and its weight 0.5 ~ 0.6 times of amount, the water that temperature is 38 ~ 40 DEG C are mixed with beating, and constant temperature steam is handled under conditions of merging temperature is 112 ~ 118 DEG C 14 ~ 16min takes out, and constant refrigeration handles 36 ~ 40min under conditions of merging temperature is 0.7 ~ 0.9 DEG C, takes out, and merging temperature is Constant temperature toasts 7 ~ 9min under conditions of 41 ~ 43 DEG C, is warming up to 75 ~ 77 DEG C of continuation constant temperature with the heating rate of 1.9 ~ 2.1 DEG C/min 11 ~ 13min is toasted, is taken out, pulverizes, obtains Chinese toon powder.
As invention further embodiment: the ant powder is prepared according to the following steps: by ant and its weight 0.8 ~ 0.9 times of amount, the ethanol solution that mass fraction is 35% ~ 37% are mixed with beating, and merging temperature is constant temperature under conditions of 81 ~ 85 DEG C 11 ~ 13min of steam treatment, with the heating rate of 3.9 ~ 4.3 DEG C/min be warming up to 151 ~ 159 DEG C of continuation constant temperature steams processing 15 ~ 17min takes out, and constant temperature toasts 28 ~ 32min under conditions of merging temperature is 93 ~ 97 DEG C, takes out, and pulverizes, obtains ant powder.
As invention further embodiment: the dried silkworm chrysalis meal is prepared according to the following steps: by silkworm chrysalis and its weight 1.4 ~ 1.6 times of amounts, the water that temperature is 55 ~ 59 DEG C are mixed with beating, and are boiled by slow fire, under conditions of magnetic field strength is 500 ~ 520mT 20 ~ 24min of magnetization treatment continues 28 ~ 32min of mild fire infusion, is spray-dried, and pulverizes, obtains dried silkworm chrysalis meal.
As invention further embodiment: a kind of preparation method of the skin whitening, moisturizing body lotion of the extract containing acacia, specifically The following steps are included:
A. heating water to temperature is 41 ~ 43 DEG C, is mixed with beating with gumbo and Grape Skin, the condition that merging temperature is 27 ~ 29 DEG C Under 40 ~ 44h of constant-temperature enclosed fermentation, be boiled by slow fire, merging temperature be 36 ~ 38 DEG C under conditions of continue it is constant-temperature enclosed fermentation 56 ~ 64h, filtering, takes filtrate, obtains fermentation liquid;
B. constant temperature 11 ~ 13min of frying in the rotary frying pan for being 65 ~ 69 DEG C by semen sojae atricolor merging temperature, is cooled to 54 ~ 56 DEG C, is added Rice continues 14 ~ 16min of constant temperature frying, is mixed with beating with fermentation liquid, and merging temperature is constant-temperature enclosed hair under conditions of 31 ~ 33 DEG C 52 ~ 58h of ferment is ultrasonically treated 26 ~ 30min under conditions of power is 310 ~ 320W, frequency is 138 ~ 144kHz, is boiled by slow fire, Being placed in temperature is 70 ~ 80h of constant-temperature enclosed fermentation under conditions of 36 ~ 38 DEG C, obtains fermentation slurry;
C. konjac glucomannan, acacia extract, Chinese toon powder, ant powder and dried silkworm chrysalis meal, mild fire are added into fermentation slurry to be heated to temperature and be 88 ~ 92 DEG C and be stirred continuously, constant refrigeration handles 70 ~ 80min under conditions of merging temperature is 0.4 ~ 0.8 DEG C, pressure be 16 ~ 18MPa, temperature are 18 ~ 20min of homogenization under conditions of 41 ~ 43 DEG C, pressure is 39 ~ 41MPa, temperature is 50 ~ 52 DEG C Under the conditions of 26 ~ 30min of homogenization, obtain the skin whitening, moisturizing body lotion of the extract containing acacia;
D. filling, it sterilizes, labelling obtains finished product.
Beneficial effects of the present invention: a kind of skin whitening, moisturizing body lotion of the extract containing acacia provided by the invention is added more Kind green natural raw material carries out processing mating reaction, does not stimulate mildly, does not add chemical addition agent, natural pollution-free, effectively The generation of heavy-metal residual phenomenon is avoided, any side effect will not be caused to human body, formula is scientific and reasonable, can effectively improve original Expect utilization efficiency, effective nutritional ingredients such as vitamin, amino acid, minerals, polysaccharide and flavones rich in, effectively supplement flesh Nutrition needed for skin enhances skin metabolic capability, improves skin oxidation resistance, effectively inhibits the precipitating of melanin and promotes black The decomposition of element, the water lock for enhancing skin protect ability, effectively avoid the generation of the dry and cracked husking phenomenon of skin, effectively supplement collagen egg White, so that skin is smooth beautiful flexible, whitening effect goes to wrinkle, and can form the protective film that strength protection acts in skin surface, To play the role of replenishing water and preserving moisture, improve skin sense, inflammation and allergy can also be adjusted with horn cell acceptor interaction, promoted Into the differentiation of horn cell;Acacia anti-oxidation efficacy ingredient in acacia extract of the invention is comprehensive and low stabilizing active at Point, pigment and volatile aroma oil component content it is high, farthest maintain the color fragrance of robiniae,flos and eliminate acacia The green taste of leaf retains the effective active composition of acacia floral leaf, has inoxidizability strong, the good feature of safety and stability is adopted The body lotion prepared with acacia extract of the invention is safe, without side-effects, newly old applied to that can effectively facilitate cell after skin Metabolism keeps skin elasticity, can improve and skin nutrition, and histiocytic activity and anti-inflammatory and anti-irritant can be improved Property, effective antibacterial is anti-oxidant, there is excellent whitening, moisturizing and senile-resistant efficacy, can effectively delaying skin aging, enable skin Skin reappears gloss and elasticity.
Specific embodiment
Illustrate the present invention with specific embodiment below, but is not limitation of the present invention.
Embodiment 1
In the embodiment of the present invention, a kind of skin whitening, moisturizing body lotion of the extract containing acacia is made of raw material from the following weight: big Rice 36 parts, 20 parts of semen sojae atricolor, 11 parts of gumbo, 26 parts of Grape Skin, 1.9 parts of konjac glucomannan, 0.44 part of acacia extract, Chinese toon powder 0.26 Part, 0.14 part of ant powder, 0.31 part of dried silkworm chrysalis meal, 70 parts of water;
The acacia extract, is prepared according to the following steps:
(1) the fresh robiniae,flos of 23 parts by weight and the fresh acacia leaf co-grinding of 14 parts by weight are beaten, merging temperature is 1.1 DEG C Under the conditions of constant refrigeration handle 21min, take out, magnetic field strength be 360mT under conditions of magnetization treatment 10min, be placed in temperature Constant refrigeration handles 46min under conditions of being 3.3 DEG C, takes out, magnetization treatment 16min under conditions of magnetic field strength is 620mT, Activation slurry must be refrigerated;
(2) the bromelain stirring of cellulase and 0.11 parts by weight that 0.24 parts by weight are added into refrigeration activation slurry is equal Even, merging temperature is enzymolysis processing 230min under conditions of 32 DEG C, and 65 parts by weight, temperature is added and stirs evenly for 49 DEG C of water, Continue mild fire infusion 40min after being boiled by slow fire, filtering obtains infusion liquid and filter residue;
(3) 34 parts by weight, mass fraction are added into filter residue to stir evenly for 51% ethanol solution, is 265W, frequency in power To be ultrasonically treated 15min under conditions of 119kHz, refluxing extraction 40min after ebuillition of heated, filtering takes filtrate, obtains refluxing extraction Liquid;
(4) merge infusion liquid and reflux extracting liquid, continue mild fire infusion 14min after being boiled by slow fire, the condition for being -30 DEG C in temperature Lower vacuum freeze drying, obtains acacia extract.
As invention further embodiment: the Chinese toon powder is prepared according to the following steps: by Chinese toon and its weight 0.5 times of amount, the water that temperature is 38 DEG C are mixed with beating, and constant temperature steam handles 14min under conditions of merging temperature is 112 DEG C, are taken out, It is placed in constant refrigeration under conditions of temperature is 0.7 DEG C and handles 36min, take out, constant temperature dries under conditions of merging temperature is 41 ~ 43 DEG C Roasting 7min is warming up to 75 DEG C of continuation constant temperature baking 11min with the heating rate of 1.9 DEG C/min, takes out, pulverize, obtain Chinese toon Powder.
As invention further embodiment: the ant powder is prepared according to the following steps: by ant and its weight 0.8 times of amount, the ethanol solution that mass fraction is 35% are mixed with beating, and constant temperature steam is handled under conditions of merging temperature is 81 DEG C 11min is warming up to 151 DEG C of continuation constant temperature steam processing 15min with the heating rate of 3.9 DEG C/min, takes out, merging temperature is 93 Constant temperature toasts 28min under conditions of DEG C, takes out, and pulverizes, obtains ant powder.
As invention further embodiment: the dried silkworm chrysalis meal is prepared according to the following steps: by silkworm chrysalis and its weight 1.4 times of amounts, the water that temperature is 55 DEG C are mixed with beating, and are boiled by slow fire, magnetization treatment under conditions of magnetic field strength is 500mT 20min continues mild fire infusion 28min, is spray-dried, and pulverizes, obtains dried silkworm chrysalis meal.
As invention further embodiment: a kind of preparation method of the skin whitening, moisturizing body lotion of the extract containing acacia, specifically The following steps are included:
A. heating water to temperature is 41 DEG C, is mixed with beating with gumbo and Grape Skin, and merging temperature is constant temperature under conditions of 27 DEG C Sealed fermenting 40h, is boiled by slow fire, and merging temperature continues constant-temperature enclosed fermentation 56h under conditions of being 36 DEG C, filters, takes filtrate, obtain Fermentation liquid;
B. constant temperature frying 11min in the rotary frying pan for being 65 DEG C by semen sojae atricolor merging temperature, is cooled to 54 DEG C, and rice is added and continues perseverance Warm frying 14min, is mixed with beating with fermentation liquid, and merging temperature is constant-temperature enclosed fermentation 52h under conditions of 31 DEG C, is in power 310W, frequency are ultrasonically treated 26min under conditions of being 138kHz, are boiled by slow fire, and constant temperature is close under conditions of merging temperature is 36 DEG C Fermentation 70h is closed, fermentation slurry is obtained;
C. konjac glucomannan, acacia extract, Chinese toon powder, ant powder and dried silkworm chrysalis meal, mild fire are added into fermentation slurry to be heated to temperature and be It 88 DEG C and is stirred continuously, constant refrigeration handles 70min under conditions of merging temperature is 0.4 DEG C, pressure is 16MPa, temperature is Homogenization 18min under conditions of 41 DEG C, homogenization 26min under conditions of pressure is 39MPa, temperature is 50 DEG C, must contain The skin whitening, moisturizing body lotion of acacia extract;
D. filling, it sterilizes, labelling obtains finished product.
Embodiment 2
In the embodiment of the present invention, a kind of skin whitening, moisturizing body lotion of the extract containing acacia is made of raw material from the following weight: big Rice 38 parts, 21 parts of semen sojae atricolor, 11.5 parts of gumbo, 27 parts of Grape Skin, 2 parts of konjac glucomannan, 0.46 part of acacia extract, Chinese toon powder 0.27 Part, 0.15 part of ant powder, 0.32 part of dried silkworm chrysalis meal, 75 parts of water;
The acacia extract, is prepared according to the following steps:
(1) the fresh robiniae,flos of 24 parts by weight and the fresh acacia leaf co-grinding of 15 parts by weight are beaten, merging temperature is 1.3 DEG C Under the conditions of constant refrigeration handle 23min, take out, magnetic field strength be 370mT under conditions of magnetization treatment 11min, be placed in temperature Constant refrigeration handles 48min under conditions of being 3.4 DEG C, takes out, magnetization treatment 17min under conditions of magnetic field strength is 630mT, Activation slurry must be refrigerated;
(2) the bromelain stirring of cellulase and 0.12 parts by weight that 0.26 parts by weight are added into refrigeration activation slurry is equal Even, merging temperature is enzymolysis processing 250min under conditions of 33 DEG C, and 70 parts by weight, temperature is added and stirs evenly for 50 DEG C of water, Continue mild fire infusion 45min after being boiled by slow fire, filtering obtains infusion liquid and filter residue;
(3) 36 parts by weight, mass fraction are added into filter residue to stir evenly for 53% ethanol solution, is 270W, frequency in power To be ultrasonically treated 16min under conditions of 122kHz, refluxing extraction 45min after ebuillition of heated, filtering takes filtrate, obtains refluxing extraction Liquid;
(4) merge infusion liquid and reflux extracting liquid, continue mild fire infusion 16min after being boiled by slow fire, the condition for being -28 DEG C in temperature Lower vacuum freeze drying, obtains acacia extract.
As invention further embodiment: the Chinese toon powder is prepared according to the following steps: by Chinese toon and its weight 0.55 times of amount, the water that temperature is 39 DEG C are mixed with beating, and constant temperature steam handles 15min under conditions of merging temperature is 115 DEG C, are taken Out, constant refrigeration handles 38min under conditions of merging temperature is 0.8 DEG C, takes out, and constant temperature dries under conditions of merging temperature is 42 DEG C Roasting 8min is warming up to 76 DEG C of continuation constant temperature baking 12min with the heating rate of 2 DEG C/min, takes out, pulverize, obtain Chinese toon powder.
As invention further embodiment: the ant powder is prepared according to the following steps: by ant and its weight 0.85 times of amount, the ethanol solution that mass fraction is 36% are mixed with beating, and constant temperature steam is handled under conditions of merging temperature is 83 DEG C 12min is warming up to 155 DEG C of continuation constant temperature steam processing 16min with the heating rate of 4.1 DEG C/min, takes out, merging temperature is 95 Constant temperature toasts 30min under conditions of DEG C, takes out, and pulverizes, obtains ant powder.
As invention further embodiment: the dried silkworm chrysalis meal is prepared according to the following steps: by silkworm chrysalis and its weight 1.5 times of amounts, the water that temperature is 57 DEG C are mixed with beating, and are boiled by slow fire, magnetization treatment under conditions of magnetic field strength is 510mT 22min continues mild fire infusion 30min, is spray-dried, and pulverizes, obtains dried silkworm chrysalis meal.
As invention further embodiment: a kind of preparation method of the skin whitening, moisturizing body lotion of the extract containing acacia, specifically The following steps are included:
A. heating water to temperature is 42 DEG C, is mixed with beating with gumbo and Grape Skin, and merging temperature is constant temperature under conditions of 28 DEG C Sealed fermenting 42h, is boiled by slow fire, and merging temperature continues constant-temperature enclosed fermentation 60h under conditions of being 37 DEG C, filters, takes filtrate, obtain Fermentation liquid;
B. constant temperature frying 12min in the rotary frying pan for being 67 DEG C by semen sojae atricolor merging temperature, is cooled to 55 DEG C, and rice is added and continues perseverance Warm frying 15min, is mixed with beating with fermentation liquid, and merging temperature is constant-temperature enclosed fermentation 55h under conditions of 32 DEG C, is in power 315W, frequency are ultrasonically treated 28min under conditions of being 141kHz, are boiled by slow fire, and constant temperature is close under conditions of merging temperature is 37 DEG C Fermentation 75h is closed, fermentation slurry is obtained;
C. konjac glucomannan, acacia extract, Chinese toon powder, ant powder and dried silkworm chrysalis meal, mild fire are added into fermentation slurry to be heated to temperature and be It 90 DEG C and is stirred continuously, constant refrigeration handles 75min under conditions of merging temperature is 0.6 DEG C, pressure is 17MPa, temperature is Homogenization 19min under conditions of 42 DEG C, homogenization 28min under conditions of pressure is 40MPa, temperature is 51 DEG C, must contain The skin whitening, moisturizing body lotion of acacia extract;
D. filling, it sterilizes, labelling obtains finished product.
Embodiment 3
In the embodiment of the present invention, a kind of skin whitening, moisturizing body lotion of the extract containing acacia is made of raw material from the following weight: big Rice 38 parts, 22 parts of semen sojae atricolor, 12 parts of gumbo, 28 parts of Grape Skin, 2.1 parts of konjac glucomannan, 0.48 part of acacia extract, Chinese toon powder 0.28 Part, 0.16 part of ant powder, 0.33 part of dried silkworm chrysalis meal, 80 parts of water;
The acacia extract, is prepared according to the following steps:
(1) the fresh robiniae,flos of 25 parts by weight and the fresh acacia leaf co-grinding of 16 parts by weight are beaten, merging temperature is 1.5 DEG C Under the conditions of constant refrigeration handle 25min, take out, magnetic field strength be 380mT under conditions of magnetization treatment 12min, be placed in temperature Constant refrigeration handles 50min under conditions of being 3.5 DEG C, takes out, magnetization treatment 18min under conditions of magnetic field strength is 640mT, Activation slurry must be refrigerated;
(2) the bromelain stirring of cellulase and 0.13 parts by weight that 0.28 parts by weight are added into refrigeration activation slurry is equal Even, merging temperature is enzymolysis processing 270min under conditions of 34 DEG C, and 75 parts by weight, temperature is added and stirs evenly for 51 DEG C of water, Continue mild fire infusion 50min after being boiled by slow fire, filtering obtains infusion liquid and filter residue;
(3) 38 parts by weight, mass fraction are added into filter residue to stir evenly for 55% ethanol solution, is 275W, frequency in power To be ultrasonically treated 17min under conditions of 125kHz, refluxing extraction 50min after ebuillition of heated, filtering takes filtrate, obtains refluxing extraction Liquid;
(4) merge infusion liquid and reflux extracting liquid, continue mild fire infusion 18min after being boiled by slow fire, the condition for being -26 DEG C in temperature Lower vacuum freeze drying, obtains acacia extract.
As invention further embodiment: the Chinese toon powder is prepared according to the following steps: by Chinese toon and its weight 0.6 times of amount, the water that temperature is 40 DEG C are mixed with beating, and constant temperature steam handles 16min under conditions of merging temperature is 118 DEG C, are taken out, It is placed in constant refrigeration under conditions of temperature is 0.9 DEG C and handles 40min, take out, constant temperature toasts under conditions of merging temperature is 43 DEG C 9min is warming up to 77 DEG C of continuation constant temperature baking 13min with the heating rate of 2.1 DEG C/min, takes out, pulverize, obtain Chinese toon powder.
As invention further embodiment: the ant powder is prepared according to the following steps: by ant and its weight 0.9 times of amount, the ethanol solution that mass fraction is 37% are mixed with beating, and constant temperature steam is handled under conditions of merging temperature is 85 DEG C 13min is warming up to 159 DEG C of continuation constant temperature steam processing 17min with the heating rate of 4.3 DEG C/min, takes out, merging temperature is 97 Constant temperature toasts 32min under conditions of DEG C, takes out, and pulverizes, obtains ant powder.
As invention further embodiment: the dried silkworm chrysalis meal is prepared according to the following steps: by silkworm chrysalis and its weight 1.6 times of amounts, the water that temperature is 59 DEG C are mixed with beating, and are boiled by slow fire, magnetization treatment under conditions of magnetic field strength is 520mT 24min continues mild fire infusion 32min, is spray-dried, and pulverizes, obtains dried silkworm chrysalis meal.
As invention further embodiment: a kind of preparation method of the skin whitening, moisturizing body lotion of the extract containing acacia, specifically The following steps are included:
A. heating water to temperature is 43 DEG C, is mixed with beating with gumbo and Grape Skin, and merging temperature is constant temperature under conditions of 29 DEG C Sealed fermenting 44h, is boiled by slow fire, and merging temperature continues constant-temperature enclosed fermentation 64h under conditions of being 38 DEG C, filters, takes filtrate, obtain Fermentation liquid;
B. constant temperature frying 13min in the rotary frying pan for being 69 DEG C by semen sojae atricolor merging temperature, is cooled to 56 DEG C, and rice is added and continues perseverance Warm frying 16min, is mixed with beating with fermentation liquid, and merging temperature is constant-temperature enclosed fermentation 58h under conditions of 33 DEG C, is in power 320W, frequency are ultrasonically treated 30min under conditions of being 144kHz, are boiled by slow fire, and constant temperature is close under conditions of merging temperature is 38 DEG C Fermentation 80h is closed, fermentation slurry is obtained;
C. konjac glucomannan, acacia extract, Chinese toon powder, ant powder and dried silkworm chrysalis meal, mild fire are added into fermentation slurry to be heated to temperature and be It 92 DEG C and is stirred continuously, constant refrigeration handles 80min under conditions of merging temperature is 0.8 DEG C, pressure is 18MPa, temperature is Homogenization 20min under conditions of 43 DEG C, homogenization 30min under conditions of pressure is 41MPa, temperature is 52 DEG C, must contain The skin whitening, moisturizing body lotion of acacia extract;
D. filling, it sterilizes, labelling obtains finished product.
Comparative example 1
A kind of skin whitening, moisturizing body lotion of the extract containing acacia, the difference from embodiment 1 is that, gumbo and perfume (or spice) are added without in raw material Chinese toon powder, other conditions are all the same.
Comparative example 2
A kind of skin whitening, moisturizing body lotion of the extract containing acacia, the difference from embodiment 1 is that, be added without in raw material Grape Skin, Ant powder and dried silkworm chrysalis meal, other conditions are all the same.
Comparative example 3
A kind of skin whitening, moisturizing body lotion of the extract containing acacia, the difference from embodiment 1 is that, acacia extraction is added without in raw material Object, other conditions are all the same.
Comparative example 4
A kind of skin whitening, moisturizing body lotion of the extract containing acacia, the difference from embodiment 1 is that, the preparation of the acacia extract The refrigeration without step (1) and magnetization treatment, other conditions are all the same in the process.
Comparative example 5
A kind of skin whitening, moisturizing body lotion of the extract containing acacia, the difference from embodiment 1 is that, the preparation of the acacia extract The processing without step (2), other conditions are all the same in the process.
Comparative example 6
Commercially available common body lotion, such as Johnson & Johnson's milky lotion
Experiment 1
Irritation and anaphylaxis experiment
Small white mouse back cuts off hair, smears body lotion by embodiment and comparative example respectively in cutting plucked position, and no painting portion Position is compared, as a result without irritation and allergic reaction;
Each 1 gram of the body lotion of Example and comparative example is applied in volunteer (18 ~ 60 years old, 90 people, every group of 10 people) gesture and facial expression, crosses 30 It is observed after minute, does not occur rubescent, dermexanthesis, foaming phenomena.
Experiment 2
The skin whitening, moisturizing body lotion whitening effect of embodiment and comparative example extract containing acacia detects
Radicals scavenging effect experiment: taking 1g embodiment and comparative example body lotion respectively, and respectively plus distilled water 100mL, dilution are standby With;Each group body lotion dilution 2mL is measured respectively and concentration is 100 μm of ol/L diphenyl picryl phenylhydrazine (DPPH) solution 2mL, first After be added in same tool plug test tube and shake up, be allowed to stand at room temperature for 30 minutes, the absorbance of sample, suppression measured under 517nm wavelength Rate processed: K%=[1- (Ai-Aj)/Ac] × 100%, Ai is the absorbance of DPPH solution and body lotion dilution, and Aj is that body lotion is dilute The absorbance of liquid and solvent is released, Ac is the absorbance of DPPH solution and solvent;
Inhibit mouse melanin cell in tyrosinase viability experiment: take 1g embodiment and comparative example body lotion respectively, respectively plus Distilled water 100mL dilutes spare;By B16Melanocyte is inoculated in 96 orifice plates, every 100 μ L of hole, and it is small to set incubator cultivation 24 When after add body lotion dilution, discard supernatant liquid after 3 days, rinsed twice with PBS, then every hole adds the 90 μ L to be containing volume fraction The PBS of 1% Triton X-100, the ultrasonication in ice bath, every 10 μ L 10mmol/L levodopa of Kong Zaijia, at 37 DEG C It is incubated for 60 minutes, the colorimetric in 475nm at, zeroing at blank well, surveys each hole absorbance value, inhibiting rate K%=(1- medicine group is averagely inhaled Shading value ÷ control group mean absorbance values) × 100%;
Inhibit mouse melanin cell melanin compound experiment: taking 1g embodiment and comparative example body lotion respectively, respectively plus distills Water 100mL dilutes spare;By the B from mouse16Melanocyte is with 1 × 105The density of a/mL is inoculated in culture dish, 37 DEG C, contain 5%CO2Under conditions of cultivate 2 days, discard supernatant liquid, add body lotion dilution, abandon supernatant after 3 days, washed with PBS It washs, every hole addition 0.5mL pancreatin, vitellophag 3 minutes, then 2mL maintaining liquid is added in every hole and terminates digestion, after piping and druming mixing, It takes out 0.5mL and does cell count, remaining cell suspension is centrifuged 5 minutes under the conditions of 2500 revs/min, discards supernatant liquid, Yu Chen NaOH solution is added in shallow lake, heating dissolves melanin, under 490nm wavelength, surveys absorbance using enzyme-linked immunosorbent assay instrument, black Pigment synthesis inhibiting rate K%=[1- (drug hole absorbance value ÷ drug hole cell density) ÷ (control wells absorbance value ÷ control wells Cell density)] × 100%;
Table 1
As it can be seen from table 1 the skin whitening, moisturizing body lotion whitening effect of present invention extract containing acacia is significant, and it is substantially better than pair Ratio.
Experiment 3
The skin whitening, moisturizing body lotion moistening effect of embodiment and comparative example extract containing acacia detects
The test of keratoderma water content
Experimental basis: QB/T 4256-2011 " cosmetics moisture-keeping efficacy evaluation guide "
Test method: it selects the age for 40 years old or so 90 people of women, is equally divided into 9 groups, every group of 10 people smear the body of corresponding group Body cream;
Recipient site: double inner forearms mark recipient site at symmetrical two, are randomly assigned as the area Tu Yang and check plot, painting sample Tested material is smeared in area, and check plot does not smear any product;
Product smears dosage: application area: 5cm × 5cm, smears dosage: 5mg/cm2
Test index: keratoderma water content (test environment: temperature: 20 DEG C, relative humidity: 30% ~ 35%);
Test procedure: subject sits quietly after 20min, (T0) keratoderma water content before test recipient site sample is smeared, so Tested material is smeared by prescribed dose afterwards, the area Tu Yang smears 2 hours, 4 hours, 8 hours, 16 hours after tested material, tests tested portion Position keratoderma water content;Test before with dry paper handkerchief wiping removal the remaining product of skin surface (smearing sample before and blank Compare position skin test before also with dry paper handkerchief scrape skin twice);During test, subject's forearm exposure, in test shape State is placed, and keeps loosening;
Table 2
From table 2 it can be seen that the skin whitening, moisturizing body lotion moistening effect of present invention extract containing acacia is significant, and it is substantially better than pair Ratio.

Claims (5)

1. a kind of skin whitening, moisturizing body lotion of extract containing acacia, which is characterized in that be made of raw material from the following weight: rice 36 ~ 38 parts, 20 ~ 22 parts of semen sojae atricolor, 11 ~ 12 parts of gumbo, 26 ~ 28 parts of Grape Skin, 1.9 ~ 2.1 parts of konjac glucomannan, acacia extract 0.44 ~ 0.48 part, 0.26 ~ 0.28 part of Chinese toon powder, 0.14 ~ 0.16 part of ant powder, 0.31 ~ 0.33 part of dried silkworm chrysalis meal, 70 ~ 80 parts of water;
The acacia extract, is prepared according to the following steps:
(1) the fresh robiniae,flos of 23 ~ 25 parts by weight and the fresh acacia leaf co-grinding of 14 ~ 16 parts by weight are beaten, merging temperature is Constant refrigeration handles 21 ~ 25min under conditions of 1.1 ~ 1.5 DEG C, takes out, and magnetizes under conditions of magnetic field strength is 360 ~ 380mT 10 ~ 12min is handled, constant refrigeration handles 46 ~ 50min under conditions of merging temperature is 3.3 ~ 3.5 DEG C, takes out, in magnetic field strength For 16 ~ 18min of magnetization treatment under conditions of 620 ~ 640mT, activation slurry must be refrigerated;
(2) cellulase of 0.24 ~ 0.28 parts by weight and the bromelain of 0.11 ~ 0.13 parts by weight is added into refrigeration activation slurry Enzyme stirs evenly, and merging temperature is 230 ~ 270min of enzymolysis processing under conditions of 32 ~ 34 DEG C, 65 ~ 75 parts by weight is added, temperature is 49 ~ 51 DEG C of water stirs evenly, and continues 40 ~ 50min of mild fire infusion after being boiled by slow fire, and filtering obtains infusion liquid and filter residue;
(3) 34 ~ 38 parts by weight, mass fraction are added into filter residue to stir evenly for 51% ~ 55% ethanol solution, are in power 265 ~ 275W, frequency are ultrasonically treated 15 ~ 17min, 40 ~ 50min of refluxing extraction after ebuillition of heated under conditions of being 119 ~ 125kHz, Filtering, takes filtrate, obtains reflux extracting liquid;
(4) merge infusion liquid and reflux extracting liquid, continue 14 ~ 18min of mild fire infusion after being boiled by slow fire, be -30 ~ -26 in temperature Vacuum freeze drying under conditions of DEG C obtains acacia extract.
2. the skin whitening, moisturizing body lotion of the extract according to claim 1 containing acacia, which is characterized in that the Chinese toon Powder is prepared according to the following steps: Chinese toon and 0.5 ~ 0.6 times of its weight amount, the water that temperature is 38 ~ 40 DEG C being mixed with beating, set Enter constant temperature steam under conditions of temperature is 112 ~ 118 DEG C and handle 14 ~ 16min, takes out, the condition that merging temperature is 0.7 ~ 0.9 DEG C Lower constant refrigeration handles 36 ~ 40min, takes out, and constant temperature toasts 7 ~ 9min under conditions of merging temperature is 41 ~ 43 DEG C, with 1.9 ~ 2.1 DEG C/heating rate of min is warming up to 75 ~ 77 DEG C of continuation constant temperature and toasts 11 ~ 13min, it takes out, pulverizes, obtain Chinese toon powder.
3. the skin whitening, moisturizing body lotion of the extract according to claim 1 containing acacia, which is characterized in that the ant Powder is prepared according to the following steps: ant and 0.8 ~ 0.9 times of its weight amount, the ethanol solution that mass fraction is 35% ~ 37% are mixed Mashing is closed, constant temperature steam handles 11 ~ 13min under conditions of merging temperature is 81 ~ 85 DEG C, with the heating speed of 3.9 ~ 4.3 DEG C/min Rate is warming up to 151 ~ 159 DEG C of continuation constant temperature steams and handles 15 ~ 17min, takes out, and merging temperature is constant temperature under conditions of 93 ~ 97 DEG C 28 ~ 32min is toasted, is taken out, pulverizes, obtains ant powder.
4. the skin whitening, moisturizing body lotion of the extract according to claim 1 containing acacia, which is characterized in that the silkworm chrysalis Powder is prepared according to the following steps: silkworm chrysalis and 1.4 ~ 1.6 times of its weight amounts, the water that temperature is 55 ~ 59 DEG C being mixed with beating, text Fire boils, 20 ~ 24min of magnetization treatment under conditions of magnetic field strength is 500 ~ 520mT, continues 28 ~ 32min of mild fire infusion, spray Mist is dry, pulverizes, obtains dried silkworm chrysalis meal.
5. the preparation method of the skin whitening, moisturizing body lotion of described in any item extracts containing acacia according to claim 1 ~ 4, special Sign is, specifically includes the following steps:
A. heating water to temperature is 41 ~ 43 DEG C, is mixed with beating with gumbo and Grape Skin, the condition that merging temperature is 27 ~ 29 DEG C Under 40 ~ 44h of constant-temperature enclosed fermentation, be boiled by slow fire, merging temperature be 36 ~ 38 DEG C under conditions of continue it is constant-temperature enclosed fermentation 56 ~ 64h, filtering, takes filtrate, obtains fermentation liquid;
B. constant temperature 11 ~ 13min of frying in the rotary frying pan for being 65 ~ 69 DEG C by semen sojae atricolor merging temperature, is cooled to 54 ~ 56 DEG C, is added Rice continues 14 ~ 16min of constant temperature frying, is mixed with beating with fermentation liquid, and merging temperature is constant-temperature enclosed hair under conditions of 31 ~ 33 DEG C 52 ~ 58h of ferment is ultrasonically treated 26 ~ 30min under conditions of power is 310 ~ 320W, frequency is 138 ~ 144kHz, is boiled by slow fire, Being placed in temperature is 70 ~ 80h of constant-temperature enclosed fermentation under conditions of 36 ~ 38 DEG C, obtains fermentation slurry;
C. konjac glucomannan, acacia extract, Chinese toon powder, ant powder and dried silkworm chrysalis meal, mild fire are added into fermentation slurry to be heated to temperature and be 88 ~ 92 DEG C and be stirred continuously, constant refrigeration handles 70 ~ 80min under conditions of merging temperature is 0.4 ~ 0.8 DEG C, pressure be 16 ~ 18MPa, temperature are 18 ~ 20min of homogenization under conditions of 41 ~ 43 DEG C, pressure is 39 ~ 41MPa, temperature is 50 ~ 52 DEG C Under the conditions of 26 ~ 30min of homogenization, obtain the skin whitening, moisturizing body lotion of the extract containing acacia;
D. filling, it sterilizes, labelling obtains finished product.
CN201811253948.2A 2018-10-26 2018-10-26 A kind of skin whitening, moisturizing body lotion of the extract containing acacia Pending CN108938512A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102210643A (en) * 2010-04-06 2011-10-12 保罗生物园科技股份有限公司 Anti-wrinkle cosmetic composition and preparation method thereof
CN104473834A (en) * 2014-11-19 2015-04-01 哈尔滨医科大学 Application of ant extract as effective component in preparation of cosmetics
CN105029603A (en) * 2015-06-24 2015-11-11 陈琳仁 Composite fresh flower, fruit, vegetable and herb enzyme, and preparation method and application thereof
CN107496295A (en) * 2017-09-12 2017-12-22 陈德兴 Anti-acne ferment facemask powder and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102210643A (en) * 2010-04-06 2011-10-12 保罗生物园科技股份有限公司 Anti-wrinkle cosmetic composition and preparation method thereof
CN104473834A (en) * 2014-11-19 2015-04-01 哈尔滨医科大学 Application of ant extract as effective component in preparation of cosmetics
CN105029603A (en) * 2015-06-24 2015-11-11 陈琳仁 Composite fresh flower, fruit, vegetable and herb enzyme, and preparation method and application thereof
CN107496295A (en) * 2017-09-12 2017-12-22 陈德兴 Anti-acne ferment facemask powder and preparation method thereof

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Application publication date: 20181207