CN109646381A - A kind of moisturizing lotion and preparation method thereof added with plant extracts - Google Patents
A kind of moisturizing lotion and preparation method thereof added with plant extracts Download PDFInfo
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- CN109646381A CN109646381A CN201910165268.3A CN201910165268A CN109646381A CN 109646381 A CN109646381 A CN 109646381A CN 201910165268 A CN201910165268 A CN 201910165268A CN 109646381 A CN109646381 A CN 109646381A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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Abstract
The invention discloses a kind of moisturizing lotion and preparation method thereof added with plant extracts.The raw material of the moisturizing lotion is made of Wild hedge rose fruit extract, monkey-bread tree pulp extract, orchid extract, cetostearyl alcohol ethylhexoate, isopropyl palmitate, epidermal growth factor, stereth -21 etc..The preparation method of the moisturizing lotion added with plant extracts is specifically that the first mixture is made through homogeneous, heating stirring in cetostearyl alcohol, trehalose etc., adding cetostearyl alcohol ethylhexoate, isopropyl palmitate etc., vacuum homogeneous obtains the second mixture in a heated condition, then stand heat preservation, be placed in emulsion pot again and epidermal growth factor be added stage by stage, Wild hedge rose fruit extract obtains final mixture, be eventually adding additive and stir to get finished emulsion.The moisturizing lotion added with plant extracts has good soothing effect, and has no toxic side effect, and has preferable application prospect in face skin nursing.
Description
Technical field
The present invention relates to cosmetic technical field, more particularly to a kind of moisturizing lotion added with plant extracts and its
Preparation method.
Background technique
Skin is made of epidermis, corium and subcutaneous tissue three parts.Epidermis is direct and extraneous contact part,
It and is the part for having most deep relationship with cosmetics.Epidermal thickness is only 0.2 millimeter, is to be piled up to constitute by horn cell
's.On the inside of skin, epidermis can be divided into basal layer, spinosity layer, stratum granulosum and cuticula again.The metabolism of skin is
It is constantly divided by the horn cell of basal layer, about 28 day period is one bout.Cuticula has moisturizing moisture
Function and the barrier function that skin internal moisture is volatilized and external foreign matter immerses is prevented, it is the natural moisturizing factor of cuticula, thin
Intercellular lipid, sodium hyaluronate largely reduce, and skin just will appear a series of problems, such as dry, coarse, decortication.Lotion is a kind of
Liquid frost class cosmetics are lotion because seeming pure white such as milk.Lotion is exactly as skin care item, maximum feature
Water content is very high, can be kept the skin wet with moment moisturizing for dry skin.In addition lotion can be formed in skin surface it is frivolous
Ventilative protective film can prevent water loss, play splendid moistening effect.Therefore the makeup water phase with simple moisturizing type
Than lotion is more suitable for using in dry season.Lotion has good moisturizing effect, also there is moistening effect, is particularly suitable for drying
Spring, use in two season of autumn, if skin be it is neutral, can also be with use in winter.Spring and autumn is in use, in addition to skin-moistening effect
Outside, extraneous dry weather can also be isolated, prevent skin moisture to be lost too fast, avoid skin dry and cracked, peeling is dry season
The skin care item of outgoing Shi Biyong.Lotion is various in style currently on the market, vdiverse in function, however but there are many problems.Some profits
Skin lotion all contains a large amount of lead substance, if skin has breakage, these harmful lead substances will pass through when smearing
Capillary of skin enters blood tissues, causes lead poisoning, influences nerve and immune system.Therefore from natural plant extracts
Angle develops the moisturizing lotion that new toxic side effect is small and effect is good and is just of great significance.
Summary of the invention
The problem of not being able to satisfy consumer demand still based on current moisturizing lotion, the present invention are provided one kind and mentioned added with plant
Take the moisturizing lotion and preparation method thereof of object.
A kind of moisturizing lotion added with plant extracts, the raw material of the moisturizing lotion by mass percentage, form
It is as follows:
Wild hedge rose fruit extract 2.5~3.5%
Monkey-bread tree pulp extract 0.8~1.6%
Orchid extract 0.5~1.5%
Cetostearyl alcohol 4.8~5.2%
Trehalose 1.8~3.8%
Glycerol 8.5~9.5%
Cetostearyl alcohol ethylhexoate 3.5~5.5%
Isopropyl palmitate 2.5~5.5%
Niacinamide 2.5~3.5%
Epidermal growth factor 1.6~1.8%
Stereth -210.12~0.18%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
The above-mentioned moisturizing lotion added with plant extracts contain Wild hedge rose fruit extract, monkey-bread tree pulp extract,
The functional components such as orchid extract, epidermal growth factor, trehalose, each functional components are possessed basic except itself is played
Other than effect, synergistic function is also unexpectedly shown, human endocrine and function can be adjusted from body metabolism level,
Fundamentally play the beautification function of moisturizing skin care.The moisturizing lotion has good soothing effect, the people suitable for dry skin
Group uses.
The Wild hedge rose fruit extract, monkey-bread tree pulp extract and orchid extract in one of the embodiments,
The preparation method comprises the following steps:
Wild hedge rose fruit, monkey-bread tree pulp and orchid are crushed respectively, are sieved, being added to weight is 30 times, volumetric concentration
For in 70~80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes and clears
The heart, filtering, then by filtrate vacuum degree be -0.08MPa under conditions of rotary evaporation, extract concentrated solution is obtained, most afterwards through cold
Jelly is dried to obtain Wild hedge rose fruit extract, monkey-bread tree pulp extract and orchid extract.
The raw material of the moisturizing lotion by mass percentage, forms as follows in one of the embodiments:
Wild hedge rose fruit extract 3.0%
Monkey-bread tree pulp extract 1.2%
Orchid extract 1.0%
Cetostearyl alcohol 5.0%
Trehalose 2.8%
Glycerol 9.0%
Cetostearyl alcohol ethylhexoate 4.5%
Isopropyl palmitate 4.0%
Niacinamide 3.0%
Epidermal growth factor 1.7%
Stereth -210.15%
Essence 0.02%
Antioxidant 0.04%
Preservative 0.15%
Deionized water surplus.
The essence is any one in ginger extrait, flavoring rose essence, lavender oil in one of the embodiments,
Kind.
The antioxidant is selected from butylated hydroxy anisole, allantoin, hydroxypropyl tetrahydro pyrrole in one of the embodiments,
Any one muttered in triol.
Any one of the preservative in Nipasol, sorbic acid, triclosan in one of the embodiments,.
The present invention also provides the preparation methods of the above-mentioned moisturizing lotion added with plant extracts, by following steps group
At:
(1) cetostearyl alcohol, trehalose, glycerol, stereth -21 are added into deionized water, according to 2000~
3000 revs/min of rate is stirred homogeneous 10~20 minutes, and mixed liquor is then warming up to 75~80 DEG C, according to 1200~
1500 revs/min of rate stirs 20~30 minutes, obtains the first mixture；
(2) cetostearyl alcohol ethylhexoate, isopropyl palmitate, niacinamide are added step (1) resulting first and mixed
It closes in object, continues to heat mixed liquor to 88~92 DEG C, the rate according to 1600~1800 revs/min is equal again under vacuum conditions
Matter 8~12 minutes, obtain the second mixture；
(3) the second mixture for obtaining step (2) stands heat preservation 30~40 minutes, is subsequently placed in emulsion pot, and to
Epidermal growth factor is added in emulsion pot, is stirred 10~15 minutes according to 2200~2400 revs/min of rates, liquid temperature to be mixed
When degree is down to 65~70 DEG C, Wild hedge rose fruit extract, monkey-bread tree pulp extract, orchid extract are added into emulsion pot,
It is stirred 8~10 minutes according to 1500~1700 revs/min of rates, obtains final mixture；
(4) after the final mixture that step (3) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 15~25 minutes according to 100~120 revs/min of rates, finished emulsion is obtained after discharging.
The preparation method of the above-mentioned moisturizing lotion added with plant extracts, process conditions are mild, controllability is strong, product matter
Amount is stablized, production cost economy, is suitable for large-scale production.
Homogeneous is carried out under the vacuum condition of -0.08~-0.1MPa in the step (2) in one of the embodiments,.
The present invention also provides application of the moisturizing lotion added with plant extracts in face skin nursing.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below in conjunction with specific embodiment,
The present invention will be described in further detail.It should be appreciated that the specific embodiments described herein are only used to explain this hair
It is bright, it is not intended to limit the present invention.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention
The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool
The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more
Any and all combinations of relevant listed item.
Raw materials used and reagent is commercially available common raw material and reagent in following embodiment.
A kind of moisturizing lotion added with plant extracts, the raw material of the moisturizing lotion by mass percentage, form
It is as follows:
Wild hedge rose fruit extract 2.5~3.5%
Monkey-bread tree pulp extract 0.8~1.6%
Orchid extract 0.5~1.5%
Cetostearyl alcohol 4.8~5.2%
Trehalose 1.8~3.8%
Glycerol 8.5~9.5%
Cetostearyl alcohol ethylhexoate 3.5~5.5%
Isopropyl palmitate 2.5~5.5%
Niacinamide 2.5~3.5%
Epidermal growth factor 1.6~1.8%
Stereth -210.12~0.18%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
Wherein, Wild hedge rose fruit is rich in skin nutrition ingredient abundant, specifically for aging, tired relaxation, dry water shortage and
It needs the skin of maintenance and designs, can nourish and motivate skin, allow skin recovery water to be full of glossy, health is plump.
Wherein, monkey-bread tree pulp extract contains a variety of constants of vitamin C, calcium, iron, potassium, magnesium and trace active ingredient.
Monkey-bread tree pulp extract has potent antioxidation, has anti-inflammatory, antibacterial characteristics, is applied in cosmetics,
With moistening effect, antioxidation and increase skin elasticity effect.
Wherein, orchid extract has antioxidant activity, can remove the active oxygen of harmful skin, helps skin to carry out new
Old metabolism restores the health of skin.
Wherein, epidermal growth factor is a kind of small molecular protein being made of 53 amino acid, and it is dynamic to be widely present in lactation
In object, there is extensive promotion cells growth activity.It can be such that the speed of growth of human skin cell accelerates, and how much is content
The quantity of skin neoblast growth and breeding is directly affected, to decide the young healthy degree of skin.
Wherein, trehalose is also known as Yeast sugar, is to be gone back as two α-D glucose molecules by non-made of hemiacetal group condensation
Originality disaccharide is a kind of safe and reliable natural carbohydrate, is also to maintain the important component of cell activity, moisturizing class cosmetics.Sea
Application of the algae sugar on cosmetics is based on it with excellent holding cell viability and the active characteristic of large biological molecule.Skin
Cell, especially epidermal cell easily dry out and cutin occur under the environment such as high temperature, high and cold, dry, intensive ultraviolet radiation
Change or even death fall off and make skin damage.Trehalose can form one layer of special protection in cell surface in this case
Film, the mucus being precipitated from film not only moisten Skin Cell, also have the function of radiateing external heat, to protect
Sheath skin will not be damaged.A large amount of research with practice have shown that, trehalose can be effectively protected epidermal cell membrane structure, and activation is thin
Born of the same parents improve skin, enable skin health natural, flexible.
The above-mentioned moisturizing lotion added with plant extracts contain Wild hedge rose fruit extract, monkey-bread tree pulp extract,
The functional components such as orchid extract, epidermal growth factor, trehalose, each functional components are possessed basic except itself is played
Other than effect, synergistic function is also unexpectedly shown, human endocrine and function can be adjusted from body metabolism level,
Fundamentally play the beautification function of moisturizing skin care.The moisturizing lotion has good soothing effect, the people suitable for dry skin
Group uses.
In a preferred embodiment, the Wild hedge rose fruit extract, monkey-bread tree pulp extract and orchid are extracted
Object the preparation method comprises the following steps:
Wild hedge rose fruit, monkey-bread tree pulp and orchid are crushed respectively, are sieved, being added to weight is 30 times, volumetric concentration
For in 70~80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes and clears
The heart, filtering, then by filtrate vacuum degree be -0.08MPa under conditions of rotary evaporation, extract concentrated solution is obtained, most afterwards through cold
Jelly is dried to obtain Wild hedge rose fruit extract, monkey-bread tree pulp extract and orchid extract.
In a preferred embodiment, the raw material of the moisturizing lotion by mass percentage, forms as follows:
Wild hedge rose fruit extract 3.0%
Monkey-bread tree pulp extract 1.2%
Orchid extract 1.0%
Cetostearyl alcohol 5.0%
Trehalose 2.8%
Glycerol 9.0%
Cetostearyl alcohol ethylhexoate 4.5%
Isopropyl palmitate 4.0%
Niacinamide 3.0%
Epidermal growth factor 1.7%
Stereth -210.15%
Essence 0.02%
Antioxidant 0.04%
Preservative 0.15%
Deionized water surplus.
In a preferred embodiment, the essence is any in ginger extrait, flavoring rose essence, lavender oil
It is a kind of.
In a preferred embodiment, the antioxidant is selected from butylated hydroxy anisole, allantoin, hydroxypropyl tetrahydro
Any one in pyrans triol.
In a preferred embodiment, the preservative is any one in Nipasol, sorbic acid, triclosan
Kind.
The present invention also provides the preparation methods of the above-mentioned moisturizing lotion added with plant extracts, by following steps group
At:
(1) cetostearyl alcohol, trehalose, glycerol, stereth -21 are added into deionized water, according to 2000~
3000 revs/min of rate is stirred homogeneous 10~20 minutes, and mixed liquor is then warming up to 75~80 DEG C, according to 1200~
1500 revs/min of rate stirs 20~30 minutes, obtains the first mixture；
(2) cetostearyl alcohol ethylhexoate, isopropyl palmitate, niacinamide are added step (1) resulting first and mixed
It closes in object, continues to heat mixed liquor to 88~92 DEG C, the rate according to 1600~1800 revs/min is equal again under vacuum conditions
Matter 8~12 minutes, obtain the second mixture；
(3) the second mixture for obtaining step (2) stands heat preservation 30~40 minutes, is subsequently placed in emulsion pot, and to
Epidermal growth factor is added in emulsion pot, is stirred 10~15 minutes according to 2200~2400 revs/min of rates, liquid temperature to be mixed
When degree is down to 65~70 DEG C, Wild hedge rose fruit extract, monkey-bread tree pulp extract, orchid extract are added into emulsion pot,
It is stirred 8~10 minutes according to 1500~1700 revs/min of rates, obtains final mixture；
(4) after the final mixture that step (3) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 15~25 minutes according to 100~120 revs/min of rates, finished emulsion is obtained after discharging.
In a preferred embodiment, it is carried out under the vacuum condition of -0.08~-0.1MPa in the step (2) equal
Matter.
The present invention also provides application of the above-mentioned moisturizing lotion added with plant extracts in face skin nursing.
Below by embodiment, the present invention is furture elucidated.It should be pointed out that the present invention is not intended to be limited to the reality
Apply example.
Embodiment 1
The moisturizing lotion formula added with plant extracts of the present embodiment is as follows:
Wild hedge rose fruit extract 2.5%
Monkey-bread tree pulp extract 0.8%
Orchid extract 0.5%
Cetostearyl alcohol 4.8%
Trehalose 1.8%
Glycerol 8.5%
Cetostearyl alcohol ethylhexoate 3.5%
Isopropyl palmitate 2.5%
Niacinamide 2.5%
Epidermal growth factor 1.6%
Stereth -210.12%
Essence 0.01%
Antioxidant 0.02%
Preservative 0.1%
Deionized water surplus.
The moisturizing lotion added with plant extracts of the present embodiment is prepared as follows:
(1) Wild hedge rose fruit, monkey-bread tree pulp and orchid are crushed respectively, is sieved, being added to weight is 30 times, volume
In the ethanol solution that concentration is 70%, ultrasonic extraction 4 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Wild hedge rose fruit extract, monkey-bread tree pulp extract and orchid extract
(2) by cetostearyl alcohol, trehalose, glycerol, stereth -21 be added into deionized water, according to 2000 turns/
The rate of minute is stirred homogeneous 10 minutes, and mixed liquor is then warming up to 75 DEG C, stirs according to 1200 revs/min of rates
20 minutes, obtain the first mixture；
(3) cetostearyl alcohol ethylhexoate, isopropyl palmitate, niacinamide are added step (2) resulting first and mixed
It closes in object, continues to heat mixed liquor to 88 DEG C, the rate under the vacuum condition of -0.08MPa according to 1600 revs/min is equal again
Matter 8 minutes, obtain the second mixture；
(4) the second mixture obtained step (3) stands heat preservation 30 minutes, is subsequently placed in emulsion pot, and to emulsification
Epidermal growth factor is added in pot, is stirred 10 minutes according to 2200 revs/min of rates, when liquid temperature to be mixed is down to 65 DEG C,
Wild hedge rose fruit extract, monkey-bread tree pulp extract, orchid extract are added into emulsion pot, according to 1500 revs/min
Rate stirs 8 minutes, obtains final mixture；
(5) after the final mixture that step (4) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 15 minutes according to 100 revs/min of rates, finished emulsion is obtained after discharging, is denoted as S1.
Embodiment 2
The moisturizing lotion formula added with plant extracts of the present embodiment is as follows:
Wild hedge rose fruit extract 3.0%
Monkey-bread tree pulp extract 1.2%
Orchid extract 1.0%
Cetostearyl alcohol 5.0%
Trehalose 2.8%
Glycerol 9.0%
Cetostearyl alcohol ethylhexoate 4.5%
Isopropyl palmitate 4.0%
Niacinamide 3.0%
Epidermal growth factor 1.7%
Stereth -210.15%
Essence 0.02%
Antioxidant 0.04%
Preservative 0.15%
Deionized water surplus.
The moisturizing lotion added with plant extracts of the present embodiment is prepared as follows:
(1) Wild hedge rose fruit, monkey-bread tree pulp and orchid are crushed respectively, is sieved, being added to weight is 30 times, volume
In the ethanol solution that concentration is 70%, ultrasonic extraction 4 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Wild hedge rose fruit extract, monkey-bread tree pulp extract and orchid extract
(2) by cetostearyl alcohol, trehalose, glycerol, stereth -21 be added into deionized water, according to 2500 turns/
The rate of minute is stirred homogeneous 15 minutes, and mixed liquor is then warming up to 77 DEG C, stirs according to 1400 revs/min of rates
25 minutes, obtain the first mixture；
(3) cetostearyl alcohol ethylhexoate, isopropyl palmitate, niacinamide are added step (2) resulting first and mixed
It closes in object, continues to heat mixed liquor to 90 DEG C, the rate under the vacuum condition of -0.09MPa according to 1700 revs/min is equal again
Matter 10 minutes, obtain the second mixture；
(4) the second mixture obtained step (3) stands heat preservation 35 minutes, is subsequently placed in emulsion pot, and to emulsification
Epidermal growth factor is added in pot, is stirred 13 minutes according to 2300 revs/min of rates, when liquid temperature to be mixed is down to 68 DEG C,
Wild hedge rose fruit extract, monkey-bread tree pulp extract, orchid extract are added into emulsion pot, according to 1600 revs/min
Rate stirs 9 minutes, obtains final mixture；
(5) after the final mixture that step (4) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 20 minutes according to 110 revs/min of rates, finished emulsion is obtained after discharging, is denoted as S2.
Embodiment 3
The moisturizing lotion formula added with plant extracts of the present embodiment is as follows:
Wild hedge rose fruit extract 3.5%
Monkey-bread tree pulp extract 1.6%
Orchid extract 1.5%
Cetostearyl alcohol 5.2%
Trehalose 3.8%
Glycerol 9.5%
Cetostearyl alcohol ethylhexoate 5.5%
Isopropyl palmitate 5.5%
Niacinamide 3.5%
Epidermal growth factor 1.8%
Stereth -210.12%
Essence 0.01%
Antioxidant 0.02%
Preservative 0.1%
Deionized water surplus.
The moisturizing lotion added with plant extracts of the present embodiment is prepared as follows:
(1) Wild hedge rose fruit, monkey-bread tree pulp and orchid are crushed respectively, is sieved, being added to weight is 30 times, volume
In the ethanol solution that concentration is 70%, ultrasonic extraction 4 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Wild hedge rose fruit extract, monkey-bread tree pulp extract and orchid extract
(2) by cetostearyl alcohol, trehalose, glycerol, stereth -21 be added into deionized water, according to 3000 turns/
The rate of minute is stirred homogeneous 20 minutes, and mixed liquor is then warming up to 80 DEG C, stirs according to 1500 revs/min of rates
30 minutes, obtain the first mixture；
(3) cetostearyl alcohol ethylhexoate, isopropyl palmitate, niacinamide are added step (2) resulting first and mixed
It closes in object, continues to heat mixed liquor to 92 DEG C, the rate under the vacuum condition of -0.1MPa according to 1800 revs/min is equal again
Matter 12 minutes, obtain the second mixture；
(4) the second mixture obtained step (3) stands heat preservation 40 minutes, is subsequently placed in emulsion pot, and to emulsification
Epidermal growth factor is added in pot, is stirred 15 minutes according to 2400 revs/min of rates, when liquid temperature to be mixed is down to 70 DEG C,
Wild hedge rose fruit extract, monkey-bread tree pulp extract, orchid extract are added into emulsion pot, according to 1700 revs/min
Rate stirs 8~10 minutes, obtains final mixture；
(5) after the final mixture that step (4) obtains is cooled to room temperature, essence, antioxidant, preservative is added, presses
It is stirred 25 minutes according to 120 revs/min of rates, finished emulsion is obtained after discharging, is denoted as S3.
Comparative example 1
Substantially with embodiment 2, difference is the formula and preparation method of the moisturizing lotion of this comparative example, does not add wild rose
Common vetch berry extract, final moisturizing lotion obtained are denoted as C1.
Comparative example 2
Substantially with embodiment 2, difference is the formula and preparation method of the moisturizing lotion of this comparative example, does not add monkey face
Packet tree pulp extract, final moisturizing lotion obtained are denoted as C2.
Comparative example 3
Substantially with embodiment 2, difference is the formula and preparation method of the moisturizing lotion of this comparative example, does not add orchid
Extract, final moisturizing lotion obtained are denoted as C3.
Comparative example 4
Substantially with embodiment 1, difference is the formula and preparation method of the moisturizing lotion of this comparative example, does not add epidermis
Growth factor, final moisturizing lotion obtained are denoted as C4.
Comparative example 5
Substantially with embodiment 1, difference is the formula and preparation method of the moisturizing lotion of this comparative example, does not add seaweed
Sugar, final moisturizing lotion obtained are denoted as C5.
Performance test
Moisturizing lotion prepared by Examples 1 to 3 and comparative example 1~5 is subjected to using effect performance test.
Select the age at 30~40 years old, the women population of dry skin is randomly divided into 8 groups, every group 15 as test object
People, each group skin of face situation, in terms of the difference that there are no significant, 1~8 group respectively in daily early, evening two
A period smears moisturizing lotion S1~S3 that the embodiment of the present invention 1~3 is prepared and the profit that comparative example 1~5 is prepared
Skin lotion C1~C5 is each primary, after being used continuously one month, carries out effect assessment using the method for marking.Full marks be 5 points, 4
~5 points of expression improvements are splendid；3~4 points of expression improvements are good；2~3 points of expression improvements are general；2 points of following tables
Show and be not affected significantly effect, last each group is made even respectively, and the specific situation that scores is as shown in table 1:
Table 1
Test result is as shown above, the moisturizing lotion of embodiment S1~S3 group and the moisturizing lotion of comparative example C1~C5 group
It compares, more excellent soothing effect is all had for user, and have no toxic side effect.And the moisturizing lotion of embodiment S2 has
There is most excellent using effect.It can be seen that from the case where embodiment and comparative example of the invention added with plant extracts
Moisturizing lotion ingredient in Wild hedge rose fruit extract, monkey-bread tree pulp extract, orchid extract, epidermal growth factor,
In the case that trehalose produces using effect and significantly affects, and mentioned component is used in conjunction with, using effect compared to
Lack any one ingredient and have and be extremely obviously improved, it is seen that produces synergistic work between above-mentioned several ingredients
With having a good application prospect.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.
Claims (9)
1. a kind of moisturizing lotion added with plant extracts, which is characterized in that the raw material of the moisturizing lotion presses quality percentage
Number meter, forms as follows:
Wild hedge rose fruit extract 2.5~3.5%
Monkey-bread tree pulp extract 0.8~1.6%
Orchid extract 0.5~1.5%
Cetostearyl alcohol 4.8~5.2%
Trehalose 1.8~3.8%
Glycerol 8.5~9.5%
Cetostearyl alcohol ethylhexoate 3.5~5.5%
Isopropyl palmitate 2.5~5.5%
Niacinamide 2.5~3.5%
Epidermal growth factor 1.6~1.8%
Stereth -210.12~0.18%
Essence 0.01~0.03%
Antioxidant 0.02~0.05%
Preservative 0.1~0.2%
Deionized water surplus.
2. the moisturizing lotion according to claim 1 added with plant extracts, which is characterized in that the Wild hedge rose fruit mentions
Take object, monkey-bread tree pulp extract and orchid extract the preparation method comprises the following steps:
Wild hedge rose fruit, monkey-bread tree pulp and orchid are crushed respectively, are sieved, being added to weight is 30 times, volumetric concentration 70
In~80% ethanol solution, ultrasonic extraction 4~6 hours at 50 DEG C, ultrasonic power 250W then takes supernatant centrifugation, mistake
Filter, then by filtrate under conditions of vacuum degree is -0.08MPa rotary evaporation, obtain extract concentrated solution, it is last freeze-dried
Obtain Wild hedge rose fruit extract, monkey-bread tree pulp extract and orchid extract.
3. the moisturizing lotion according to claim 1 added with plant extracts, which is characterized in that the moisturizing lotion
Raw material by mass percentage, forms as follows:
Wild hedge rose fruit extract 3.0%
Monkey-bread tree pulp extract 1.2%
Orchid extract 1.0%
Cetostearyl alcohol 5.0%
Trehalose 2.8%
Glycerol 9.0%
Cetostearyl alcohol ethylhexoate 4.5%
Isopropyl palmitate 4.0%
Niacinamide 3.0%
Epidermal growth factor 1.7%
Stereth -210.15%
Essence 0.02%
Antioxidant 0.04%
Preservative 0.15%
Deionized water surplus.
4. described in any item moisturizing lotions added with plant extracts according to claim 1~3, which is characterized in that described
Any one of essence in ginger extrait, flavoring rose essence, lavender oil.
5. described in any item moisturizing lotions added with plant extracts according to claim 1~3, which is characterized in that described
Any one of antioxidant in butylated hydroxy anisole, allantoin, hydroxypropyl oxinane triol.
6. described in any item moisturizing lotions added with plant extracts according to claim 1~3, which is characterized in that described
Any one of preservative in Nipasol, sorbic acid, triclosan.
7. a kind of preparation method of the moisturizing lotion as described in any one of claims 1 to 6 added with plant extracts, special
Sign is, comprises the steps of:
(1) cetostearyl alcohol, trehalose, glycerol, stereth -21 are added into deionized water, according to 2000~3000
Rev/min rate be stirred homogeneous 10~20 minutes, mixed liquor is then warming up to 75~80 DEG C, according to 1200~1500
Rev/min rate stir 20~30 minutes, obtain the first mixture；
(2) step (1) resulting first mixture is added in cetostearyl alcohol ethylhexoate, isopropyl palmitate, niacinamide
In, continue to heat mixed liquor to 88~92 DEG C, under vacuum conditions according to 1600~1800 revs/min of rate homogeneous 8 again
~12 minutes, obtain the second mixture；
(3) the second mixture obtained step (2) stands heat preservation 30~40 minutes, is subsequently placed in emulsion pot, and to emulsification
Epidermal growth factor is added in pot, is stirred 10~15 minutes according to 2200~2400 revs/min of rates, liquid temperature drop to be mixed
When to 65~70 DEG C, Wild hedge rose fruit extract, monkey-bread tree pulp extract, orchid extract are added into emulsion pot, according to
1500~1700 revs/min of rate stirs 8~10 minutes, obtains final mixture；
(4) after the final mixture that step (3) obtains is cooled to room temperature, essence, antioxidant, preservative is added, according to 100
~120 revs/min of rate stirs 15~25 minutes, and finished emulsion is obtained after discharging.
8. the preparation method of the moisturizing lotion according to claim 7 added with plant extracts, which is characterized in that described
Step carries out homogeneous under the vacuum condition of -0.08~-0.1MPa in (2).
9. described in any item moisturizing lotions added with plant extracts are in face skin nursing according to claim 1~6
Application.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114303944A (en) * | 2020-09-30 | 2022-04-12 | 伽蓝（集团）股份有限公司 | Culture medium for callus of rosa tenuifolia, extract, preparation method and application |
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2019
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114303944A (en) * | 2020-09-30 | 2022-04-12 | 伽蓝（集团）股份有限公司 | Culture medium for callus of rosa tenuifolia, extract, preparation method and application |
| CN114303944B (en) * | 2020-09-30 | 2023-08-11 | 伽蓝（集团）股份有限公司 | Callus culture medium and extract of rosa tenuifolia, preparation method and application |
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Application publication date: 20190419 |