CN108785174A - A kind of plain face frost and preparation method thereof rich in grapefruit abstract - Google Patents

A kind of plain face frost and preparation method thereof rich in grapefruit abstract Download PDF

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CN108785174A
CN108785174A CN201810844185.2A CN201810844185A CN108785174A CN 108785174 A CN108785174 A CN 108785174A CN 201810844185 A CN201810844185 A CN 201810844185A CN 108785174 A CN108785174 A CN 108785174A
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parts
shaddock
rich
grapefruit
component
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傅曼琼
戴海民
付杰
袁翠华
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Dapu Tongmei Industrial Co Ltd
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Dapu Tongmei Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/29Titanium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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Abstract

The present invention relates to shaddock deep process technology fields, more particularly to a kind of plain face frost and preparation method thereof rich in grapefruit abstract comprising the components such as 2-5 parts of 8-20 parts of emulsifier, ivory white powder and/or titanium dioxide, 2-6 parts of amino acid humectant, 25-45 parts of shaddock hydrosol, 15-25 parts of shaddock essential oil and antiseptic.Shaddock hydrosol in formula and shaddock essential oil, it is so that the shaddock ped of Meizhou golden-pomelo is handled through special process and extracts the naringenin essence extracted, with whitening spot-removing, anti-acne, a variety of unique effects such as grease, antiphlogistic antibacterial, antiallergy, anti-oxidant are adjusted, and raw material is natural plant raw material, performance is mild, it is non-stimulated to skin, it is easy to absorb, quality is good, preparation process is simple, it can be achieved that large-scale industrial production.

Description

A kind of plain face frost and preparation method thereof rich in grapefruit abstract
Technical field
The present invention relates to shaddock deep process technology fields, and in particular to a kind of plain face frost and its system rich in grapefruit abstract Preparation Method.
Background technology
As domestic consumer to the cognition of cosmetic industry and is familiar with, people are more and more to safe and healthy, effective Care product focus more on, can be to people especially using extract in natural plants as the natural plant cosmetics of raw material Body skin plays the effects that nutrition protection and beauty treatment, and the functional component that irritation will not be caused to damage to skin.BB is white, is The abbreviation of Blemish Balm, effect mainly hide the flaw, adjust the colour of skin, is sun-proof, careful pore, can create nude look effect Feel.BB frosts itself have maintenance and hide the dual identity of the flaw, ignore the impression of skin to achieve the effect that hide the flaw, because And the functional product that natural component is extracted from plant is the Development Trend of the naked adornment skin care item of a new generation, also more science and Environmental protection.
Shaddock (scientific name:Citrus maxima) be Citrus paradisi Macfadyen ripening fruits, originate in southern region of China, Fruit sour-sweet Liang Run, it is full of nutrition;Its pericarp, pomelo flower can all be used as medicine.Wherein, the soil moisture of East Guangdong Meizhou, soil moisture and Soil pH originates in the Meizhou golden-pomelo of Meizhou suitable for shaddock growth and development, and fruit is big, good appearance;It is peel smooth, neat and well spaced, clean Only;Pulp sweetness is tasty and refreshing, there is sweet taste, thus has singing the praises of for " king in shaddock ".Shaddock is rich in nutriment and higher medicinal valence Value, the work rich in multiple beneficials health such as various active polysaccharide, flavones, pectin, natural pigment, essential oil especially in pomelo peel Property ingredient, and higher than the content in shaddock fruit.However, shaddock still has fresh weight 20~30% after people are edible and produce and process Shaddock ped can not be used.These shaddock peds are dried, burned or are directly thrown away as waste mostly, are not only made to ecological environment At serious pollution, but also resource abundant in shaddock ped is wasted significantly.Extract of the shaddock pericarp after processing has A variety of beauty functions such as whitening spot-removing, antiphlogistic antibacterial, antiallergy, anti-oxidant are extraordinary natural plants cosmetic materials, but Research there has been no the extract for processing shaddock pericarp as raw material applied to cosmetics at present.
Invention content
It is an object of the invention to be directed to deficiency in the prior art, and provide a kind of plain face frost rich in grapefruit abstract And preparation method thereof, the shaddock hydrosol and shaddock essential oil added in formula is the shaddock ped with Meizhou golden-pomelo through special process Processing and extract the naringenin essence that extracts, obtained plain face frost not only have whitening spot-removing, antiphlogistic antibacterial, antiallergy, A variety of beauty functions such as anti-oxidant, and raw material is natural plant composition, and performance is mild, non-stimulated to skin.
The purpose of the present invention is achieved through the following technical solutions:
A kind of plain face frost rich in grapefruit abstract is provided, the raw material of following parts by weight is included:
Component A:
B component:
Component C:
15-25 parts of shaddock essential oil
0.5-2 parts of antiseptic
0.5-1.5 parts of thickener.
In above-mentioned technical proposal, a kind of plain face frost rich in grapefruit abstract includes the raw material of following parts by weight:
Component A:
B component:
Component C:
15-25 parts of shaddock essential oil
0.5-2 parts of antiseptic
0.5-1.5 parts of thickener.
In above-mentioned technical proposal, the shaddock hydrosol is made through distillation by the raw material of following parts by weight:Grapefruit flower 3-8 80-120 parts of part, 3-8 parts of pomelo peel and pure water.
In above-mentioned technical proposal, the shaddock essential oil is made by distillation extraction using fresh Meizhou golden-pomelo skin.
In above-mentioned technical proposal, B component further includes 0.8-2 parts of Chinese herbal medicine extract, and the Chinese herbal medicine extract is sweet Careless extract and/or ginseng extract.
In above-mentioned technical proposal, the emulsifier is cetyl dimethicone and/or C12-20 alkyl glucosides.
In above-mentioned technical proposal, the antiseptic is the mixture of sorbic acid and bisabolol.
In above-mentioned technical proposal, the thickener is lecithin.
The present invention also provides a kind of preparation methods of the plain face frost rich in grapefruit abstract, include the following steps:
Step a, the emulsion of component A is prepared:
Emulsifier, saualane, isononyl isononanoate, ivory white powder and/or titanium dioxide are weighed by weight, are added to emulsification In cylinder, stirring is opened, and be heated to 80-85 DEG C, so that emulsifying raw material is uniformly dispersed, obtain emulsion, it is spare;
Step b, the mixed liquor of B component is prepared:
B1 3-8 parts of 3-8 parts of grapefruit flower and pomelo peel) are taken, 80-120 parts of pure water is added, then under the conditions of 95-100 DEG C 2-3h is distilled, shaddock hydrosol is made;
B2 purified water, glycerine, butanediol, biological carbohydrate gum, amino acid humectant and shaddock hydrosol) are weighed by weight, are stirred Mixing is mixed, and is heated to 80-85 DEG C, raw material is made all to be uniformly dissolved, obtains mixed liquor, it is spare;
Step c, shaddock essential oil is prepared:
C1 the fresh shaddock fruit of Meizhou golden-pomelo) is taken, shaddock fruit crust is cleaned, it is spare;
C2) by weight, 2-4 parts of 15-25 parts of brown sugar, 8-12 parts of brown sugar, brown sugar or honey, Meizhou golden-pomelo skin 75- are taken 85 parts, 8-12 parts of fragrant citrus pericarp, 3-8 parts of orange peel, 2-4 parts of tea seed, 0.5-1.5 parts of grapefruit flower, 0.3-0.8 parts of shaddock leaf, rose 800-1200 parts of 0.3-0.8 parts of flower and pure water are packed into sealing container through spontaneous fermentation 1-3, then filter after mixing, Shaddock ferment is obtained, shaddock ferment and pure water are then mixed and made into shaddock enzyme liquid;
C3) the fresh shaddock fruit of step c1 is put into the shaddock enzyme liquid and is soaked for a period of time, then cleaning, airing; The step is crucial, using shaddock enzyme liquid soaking and washing, can thoroughly remove pesticide residue on pomelo peel, bacterium, worm's ovum, Virus etc., to ensure natural, pollution-free, the non-stimulated better quality of the derived essential oil subsequently extracted from shaddock crust, and And the cleaning agent for using chemical reagent is compared, and it is more environmentally-friendly, avoid environmental pollution.
C4 the shaddock fruit after drying) is taken, ecto-entad, which is cut, takes shaddock crust, is subsequently processed into the pomelo peel of sheet or filiform, Suitable boiler is chosen according to the weight of pomelo peel after weighing, boiler volume is 30-50L needed for per kilogram pomelo peel;
C5 pomelo peel) is poured into boiler, the pure water that isodose is added carries out distillation extraction, obtains the oil of shaddock ped fragrance Aqueous mixtures after detaching oil water mixture, obtain shaddock essential oil;
Step d, mixing dispersion:
The emulsion of step a is poured into the mixed liquor of step b, keeps 80-85 DEG C of constant temperature, stirred while pouring into, Keep raw material evenly dispersed, grainless obtains dispersion liquid;
Step e, component C is added:
When the dispersion liquid of step d is cooled to 40 DEG C or less, shaddock essential oil, antiseptic and thickening are added into dispersion liquid Agent then proceedes to stirring 30-60min, and is adjusted to required viscosity to get white to the plain face rich in grapefruit abstract.
In above-mentioned technical proposal, in step c2, the mass ratio of shaddock ferment and clear water is 1:(90-110);
In step c3, soaking time 15-40min;
In step c4, the shaddock fruit after drying, ecto-entad is taken to cut the shaddock crust for taking 1-5mm thickness, be subsequently processed into 5- The sheet of 10mm thickness or the pomelo peel of filiform;Shaddock oil vacuole can be quickly obtained in follow-up distillation in this way, and then is quickly made Shaddock essential oil is extracted in follow-up distillation extraction, is shortened extraction time, is thus greatly shortened production cycle, and yield It is high.
In step c5, the time of distillation extraction is 40-100min.
Beneficial effects of the present invention:
A kind of plain face frost and preparation method thereof rich in grapefruit abstract of the present invention, has the following advantages:(1) formula group Be added to shaddock hydrosol in point B, shaddock essential oil be added in component C, both ingredients be using the shaddock ped of Meizhou golden-pomelo as Then raw material extracts the naringenin essence extracted, makes the aurantiin contained in shaddock ped by the special process processing to shaddock ped It is extracted etc. a large amount of physiological activators, the active material penetration is strong, 300 microns of energy skin permeation surface layer, to have Effect removal melanin has whitening spot-removing, anti-acne, repairs skin blemishes, adjusts grease, antiphlogistic antibacterial, antiallergy, anti-oxidant etc. A variety of unique effects, shaddock essential oil can also play the effect of promoting toxin expelling, promoting blood circulation channels and collaterals, and the shaddock added in being formulated Hydrosol and shaddock essential oil are pure plant raw material, and performance is mild, non-stimulated to skin, are easy to skin absorption, improve skin quality, Using effect is notable;(2) present invention uses special shaddock enzyme liquid soaking and washing to shaddock ped, and shaddock ferment is by shaddock ped pomace It is made Deng by spontaneous fermentation, a large amount of organized enzymes can be generated, can thoroughly remove pesticide residue on shaddock ped, bacterium, worm Ovum, virus etc., to ensure that the active constituent extracted from shaddock ped has natural, pollution-free, non-stimulated quality;(3) this hair Bright preparation process is simple, and grapefruit abstract can be more evenly distributed in emulsification system, and stability is good, to equipment requirement Low, with short production cycle, yield is high, it can be achieved that industrial scale produces.
Specific implementation mode
With reference to specific embodiment, the present invention is described in further detail, but does not constitute to any of the present invention Limitation.
Embodiment 1:
A kind of preparation method of plain face frost rich in grapefruit abstract of the present embodiment is as follows, includes the following steps:
Step a, the emulsion of component A is prepared:
10 parts of cetyl dimethicone, 8 parts of saualane, 5 parts of isononyl isononanoate, titanium dioxide are weighed by weight It 2 parts, is added into emulsion tank, opens stirring, and be heated to 80 DEG C, so that emulsifying raw material is uniformly dispersed, obtain emulsion, it is spare;
Step b, the mixed liquor of B component is prepared:
B1 5 parts of 3 parts of grapefruit flower and pomelo peel) are taken, 80 parts of pure water is added, then distills 3h under the conditions of 95 DEG C, is made Shaddock hydrosol;
B2 10 parts of purified water, 3 parts of glycerine, 2 parts of butanediol, biological 1 part of carbohydrate gum, amino acid humectant 3) are weighed by weight 30 parts of part and shaddock hydrosol, are stirred, and be heated to 80 DEG C, raw material are made all to be uniformly dissolved, obtain mixed liquor, spare;
Step c, shaddock essential oil is prepared:
C1 the fresh shaddock fruit of Meizhou golden-pomelo) is taken, shaddock fruit crust is cleaned, it is spare;
C2) by weight, 15 parts of brown sugar, 8 parts of brown sugar, 2 parts of brown sugar, 75 parts of Meizhou golden-pomelo skin, 8 parts of fragrant citrus pericarp, tangerine are taken 800 parts of 3 parts of sub- skin, 2 parts of tea seed, 1 part of grapefruit flower, 0.5 part of shaddock leaf, 0.3 part of rose and pure water, are packed into after mixing Then sealing container is filtered through spontaneous fermentation 1-3, obtain shaddock ferment, then by shaddock ferment and pure water according to quality Than being 1:90 are mixed and made into shaddock enzyme liquid;
C3) the fresh shaddock fruit of step c1 is put into the shaddock enzyme liquid and impregnates 15min, then cleaning, airing;
C4 it) takes the shaddock fruit after drying, ecto-entad to cut the shaddock crust for taking 2mm thickness, is then machined to 5mm thickness with chopping Sheet or filiform pomelo peel, suitable boiler is chosen according to the weight of pomelo peel after weighing, needed for per kilogram pomelo peel Boiler volume is 30-50L;
C5 pomelo peel) is poured into boiler, the pure water that isodose is added carries out distillation extraction 100min, obtains shaddock ped perfume The oil water mixture of taste after detaching oil water mixture, obtains shaddock essential oil;
Step d, mixing dispersion:
The emulsion of step a is poured into the mixed liquor of step b, keeps 80 DEG C of constant temperature, stirred while pouring into, make original Expect evenly dispersed, grainless obtains dispersion liquid;
Step e, component C is added:
When the dispersion liquid of step d is cooled to 40 DEG C or less, 15 parts of shaddock essential oil, sorbic acid 0.5 are added into dispersion liquid 1.5 parts of part, 0.5 part of bisabolol and lecithin then proceed to stirring 60min, and are adjusted to required viscosity to get to rich in shaddock The plain face frost of seed extract.
Embodiment 2:
A kind of preparation method of plain face frost rich in grapefruit abstract of the present embodiment is as follows, includes the following steps:
Step a, the emulsion of component A is prepared:
15 parts of C12-20 alkyl glucosides, 10 parts of saualane, 3 parts of isononyl isononanoate, ivory white powder 1 are weighed by weight Part, 3 parts of titanium dioxide are added into emulsion tank, open stirring, and be heated to 82 DEG C, so that emulsifying raw material is uniformly dispersed, emulsified Liquid, it is spare;
Step b, the mixed liquor of B component is prepared:
B1 3 parts of 5 parts of grapefruit flower and pomelo peel) are taken, 100 parts of pure water is added, then distills 2.5h under the conditions of 98 DEG C, is made Obtain shaddock hydrosol;
B2 18 parts of purified water, 6 parts of glycerine, 1 part of butanediol, biological 3 parts of carbohydrate gum, amino acid humectant 4) are weighed by weight Part, 35 parts of shaddock hydrosol, 1 part of licorice and 1 part of ginseng extract, are stirred, and be heated to 82 DEG C, keep raw material whole It is uniformly dissolved, obtains mixed liquor, it is spare;
Step c, shaddock essential oil is prepared:
C1 the fresh shaddock fruit of Meizhou golden-pomelo) is taken, shaddock fruit crust is cleaned, it is spare;
C2) by weight, take 20 parts of brown sugar, 10 parts of brown sugar, 3 parts of honey, 80 parts of Meizhou golden-pomelo skin, 10 parts of fragrant citrus pericarp, 1000 parts of 5 parts of orange peel, 3 parts of tea seed, 0.5 part of grapefruit flower, 0.8 part of shaddock leaf, 0.8 part of rose and pure water are uniformly mixed It is packed into sealing container afterwards through spontaneous fermentation 1-3, then filters, obtains shaddock ferment, then press shaddock ferment and pure water It is 1 according to mass ratio:110 are mixed and made into shaddock enzyme liquid;
C3) the fresh shaddock fruit of step c1 is put into the shaddock enzyme liquid and impregnates 25min, then cleaning, airing;
C4 it) takes the shaddock fruit after drying, ecto-entad to cut the shaddock crust for taking 3mm thickness, is then machined to 8mm thickness with chopping Sheet or filiform pomelo peel, suitable boiler is chosen according to the weight of pomelo peel after weighing, needed for per kilogram pomelo peel Boiler volume is 30-50L;
C5 pomelo peel) is poured into boiler, the pure water that isodose is added carries out distillation extraction 80min, obtains shaddock ped perfume The oil water mixture of taste after detaching oil water mixture, obtains shaddock essential oil;
Step d, mixing dispersion:
The emulsion of step a is poured into the mixed liquor of step b, keeps 82 DEG C of constant temperature, stirred while pouring into, make original Expect evenly dispersed, grainless obtains dispersion liquid;
Step e, component C is added:
When the dispersion liquid of step d is cooled to 40 DEG C or less, be added into dispersion liquid 18 parts of shaddock essential oil, 1 part of sorbic acid, 0.5 part of 0.5 part of bisabolol and lecithin then proceed to stirring 50min, and are adjusted to required viscosity to get to rich in shaddock The plain face frost of extract.
Embodiment 3:
A kind of preparation method of plain face frost rich in grapefruit abstract of the present embodiment is as follows, includes the following steps:
Step a, the emulsion of component A is prepared:
Weigh by weight 10 parts of cetyl dimethicone, 8 parts of C12-20 alkyl glucosides, 13 parts of saualane, 6 parts of isononyl isononanoate, 3 parts of ivory white powder are added into emulsion tank, open stirring, and be heated to 83 DEG C, make emulsifying raw material point It dissipates uniformly, obtains emulsion, it is spare;
Step b, the mixed liquor of B component is prepared:
B1 8 parts of 8 parts of grapefruit flower and pomelo peel) are taken, 120 parts of pure water is added, then distills 2h under the conditions of 100 DEG C, is made Obtain shaddock hydrosol;
B2 14 parts of purified water, 5 parts of glycerine, 3 parts of butanediol, biological 2 parts of carbohydrate gum, amino acid humectant 2) are weighed by weight 0.8 part of part, 40 parts of shaddock hydrosol and licorice, are stirred, and be heated to 83 DEG C, so that raw material is all uniformly dissolved, obtain It is spare to mixed liquor;
Step c, shaddock essential oil is prepared:
C1 the fresh shaddock fruit of Meizhou golden-pomelo) is taken, shaddock fruit crust is cleaned, it is spare;
C2) by weight, take 25 parts of brown sugar, 12 parts of brown sugar, 4 parts of brown sugar, 85 parts of Meizhou golden-pomelo skin, 12 parts of fragrant citrus pericarp, 1200 parts of 8 parts of orange peel, 4 parts of tea seed, 1.5 parts of grapefruit flower, 0.8 part of shaddock leaf, 0.8 part of rose and pure water are uniformly mixed It is packed into sealing container afterwards through spontaneous fermentation 1-3, then filters, obtains shaddock ferment, then press shaddock ferment and pure water It is 1 according to mass ratio:100 are mixed and made into shaddock enzyme liquid;
C3) the fresh shaddock fruit of step c1 is put into the shaddock enzyme liquid and impregnates 30min, then cleaning, airing;
C4 it) takes the shaddock fruit after drying, ecto-entad to cut the shaddock crust for taking 4mm thickness, is then machined to 6mm thickness with chopping Sheet or filiform pomelo peel, suitable boiler is chosen according to the weight of pomelo peel after weighing, needed for per kilogram pomelo peel Boiler volume is 30-50L;
C5 pomelo peel) is poured into boiler, the pure water that isodose is added carries out distillation extraction 60min, obtains shaddock ped perfume The oil water mixture of taste after detaching oil water mixture, obtains shaddock essential oil;
Step d, mixing dispersion:
The emulsion of step a is poured into the mixed liquor of step b, keeps 83 DEG C of constant temperature, stirred while pouring into, make original Expect evenly dispersed, grainless obtains dispersion liquid;
Step e, component C is added:
When the dispersion liquid of step d is cooled to 40 DEG C or less, 22 parts of shaddock essential oil, sorbic acid 0.3 are added into dispersion liquid 1 part of part, 0.2 part of bisabolol and lecithin then proceed to stirring 40min, and are adjusted to required viscosity to get to rich in shaddock The plain face frost of extract.
Embodiment 4:
A kind of preparation method of plain face frost rich in grapefruit abstract of the present embodiment is as follows, includes the following steps:
Step a, the emulsion of component A is prepared:
Weigh by weight 10 parts of cetyl dimethicone, 10 parts of C12-20 alkyl glucosides, 15 parts of saualane, 3 parts of 8 parts of isononyl isononanoate, ivory white powder 2 and titanium dioxide are added into emulsion tank, open stirring, and be heated to 85 DEG C, make Emulsifying raw material is uniformly dispersed, and obtains emulsion, spare;
Step b, the mixed liquor of B component is prepared:
B1 4 parts of 6 parts of grapefruit flower and pomelo peel) are taken, 110 parts of pure water is added, then distills 2.3h under the conditions of 99 DEG C, is made Obtain shaddock hydrosol;
B2 20 parts of purified water, 4 parts of glycerine, 2 parts of butanediol, biological 2 parts of carbohydrate gum, amino acid humectant 5) are weighed by weight 1.5 parts of part, 25 parts of shaddock hydrosol and ginseng extract, are stirred, and be heated to 85 DEG C, so that raw material is all uniformly dissolved, obtain It is spare to mixed liquor;
Step c, shaddock essential oil is prepared:
C1 the fresh shaddock fruit of Meizhou golden-pomelo) is taken, shaddock fruit crust is cleaned, it is spare;
C2) by weight, take 22 parts of brown sugar, 11 parts of brown sugar, 3 parts of honey, 82 parts of Meizhou golden-pomelo skin, 11 parts of fragrant citrus pericarp, 900 parts of 6 parts of orange peel, 3 parts of tea seed, 1.2 parts of grapefruit flower, 0.6 part of shaddock leaf, 0.3 part of rose and pure water, after mixing Sealing container is packed into through spontaneous fermentation 1-3, then filters, obtains shaddock ferment, then by shaddock ferment and pure water according to Mass ratio is 1:100 are mixed and made into shaddock enzyme liquid;
C3) the fresh shaddock fruit of step c1 is put into the shaddock enzyme liquid and impregnates 40min, then cleaning, airing;
C4 the shaddock fruit after drying) is taken, the shaddock crust for taking 5mm thickness is cut by ecto-entad, is then machined to 5mm with chopping The pomelo peel of thick sheet or filiform, suitable boiler, per kilogram pomelo peel institute are chosen after weighing according to the weight of pomelo peel It is 30-50L to need boiler volume;
C5 pomelo peel) is poured into boiler, the pure water that isodose is added carries out distillation extraction 40min, obtains shaddock ped perfume The oil water mixture of taste after detaching oil water mixture, obtains shaddock essential oil;
Step d, mixing dispersion:
The emulsion of step a is poured into the mixed liquor of step b, keeps 85 DEG C of constant temperature, stirred while pouring into, make original Expect evenly dispersed, grainless obtains dispersion liquid;
Step e, component C is added:
When the dispersion liquid of step d is cooled to 40 DEG C or less, 25 parts of shaddock essential oil, sorbic acid 0.5 are added into dispersion liquid 1 part of part, 0.5 part of bisabolol and lecithin then proceed to stirring 30min, and are adjusted to required viscosity to get to rich in shaddock The plain face frost of extract.
Embodiment provided above is the better embodiment of the present invention, only is used for facilitating illustrating the present invention, not to this hair It is bright to make any form of restriction, any those of ordinary skill in the art, if not departing from the put forward skill of the present invention In the range of art feature, using the equivalent embodiment for locally changing or modifying made by disclosed technology contents, and Without departing from the technical feature content of the present invention, in the range of still falling within the technology of the present invention feature.

Claims (10)

1. a kind of plain face frost rich in grapefruit abstract, it is characterised in that:Include the raw material of following parts by weight:
Component A:
8-20 parts of emulsifier
8-15 parts of saualane
3-8 parts of isononyl isononanoate
2-5 parts of ivory white powder and/or titanium dioxide;
B component:
10-20 parts of purified water
3-8 parts of glycerine
1-3 parts of butanediol
Biological carbohydrate gum 1-3 parts
2-6 parts of amino acid humectant
25-45 parts of shaddock hydrosol;
Component C:
15-25 parts of shaddock essential oil
0.5-2 parts of antiseptic
0.5-1.5 parts of thickener.
2. a kind of plain face frost rich in grapefruit abstract according to claim 1, it is characterised in that:Including following parts by weight Raw material:
Component A:
10-18 parts of emulsifier
8-13 parts of saualane
3-8 parts of isononyl isononanoate
2-4 parts of ivory white powder and/or titanium dioxide
B component:
10-18 parts of purified water
3-6 parts of glycerine
1-3 parts of butanediol
Biological carbohydrate gum 1-3 parts
2-6 parts of amino acid humectant
25-40 parts of shaddock hydrosol
Component C:
15-25 parts of shaddock essential oil
0.5-2 parts of antiseptic
0.5-1.5 parts of thickener.
3. a kind of plain face frost rich in grapefruit abstract according to claim 1 or 2, it is characterised in that:The shaddock is pure Dew is made through distillation by the raw material of following parts by weight:80-120 parts of 3-8 parts of grapefruit flower, 3-8 parts of pomelo peel and pure water.
4. a kind of plain face frost rich in grapefruit abstract according to claim 1 or 2, it is characterised in that:The shaddock essence Oil is made by distillation extraction using fresh Meizhou golden-pomelo skin.
5. a kind of skin care item rich in grapefruit abstract according to claim 1 or 2, it is characterised in that:B component further includes 0.8-2 parts of Chinese herbal medicine extract, the Chinese herbal medicine extract are licorice and/or ginseng extract.
6. a kind of plain face frost rich in grapefruit abstract according to claim 1 or 2, it is characterised in that:The emulsifier For cetyl dimethicone and/or C12-20 alkyl glucosides.
7. a kind of plain face frost rich in grapefruit abstract according to claim 1 or 2, it is characterised in that:The antiseptic For the mixture of sorbic acid and bisabolol.
8. a kind of plain face frost rich in grapefruit abstract according to claim 1 or 2, it is characterised in that:The thickener For lecithin.
9. a kind of preparation method of plain face frost rich in grapefruit abstract as described in claim 1 to 8 any one, including with Lower step:
Step a, the emulsion of component A is prepared:
Emulsifier, saualane, isononyl isononanoate, ivory white powder and/or titanium dioxide are weighed by weight, are added to emulsion tank In, stirring is opened, and be heated to 80-85 DEG C, so that emulsifying raw material is uniformly dispersed, obtain emulsion, it is spare;
Step b, the mixed liquor of B component is prepared:
B1 3-8 parts of 3-8 parts of grapefruit flower and pomelo peel) are taken, 80-120 parts of pure water is added, is then distilled under the conditions of 95-100 DEG C Shaddock hydrosol is made in 2-3h;
B2 it is mixed that purified water, glycerine, butanediol, biological carbohydrate gum, amino acid humectant and shaddock hydrosol, stirring) are weighed by weight It closes, and is heated to 80-85 DEG C, so that raw material is all uniformly dissolved, obtain mixed liquor, it is spare;
Step c, shaddock essential oil is prepared:
C1 the fresh shaddock fruit of Meizhou golden-pomelo) is taken, shaddock fruit crust is cleaned, it is spare;
C2) by weight, take 2-4 parts of 15-25 parts of brown sugar, 8-12 parts of brown sugar, brown sugar or honey, 75-85 parts of Meizhou golden-pomelo skin, 8-12 parts of fragrant citrus pericarp, 3-8 parts of orange peel, 2-4 parts of tea seed, 0.5-1.5 parts of grapefruit flower, 0.3-0.8 parts of shaddock leaf, rose 0.3- 0.8 part and 800-1200 parts of pure water are packed into sealing container through spontaneous fermentation 1-3, then filter, obtain shaddock after mixing Then shaddock ferment and pure water are mixed and made into shaddock enzyme liquid by sub- ferment;
C3) the fresh shaddock fruit of step c1 is put into the shaddock enzyme liquid and is soaked for a period of time, then cleaning, airing;
C4 the shaddock fruit after drying) is taken, ecto-entad, which is cut, takes shaddock crust, is subsequently processed into the pomelo peel of sheet or filiform, weighs Suitable boiler is chosen according to the weight of pomelo peel afterwards, boiler volume is 30-50L needed for per kilogram pomelo peel;
C5 pomelo peel) is poured into boiler, the pure water that isodose is added carries out distillation extraction, and the grease for obtaining shaddock ped fragrance is mixed Object is closed, after oil water mixture is detached, obtains shaddock essential oil;
Step d, mixing dispersion:
The emulsion of step a is poured into the mixed liquor of step b, keeps 80-85 DEG C of constant temperature, stirred while pouring into, make original Expect evenly dispersed, grainless obtains dispersion liquid;
Step e, component C is added:
When the dispersion liquid of step d is cooled to 40 DEG C or less, shaddock essential oil, antiseptic and thickener are added into dispersion liquid, so After continue stir 30-60min, and be adjusted to required viscosity to get to rich in grapefruit abstract plain face frost.
10. a kind of preparation method of plain face frost rich in grapefruit abstract according to claim 9, it is characterised in that:Step In rapid c2, the mass ratio of shaddock ferment and clear water is 1:(90-110);In step c3, soaking time 15-40min;Step c4 In, it takes the shaddock fruit after drying, ecto-entad to cut the shaddock crust for taking 1-5mm thickness, is subsequently processed into the sheet or silk of 5-10mm thickness The pomelo peel of shape;In step c5, the time of distillation extraction is 40-100min.
CN201810844185.2A 2018-07-27 2018-07-27 A kind of plain face frost and preparation method thereof rich in grapefruit abstract Pending CN108785174A (en)

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CN111803430A (en) * 2020-08-14 2020-10-23 广州致美日化科技有限公司 Face-beautifying cream and preparation method thereof
CN114287547A (en) * 2021-12-30 2022-04-08 北京康比特体育科技股份有限公司 Acne-removing and whitening beverage and preparation method thereof

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CN111803430A (en) * 2020-08-14 2020-10-23 广州致美日化科技有限公司 Face-beautifying cream and preparation method thereof
CN114287547A (en) * 2021-12-30 2022-04-08 北京康比特体育科技股份有限公司 Acne-removing and whitening beverage and preparation method thereof

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Application publication date: 20181113