CN106036274A - Eucommia and blueberry composite fruit juice containing inonotus obliquus polyphenol purified product and preparation method of composite fruit juice - Google Patents

Eucommia and blueberry composite fruit juice containing inonotus obliquus polyphenol purified product and preparation method of composite fruit juice Download PDF

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Publication number
CN106036274A
CN106036274A CN201610396338.2A CN201610396338A CN106036274A CN 106036274 A CN106036274 A CN 106036274A CN 201610396338 A CN201610396338 A CN 201610396338A CN 106036274 A CN106036274 A CN 106036274A
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fruit juice
blue berry
blueberry
composite
eucommia
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李峰
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Funan Anhui Chang Hui Food Co Ltd
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Funan Anhui Chang Hui Food Co Ltd
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52—Adding ingredients
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/80—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by adsorption
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention discloses eucommia and blueberry composite fruit juice containing inonotus obliquus polyphenol purified products. The eucommia and blueberry composite fruit juice is prepared from components in parts by weight as follows: 120-130 parts of blueberry fruits, 21-22 parts of eucommia flowers, 22-23 parts of flowers of masson pine, 23-24 parts of tea flowers, 4-5 parts of lutein, 7-8 parts of isomaltulose, 10-11 parts of water-soluble coffee polyphenols, 12-13 parts of the inonotus obliquus polyphenol purified products and the like. The blueberry and zymolytic alcohol extracts of the eucommia flowers, the flowers of masson pine and the tea flowers are matched, and the composite blueberry fruit juice is prepared and has the efficacy of reducing blood pressure collaboratively, relieving fatigue and visual fatigue, improving the memory and the like; besides, the composite fruit juice has taste different from single blueberry fruit juice and has certain unique flower fragrance; the oxidation resistance and the stability of the composite fruit juice are enhanced by means of water-soluble coffee polyphenols and the inonotus obliquus polyphenol purified products, the nutrition of the blueberry fruit juice is enriched by means of the zymolytic alcohol extracts of the eucommia flowers, the flowers of masson pine and the tea flowers, and the eucommia and blueberry composite fruit juice has better nutritional and health-care efficacy.

Description

A kind of Cortex Eucommiae blue berry composite fruit juice containing Inonqqus obliquus polyphenol purified and preparation thereof Method
Technical field
The present invention relates to blue berry deep process technology field, particularly relate to a kind of Cortex Eucommiae containing Inonqqus obliquus polyphenol purified blue Certain kind of berries composite fruit juice and preparation method thereof.
Background technology
Blue berry formal name used at school Pericarpium Citri tangerinae, belongs to Ericaceae genus vaccinium plant.Blueberry is except outer the most extremely strong medicinal for eating raw Being worth and alimentary health-care function, international food and agricultural organization is classified as one of big health food of the mankind five.Blue berry is in wild acinus Superfine product, its nutritive value, far above the fruit such as Fructus Mali pumilae, Fructus Vitis viniferae, Fructus Citri tangerinae, can be rated as " king of world's fruit ", is the world in recent years The with the fastest developing speed Third Class Fruit-tree kind integrating nutrition and health care, is first-class health food, and fashionable America and Europe is each State, enjoys the high praise of people and likes.
In Blueberry in addition to conventional sugar, acid and vitamin C, rich in vitamin E, vitamin A, vitamin B complex, The mineral elements such as SOD, arbutin, protein, anthocyanin, edible fiber and abundant potassium, ferrum, zinc, calcium.
Anthocyanidin contained by blue berry is that among all of fruit and vegetables, content is the highest, as every in high clump blue berry 100 grams In fruit, anthocyanidin content reaches hundreds of milligram.The part that the anthocyanidin of blue berry is the abundantest is exactly in its distinctive purple peel portion Position.Blueberry pomace, as the by-product of blue berry industry, abandons as refuse mostly.Blueberry pomace contain abundant Polyphenols and Flavone compound, especially anthocyanidin, about 42% remains in marc, if directly being abandoned by these blueberry pomaces is one Plant the waste of resource.Furthermore, in blueberry fresh fruit, the content of blue berry seed is about 3%, and blue berry seed fills the blue berry seed oil made, rich in relatively A high proportion of unsaturated fatty acid, can reduce cholesterol level, protection vision, nootropics, to cardiovascular and cerebrovascular vessel and cancer etc. Disease has positive preventive and therapeutic effect, about produces a few kiloton blue berry seed every year, and it is most of in blue berry machining chain All go out of use；This not only causes the huge waste of resource, also pollutes the environment.But up to the present, worldwide Research to blue berry seed and the exploitation to it are less.Further, owing to, in ripe blue berry, organic acid and tannin content enrich, saccharic acid Ratio up to 2.35, fruit juice pH2.6, so directly sensory experience is sour and astringent.Consequently leads to the blue berry of tradition blue berry processing The fragrance of juice is relatively weak.How to utilize and make full use of rate blueberry peel slag, seed slag and sarcocarp slag and produce nutrition, high-quality The high-quality of blueberry juice drink comprehensive utilization and blue berry fruit juice to realizing blue berry efficiently produces blue berry deep processing enterprise There is important value.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of Du containing Inonqqus obliquus polyphenol purified Secondary blue berry composite fruit juice and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of Cortex Eucommiae blue berry composite fruit juice containing Inonqqus obliquus polyphenol purified, including following parts by weight of component: blue berry 120- 130, calcining Concha Ostreae 19-20, pectase 10-11, eucommia flower 21-22, horse hair Flos pini 22-23, Flos Camelliae sinensis 23-24, cellulose Enzyme 7-8, citric acid 9-10, phylloxanthin 4-5, hydroxyl isomaltulose 7-8, water soluble coffee polyphenol 10-11, Inonqqus obliquus polyphenol are pure Compound 12-13, xanthan gum 2-3, kieselguhr 15-16, the ethanol water of appropriate concentration 10%, appropriate water, appropriate dioxygen Water.
A kind of Cortex Eucommiae fruit blue berry composite fruit juice preparation method containing Inonqqus obliquus polyphenol purified, comprises the following steps:
(1) calcining Concha Ostreae is put into ball milling 30min in ball mill and obtains ultra micro calcining oyster shell powder to micron dimension, by blue berry Adding after removing decayed fruit in tank, in tank, stirring adds ultra micro calcining oyster shell powder continuously stirred 15min, pulls out fresh Blue berry, and precipitate that to dry ultra micro calcining oyster shell powder standby, with clear water strength spray irrigation remove rhizome and decayed fruit, Fresh blue berry is standby；Fresh blue berry is first prepared granular size with grater with beating crusher pulverization process 40min consistent Blue berry crushes thing, this blue berry crushes thing pulper process 30min and carries out Particle pollution process, obtain blueberry pulp thing, should Blueberry pulp thing adds pectase and the water of gross weight 1-1.2 times, at 40 DEG C after mix and blend 1h, uses 650W microwave auxiliary Help process 2 times, each 15min, use milling process to squeeze the juice afterwards, carry out coarse filtration with the screen cloth of aperture 0.5mm, must be rich in flower Blue or green element blue berry fruit juice and blueberry pomace are standby；
(2), after eucommia flower, horse hair Flos pini, Flos Camelliae sinensis first being rinsed well with clear water, put in super micron mill and pulverize Process 30min, afterwards with the ethanol water of the concentration 10% of blueberry pomace, citric acid, cellulase and gross weight 1-2 times, Mixing and stirring, after using ultrasonic Treatment 1h of 100W, carries out hollow-fibre membrane hyperfiltration treatment, obtains complex liquid and alcohol extraction Rear composite slag；Complex liquid is carried out at 15 DEG C heat alcohol extraction 1h obtain rich in blue berry seed oil complex liquid standby；
(3) it is gross weight by first using vacuum drier dried 20-30min to moisture after composite slag after alcohol extraction 5%, use ball mill ball-milling treatment 30min, obtain ultramicronising and be combined ground-slag, ultramicronising is combined ground-slag, kieselguhr and step (1) the ultra micro calcining oyster shell powder mixing and stirring that precipitation obtains, first stirs dried 50min at 40 DEG C, exists afterwards Add the hydrogen peroxide mixing and stirring of gross weight 8%, obtain compound, this compound is put in control-temperature electric heating set and first uses often The intensification mode of heating of minutes 2 DEG C is heated with stirring to 110 DEG C of preliminary carbonizations and processes 20min, then temperature is raised and controls 180-190 DEG C, through 80-90min carbonization, then ball mill ball-milling treatment 30min, obtain marc base composite activated carbon standby With；
(4) amount of will be enriched in anthocyanidin blue berry fruit juice, the complex liquid rich in blue berry seed oil, phylloxanthin, hydroxyl isomaltulose, water solublity Coffee polyphenols, Inonqqus obliquus polyphenol purified are mixed and heated to 82-85 DEG C, are being rapidly cooled to 38 DEG C, during cooling Add marc base composite activated carbon mix and blend, stand 2-3h afterwards, take supernatant liquid, add xanthan gum mix and blend equal Even, obtain composite fruit juice standby；
(5) this composite fruit juice is heated rapidly on 98 DEG C, maintains 5s to carry out high-temperature instantaneous sterilization, use filling machine rapid afterwards Load the vial sterilized, seal while hot, be rapidly cooled to 38 DEG C after sealing, to obtain final product.
The invention have the advantage that the present invention uses blue berry to coordinate eucommia flower, Pollen of Masson Pine, Flos Camelliae sinensis enzymolysis ethanol extract system Standby composite blueberry fruit juice, has collaborative blood pressure lowering, lessens fatigue, alleviates visual fatigue, improves the effects such as memory；The most also Give the taste that single blue berry fruit juice is different so that it is there is certain unique flowery odour；The water soluble coffee polyphenol of employing, Pyropolyporus fomentarius (L.ex Fr.) Teng Pore fungi polyphenol purified enhances non-oxidizability and the stability of composite fruit juice, stablizes its effect；Use eucommia flower, horse hair Flos pini Powder, Flos Camelliae sinensis enzymolysis ethanol extract enrich the nutrition of blue berry fruit juice, it is achieved that the regulation of blue berry fruit juice sugariness, have preferably battalion Supporting health-care effect, preparation gets up to be also convenient for being easily achieved；Cause for the skin slag in the blue berry fruit juice course of processing, meat slag, seed slag Waste problem, use the supplementary means such as microwave, ultrasound wave and eucommia flower, Pollen of Masson Pine, Flos Camelliae sinensis and blueberry nutrient thing Intermiscibility between matter, has the most fully carried out including anthocyanidin and the extraction of blue berry seed oil, has enriched this composite fruit juice Nutrition；For removing the slag after nutrition, carry out the preparation of marc matrix activated carbon, and used it for composite fruit clarification of juice, it is achieved Making full use of of resource, meanwhile, decreases the usage amount of single clarifier the most to a certain extent, reaches preferably to clarify effect Really；The comprehensive high-efficiency achieving blue berry develops.The fiber content that prepared marc matrix activated carbon combines micronizing is few Marc, hydrogen peroxide and kieselguhr, calcining oyster shell powder, pore structure is flourishing, it is possible to realize the efficient clarification of composite fruit juice Absorption.
Detailed description of the invention
A kind of Cortex Eucommiae blue berry composite fruit juice containing Inonqqus obliquus polyphenol purified, including following parts by weight of component: blue berry 120, calcining Concha Ostreae 19, pectase 10, eucommia flower 21, horse hair Flos pini 22, Flos Camelliae sinensis 23, cellulase 7, citric acid 9, leaf Huang Element 4, hydroxyl isomaltulose 7, water soluble coffee polyphenol 10, Inonqqus obliquus polyphenol purified 12, xanthan gum 2, kieselguhr 15, appropriate The ethanol water of concentration 10%, appropriate water, appropriate hydrogen peroxide.
A kind of Cortex Eucommiae fruit blue berry composite fruit juice preparation method containing Inonqqus obliquus polyphenol purified, comprises the following steps:
(1) calcining Concha Ostreae is put into ball milling 30min in ball mill and obtains ultra micro calcining oyster shell powder to micron dimension, by blue berry Adding after removing decayed fruit in tank, in tank, stirring adds ultra micro calcining oyster shell powder continuously stirred 15min, pulls out fresh Blue berry, and precipitate that to dry ultra micro calcining oyster shell powder standby, with clear water strength spray irrigation remove rhizome and decayed fruit, Fresh blue berry is standby；Fresh blue berry is first prepared granular size with grater with beating crusher pulverization process 40min consistent Blue berry crushes thing, this blue berry crushes thing pulper process 30min and carries out Particle pollution process, obtain blueberry pulp thing, should Blueberry pulp thing adds pectase and the water of gross weight 1 times, at 40 DEG C after mix and blend 1h, uses at 650W microwave-assisted Manage 2 times, each 15min, use milling process to squeeze the juice afterwards, carry out coarse filtration with the screen cloth of aperture 0.5mm, must be rich in anthocyanidin Blue berry fruit juice and blueberry pomace are standby；
(2), after eucommia flower, horse hair Flos pini, Flos Camelliae sinensis first being rinsed well with clear water, put in super micron mill and pulverize Process 30min, afterwards with the ethanol water of the concentration 10% of blueberry pomace, citric acid, cellulase and gross weight 1 times, mixed Conjunction stirs, and after using ultrasonic Treatment 1h of 100W, carries out hollow-fibre membrane hyperfiltration treatment, after obtaining complex liquid and alcohol extraction Composite slag；Complex liquid is carried out at 15 DEG C heat alcohol extraction 1h obtain rich in blue berry seed oil complex liquid standby；
(3) it is the 5% of gross weight by first using vacuum drier dried 20min after composite slag after alcohol extraction to moisture, adopts By ball mill ball-milling treatment 30min, obtain ultramicronising and be combined ground-slag, ultramicronising is combined ground-slag, kieselguhr and step (1) precipitation The ultra micro calcining oyster shell powder mixing and stirring obtained, first stirs dried 50min at 40 DEG C, is adding gross weight afterwards The hydrogen peroxide mixing and stirring of amount 8%, obtains compound, is put in by this compound in control-temperature electric heating set and first uses 2 DEG C per minute Intensification mode of heating is heated with stirring to 110 DEG C of preliminary carbonizations and processes 20min, then temperature is raised and controls at 180 DEG C, warp 80min carbonization, then ball mill ball-milling treatment 30min, obtain marc base composite activated carbon standby；
(4) amount of will be enriched in anthocyanidin blue berry fruit juice, the complex liquid rich in blue berry seed oil, phylloxanthin, hydroxyl isomaltulose, water solublity Coffee polyphenols, Inonqqus obliquus polyphenol purified are mixed and heated to 82 DEG C, are being rapidly cooled to 38 DEG C, add during cooling Marc base composite activated carbon mix and blend, stands 2h afterwards, takes supernatant liquid, add xanthan gum mixing and stirring, Composite fruit juice is standby；
(5) this composite fruit juice is heated rapidly on 98 DEG C, maintains 5s to carry out high-temperature instantaneous sterilization, use filling machine rapid afterwards Load the vial sterilized, seal while hot, be rapidly cooled to 38 DEG C after sealing, to obtain final product.

Claims (2)

1. the Cortex Eucommiae blue berry composite fruit juice containing Inonqqus obliquus polyphenol purified, it is characterised in that include following weight portion group Point: blue berry 120-130, calcining Concha Ostreae 19-20, pectase 10-11, eucommia flower 21-22, horse hair Flos pini 22-23, Flos Camelliae sinensis 23-24, cellulase 7-8, citric acid 9-10, phylloxanthin 4-5, hydroxyl isomaltulose 7-8, water soluble coffee polyphenol 10-11, birch Brown pore fungi polyphenol purified 12-13, xanthan gum 2-3, kieselguhr 15-16, the ethanol water of appropriate concentration 10%, appropriate Water, appropriate hydrogen peroxide.
2. one kind containing Inonqqus obliquus polyphenol purified the Cortex Eucommiae fruit blue berry composite fruit juice preparation method, it is characterised in that include with Lower step:
(1) calcining Concha Ostreae is put into ball milling 30min in ball mill and obtains ultra micro calcining oyster shell powder to micron dimension, by blue berry Adding after removing decayed fruit in tank, in tank, stirring adds ultra micro calcining oyster shell powder continuously stirred 15min, pulls out fresh Blue berry, and precipitate that to dry ultra micro calcining oyster shell powder standby, with clear water strength spray irrigation remove rhizome and decayed fruit, Fresh blue berry is standby；Fresh blue berry is first prepared granular size with grater with beating crusher pulverization process 40min consistent Blue berry crushes thing, this blue berry crushes thing pulper process 30min and carries out Particle pollution process, obtain blueberry pulp thing, should Blueberry pulp thing adds pectase and the water of gross weight 1-1.2 times, at 40 DEG C after mix and blend 1h, uses 650W microwave auxiliary Help process 2 times, each 15min, use milling process to squeeze the juice afterwards, carry out coarse filtration with the screen cloth of aperture 0.5mm, must be rich in flower Blue or green element blue berry fruit juice and blueberry pomace are standby；
(2), after eucommia flower, horse hair Flos pini, Flos Camelliae sinensis first being rinsed well with clear water, put in super micron mill and pulverize Process 30min, afterwards with the ethanol water of the concentration 10% of blueberry pomace, citric acid, cellulase and gross weight 1-2 times, Mixing and stirring, after using ultrasonic Treatment 1h of 100W, carries out hollow-fibre membrane hyperfiltration treatment, obtains complex liquid and alcohol extraction Rear composite slag；Complex liquid is carried out at 15 DEG C heat alcohol extraction 1h obtain rich in blue berry seed oil complex liquid standby；
(3) it is gross weight by first using vacuum drier dried 20-30min to moisture after composite slag after alcohol extraction 5%, use ball mill ball-milling treatment 30min, obtain ultramicronising and be combined ground-slag, ultramicronising is combined ground-slag, kieselguhr and step (1) the ultra micro calcining oyster shell powder mixing and stirring that precipitation obtains, first stirs dried 50min at 40 DEG C, exists afterwards Add the hydrogen peroxide mixing and stirring of gross weight 8%, obtain compound, this compound is put in control-temperature electric heating set and first uses often The intensification mode of heating of minutes 2 DEG C is heated with stirring to 110 DEG C of preliminary carbonizations and processes 20min, then temperature is raised and controls 180-190 DEG C, through 80-90min carbonization, then ball mill ball-milling treatment 30min, obtain marc base composite activated carbon standby With；
(4) amount of will be enriched in anthocyanidin blue berry fruit juice, the complex liquid rich in blue berry seed oil, phylloxanthin, hydroxyl isomaltulose, water solublity Coffee polyphenols, Inonqqus obliquus polyphenol purified are mixed and heated to 82-85 DEG C, are being rapidly cooled to 38 DEG C, during cooling Add marc base composite activated carbon mix and blend, stand 2-3h afterwards, take supernatant liquid, add xanthan gum mix and blend equal Even, obtain composite fruit juice standby；
(5) this composite fruit juice is heated rapidly on 98 DEG C, maintains 5s to carry out high-temperature instantaneous sterilization, use filling machine rapid afterwards Load the vial sterilized, seal while hot, be rapidly cooled to 38 DEG C after sealing, to obtain final product.
CN201610396338.2A 2016-06-07 2016-06-07 Eucommia and blueberry composite fruit juice containing inonotus obliquus polyphenol purified product and preparation method of composite fruit juice Pending CN106036274A (en)

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CN107616208A (en) * 2017-09-01 2018-01-23 合肥学院 Blueberry moon cake and preparation method thereof
CN110643582A (en) * 2019-09-29 2020-01-03 浙江工业大学 Method for extracting SOD from fresh sea-buckthorn fruit
CN113016968A (en) * 2021-05-12 2021-06-25 黑龙江八一农垦大学 Inonotus obliquus and coarse cereal composite beverage

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CN104273600A (en) * 2013-07-11 2015-01-14 全武 Novel fresh fruit juice beverage
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CN104273600A (en) * 2013-07-11 2015-01-14 全武 Novel fresh fruit juice beverage
CN104187964A (en) * 2014-08-19 2014-12-10 王慧君 Cabbage compound fruit and vegetable juice and preparation method thereof
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107616208A (en) * 2017-09-01 2018-01-23 合肥学院 Blueberry moon cake and preparation method thereof
CN110643582A (en) * 2019-09-29 2020-01-03 浙江工业大学 Method for extracting SOD from fresh sea-buckthorn fruit
CN113016968A (en) * 2021-05-12 2021-06-25 黑龙江八一农垦大学 Inonotus obliquus and coarse cereal composite beverage

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Application publication date: 20161026