CN108096047A - Domiphen bromide xylitol combination of acidic mouthwash and preparation method thereof - Google Patents
Domiphen bromide xylitol combination of acidic mouthwash and preparation method thereof Download PDFInfo
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- CN108096047A CN108096047A CN201810137128.0A CN201810137128A CN108096047A CN 108096047 A CN108096047 A CN 108096047A CN 201810137128 A CN201810137128 A CN 201810137128A CN 108096047 A CN108096047 A CN 108096047A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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Abstract
The invention discloses a kind of Domiphen bromide xylitol combination of acidic mouthwash, component includes：Sweetener 0.1%~5%；Acid 0.01%~0.3%；Moisturizer 2%~15%；Essence 0.05%~0.5%；Solubilizer 0.5%~2.5%；Bacteriostatic agent 0.02%~0.05%；Preservative 0.1%~0.4%；Deionized water surplus；The PH of the mouthrinse product is 3~5.Sweetener and acid are added in into stirring and dissolving in water deionization, then moisturizer is added in aqueous solution；Solubilizer and essence are stirred to form uniform oily solution；In the state of stirring, oily solution is slowly added into water-soluble clarified solution；Bacteriostatic agent, preservative are added in aqueous solution, are mixed evenly；Stand 24 it is small when, filtering, after aseptic process PH be 3~5 mouthwash finished product.Acid environment, it is easier to the adhesion of tooth and staining be made to have clean more thorough effect, while xylitol can carry out antieurodontic effect.
Description
Technical field
The present invention relates to oral care product technical field more particularly to a kind of Domiphen bromide xylitol combination of acidic mouthwashes
And preparation method thereof.
Background technology
With the improvement of living standards, people increasingly improve the attention rate of oral health, common oral care is also no longer
It is confined to brush teeth twice sooner or later, the species and form demand to oral care product tend to diversification and fashion-orientation.Mouthwash is
Through into the necessity in for people's lives, it is easy to use, and effect can be equal to toothpaste, and use is more convenient than toothpaste, but mesh
The mouthwash of preceding market often act on it is single, and for a long time use protective effect is not had to tooth.It is also, existing at present
The acid-base value of mouthwash be generally neutrality, main function include antibacterial bacteriostatic, improve oral peculiar smell, anti-inflammatory, cleaning oral cavity it is thin
Bacterium and tartar etc., species include Chinese medicine draft class, natural plant extracts class and drug ingedient composite class.
CN102988206 A disclose a kind of deodorant mouth wash, it is by lemon oil, perilla herb oil, peppermint oil, ethyl alcohol, phosphorus
Sour hydrogen calcium anhydrous salt, sorbierite, xylitol and distilled water mixed preparing form, and the parts by weight of each component are：Lemon oil：1-
2 parts；Perilla herb oil：1-2 parts；Peppermint oil：1-2 parts；Ethyl alcohol：10-20 parts；Calcium monohydrogen phosphate anhydrous salt：1-2 parts；Sorbierite：1-
2 parts；Xylitol：1-2 parts；Distilled water：80-100 parts.A kind of deodorant mouth wash of the present invention, not only with stronger
The effect of halitosis is removed, while permanent tooth can also be played the role of.
CN105395422 A disclose antibacterial anti-inflammatory mouthwash, are made of the raw material of following parts by weight：Radix Glycyrrhizae 3-5
Part, 2-5 parts of dried orange peel, 5-10 parts of Radix Notoginseng, 0.5-1 parts of rose extract, 0.5-1 parts of caryophyllus oil, Honegsukle flower P.E 0.5-
1 part, 2-5 parts of Flos Chrysanthemi Indici extract, 1-3 parts of green-tea extract, 70-75 parts of soda water.The present invention has antibacterial anti-inflammatory
Effect, cleaning oral cavity are killed except microorganism and tartar, eliminate oral peculiar smell, and product itself is free of preservative, can be with long-time service.
103893026 A of CN disclose a kind of for oral cleaning and the mouthwash of health care.Each component and its weight are：
Small active peptides 0.2%-2%, glycerine 5%-15%, rilanit special 0.5%-2%, chlorhexidine gluconate 0.05%-0.5%,
Xylitol 2.5%-10%, potassium sorbate 0.1%-0.3%, Sucralose 0.01%-0.03%, menthol 0.025%-0.1%, sweet tea
Orange essence 0.025%-0.1%, ethyl alcohol 1%-15%, remaining is distilled water.The mouthwash of the present invention not only has suppression to human oral cavity
Bacterium and cleaning action, and small active peptides are used in combination with chlorhexidine gluconate and are repaiied with anti-inflammatory, acceleration mucous membrane of mouth
Again, the effects that treatment canker sore.
103385821 A of CN are related to a kind of mouthwash of in-depth tartar removal, and constituent has：Glycerine, polyoxypropylene,
Western pyrrole chloramines, peppermint, motherwort extracting solution, tea polyphenols, strontium chloride, deionized water.The present invention can be with deep layer cleaning tartar, inhibition
Oral bacteria grows, removes implication, tooth-whitening, inhibits dental plaque generation, while to treatment gingivitis, periodontitis, canker sore
Wait oral inflammations that there is certain alleviation, cure.
Various mouthwashes described in above-mentioned patent, although play the antibacterial anti-inflammatory to tooth and oral cavity, cleaning oral cavity and
Tooth and the effect for being effectively improved oral peculiar smell, but it is substantially neutrality, it is well known that tartar and dental surface it is glutinous
The staining of object and long-term accumulation can not remove in a short time, although above-mentioned technological means can remove part
Swill and tartar, but be intended to thoroughly remove, the stainings such as crock, tooth Huang can not be removed by brushing teeth sooner or later,
It is even more to be difficult to thorough removing by the way of gargling.Therefore, the adhesion of tooth how effectively, quickly, is thoroughly realized
With the removing of staining, while antieurodontic purpose can be carried out, be restrict current mouth cavity daily nursing industry one
Problem, and the mouthwash of pure Chinese medicine ingredient primarily serves the effect of reparation, anti-inflammatory, and also it is past to act on external Chinese medicine effect
Toward slowly, it is not obvious for the effect of bacteriostasis antibiosis.
The content of the invention
It in view of the deficienciess of the prior art, can be to oral cavity the technical problem to be solved by the invention is to provide one kind
While cleaning, dispel implication and bacteria resistance function, it is easier to make the adhesion of tooth and staining have it is clean more thoroughly,
There is Domiphen bromide xylitol combination of acidic mouthwash of anti-decayed tooth effect and preparation method thereof simultaneously.
In order to solve the above technical problems, the technical solution used in the present invention is：A kind of Domiphen bromide xylitol combination of acidic
Mouthwash, by forming following weight percentage components：
Sweetener 0.1%~5%；
Acid 0.01%~0.3%；
Moisturizer 2%~15%；
Essence 0.05%~0.5%；
Solubilizer 0.5%~2.5%；
Bacteriostatic agent 0.02%~0.05%；
Preservative 0.1%~0.4%；
Deionized water surplus；
The PH of the mouthrinse product is 3~5.
Above-mentioned Domiphen bromide xylitol combination of acidic mouthwash, by forming following weight percentage components：
Sweetener 2%；
Acid 0.1%；
Moisturizer 8%；
Essence 0.3%；
Solubilizer 1.5%；
Bacteriostatic agent 0.03%；
Preservative 0.2%；
Deionized water surplus；
The PH of the mouthrinse product is 4.
Above-mentioned Domiphen bromide xylitol combination of acidic mouthwash, the sweetener are xylitol, acid for citric acid or
Malic acid, moisturizer are one or more of glycerine, sorbierite, propylene glycol, and essence is the water such as green tea, spearmint, honey peach
Fruity or the fragrance of a flower, solubilizer are polysorbas20 or Cremophor RH40, and preservative is potassium sorbate, sodium benzoate, oxybenzene first
One or more of ester, bacteriostatic agent are Domiphen bromide.
Above-mentioned Domiphen bromide xylitol combination of acidic mouthwash, the mouthwash are 0.5% also added with weight percent
Coolant agent.
Above-mentioned Domiphen bromide xylitol combination of acidic mouthwash, the coolant agent are menthol.
A kind of method for preparing Domiphen bromide xylitol combination of acidic mouthwash, includes the following steps：
（1）, sweetener and acid are added in stirring and dissolving in water deionization, then moisturizer is added in aqueous solution, stirring is equal
It is even and form finely dispersed water-soluble clarified solution；
（2）, solubilizer and essence stirred to form uniform oily solution；
（3）, in the state of stirring, oily solution is slowly added into water-soluble clarified solution, be uniformly mixed；
（4）, by bacteriostatic agent, preservative add in step（3）In the aqueous solution of acquisition, it is mixed evenly；
（5）, stop stirring, stand 24 it is small when, filtering, after aseptic process PH be 3~5 mouthwash finished product.
The preparation method of above-mentioned Domiphen bromide xylitol combination of acidic mouthwash, the step（2）Middle addition weight percent
Than the coolant agent for 0.5%.
The preparation method of above-mentioned Domiphen bromide xylitol combination of acidic mouthwash, the sweetener be xylitol, acid
For citric acid or malic acid, moisturizer is glycerine, one or more of sorbierite, propylene glycol, essence is green tea, spearmint,
The fruit such as honey peach are fragrant or the fragrance of a flower, solubilizer are polysorbas20 or Cremophor RH40, and preservative is potassium sorbate, benzoic acid
One or more of sodium, methyl hydroxybenzoate, bacteriostatic agent are Domiphen bromide.
The preparation method of above-mentioned Domiphen bromide xylitol combination of acidic mouthwash, the coolant agent are menthol.
The advantages of Domiphen bromide xylitol combination of acidic mouthwash of the present invention and preparation method thereof is：Add Domiphen bromide and cool taste
Agent can be grown with deep layer cleaning tartar, inhibition oral bacteria, remove implication, tooth-whitening, inhibit dental plaque generation, while to controlling
Treating the oral inflammations such as gingivitis, periodontitis, canker sore has effects that certain alleviation, cures.And it to oral cleaning, dispels
While implication and bacteria resistance function, acid environment, it is easier to make the adhesion of tooth and staining have it is clean more thorough
The effect of bottom, while xylitol can carry out antieurodontic effect.
Specific embodiment
The present invention is described in further details with reference to specific embodiment；
Embodiment 1：
A kind of Domiphen bromide xylitol combination of acidic mouthwash, by forming following weight percentage components：Sweetener 0.1%；Tart flavour
Agent 0.01%；Moisturizer 2%；Essence 0.05%；Solubilizer 0.5%；Bacteriostatic agent 0.02%；Preservative 0.1%；Coolant agent 0.5%；Go from
Sub- water surplus；The PH of the mouthrinse product is 5.Sweetener is xylitol, and acid is citric acid, and moisturizer is glycerine, mountain
Pears alcohol, essence are the green tea fragrance of a flower, and solubilizer is polysorbas20, and coolant agent is menthol, and preservative is potassium sorbate, and bacteriostatic agent is degree
Meter Fen.
The method that the present invention prepares Domiphen bromide xylitol combination of acidic mouthwash, includes the following steps：
（1）, sweetener and acid are added in stirring and dissolving in water deionization, then moisturizer is added in aqueous solution, stirring is equal
It is even and form finely dispersed water-soluble clarified solution；
（2）, solubilizer, essence and coolant agent stirred to form uniform oily solution；
（3）, in the state of stirring, oily solution is slowly added into water-soluble clarified solution, be uniformly mixed；
（4）, by bacteriostatic agent, preservative add in step（3）In the aqueous solution of acquisition, it is mixed evenly；
（5）, stop stirring, stand 24 it is small when, filtering, after aseptic process PH be 5 mouthwash finished product.
Sweetener is xylitol, and acid is citric acid, and moisturizer is glycerine, sorbierite, and essence is the green tea fragrance of a flower, solubilized
Agent is polysorbas20, and coolant agent is menthol, and preservative is potassium sorbate, and bacteriostatic agent is Domiphen bromide.
Embodiment 2：
A kind of Domiphen bromide xylitol combination of acidic mouthwash, by forming following weight percentage components：
Sweetener 2%；Acid 0.1%；Moisturizer 8%；Essence 0.3%；Solubilizer 1.5%；Bacteriostatic agent 0.03%；Preservative 0.2%；
Coolant agent 0.5%；Deionized water surplus；The PH of the mouthrinse product is 4.
Sweetener is xylitol, and acid is malic acid, and moisturizer is sorbierite, propylene glycol, and essence is the spearmint fragrance of a flower,
Solubilizer is Cremophor RH40, and coolant agent is menthol, and preservative is sodium benzoate, methyl hydroxybenzoate, and bacteriostatic agent is degree
Meter Fen.
The method that the present invention prepares Domiphen bromide xylitol combination of acidic mouthwash, includes the following steps：
（1）, sweetener and acid are added in stirring and dissolving in water deionization, then moisturizer is added in aqueous solution, stirring is equal
It is even and form finely dispersed water-soluble clarified solution；
（2）, solubilizer, essence and coolant agent stirred to form uniform oily solution；
（3）, in the state of stirring, oily solution is slowly added into water-soluble clarified solution, be uniformly mixed；
（4）, by bacteriostatic agent, preservative add in step（3）In the aqueous solution of acquisition, it is mixed evenly；
（5）, stop stirring, stand 24 it is small when, filtering, after aseptic process PH be 4 mouthwash finished product.
The sweetener is xylitol, and acid is malic acid, and moisturizer is sorbierite, propylene glycol, and essence is spearmint
The fragrance of a flower, solubilizer are Cremophor RH40, and coolant agent is menthol, and preservative is sodium benzoate, methyl hydroxybenzoate, bacteriostatic agent
For Domiphen bromide.
Embodiment 3：
A kind of Domiphen bromide xylitol combination of acidic mouthwash, by forming following weight percentage components：Sweetener 5%；Acid
0.3%；Moisturizer 15%；Essence 0.5%；Solubilizer 2.5%；Bacteriostatic agent 0.05%；Preservative 0.4%；Coolant agent 0.5%；Deionized water
Surplus；The PH of the mouthrinse product is 3.
The sweetener is xylitol, and acid is citric acid, and moisturizer is glycerine, propylene glycol, and essence is honey peach water
Fruity, solubilizer are polysorbas20, and coolant agent is menthol, and preservative is potassium sorbate, methyl hydroxybenzoate, and bacteriostatic agent is Domiphen bromide.
The method that the present invention prepares Domiphen bromide xylitol combination of acidic mouthwash, includes the following steps：
（1）, sweetener and acid are added in stirring and dissolving in water deionization, then moisturizer is added in aqueous solution, stirring is equal
It is even and form finely dispersed water-soluble clarified solution；
（2）, solubilizer, essence and coolant agent stirred to form uniform oily solution；
（3）, in the state of stirring, oily solution is slowly added into water-soluble clarified solution, be uniformly mixed；
（4）, by bacteriostatic agent, preservative add in step（3）In the aqueous solution of acquisition, it is mixed evenly；
（5）, stop stirring, stand 24 it is small when, filtering, after aseptic process PH be 3 mouthwash finished product.
The sweetener is xylitol, and acid is citric acid, and moisturizer is glycerine, propylene glycol, and essence is honey peach water
Fruity, solubilizer are polysorbas20, and coolant agent is menthol, and preservative is potassium sorbate, methyl hydroxybenzoate, and bacteriostatic agent is Domiphen bromide.
Certainly, it is limitation of the present invention that above description, which is not, and the present invention is also not limited to the example above, the art
Those of ordinary skill, in the essential scope of the present invention, the variations, modifications, additions or substitutions made should all belong to the present invention
Protection domain.
Claims (9)
1. a kind of Domiphen bromide xylitol combination of acidic mouthwash, which is characterized in that by forming following weight percentage components：
Sweetener 0.1%~5%；
Acid 0.01%~0.3%；
Moisturizer 2%~15%；
Essence 0.05%~0.5%；
Solubilizer 0.5%~2.5%；
Bacteriostatic agent 0.02%~0.05%；
Preservative 0.1%~0.4%；
Deionized water surplus；
The PH of the mouthrinse product is 3~5.
2. Domiphen bromide xylitol combination of acidic mouthwash according to claim 1, it is characterized in that, by following weight percent
Component composition：
Sweetener 2%；
Acid 0.1%；
Moisturizer 8%；
Essence 0.3%；
Solubilizer 1.5%；
Bacteriostatic agent 0.03%；
Preservative 0.2%；
Deionized water surplus；
The PH of the mouthrinse product is 4.
3. Domiphen bromide xylitol combination of acidic mouthwash according to claim 1, it is characterized in that：The sweetener is xylose
Alcohol, acid are citric acid or malic acid, and moisturizer is one or more of glycerine, sorbierite, propylene glycol, and essence is green
The fruit such as tea, spearmint, honey peach are fragrant or the fragrance of a flower, solubilizer are polysorbas20 or Cremophor RH40, and preservative is sorb
One or more of sour potassium, sodium benzoate, methyl hydroxybenzoate, bacteriostatic agent are Domiphen bromide.
4. Domiphen bromide xylitol combination of acidic mouthwash according to claim 1, it is characterized in that：The mouthwash also adds
There is the coolant agent that weight percent is 0.5%.
5. Domiphen bromide xylitol combination of acidic mouthwash according to claim 4, it is characterized in that：The coolant agent is peppermint
Alcohol.
A kind of 6. method for preparing Domiphen bromide xylitol combination of acidic mouthwash, which is characterized in that include the following steps：
（1）, sweetener and acid are added in stirring and dissolving in water deionization, then moisturizer is added in aqueous solution, stirring is equal
It is even and form finely dispersed water-soluble clarified solution；
（2）, solubilizer, essence stirred to form uniform oily solution；
（3）, in the state of stirring, oily solution is slowly added into water-soluble clarified solution, be uniformly mixed；
（4）, by bacteriostatic agent, preservative add in step（3）In the aqueous solution of acquisition, it is mixed evenly；
（5）, stop stirring, stand 24 it is small when, filtering, after aseptic process PH be 3~5 mouthwash finished product.
7. the preparation method of Domiphen bromide xylitol combination of acidic mouthwash according to claim 6, it is characterized in that：The step
Suddenly（2）The coolant agent that middle addition weight percent is 0.5%.
8. the preparation method of Domiphen bromide xylitol combination of acidic mouthwash according to claim 6, it is characterized in that：The sweet tea
Taste agent is xylitol, and acid is citric acid or malic acid, and moisturizer is glycerine, sorbierite, one or more of propylene glycol,
Essence is the fruit such as green tea, spearmint, honey peach is fragrant or the fragrance of a flower, and solubilizer is polysorbas20 or Cremophor RH40, cool taste
Agent is menthol, and preservative is one or more of potassium sorbate, sodium benzoate, methyl hydroxybenzoate, and bacteriostatic agent is Domiphen bromide.
9. the preparation method of Domiphen bromide xylitol combination of acidic mouthwash according to claim 7, it is characterized in that：It is described cool
Taste agent is menthol.
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Cited By (5)
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| CN109010098A (en) * | 2018-10-23 | 2018-12-18 | 郑州吉尔康消毒制品有限公司 | Antimicrobial mouthwash and preparation method thereof |
| CN112245317A (en) * | 2020-09-07 | 2021-01-22 | 广州雨晓生物制品有限公司 | Mouthwash |
| CN112675261A (en) * | 2021-01-05 | 2021-04-20 | 安徽中医药大学第一附属医院(安徽省中医院) | Traditional Chinese medicine mouth wash capable of diminishing inflammation and promoting fluid production and preparation method thereof |
| CN113499272A (en) * | 2021-09-05 | 2021-10-15 | 广州市九叶化妆品有限公司 | Chlorhexidine gluconate-containing mouthwash and preparation method thereof |
| CN113712863A (en) * | 2021-08-27 | 2021-11-30 | 广东南方洁灵科技实业有限公司 | Mild and non-irritant oral mouthwash and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109010098A (en) * | 2018-10-23 | 2018-12-18 | 郑州吉尔康消毒制品有限公司 | Antimicrobial mouthwash and preparation method thereof |
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| CN113712863A (en) * | 2021-08-27 | 2021-11-30 | 广东南方洁灵科技实业有限公司 | Mild and non-irritant oral mouthwash and preparation method thereof |
| CN113499272A (en) * | 2021-09-05 | 2021-10-15 | 广州市九叶化妆品有限公司 | Chlorhexidine gluconate-containing mouthwash and preparation method thereof |
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Application publication date: 20180601 |