CN108046833A - 一种具有多孔发热膜结构的陶瓷加热体的制备工艺 - Google Patents

一种具有多孔发热膜结构的陶瓷加热体的制备工艺 Download PDF

Info

Publication number
CN108046833A
CN108046833A CN201711394637.3A CN201711394637A CN108046833A CN 108046833 A CN108046833 A CN 108046833A CN 201711394637 A CN201711394637 A CN 201711394637A CN 108046833 A CN108046833 A CN 108046833A
Authority
CN
China
Prior art keywords
porous
matrix
slurry
ceramic
membrane structure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201711394637.3A
Other languages
English (en)
Other versions
CN108046833B (zh
Inventor
丁毅
程宏生
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenzhen ALD Technology Co Ltd
Original Assignee
ALD Group Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ALD Group Ltd filed Critical ALD Group Ltd
Priority to CN201711394637.3A priority Critical patent/CN108046833B/zh
Priority to PCT/CN2018/074111 priority patent/WO2019119611A1/zh
Publication of CN108046833A publication Critical patent/CN108046833A/zh
Priority to US16/906,518 priority patent/US11498875B2/en
Application granted granted Critical
Publication of CN108046833B publication Critical patent/CN108046833B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81—Coating or impregnation
    • C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
    • C04B41/90—Coating or impregnation for obtaining at least two superposed coatings having different compositions at least one coating being a metal
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/62625—Wet mixtures
    • C04B35/6264—Mixing media, e.g. organic solvents
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62218—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining ceramic films, e.g. by using temporary supports
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/62222—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining ceramic coatings
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/6261—Milling
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/62625—Wet mixtures
    • C04B35/6263—Wet mixtures characterised by their solids loadings, i.e. the percentage of solids
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/62645—Thermal treatment of powders or mixtures thereof other than sintering
    • C04B35/6265—Thermal treatment of powders or mixtures thereof other than sintering involving reduction or oxidation
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632—Organic additives
    • C04B35/636—Polysaccharides or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64—Burning or sintering processes
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/06—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by burning-out added substances by burning natural expanding materials or by sublimating or melting out added substances
    • C04B38/063—Preparing or treating the raw materials individually or as batches
    • C04B38/0635—Compounding ingredients
    • C04B38/0645—Burnable, meltable, sublimable materials
    • C04B38/0675—Vegetable refuse; Cellulosic materials, e.g. wood chips, cork, peat, paper
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/08—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by adding porous substances
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/4505—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements characterised by the method of application
    • C04B41/455—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements characterised by the method of application the coating or impregnating process including a chemical conversion or reaction
    • C04B41/4558—Coating or impregnating involving the chemical conversion of an already applied layer, e.g. obtaining an oxide layer by oxidising an applied metal layer
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/4578—Coating or impregnating of green ceramics or unset concrete
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/4582—Porous coatings, e.g. coating containing porous fillers
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/51—Metallising, e.g. infiltration of sintered ceramic preforms with molten metal
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81—Coating or impregnation
    • C04B41/85—Coating or impregnation with inorganic materials
    • C04B41/88—Metals
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54—Particle size related information
    • C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5454—Particle size related information expressed by the size of the particles or aggregates thereof nanometer sized, i.e. below 100 nm
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/612—Machining
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6562—Heating rate
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567—Treatment time
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/658—Atmosphere during thermal treatment
    • C04B2235/6583—Oxygen containing atmosphere, e.g. with changing oxygen pressures
    • C04B2235/6585—Oxygen containing atmosphere, e.g. with changing oxygen pressures at an oxygen percentage above that of air
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
    • C04B2235/661—Multi-step sintering

Abstract

本发明公开了一种具有多孔发热膜结构的陶瓷加热体的制备工艺，涉及加热体的制备工艺技术领域；该工艺包括混料、球磨、托盘、成型与干燥、烧结、灌蜡、机加工、涂覆、金属化烧结、接电极；本发明的有益效果是：整个制造工艺简单，通过采用箱式炉在氧化气氛和常压下烧结胚体，制得的加热体加热均匀且加热效率高。

Description

一种具有多孔发热膜结构的陶瓷加热体的制备工艺
技术领域
本发明涉及加热体的制备工艺技术领域，更具体的说，本发明涉及一种具有多孔发热膜结构的陶瓷加热体的制备工艺。
背景技术
氮化硅发热片是一种结合高性能氮化硅陶瓷基体和长寿命大功率的高温金属发热丝的器件，其具有体积小，功率大和热效率高等特点，同时通过氮化硅发热片产热也被证明是一种安全可靠的发热方式。
目前，传统的氮化硅陶瓷加热片是将钨丝埋在氮化硅粉末内成型成片状体热压烧结而成，此工艺生产的加热器由于受工艺限制，钨丝很难定位，成型过程中造成位置偏移，造成加热器整体传热不均，同时由于钨丝与氮化硅粉体有明显的界面，烧结后很难成为一体，钨丝与陶瓷接触面形成空隙，加热过程中形成局部氧化，降低发热片的使用寿命。
目前氮化硅陶瓷加热片的烧结也有采用反应烧结，然而反应烧结致密度差，力学性能差，加热体的加热不均匀。
发明内容
为了克服现有技术的不足，本发明提供一种具有多孔发热膜结构的陶瓷加热体的制备工艺，该制备工艺所制得的加热体加热均匀，且加热效率高。
本发明解决其技术问题所采用的技术方案是：一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其改进之处在于：该工艺包括以下的步骤：
A、混料：按质量百分比称取15-55%的硅藻土、5-25%的淀粉、0-2%的纳米二氧化硅溶液、40-70%的去离子水并混合搅拌均匀，制得陶瓷基体浆料；
按质量百分比称取15-40%的电阻浆料、30-60%的淀粉、10-30%的有机溶剂并混和搅拌均匀，制得有造孔剂的电阻浆料；
B、球磨：向步骤A中制得的陶瓷基体浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为4-24h；
向步骤A中制得的电阻浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为24-48h；
C、将步骤B中湿法球磨后的陶瓷基体浆料在真空条件下进行脱泡；
将步骤B中湿法球磨后的电阻浆料在真空条件下进行脱泡；
D、成型与干燥：将步骤C中制得的陶瓷基体浆料用浇注机浇注制成所需形状的陶瓷基体，并将陶瓷基体进行干燥，以形成胚体；
E、烧结：将步骤D制得的坯体置于石墨坩埚中，并埋入隔离粉，此后用箱式炉将埋于隔离粉中的坯体在常压下进行烧结，烧结气氛为氧气，坯体烧结制得多孔陶瓷加热体基体半成品；
F、灌蜡：将石蜡用加热筒液化，将步骤E制得的多孔陶瓷加热体基体半成品完全浸入到液化的石蜡中1-5h，之后在常温下冷却4-24h得到含有石蜡的多孔陶瓷加热体基体；
G、机加工：将步骤F中制得的含有石蜡的多孔陶瓷加热体基体进行机加工，去除多孔陶瓷加热体基体外表面的石蜡层；
H、涂覆：将步骤C中制得的电阻浆料按所需厚度涂覆于在步骤G中制得的多孔陶瓷加热体基体的外表面，电阻浆料在陶瓷基体表面形成一层发热膜；
I、金属化烧结：将步骤H中制得的具有发热膜结构的多孔陶瓷加热体基体置于石墨坩埚中，此后置于烧结炉中进行排蜡和多孔电阻发热膜的金属化烧结；
J、接电极：将步骤I中制得的加热体坯体两端进行表面镀镍处理，再于镀镍处理后的部位进行钎焊引出电极，制得多孔陶瓷加热体成品。
进一步的，所述的步骤A中，陶瓷基体浆料由以下质量百分比的原料组成：
硅藻土21%
淀粉16%
纳米二氧化硅溶液1%
去离子水62%。
进一步的，所述的步骤A中，电阻浆料由以下质量百分比的原料组成：
电阻浆料30%
淀粉45%
有机溶剂25%。
进一步的，所述的步骤A中，陶瓷基体浆料由以下质量百分比的原料组成：
硅藻土15%
淀粉15%
去离子水70%。
进一步的，所述的步骤A中，电阻浆料由以下质量百分比的原料组成：
电阻浆料40%
淀粉30%
有机溶剂30%。
进一步的，所述的步骤A中，陶瓷基体浆料由以下质量百分比的原料组成：
硅藻土50%
淀粉8%
纳米二氧化硅溶液2%
去离子水40%。
进一步的，所述的步骤A中，电阻浆料由以下质量百分比的原料组成：
电阻浆料30%
淀粉50%
有机溶剂20%。
进一步的，所述的步骤E中，对胚体进行烧结时的烧结温度为900-1400℃，升温速率为1-20℃/min，保温时间为2-12h。
进一步的，所述的步骤I中，金属化烧结的升温速率为1-5℃/min，金属化烧结温度为800-1000℃，时间为1-2h。
本发明的有益效果是：本发明提供了一种具有多孔发热膜结构的陶瓷加热体的制备工艺，该工艺依次通过混料、球磨、托盘、成型与干燥、烧结、灌蜡、机加工、涂覆、金属化烧结、接电极，整个制造工艺简单，通过采用箱式炉在氧化气氛和常压下烧结胚体，制得的加热体加热均匀且加热效率高。
附图说明
图1为本发明的一种具有多孔发热膜结构的陶瓷加热体的制备工艺的工艺流程图。
具体实施方式
下面结合附图和实施例对本发明进一步说明。
以下将结合实施例和附图对本发明的构思、具体结构及产生的技术效果进行清楚、完整地描述，以充分地理解本发明的目的、特征和效果。显然，所描述的实施例只是本发明的一部分实施例，而不是全部实施例，基于本发明的实施例，本领域的技术人员在不付出创造性劳动的前提下所获得的其他实施例，均属于本发明保护的范围。另外，专利中涉及到的所有联接/连接关系，并非单指构件直接相接，而是指可根据具体实施情况，通过添加或减少联接辅件，来组成更优的联接结构。本发明创造中的各个技术特征，在不互相矛盾冲突的前提下可以交互组合。
实施例1
参照图1所示，本发明揭示了一种具有多孔发热膜结构的陶瓷加热体的制备工艺，具体的，该工艺包括以下的步骤：
A、混料：按质量百分比称取21%的硅藻土、16%的淀粉、1%的纳米二氧化硅溶液、62%的去离子水并混合搅拌均匀，制得陶瓷基体浆料；
按质量百分比称取30%的电阻浆料、45%的淀粉、25%的有机溶剂并混和搅拌均匀，制得有造孔剂的电阻浆料；
B、球磨：向步骤A中制得的陶瓷基体浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为24h；向步骤A中制得的电阻浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为48h；
C、脱泡：将步骤B中湿法球磨后的陶瓷基体浆料在真空条件下进行脱泡；将步骤B中湿法球磨后的电阻浆料在真空条件下进行脱泡；
D、成型与干燥：将步骤C中制得的陶瓷基体浆料用浇注机浇注制成所需形状的陶瓷基体，并将陶瓷基体进行干燥，以形成胚体；
E、烧结：将步骤D制得的坯体置于石墨坩埚中，并埋入隔离粉，此后用箱式炉将埋于隔离粉中的坯体在常压下进行烧结，烧结气氛为氧气，升温速率为5℃/min，烧结温度为1200℃，保温时间为2h，坯体烧结制得多孔陶瓷加热体基体半成品；
F、灌蜡：将石蜡用加热筒液化，将步骤E制得的多孔陶瓷加热体基体半成品完全浸入到液化的石蜡中5h，之后在常温下冷却24h得到含有石蜡的多孔陶瓷加热体基体；
G、机加工：将步骤F中制得的含有石蜡的多孔陶瓷加热体基体进行机加工，去除多孔陶瓷加热体基体外表面的石蜡层；
H、涂覆：将步骤C中制得的电阻浆料按所需厚度涂覆于在步骤G中制得的多孔陶瓷加热体基体的外表面，电阻浆料在陶瓷基体表面形成一层发热膜；
I、金属化烧结：将步骤H中制得的具有发热膜结构的多孔陶瓷加热体基体置于石墨坩埚中，此后置于烧结炉中进行排蜡和多孔电阻发热膜的金属化烧结，其中升温速率为2℃/min，金属化烧结温度为850℃，时间为1h；
J、接电极：将步骤I中制得的加热体坯体两端进行表面镀镍处理，再于镀镍处理后的部位进行钎焊引出电极，制得多孔陶瓷加热体成品。
实施例2
参照图1所示，本发明揭示了一种具有多孔发热膜结构的陶瓷加热体的制备工艺，具体的，该工艺包括以下的步骤：
A、混料：按质量百分比称取15%的硅藻土、15%的淀粉、70%的去离子水并混合搅拌均匀，制得陶瓷基体浆料；
按质量百分比称取40%的电阻浆料、30%的淀粉、30%的有机溶剂并混和搅拌均匀，制得有造孔剂的电阻浆料；
B、球磨：向步骤A中制得的陶瓷基体浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为14h；
向步骤A中制得的电阻浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为36h；
C、脱泡：将步骤B中湿法球磨后的陶瓷基体浆料在真空条件下进行脱泡；将步骤B中湿法球磨后的电阻浆料在真空条件下进行脱泡；
D、成型与干燥：将步骤C中制得的陶瓷基体浆料用浇注机浇注制成所需形状的陶瓷基体，并将陶瓷基体进行干燥，以形成胚体；
E、烧结：将步骤D制得的坯体置于石墨坩埚中，并埋入隔离粉，此后用箱式炉将埋于隔离粉中的坯体在常压下进行烧结，烧结气氛为氧气，坯体烧结制得多孔陶瓷加热体基体半成品；对胚体进行烧结时的烧结温度为900℃，升温速率为1℃/min，保温时间为2h；
F、灌蜡：将石蜡用加热筒液化，将步骤E制得的多孔陶瓷加热体基体半成品完全浸入到液化的石蜡中1h，之后在常温下冷却4h得到含有石蜡的多孔陶瓷加热体基体；
G、机加工：将步骤F中制得的含有石蜡的多孔陶瓷加热体基体进行机加工，去除多孔陶瓷加热体基体外表面的石蜡层；
H、涂覆：将步骤C中制得的电阻浆料按所需厚度涂覆于在步骤G中制得的多孔陶瓷加热体基体的外表面，电阻浆料在陶瓷基体表面形成一层发热膜；
I、金属化烧结：将步骤H中制得的具有发热膜结构的多孔陶瓷加热体基体置于石墨坩埚中，此后置于烧结炉中进行排蜡和多孔电阻发热膜的金属化烧结；金属化烧结的升温速率为1℃/min，金属化烧结温度为 800℃，时间为1h；
J、接电极：将步骤I中制得的加热体坯体两端进行表面镀镍处理，再于镀镍处理后的部位进行钎焊引出电极，制得多孔陶瓷加热体成品。
实施例3
参照图1所示，本发明揭示了一种具有多孔发热膜结构的陶瓷加热体的制备工艺，具体的，该工艺包括以下的步骤：
A、混料：按质量百分比称取50%的硅藻土、8%的淀粉、2%的纳米二氧化硅溶液、40%的去离子水并混合搅拌均匀，制得陶瓷基体浆料；
按质量百分比称取30%的电阻浆料、50%的淀粉、20%的有机溶剂并混和搅拌均匀，制得有造孔剂的电阻浆料；
B、球磨：向步骤A中制得的陶瓷基体浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为4h；
向步骤A中制得的电阻浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为24h；
C、脱泡：将步骤B中湿法球磨后的陶瓷基体浆料在真空条件下进行脱泡；
将步骤B中湿法球磨后的电阻浆料在真空条件下进行脱泡；
D、成型与干燥：将步骤C中制得的陶瓷基体浆料用浇注机浇注制成所需形状的陶瓷基体，并将陶瓷基体进行干燥，以形成胚体；
E、烧结：将步骤D制得的坯体置于石墨坩埚中，并埋入隔离粉，此后用箱式炉将埋于隔离粉中的坯体在常压下进行烧结，烧结气氛为氧气，坯体烧结制得多孔陶瓷加热体基体半成品；对胚体进行烧结时的烧结温度为1400℃，升温速率为20℃/min，保温时间为12h；
F、灌蜡：将石蜡用加热筒液化，将步骤E制得的多孔陶瓷加热体基体半成品完全浸入到液化的石蜡中3h，之后在常温下冷却14h得到含有石蜡的多孔陶瓷加热体基体；
G、机加工：将步骤F中制得的含有石蜡的多孔陶瓷加热体基体进行机加工，去除多孔陶瓷加热体基体外表面的石蜡层；
H、涂覆：将步骤C中制得的电阻浆料按所需厚度涂覆于在步骤G中制得的多孔陶瓷加热体基体的外表面，电阻浆料在陶瓷基体表面形成一层发热膜；
I、金属化烧结：将步骤H中制得的具有发热膜结构的多孔陶瓷加热体基体置于石墨坩埚中，此后置于烧结炉中进行排蜡和多孔电阻发热膜的金属化烧结；金属化烧结的升温速率为5℃/min，金属化烧结温度为 1000℃，时间为2h；
J、接电极：将步骤I中制得的加热体坯体两端进行表面镀镍处理，再于镀镍处理后的部位进行钎焊引出电极，制得多孔陶瓷加热体成品。
综上所述，本发明提供了一种具有多孔发热膜结构的陶瓷加热体的制备工艺，该工艺依次通过混料、球磨、托盘、成型与干燥、烧结、灌蜡、机加工、涂覆、金属化烧结、接电极制得陶瓷加热体，整个制造工艺简单，通过采用箱式炉在氧化气氛和常压下烧结胚体，制得的陶瓷加热体加热均匀且加热效率高。
以上是对本发明的较佳实施进行了具体说明，但本发明创造并不限于所述实施例，熟悉本领域的技术人员在不违背本发明精神的前提下还可做出种种的等同变形或替换，这些等同的变形或替换均包含在本申请权利要求所限定的范围内。

Claims (9)

1.一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：该工艺包括以下的步骤：
A、混料：按质量百分比称取15-55%的硅藻土、5-25%的淀粉、0-2%的纳米二氧化硅溶液、40-70%的去离子水，混合搅拌均匀，制得陶瓷基体浆料；
按质量百分比称取15-40%的电阻浆料、30-60%的淀粉、10-30%的有机溶剂并混和搅拌均匀，制得有造孔剂的电阻浆料；
B、球磨：向步骤A中制得的陶瓷基体浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为4-24h；
向步骤A中制得的电阻浆料加入研磨球，并放入球磨罐中进行湿法球磨，湿法球磨的时间为24-48h；
C、脱泡：将步骤B中湿法球磨后的陶瓷基体浆料在真空条件下进行脱泡；
将步骤B中湿法球磨后的电阻浆料在真空条件下进行脱泡；
D、成型与干燥：将步骤C中制得的陶瓷基体浆料用浇注机浇注制成所需形状的陶瓷基体，并将陶瓷基体进行干燥，以形成胚体；
E、烧结：将步骤D制得的坯体置于石墨坩埚中，并埋入隔离粉，此后用箱式炉将埋于隔离粉中的坯体在常压下进行烧结，烧结气氛为氧气，坯体烧结制得多孔陶瓷加热体基体半成品；
F、灌蜡：将石蜡用加热筒液化，将步骤E制得的多孔陶瓷加热体基体半成品完全浸入到液化的石蜡中1-5h，之后在常温下冷却4-24h得到含有石蜡的多孔陶瓷加热体基体；
G、机加工：将步骤F中制得的含有石蜡的多孔陶瓷加热体基体进行机加工，去除多孔陶瓷加热体基体外表面的石蜡层；
H、涂覆：将步骤C中制得的电阻浆料按所需厚度涂覆于在步骤G中制得的多孔陶瓷加热体基体的外表面，电阻浆料在陶瓷基体表面形成一层发热膜；
I、金属化烧结：将步骤H中制得的具有发热膜结构的多孔陶瓷加热体基体置于石墨坩埚中，此后置于烧结炉中进行排蜡和多孔电阻发热膜的金属化烧结；
J、 接电极：将步骤I中制得的加热体坯体两端进行表面镀镍处理，再于镀镍处理后的部位进行钎焊引出电极，制得多孔陶瓷加热体成品。
2.根据权利要求1所述的一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：所述的步骤A中，陶瓷基体浆料由以下质量百分比的原料组成：
硅藻土21%
淀粉16%
纳米二氧化硅溶液1%
去离子水62%。
3.根据权利要求2所述的一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：所述的步骤A中，电阻浆料由以下质量百分比的原料组成：
电阻浆料30%
淀粉45%
有机溶剂25%。
4.根据权利要求1所述的一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：所述的步骤A中，陶瓷基体浆料由以下质量百分比的原料组成：
硅藻土15%
淀粉15%
去离子水70%。
5.根据权利要求4所述的一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：所述的步骤A中，电阻浆料由以下质量百分比的原料组成：
电阻浆料40%
淀粉30%
有机溶剂30%。
6.根据权利要求1所述的一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：所述的步骤A中，陶瓷基体浆料由以下质量百分比的原料组成：
硅藻土50%
淀粉8%
纳米二氧化硅溶液2%
去离子水40%。
7.根据权利要求6所述的一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：所述的步骤A中，电阻浆料由以下质量百分比的原料组成：
电阻浆料30%
淀粉50%
有机溶剂20%。
8.根据权利要求1所述的一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：所述的步骤E中，对胚体进行烧结时的烧结温度为900-1400℃，升温速率为1-20℃/min，保温时间为2-12h。
9.根据权利要求1所述的一种具有多孔发热膜结构的陶瓷加热体的制备工艺，其特征在于：所述的步骤I中，金属化烧结的升温速率为1-5℃/min，金属化烧结温度为800-1000℃，时间为1-2h。
CN201711394637.3A 2017-12-21 2017-12-21 一种具有多孔发热膜结构的陶瓷加热体的制备工艺 Active CN108046833B (zh)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN201711394637.3A CN108046833B (zh) 2017-12-21 2017-12-21 一种具有多孔发热膜结构的陶瓷加热体的制备工艺
PCT/CN2018/074111 WO2019119611A1 (zh) 2017-12-21 2018-01-25 一种具有多孔发热膜结构的陶瓷加热体的制备工艺
US16/906,518 US11498875B2 (en) 2017-12-21 2020-06-19 Method for fabricating a ceramic heating body with porous heating film

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711394637.3A CN108046833B (zh) 2017-12-21 2017-12-21 一种具有多孔发热膜结构的陶瓷加热体的制备工艺

Publications (2)

Publication Number Publication Date
CN108046833A true CN108046833A (zh) 2018-05-18
CN108046833B CN108046833B (zh) 2020-06-30

Family

ID=62131197

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711394637.3A Active CN108046833B (zh) 2017-12-21 2017-12-21 一种具有多孔发热膜结构的陶瓷加热体的制备工艺

Country Status (3)

Country Link
US (1) US11498875B2 (zh)
CN (1) CN108046833B (zh)
WO (1) WO2019119611A1 (zh)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110041096A (zh) * 2019-01-16 2019-07-23 深圳陶陶科技有限公司 硅藻土基多孔陶瓷及其制备方法和系统
CN112413023A (zh) * 2020-11-20 2021-02-26 贵州新安航空机械有限责任公司 薄片粉末冶金刹车盘的加工方法
CN115028473A (zh) * 2022-05-06 2022-09-09 深圳市吉迩技术有限公司 覆有金属涂层的多孔陶瓷的制备方法及气溶胶生成装置
CN115974592A (zh) * 2021-10-14 2023-04-18 深圳市卓力能技术有限公司 发热体的金属化处理方法、发热体及气溶胶产生装置
CN116944493A (zh) * 2023-08-03 2023-10-27 广东奇砺新材料科技有限公司 一种金属浆料、具有凹凸表面的发热元件及气雾发生器

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112420240B (zh) * 2020-11-20 2022-11-11 深圳顺络电子股份有限公司 电极浆料及其制作方法、电子烟加热体及其制作方法
CN112592200B (zh) * 2020-12-18 2023-06-27 惠州市新泓威科技有限公司 雾化芯用纳米多孔陶瓷及其制备方法
CN112548100B (zh) * 2020-12-24 2022-05-17 南京航空航天大学 一种仿生定向有序叠层复合材料的制备方法
CN113072390A (zh) * 2021-03-16 2021-07-06 上海梦泺企业管理咨询有限公司 一种多孔陶瓷加热体及其制备方法
CN114180973B (zh) * 2021-12-27 2023-05-26 重庆石墨烯研究院有限公司 一种石墨烯陶瓷发热板的制备方法
WO2024027354A1 (zh) * 2022-08-04 2024-02-08 常州市派腾电子技术服务有限公司 雾化芯、雾化器、气溶胶发生装置及雾化芯制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04188652A (ja) * 1990-11-19 1992-07-07 Shinko Electric Ind Co Ltd 高周波素子用パッケージの製造方法と高周波素子用パッケージ
US20040187297A1 (en) * 2003-03-27 2004-09-30 E Touch Corporation Method of fabricating a polymer resistor in an interconnection via
CN101265123A (zh) * 2008-04-18 2008-09-17 南京工业大学 一种小孔径陶瓷膜的制备方法
CN104860681A (zh) * 2014-02-26 2015-08-26 东莞市国研电热材料有限公司 一种叠层式陶瓷加热体及其制备工艺
CN104860682A (zh) * 2014-02-26 2015-08-26 东莞市国研电热材料有限公司 一种叠层共烧的陶瓷加热体的制备工艺

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS577215A (en) * 1980-06-16 1982-01-14 Ngk Insulators Ltd Preparation of ceramic honeycomb filter
CN102034877A (zh) * 2009-09-30 2011-04-27 比亚迪股份有限公司 一种太阳能电池用导电浆料及其制备方法
US8974722B1 (en) * 2013-03-15 2015-03-10 Ibiden Co., Ltd. Method for manufacturing aluminum-titanate-based ceramic honeycomb structure
CN104014195B (zh) * 2014-05-06 2015-12-30 三达膜科技（厦门）有限公司 一种涂层复合陶瓷滤芯的制备方法
CN107010934B (zh) * 2017-04-20 2018-08-24 深圳市卓力能电子有限公司 一种微孔陶瓷及微孔陶瓷加热棒的制备方法
CN108059479B (zh) * 2017-12-21 2020-09-15 深圳市卓力能电子有限公司 一种新型多孔陶瓷加热体的制备工艺

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04188652A (ja) * 1990-11-19 1992-07-07 Shinko Electric Ind Co Ltd 高周波素子用パッケージの製造方法と高周波素子用パッケージ
US20040187297A1 (en) * 2003-03-27 2004-09-30 E Touch Corporation Method of fabricating a polymer resistor in an interconnection via
CN101265123A (zh) * 2008-04-18 2008-09-17 南京工业大学 一种小孔径陶瓷膜的制备方法
CN104860681A (zh) * 2014-02-26 2015-08-26 东莞市国研电热材料有限公司 一种叠层式陶瓷加热体及其制备工艺
CN104860682A (zh) * 2014-02-26 2015-08-26 东莞市国研电热材料有限公司 一种叠层共烧的陶瓷加热体的制备工艺

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110041096A (zh) * 2019-01-16 2019-07-23 深圳陶陶科技有限公司 硅藻土基多孔陶瓷及其制备方法和系统
CN112413023A (zh) * 2020-11-20 2021-02-26 贵州新安航空机械有限责任公司 薄片粉末冶金刹车盘的加工方法
CN112413023B (zh) * 2020-11-20 2022-11-08 贵州新安航空机械有限责任公司 薄片粉末冶金刹车盘的加工方法
CN115974592A (zh) * 2021-10-14 2023-04-18 深圳市卓力能技术有限公司 发热体的金属化处理方法、发热体及气溶胶产生装置
CN115974592B (zh) * 2021-10-14 2024-03-29 深圳市卓力能技术有限公司 发热体的金属化处理方法、发热体及气溶胶产生装置
CN115028473A (zh) * 2022-05-06 2022-09-09 深圳市吉迩技术有限公司 覆有金属涂层的多孔陶瓷的制备方法及气溶胶生成装置
CN115028473B (zh) * 2022-05-06 2024-02-09 深圳市吉迩技术有限公司 覆有金属涂层的多孔陶瓷的制备方法及气溶胶生成装置
CN116944493A (zh) * 2023-08-03 2023-10-27 广东奇砺新材料科技有限公司 一种金属浆料、具有凹凸表面的发热元件及气雾发生器
CN116944493B (zh) * 2023-08-03 2024-02-13 广东奇砺新材料科技有限公司 一种气雾发生器

Also Published As

Publication number Publication date
US11498875B2 (en) 2022-11-15
US20200317585A1 (en) 2020-10-08
WO2019119611A1 (zh) 2019-06-27
CN108046833B (zh) 2020-06-30

Similar Documents

Publication Publication Date Title
CN108046833A (zh) 一种具有多孔发热膜结构的陶瓷加热体的制备工艺
CN107182139B (zh) 一种金属膜多孔陶瓷发热体及其应用
CN104058772B (zh) 一种陶瓷复合材料基板及其制备工艺
CN107935634A (zh) 一种难熔金属化合物高温抗氧化涂层及其制备方法
CN108059462A (zh) 一种新型多孔发热陶瓷的制备工艺
CN104844221B (zh) 一种大尺寸氮化铝陶瓷基板的制备方法
CN101913879B (zh) 氮化硅材料及其制备方法和氮化硅发热器件及其制备方法
CN108838504B (zh) 一种用于扩散连接碳化硅陶瓷的复合中间层及其连接工艺
CN105884394A (zh) 一种低温制备多孔碳化硅支撑体的方法
CN108059479A (zh) 一种新型多孔陶瓷加热体的制备工艺
CN106083061A (zh) 一种激光烧结快速成型碳化硅陶瓷的制备方法
CN107963890B (zh) 一种氮化钛多孔导电陶瓷的制备方法
CN108249952A (zh) 一种多孔陶瓷承烧板的制备方法
CN104163640B (zh) 低压铸造用高纯氮化硅陶瓷升液管的微波烧结制备方法
CN101117295A (zh) 一种制备泡沫陶瓷过滤器的方法及用该方法制备的过滤器
CN110903074A (zh) 一种碳化硅基体表面高温抗氧化涂层及其制备方法
CN106478081A (zh) 真空碳热还原强化熔融石英高温性能的方法
CN107673761A (zh) 一种大规格致密碳化硅陶瓷板的制备方法
CN105801108B (zh) 一种三维孔道结构锂基块体氚增值剂材料的制备方法
CN104016663A (zh) 一种氧化铅陶瓷芯块的微波烧结方法
CN104162661B (zh) 一种微波烧结Al2O3-TiC-TiN微米复合陶瓷刀具材料的方法
CN109732088A (zh) 一种抗热震性能高的新型复合陶瓷及其加工工艺
CN108046834A (zh) 一种具有镶嵌结构的多孔陶瓷加热体的制备工艺
CN104860691A (zh) 高强度氮化硅铁窑具的制备方法
CN106187249B (zh) 一种高热稳定性的电热陶瓷及其制备工艺

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
CP03 Change of name, title or address
CP03 Change of name, title or address

Address after: 518100 1st, 2nd, 3rd, 4th and 5th floors of workshop B, No.2, Gongye 3rd road, Langxin community, Shiyan street, Bao'an District, Shenzhen City, Guangdong Province

Patentee after: Shenzhen zhuolineng Technology Co.,Ltd.

Address before: 518000 workshop B, No.2, Gongye 3rd road, Shixin community, Shiyan street, Bao'an District, Shenzhen City, Guangdong Province

Patentee before: Shenzhen Zhuolineng Electronics Co.,Ltd.

CP03 Change of name, title or address
CP03 Change of name, title or address

Address after: 518100 workshop B, No.2, Gongye 3rd road, Langxin community, Shiyan street, Bao'an District, Shenzhen City, Guangdong Province

Patentee after: Shenzhen zhuolineng Technology Co.,Ltd.

Address before: 518100 1st, 2nd, 3rd, 4th and 5th floors of workshop B, No.2, Gongye 3rd road, Langxin community, Shiyan street, Bao'an District, Shenzhen City, Guangdong Province

Patentee before: Shenzhen zhuolineng Technology Co.,Ltd.