CN107793044A - 在线稳定化学钢化玻璃表面压应力的方法 - Google Patents
在线稳定化学钢化玻璃表面压应力的方法 Download PDFInfo
- Publication number
- CN107793044A CN107793044A CN201610780982.XA CN201610780982A CN107793044A CN 107793044 A CN107793044 A CN 107793044A CN 201610780982 A CN201610780982 A CN 201610780982A CN 107793044 A CN107793044 A CN 107793044A
- Authority
- CN
- China
- Prior art keywords
- glass
- salt bath
- stabilizer
- bearing stress
- tempering
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 37
- 239000005341 toughened glass Substances 0.000 title claims abstract description 29
- 239000011521 glass Substances 0.000 claims abstract description 94
- 150000003839 salts Chemical class 0.000 claims abstract description 68
- 238000005496 tempering Methods 0.000 claims abstract description 56
- 239000003381 stabilizer Substances 0.000 claims abstract description 39
- 230000003014 reinforcing effect Effects 0.000 claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 8
- 239000000463 material Substances 0.000 claims description 19
- 229910001220 stainless steel Inorganic materials 0.000 claims description 15
- 239000010935 stainless steel Substances 0.000 claims description 15
- 229910000831 Steel Inorganic materials 0.000 claims description 12
- 239000010959 steel Substances 0.000 claims description 12
- 238000010276 construction Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 24
- 239000000126 substance Substances 0.000 abstract description 17
- 239000012535 impurity Substances 0.000 abstract description 5
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 76
- 235000010333 potassium nitrate Nutrition 0.000 description 38
- 239000004323 potassium nitrate Substances 0.000 description 38
- 239000005336 safety glass Substances 0.000 description 18
- 150000002500 ions Chemical class 0.000 description 8
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 7
- 239000011734 sodium Substances 0.000 description 7
- IRPDISVJRAYFBI-UHFFFAOYSA-N nitric acid;potassium Chemical compound [K].O[N+]([O-])=O IRPDISVJRAYFBI-UHFFFAOYSA-N 0.000 description 6
- 238000005342 ion exchange Methods 0.000 description 5
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 229910052744 lithium Inorganic materials 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 3
- 229910052681 coesite Inorganic materials 0.000 description 3
- 230000006835 compression Effects 0.000 description 3
- 238000007906 compression Methods 0.000 description 3
- 229910052906 cristobalite Inorganic materials 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 239000011152 fibreglass Substances 0.000 description 3
- 229910001416 lithium ion Inorganic materials 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 229910052682 stishovite Inorganic materials 0.000 description 3
- 229910052905 tridymite Inorganic materials 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 238000010257 thawing Methods 0.000 description 2
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical compound [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 description 1
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- -1 and stirs Uniformly Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000005357 flat glass Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 229910003002 lithium salt Inorganic materials 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 150000002927 oxygen compounds Chemical class 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 229910001415 sodium ion Inorganic materials 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B27/00—Tempering or quenching glass products
- C03B27/02—Tempering or quenching glass products using liquid
- C03B27/03—Tempering or quenching glass products using liquid the liquid being a molten metal or a molten salt
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C21/00—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface
- C03C21/001—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions
- C03C21/002—Treatment of glass, not in the form of fibres or filaments, by diffusing ions or metals in the surface in liquid phase, e.g. molten salts, solutions to perform ion-exchange between alkali ions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Surface Treatment Of Glass (AREA)
Abstract
Description
批次 | 表面压应力/Mpa |
第一批 | 823 |
第二批 | 821 |
第三批 | 819 |
第四批 | 822 |
第五批 | 817 |
第六批 | 818 |
批次 | 表面压应力/Mpa |
第一批 | 823 |
第二批 | 821 |
第三批 | 819 |
第四批 | 820 |
第五批 | 817 |
第六批 | 825 |
第七批 | 820 |
第八批 | 818 |
第九批 | 817 |
第十批 | 819 |
Claims (7)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610780982.XA CN107793044B (zh) | 2016-08-30 | 2016-08-30 | 在线稳定化学钢化玻璃表面压应力的方法 |
PCT/CN2017/099520 WO2018041102A1 (zh) | 2016-08-30 | 2017-08-29 | 在线稳定化学钢化玻璃表面压应力的方法 |
US15/800,122 US10618841B2 (en) | 2016-08-30 | 2017-11-01 | On-line method for stabilizing surface compressive stress of chemically-tempered glass |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610780982.XA CN107793044B (zh) | 2016-08-30 | 2016-08-30 | 在线稳定化学钢化玻璃表面压应力的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN107793044A true CN107793044A (zh) | 2018-03-13 |
CN107793044B CN107793044B (zh) | 2020-07-03 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610780982.XA Active CN107793044B (zh) | 2016-08-30 | 2016-08-30 | 在线稳定化学钢化玻璃表面压应力的方法 |
Country Status (2)
Country | Link |
---|---|
CN (1) | CN107793044B (zh) |
WO (1) | WO2018041102A1 (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112608033A (zh) * | 2020-09-12 | 2021-04-06 | 重庆鑫景特种玻璃有限公司 | 一种化学强化微晶玻璃及强化方法 |
CN113165968A (zh) * | 2018-11-30 | 2021-07-23 | 康宁股份有限公司 | 输送固体化学物质及在熔融盐浴中保留淤渣的设备和方法 |
CN113480196A (zh) * | 2021-07-30 | 2021-10-08 | Oppo广东移动通信有限公司 | 用于玻璃强化的组合物及其制备方法和玻璃强化方法 |
CN116354619A (zh) * | 2019-10-16 | 2023-06-30 | 重庆鑫景特种玻璃有限公司 | 无硅盐浴提纯添加剂材料及其使用方法 |
CN116768493A (zh) * | 2020-09-12 | 2023-09-19 | 重庆鑫景特种玻璃有限公司 | 无硼、无磷高稳定性的离子筛及其制备和应用 |
Citations (7)
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CN101372393A (zh) * | 2007-08-20 | 2009-02-25 | 比亚迪股份有限公司 | 一种玻璃化学强化的催化剂、制备方法及其应用 |
CN101372392A (zh) * | 2007-08-20 | 2009-02-25 | 比亚迪股份有限公司 | 一种用于玻璃化学强化的催化剂及其应用 |
CN102092940A (zh) * | 2009-12-11 | 2011-06-15 | 肖特公开股份有限公司 | 用于触摸屏的铝硅酸盐玻璃 |
CN102167507A (zh) * | 2010-02-26 | 2011-08-31 | 肖特玻璃科技(苏州)有限公司 | 用于3d紧密模压的薄锂铝硅玻璃 |
WO2014045979A1 (ja) * | 2012-09-18 | 2014-03-27 | 旭硝子株式会社 | 化学強化ガラスの製造方法 |
CN104640821A (zh) * | 2012-09-18 | 2015-05-20 | 旭硝子株式会社 | 玻璃化学强化用熔融盐的再生方法和强化玻璃的制造方法 |
CN104788013A (zh) * | 2015-04-13 | 2015-07-22 | 北京航玻新材料技术有限公司 | 化学钢化及去除化学钢化硝酸钾熔盐中杂质的方法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104743866B (zh) * | 2013-12-30 | 2018-06-26 | 深圳市力沣实业有限公司 | 一种化学强化盐浴添加剂及其制备方法 |
CN103864283A (zh) * | 2014-03-10 | 2014-06-18 | 中国洛阳浮法玻璃集团有限责任公司 | 一种薄玻璃化学钢化的离子交换工艺及熔盐 |
CN204702649U (zh) * | 2015-05-30 | 2015-10-14 | 广东特纳江玻实业发展有限公司 | 一种用于玻璃钢化炉的吊篮 |
-
2016
- 2016-08-30 CN CN201610780982.XA patent/CN107793044B/zh active Active
-
2017
- 2017-08-29 WO PCT/CN2017/099520 patent/WO2018041102A1/zh active Application Filing
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101372393A (zh) * | 2007-08-20 | 2009-02-25 | 比亚迪股份有限公司 | 一种玻璃化学强化的催化剂、制备方法及其应用 |
CN101372392A (zh) * | 2007-08-20 | 2009-02-25 | 比亚迪股份有限公司 | 一种用于玻璃化学强化的催化剂及其应用 |
CN102092940A (zh) * | 2009-12-11 | 2011-06-15 | 肖特公开股份有限公司 | 用于触摸屏的铝硅酸盐玻璃 |
CN102167507A (zh) * | 2010-02-26 | 2011-08-31 | 肖特玻璃科技(苏州)有限公司 | 用于3d紧密模压的薄锂铝硅玻璃 |
WO2014045979A1 (ja) * | 2012-09-18 | 2014-03-27 | 旭硝子株式会社 | 化学強化ガラスの製造方法 |
CN104640821A (zh) * | 2012-09-18 | 2015-05-20 | 旭硝子株式会社 | 玻璃化学强化用熔融盐的再生方法和强化玻璃的制造方法 |
CN104788013A (zh) * | 2015-04-13 | 2015-07-22 | 北京航玻新材料技术有限公司 | 化学钢化及去除化学钢化硝酸钾熔盐中杂质的方法 |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113165968A (zh) * | 2018-11-30 | 2021-07-23 | 康宁股份有限公司 | 输送固体化学物质及在熔融盐浴中保留淤渣的设备和方法 |
CN116354619A (zh) * | 2019-10-16 | 2023-06-30 | 重庆鑫景特种玻璃有限公司 | 无硅盐浴提纯添加剂材料及其使用方法 |
CN116354619B (zh) * | 2019-10-16 | 2024-01-30 | 重庆鑫景特种玻璃有限公司 | 无硅盐浴提纯添加剂材料及其使用方法 |
CN112608033A (zh) * | 2020-09-12 | 2021-04-06 | 重庆鑫景特种玻璃有限公司 | 一种化学强化微晶玻璃及强化方法 |
CN116768493A (zh) * | 2020-09-12 | 2023-09-19 | 重庆鑫景特种玻璃有限公司 | 无硼、无磷高稳定性的离子筛及其制备和应用 |
CN113480196A (zh) * | 2021-07-30 | 2021-10-08 | Oppo广东移动通信有限公司 | 用于玻璃强化的组合物及其制备方法和玻璃强化方法 |
Also Published As
Publication number | Publication date |
---|---|
WO2018041102A1 (zh) | 2018-03-08 |
CN107793044B (zh) | 2020-07-03 |
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Address after: 400700 No.78, Yunwu Road, Beibei District, Chongqing Applicant after: Xiameixi technology partnership (limited partnership) of Liangjiang New District, Chongqing Address before: 400700 No.78, Yunwu Road, Beibei District, Chongqing Applicant before: Xiameixi technology partnership (limited partnership) of Liangjiang New District, Chongqing |
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Effective date of registration: 20200825 Address after: No.78 Yunwu Road, Shuitu hi tech Industrial Park, Beibei District, Chongqing Patentee after: CHONGQING XINJING SPECIAL GLASS Co.,Ltd. Address before: 400700 No.78, Yunwu Road, Beibei District, Chongqing Patentee before: Xiameixi technology partnership (L.P.) of Liangjiang New District, Chongqing |
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