CN107646912A - A kind of grape tree planting insecticide and preparation method thereof - Google Patents
A kind of grape tree planting insecticide and preparation method thereof Download PDFInfo
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- CN107646912A CN107646912A CN201710977424.7A CN201710977424A CN107646912A CN 107646912 A CN107646912 A CN 107646912A CN 201710977424 A CN201710977424 A CN 201710977424A CN 107646912 A CN107646912 A CN 107646912A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Pest Control & Pesticides (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of grape tree planting insecticide and preparation method thereof, is related to planting fruit trees technical field, includes the raw material of following parts by weight：60 ~ 80 parts of Dalmatian chrysanthemum, 50 ~ 60 parts of cordate houttuynia, 30 ~ 40 parts of garlic, 20 ~ 30 parts of radix glycyrrhizae, 20 ~ 30 parts of the coptis, 40 ~ 50 parts of kuh-seng, 30 ~ 40 parts of the root of langdu, 50 ~ 60 parts of Celastrus angulatus, 20 ~ 30 parts of Fourstamen Stephania Root, 30 ~ 40 parts of nicotine, 20 ~ 30 parts of rhizome of chuanxiong, 10 ~ 15 parts of emulsifying agent, 6 ~ 10 parts of stabilizer；Preparation method includes：（1）, Feedstock treating；（2）, extraction；（3）, filtrate concentration；（4）, spray drying；（5）, dry；（6）, packaging.The longevity of residure of the invention is short, extraneous or be easily degraded in vivo, reduce the Harmful Residue on grape surface, plants out the grape without hormone and without chemical contamination.
Description
Technical field
The present invention relates to planting fruit trees technical field, and in particular to a kind of grape tree planting insecticide and its preparation side
Method.
Background technology
Grape nutritive value enriches, and is a kind of very strong fruit of nourishing.Grape juice is described as " vegetable milk " by scientist.Portugal
Grape trace element containing protein, carbohydrate, crude fibre, calcium, phosphorus, iron, potassium etc. is outer, and containing carrotene, vitamin B1,
Vitamin B2, vitamin C, citrin, nicotinic acid etc., in addition, ten several amino acids and volume fruit also containing needed by human body
Acid.Grape sugar content is high, based on glucose.Therefore, grape is often eaten, has benefiting action to neurasthenia and fatigue.
Grape is in plantation growth period mainly by the insect pests such as thrips, aphid, noctuid, coccid, green plant bug, the insect pest phenomenon of wine-growing
The quantity of grape fruit is not only influenceed, more influences the quality of grape fruit.
The prevention and controls of insect have many kinds, but people are for convenience and quick at present, are typically chosen and spray insecticide, existing
It is largely that a variety of chemical substances are made by hybrid reaction to have technology Pesticides.During pesticide spraying, grape has agriculture on surface
Medicine residue, when eating, certain harm is caused to people's body.
The content of the invention
For in the prior art the defects of, it is an object of the invention to provide a kind of grape tree planting insecticide and its preparation
Method, the Chinese herbal medicine extract matter longevity of residure is short, extraneous or be easily degraded in vivo, reduces the Harmful Residue on grape surface, kind
Plant no hormone and the grape without chemical contamination.
The invention provides following technical scheme：A kind of grape tree planting insecticide, including following parts by weight
Raw material：60~80 parts of Dalmatian chrysanthemum, 50~60 parts of cordate houttuynia, 30~40 parts of garlic, 20~30 parts of radix glycyrrhizae, 20~30 parts of the coptis,
40~50 parts of kuh-seng, 30~40 parts of the root of langdu, 50~60 parts of Celastrus angulatus, 20~30 parts of Fourstamen Stephania Root, 30~40 parts of nicotine, rhizome of chuanxiong 20
~30 parts, 10~15 parts of emulsifying agent, 6~10 parts of stabilizer.
Preferably, 70 parts of the Dalmatian chrysanthemum, 60 parts of cordate houttuynia, 38 parts of garlic, 30 parts of radix glycyrrhizae, 25 parts of the coptis, kuh-seng 48
Part, 36 parts of the root of langdu, 55 parts of Celastrus angulatus, 28 parts of Fourstamen Stephania Root, 30 parts of nicotine, 20 parts of rhizome of chuanxiong, 12 parts of emulsifying agent, 8 parts of stabilizer.
Preferably, the emulsifying agent is the one or more in tween, Arabic gum, poloxamer.
Preferably, the stabilizer is creatinine, glycine, niacinamide, the one or more of Sodium Caprylate.
The present invention also provides a kind of grape tree planting method for producing insecticide, comprises the following steps：
(1), Feedstock treating：Each raw material is weighed by above-mentioned parts by weight, each raw material is respectively placed in pulverizer and carries out powder
It is broken, except emulsifying agent and stabilizer, it is well mixed；
(2), extract：Add the ethanol of 5~10 times of parts by weight into mixed material, heating-up temperature is to 50~60 Celsius
Degree, lasting stirring, is soaked 20~30 hours, filtering, obtains filtrate and filter residue, and the second of 2~5 times of parts by weight is added into filter residue
Alcohol, heating-up temperature lasting stirring, are soaked 10~20 hours, secondary soak extraction to 50~60 degrees Celsius, filtering, obtain filtrate, and
Mixed with foregoing filtrate, it is standby；
(3), filtrate concentrates：Emulsifying agent and stabilizer are added in mixed filtrate, after stirring 2~3 hours, using rotation
Turn evaporimeter to concentrate mixed liquor, concentrate 0.5~1 hour；
(4), it is spray-dried：Concentration filtrate is sent into spray dryer, preparation forms extract powder；
(5), dry：Extract powder is put into drying box and is dried, temperature is 90~100 degrees Celsius, and it is small to dry 1~2
When, obtain solid particle；
(6), pack：After the solid particle of above-mentioned acquisition is cooled into room temperature, it is put into air-locked aluminium foil bag, sealing is protected
Deposit, you can.
Preferably, the raw material particle size in the step (1) is crushed to 50~150 mesh.
Preferably, the ethanol in the step (2) is the ethanol water of mass fraction 70%~85%.
Preferably, the mixing speed in the step (2) is 300~500r/min.
Beneficial effects of the present invention：The Chinese herbal medicine extract matter longevity of residure is short, extraneous or be easily degraded in vivo, reduces grape
The Harmful Residue on surface, the grape without hormone and without chemical contamination is planted out, it is specific as follows：
(1), the raw material of insecticide of the invention is the Nature material, and composition is nontoxic, noresidue, nuisanceless, and this
Invention desinsection agent and process for producing same is simple, easily operated, and production cost is low, easy to use.
(2), the suitable insecticide of the present invention is short using the Chinese herbal medicine extract component longevity of residure, is easily divided by sunlight or microbial action
Advantage is solved, poisoning will not be produced during use, can accordingly reduce pollution of the agricultural chemicals to environment.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments are merely to illustrate the present invention and not had to
In limitation the scope of the present invention.
Embodiment 1
A kind of grape tree planting insecticide, including the raw material with parts by weight：
70 parts of Dalmatian chrysanthemum, 60 parts of cordate houttuynia, 38 parts of garlic, 30 parts of radix glycyrrhizae, 25 parts of the coptis, 48 parts of kuh-seng, 36 parts of the root of langdu,
55 parts of Celastrus angulatus, 28 parts of Fourstamen Stephania Root, 30 parts of nicotine, 20 parts of rhizome of chuanxiong, 12 parts of emulsifying agent, 8 parts of stabilizer.
Wherein, emulsifying agent is tween.
Wherein, stabilizer is glycine.
A kind of grape tree planting method for producing insecticide is also provided in the present embodiment, comprised the following steps：
(1), Feedstock treating：Each raw material is weighed by above-mentioned parts by weight, each raw material is respectively placed in pulverizer and carries out powder
It is broken, it is well mixed, except emulsifying agent and stabilizer；
(2), extract：The ethanol of 5 times of parts by weight is added into mixed material, heating-up temperature continues to 50 degrees Celsius
Stirring, soak 20 hours, filtering, obtain filtrate and filter residue, the ethanol of 2 times of parts by weight, heating-up temperature to 50 are added into filter residue
Degree Celsius, lasting stirring, soak 10 hours, secondary soak extraction, filtering, obtain filtrate, and mixed with foregoing filtrate, it is standby；
(3), filtrate concentrates：Emulsifying agent and stabilizer are added in mixed filtrate, after stirring 2 hours, using rotation
Evaporimeter concentrates to mixed liquor, concentrates 0.5 hour；
(4), it is spray-dried：Concentration filtrate is sent into spray dryer, preparation forms extract powder；
(5), dry：Extract powder is put into drying box and is dried, temperature is 90 degrees Celsius, is dried 1 hour, consolidate
Body particle；
(6), pack：After the solid particle of above-mentioned acquisition is cooled into room temperature, it is put into air-locked aluminium foil bag, sealing is protected
Deposit, you can.
Raw material particle size in step (1) is crushed to 50 mesh.
Ethanol in step (2) is the ethanol water of mass fraction 70%.
Mixing speed in step (2) is 300~500r/min.
Embodiment 2
A kind of grape tree planting insecticide, including the raw material with parts by weight：
60 parts of Dalmatian chrysanthemum, 50 parts of cordate houttuynia, 30 parts of garlic, 20 parts of radix glycyrrhizae, 20 parts of the coptis, 40 parts of kuh-seng, 30 parts of the root of langdu,
50 parts of Celastrus angulatus, 20 parts of Fourstamen Stephania Root, 30 parts of nicotine, 20 parts of rhizome of chuanxiong, 10 parts of emulsifying agent, 6 parts of stabilizer.
Wherein, emulsifying agent is the mixture of tween and Arabic gum.
Wherein, stabilizer is the mixture of niacinamide and Sodium Caprylate.
A kind of grape tree planting method for producing insecticide is also provided in the present embodiment, comprised the following steps：
(1), Feedstock treating：Each raw material is weighed by above-mentioned parts by weight, each raw material is respectively placed in pulverizer and carries out powder
It is broken, except emulsifying agent and stabilizer, it is well mixed；
(2), extract：The ethanol of 10 times of parts by weight is added into mixed material, heating-up temperature continues to 60 degrees Celsius
Stirring, soak 30 hours, filtering, obtain filtrate and filter residue, the ethanol of 5 times of parts by weight, heating-up temperature to 60 are added into filter residue
Degree Celsius, lasting stirring, soak 20 hours, secondary soak extraction, filtering, obtain filtrate, and be well mixed with foregoing filtrate, it is standby
With；
(3), filtrate concentrates：Emulsifying agent and stabilizer are added after mixing in filtrate, after stirring 3 hours, using rotation steaming
Hair instrument concentrates to mixed liquor, concentrates 1 hour；
(4), it is spray-dried：Concentration filtrate is sent into spray dryer, preparation forms extract powder；
(5), dry：Extract powder is dried, temperature is 100 degrees Celsius, dries 2 hours, obtains solid particle；
(6), pack：After the solid particle of above-mentioned acquisition is cooled into room temperature, it is put into air-locked aluminium foil bag, sealing is protected
Deposit, you can.
Raw material particle size in step (1) is crushed to 150 mesh.
Ethanol in step (2) is the ethanol water of mass fraction 85%.
Mixing speed in step (2) is 500r/min.
Embodiment 3
A kind of grape tree planting insecticide, including the raw material with parts by weight：
80 parts of Dalmatian chrysanthemum, 60 parts of cordate houttuynia, 40 parts of garlic, 30 parts of radix glycyrrhizae, 30 parts of the coptis, 50 parts of kuh-seng, 40 parts of the root of langdu,
60 parts of Celastrus angulatus, 30 parts of Fourstamen Stephania Root, 40 parts of nicotine, 30 parts of rhizome of chuanxiong, 15 parts of emulsifying agent, 10 parts of stabilizer.
Wherein, emulsifying agent is Arabic gum.
Wherein, stabilizer is creatinine.
A kind of grape tree planting method for producing insecticide is also provided in the present embodiment, comprised the following steps：
(1), Feedstock treating：Each raw material is weighed by above-mentioned parts by weight, each raw material is respectively placed in pulverizer and carries out powder
It is broken, it is well mixed, except emulsifying agent and stabilizer；
(2), extract：The ethanol of 8 times of parts by weight is added into mixed material, heating-up temperature continues to 55 degrees Celsius
Stirring, soak 28 hours, filtering, obtain filtrate and filter residue, filter residue is added to the ethanol of 3 times of parts by weight, heating-up temperature to 55 is taken the photograph
Family name's degree, lasting stirring, soaks 18 hours, secondary soak extraction, filtering, obtains filtrate, and is well mixed with foregoing filtrate, standby；
(3), filtrate concentrates：Emulsifying agent and stabilizer are added after mixing in filtrate, after stirring 2.5 hours, using rotation
Evaporimeter concentrates to mixed liquor, concentrates 50 minutes；
(4), it is spray-dried：Concentration filtrate is sent into spray dryer, preparation forms extract powder；
(5), dry：Extract powder is put into drying box and is dried, temperature is 98 degrees Celsius, is dried 2 hours, consolidate
Body particle；
(6), pack：After the solid particle of above-mentioned acquisition is cooled into room temperature, it is put into air-locked aluminium foil bag, sealing is protected
Deposit, you can.
Raw material particle size in step (1) is crushed to 130 mesh.
Ethanol in step (2) is the ethanol water of mass fraction 78%.
Mixing speed in step (2) is 380r/min.
Embodiment 4
A kind of grape tree planting insecticide, including the raw material with parts by weight：
78 parts of Dalmatian chrysanthemum, 55 parts of cordate houttuynia, 38 parts of garlic, 27 parts of radix glycyrrhizae, 26 parts of the coptis, 41 parts of kuh-seng, 39 parts of the root of langdu,
57 parts of Celastrus angulatus, 22 parts of Fourstamen Stephania Root, 35 parts of nicotine, 26 parts of rhizome of chuanxiong, 12 parts of emulsifying agent, 9 parts of stabilizer.
Wherein, emulsifying agent is tween and mixtures of poloxamers.
Wherein, stabilizer is Sodium Caprylate.
A kind of grape tree planting method for producing insecticide is also provided in the present embodiment, comprised the following steps：
(1), Feedstock treating：Each raw material is weighed by above-mentioned parts by weight, each raw material is respectively placed in pulverizer and carries out powder
It is broken, it is well mixed, except emulsifying agent and stabilizer；
(2), extract：The ethanol of 6 times of parts by weight is added into mixed material, heating-up temperature continues to 58 degrees Celsius
Stirring, soak 25 hours, filtering, obtain filtrate and filter residue, the ethanol of 4 times of parts by weight, heating-up temperature to 53 are added into filter residue
Degree Celsius, lasting stirring, soak 18 hours, secondary soak extraction, obtain filtrate, and be well mixed with foregoing filtrate, it is standby；
(3), filtrate concentrates：Emulsifying agent and stabilizer are added in mixed filtrate, after stirring 2.6 hours, using rotation
Turn evaporimeter to concentrate mixed liquor, concentrate 0.8 hour；
(4), it is spray-dried：Concentration filtrate is sent into spray dryer, preparation forms extract powder；
(5), dry：Extract powder is put into drying box and is dried, temperature is 99 degrees Celsius, dries 1.5 hours, obtains
Solid particle；
(6), pack：After the solid particle of above-mentioned acquisition is cooled into room temperature, it is put into air-locked aluminium foil bag, sealing is protected
Deposit, you can.
Raw material particle size in step (1) is crushed to 120 mesh.
Ethanol in step (2) is the ethanol water of mass fraction 75%.
Mixing speed in step (2) is 450r/min.
Application Example
Will the grape tree planting insecticide as made from above-described embodiment 1-4, press 1 with parts by weight and water:1000 ratio
Preparation is diluted, is sprayed on grape timbo branch of the same area, observes its insect preventive effect situation, is recorded in table 1 below；
Comparative example：The vine of any insecticide is not sprayed
Table 1
From table 1 it follows that grape tree planting insecticide provided by the invention is to a variety of of the frequent appearance of vine
For the preventive effect of insect more than 80%, this illustrates that grape tree planting insecticide of the present invention can in grape tree planting
With.
Claims (8)
1. a kind of grape tree planting insecticide, it is characterised in that include the raw material of following parts by weight：60 ~ 80 parts of Dalmatian chrysanthemum,
50 ~ 60 parts of cordate houttuynia, 30 ~ 40 parts of garlic, 20 ~ 30 parts of radix glycyrrhizae, 20 ~ 30 parts of the coptis, 40 ~ 50 parts of kuh-seng, 30 ~ 40 parts of the root of langdu,
50 ~ 60 parts of Celastrus angulatus, 20 ~ 30 parts of Fourstamen Stephania Root, 30 ~ 40 parts of nicotine, 20 ~ 30 parts of rhizome of chuanxiong, 10 ~ 15 parts of emulsifying agent, stabilizer 6 ~ 10
Part.
2. grape tree planting insecticide according to claim 1, it is characterised in that 70 parts of the Dalmatian chrysanthemum, cordate houttuynia
60 parts, 38 parts of garlic, 30 parts of radix glycyrrhizae, 25 parts of the coptis, 48 parts of kuh-seng, 36 parts of the root of langdu, 55 parts of Celastrus angulatus, 28 parts of Fourstamen Stephania Root, cigarette
30 parts of alkali, 20 parts of rhizome of chuanxiong, 12 parts of emulsifying agent, 8 parts of stabilizer.
3. grape tree planting insecticide according to claim 1, it is characterised in that the emulsifying agent is tween, I
One or more in primary glue, poloxamer.
4. grape tree planting insecticide according to claim 1, it is characterised in that the stabilizer is creatinine, sweet ammonia
Acid, niacinamide, the one or more of Sodium Caprylate.
5. the method that one kind prepares the grape tree planting insecticide as described in claim 1 ~ 4, it is characterised in that including following
Step：
（1）, Feedstock treating：Each raw material is weighed by above-mentioned parts by weight, each raw material is respectively placed in pulverizer and crushed, is mixed
Close uniformly, except emulsifying agent and stabilizer；
（2）, extraction：The ethanol of 5 ~ 10 times of parts by weight is added into mixed material, heating-up temperature is held to 50 ~ 60 degrees Celsius
Continuous stirring, is soaked 20 ~ 30 hours, filtering, obtains filtrate and filter residue, and the ethanol of 2 ~ 5 times of parts by weight, heating temperature are added into filter residue
Degree lasting stirring, soaks 10 ~ 20 hours, secondary soak extraction, filtering to 50 ~ 60 degrees Celsius, obtains filtrate, and with foregoing filtrate
Mixing, it is standby；
（3）, filtrate concentration：Emulsifying agent and stabilizer are added in mixed filtrate, after stirring 2 ~ 3 hours, steamed using rotation
Hair instrument concentrates to mixed liquor, concentrates 0.5 ~ 1 hour；
（4）, spray drying：Concentration filtrate is sent into spray dryer, preparation forms extract powder；
（5）, dry：Extract powder is put into drying box and is dried, temperature is 90 ~ 100 degrees Celsius, dries 1 ~ 2 hour, obtains
Solid particle；
（6）, packaging：After the solid particle of above-mentioned acquisition is cooled into room temperature, it is put into air-locked aluminium foil bag, is sealed,
.
6. grape tree planting method for producing insecticide according to claim 5, it is characterised in that the step（1）
In raw material particle size be crushed to 50 ~ 150 mesh.
7. grape tree planting method for producing insecticide according to claim 5, it is characterised in that the step（2）
In ethanol be mass fraction 70% ~ 85% ethanol water.
8. grape tree planting method for producing insecticide according to claim 5, it is characterised in that the step（2）
In mixing speed be 300 ~ 500r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710977424.7A CN107646912A (en) | 2017-10-17 | 2017-10-17 | A kind of grape tree planting insecticide and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710977424.7A CN107646912A (en) | 2017-10-17 | 2017-10-17 | A kind of grape tree planting insecticide and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107646912A true CN107646912A (en) | 2018-02-02 |
Family
ID=61119050
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|---|---|---|---|
| CN201710977424.7A Pending CN107646912A (en) | 2017-10-17 | 2017-10-17 | A kind of grape tree planting insecticide and preparation method thereof |
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| CN (1) | CN107646912A (en) |
Cited By (2)
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| CN108703162A (en) * | 2018-08-09 | 2018-10-26 | 徐州万盛现代农业发展有限公司 | A kind of grape insecticide and preparation method thereof |
| CN112042682A (en) * | 2020-09-07 | 2020-12-08 | 衡东林馨农林科技开发有限责任公司 | Preparation method of plant insecticide for fruit tree planting |
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| CN108703162A (en) * | 2018-08-09 | 2018-10-26 | 徐州万盛现代农业发展有限公司 | A kind of grape insecticide and preparation method thereof |
| CN112042682A (en) * | 2020-09-07 | 2020-12-08 | 衡东林馨农林科技开发有限责任公司 | Preparation method of plant insecticide for fruit tree planting |
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