CN101971972A - Preparation method for simultaneously extracting Tibet barley serum and Tibet barley dietary fiber - Google Patents
Preparation method for simultaneously extracting Tibet barley serum and Tibet barley dietary fiber Download PDFInfo
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- CN101971972A CN101971972A CN2010105011485A CN201010501148A CN101971972A CN 101971972 A CN101971972 A CN 101971972A CN 2010105011485 A CN2010105011485 A CN 2010105011485A CN 201010501148 A CN201010501148 A CN 201010501148A CN 101971972 A CN101971972 A CN 101971972A
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Abstract
The invention provides a preparation method for simultaneously extracting Tibet barley serum and Tibet barley dietary fiber. The method sequentially comprises the following steps of: cleaning tender Tibet barley leaves, soaking the cleaned leaves into hot water for enzyme inactivation and sterilization, cleaning the leaves again, and dry-pressing the leaves; then performing supercritical extraction, and collecting an extraction component containing the Tibet barley serum and an extraction component containing the Tibet barley dietary fiber respectively; performing low-temperature grinding and spray drying on the extraction component containing the Tibet barley serum to obtain powdery Tibet barley serum; and performing high-speed centrifugal dehydration, constant-temperature drying and super-micro crushing on the extraction component containing the Tibet barley dietary fiber to obtain powdery Tibet barley dietary fiber. The method ensures the reality of products, reduces the cost of raw materials, and has no pollution.
Description
Technical field
The present invention relates to technical field of bioengineering, be specifically related to a kind of preparation method who extracts highland barley young leaf green juice and barley diet fiber simultaneously.
Background technology
In recent years, medical expert both domestic and external, nutrition expert have high evaluation to barley leaf based food in effect aspect medical science and the health care.Barley young leaf is the seedling of barley growth to 20～30cm, and the contained various nutrients of the seedling in this period are the abundantest.Country such as the fashionable Japan of barley young leaf green juice series products, Taiwan and America and Europe history of existing more than ten years.
Highland barley is a kind of cereal crop of grass family Hordeum, and because of coetonium shell in it separates, seed is exposed, so claim hull-less barley, highland barley, Mi Damai again.Highland barley had long cultivation history in the Qinghai-Tibet Platean, apart from modern existing about 3500.Highland barley mainly is distributed in the state, Ganzi in China Tibet, Qinghai, Sichuan and Aba state, the enlightening celebrating in Yunnan, the areas such as Gannan in Gansu.Highland barley has abundant nutritive value and outstanding health-care effect.In the Qinghai-Tibet Platean of high and cold anoxic, be no lack of the centenarian why, this is undivided with the medical health care function effect that normal food highland barley and highland barley are given prominence to.Put down in writing according to supplement to the Herbal: highland barley, during the therapeutic method to keep the adverse qi flowing downward is wide, strong lean power, dehumidifying sweating, antidiarrheal.Tibetan medicine's ancient books and records " brilliant pearl book on Chinese herbal medicine " more highland barley as a kind of important drugs, be used for the treatment of multiple disease.Up-to-date studies show that, highland barley is rich in beta glucan, dietary fiber, vegetable protein, trace element, amylopectin and active mineral matter.Highland barley young leaf green juice (Tibet Barley Serum) and barley diet fiber (Tibet Barley Dietary Fiber) they are that two kinds of equilibriums contain the plain and tens kinds of trace elements of the big basic nutritions of needed by human body six, have remarkable toxin expelling effect, but and the high alkalinity pure natural healthy food of vegetative cell.The undesirable health status that highland barley young leaf green juice and barley diet fiber can improve comprises: cardiovascular and cerebrovascular diseases such as constipation, halitosis, body odor, obesity, diabetes, uremia, hypertension, artery sclerosis, cancer, osteoporosis, calculosis, ulcerate disease, other chronic inflammations, gout, liver diseases, anaemia, climacteric metancholia, pregnant and lying-in women's skin are given birth to acne, coarse, allergy, lassitude and weak etc.
Highland barley young leaf green juice main component and effect: 1. natural complex and mineral matter: contain abundant natural thiamine (vitamin B1), riboflavin (vitamin B2), niacin, vitamin E etc., these materials are grown promoting health all positive interactively, contains a large amount of active mineral matters simultaneously.2. the king of base-forming food (balance blood pH): human 80% disease is relevant with acidic constitution, and acidic constitution is the source of all kinds of diseases and ailments, and the basicity of highland barley young leaf green juice is up to 66.5, can in body inner acidic toxin, Balancing effectively improves acidic constitution.3. chlorophyll: contain the chlorophyll that the international nutritionist of abundant quilt is called " green blood " in the highland barley young leaf green juice.Chlorophyllous structure is closely similar with the red blood cell of human body, therefore is called as " green blood ".Chlorophyll has the very strong body odor function that neutralizes a toxin, purifies the blood, eliminates, and also has the bactericidal antiphlogistic effect simultaneously, can be to a lot of inflammation, and as chafing, wound, cureless gastric ulcer, enteritis all have an unexpected effect.Chlorophyll can stop in the body metabolism process and produces sulfide, therefore can be to halitosis, and underarm odor has good deodorization.4. organized enzyme: also have multiple biology enzyme in the highland barley young leaf green juice, effectively poisonous peroxide in the decomposer promotes wastes metabolism, as SOD organized enzyme antioxidant content etc., can get rid of pesticidal toxin, the opposing free radical.5. protein: the highland barley young leaf green juice contains the quality plant protein that human body easily absorbs.If highland barley is leaf dietary fiber main component and effect: contain natural soluble dietary fiber about 90% 1.: effectively skin maintenance of dietary fiber, increase satiety, and help the control body weight, and can improve hypertension, diabetes, fatty liver, symptoms such as artery sclerosis reduce and suffer from the cancer risk.2. contain a certain amount of protein, vitamin and mineral matter.
In the prior art, the barley young leaf series products adopts the vulgare of executing chemical fertilizer or wheat leaf as raw material, and its preparation technology carries out crushing packing after adopting the conventional method drying usually again.In order to shorten the growth time of barley or wheat, increase output, people use the synthetic fertilizer of chemical industry usually; The use of chemical fertilizer has weakened the production capacity and the resistant to diseases and insects in crops, beneficial trace elements can not effectively be absorbed by crop on the one hand a large amount of soil, cause the crops that disease and pest easily takes place on the other hand, thereby increased the possibility of using agricultural chemicals, the indirect harm that has caused residues of pesticides and to the pollution of environment.The barley young leaf series products uses the conventional drying method, the vitamins and other nutritious components in the as easy as rolling off a log destruction product of the high temperature in its dry run in process of production.Barley young leaf series products on the market does not separate the nutriment of different efficacies mostly in addition, thereby can not provide nutritious supplementary pharmaceutical for different crowds targetedly.
The present invention overcomes the above defective of prior art, with the highland barley tender leaf from the Qinghai-Tibet Platean is raw material, whole process does not add other animal derived additives, guaranteed the Islamic of product, also guaranteed the green non-pollution of product, the goods that extremely need for Muslim country and countries in the world food, health products circle.Simultaneously, the present invention can keep the nutritional labeling in the highland barley tender leaf effectively, reduces cost of material, and is pollution-free, is fit to suitability for industrialized production.
Summary of the invention
The invention provides a kind of preparation method who extracts highland barley young leaf green juice and barley diet fiber simultaneously, it is characterized in that, may further comprise the steps successively:
(1) highland barley tender leaf is placed to soak in the hot water and is killed the enzyme sterilization after cleaning, and after cleaning once more, press dry with press drier;
(2) highland barley tender leaf after will pressing dry carries out supercritical extract, collects the extracted component that contains the highland barley young leaf green juice, the extracted component that contains dietary fiber respectively;
(3) the described extracted component that contains the highland barley young leaf green juice is carried out cryogrinding, spray-dried after, obtain pulverous highland barley young leaf green juice;
(4) the described extracted component that contains dietary fiber is carried out the high speed centrifugation dehydration, after freeze-day with constant temperature, ultramicro grinding, obtain Powdered barley diet fiber.
Described highland barley tender leaf among the present invention is 20～30 centimetres the tender seedling of highland barley of growing to from the Qinghai-Tibet Platean.Described highland barley tender leaf is the secondary tender leaf that highland barley regrows after harvesting.
Be to adopt 85 ℃ of pure water to soak in the step described in the present invention (1).Among the present invention, the powder in the described step (3) behind the cryogrinding is more than 200 orders.Powder in the described step (4) after the ultramicro grinding is the above homogeneous powder of 160 orders.
The present invention adopts supercritical extraction method, and the highland barley leaf after pressing dry is divided into three parts, and a part is that the extracted component, the part that contain the highland barley young leaf green juice are a spot of residue for extracted component, the another part that contains dietary fiber.Collect the extracted component that contains the highland barley young leaf green juice respectively, contain the extracted component of dietary fiber.The present invention adopts the way of supercritical extract to extract two kinds of nutritional labelings, overall process is without organic solvent, the vehicle substance of exhausted noresidue, thus prevented the existence of harmful thing in the leaching process and, guaranteed 100% pure natural property the pollution of environment.
The present invention adopts 80 ℃ of pure water to soak, and makes the color of the enzyme deactivation maintenance highland barley leaf in the highland barley leaf on the one hand, plays oxidizing ferment in the deactivation highland barley tender leaf, avoids the rotten effect of product, also plays sterilization on the other hand.
The present invention adopts highland barley tender leaf from Qinghai-Tibet highland barley producing region as raw material, guaranteed the green non-pollution of product on the one hand, owing to the particularity of highland barley, the highland barley young leaf green juice of extraction and barley diet fiber have abundanter more fully nutrition than the like product that extracts from barley on the other hand.Do not add other animal derived additive and organic solvents in the whole process of preparation of the present invention, guaranteed the Islamic of product,, guaranteed the green non-pollution of product simultaneously yet for Muslim country and countries in the world health care of food product circle provide the goods that very need.And, only use running water and pure water among the preparation method of the present invention, do not use other chemical reagent, also do not produce the waste residue and liquid waste gas of contaminated environment in the technical process, protected the ecological environment in the highland barley place of production well.
What the present invention adopted extracts the highland barley young leaf green juice with low temperature colloidal grinding technology, has kept the nutritional labeling in the highland barley tender leaf effectively, has avoided extreme condition to cause the loss of food nourishment composition.Adopt the recovery rate of its nutritional labeling of preparation method of the present invention can reach more than 95%, effectively control production cost.The present invention adopts superfine communication technique, efficiently solves inhomogeneous, the inconsistent technical problem of granularity shape of product pulverizing that conventional breaking method causes, thereby prepares the above homogeneous powder of 160 orders easily.Use technology of the present invention, from the secondary tender leaf that gathers in the back regrowth, can also extract highland barley young leaf green juice and barley diet fiber, further reduced cost of material, be fit to suitability for industrialized production.
The specific embodiment
Below in conjunction with the specific embodiment the present invention is described in further detail.
Preparation were established of the present invention mainly comprises:
Tender seedling → the preliminary treatment of the highland barley of 20～30cm → 80 ℃ sterilization soaks → press dry → supercritical extract → obtain extracted component →
Preparation method of the present invention, detailed process is as follows:
(1) harvesting is from 20～30 centimetres the tender seedling of highland barley that grows into of Qinghai-Tibet Platean, and transports to workshop in harvested 30 minutes.Wash after rejecting impurity.The highland barley tender leaf of cleaning is put into 80 ℃ of pure water and was soaked 3 minutes, kills the enzyme sterilization.Take out the back and use pure water rinsing, be cooled to room temperature rapidly, press dry with press drier then.
(2) the highland barley leaf after pressing dry enters and carries out supercritical extract in the SFE equipment, collects the extracted component that contains the highland barley young leaf green juice, the extracted component that contains dietary fiber.
(3) refrigerated brine of unlatching colloid mill adds 45% pure water of measuring in the extracted component that contains the highland barley young leaf green juice, grind, and adjusts the colloid mill fineness gradually, until being ground to more than 200 orders.Ground material is delivered to immediately and carries out spray-drying between spray-drying, keeps between 80 to 85 ℃ of the EATs below 172 ℃, leaving air temp, and the material of grinding was finished drying in 1 hour.The powder that spray-drying is collected is product highland barley young leaf green juice, and finished product is detected back packing warehouse-in.
(4) extracted component that contains dietary fiber collected of supercritical extract enters supercentrifuge and dewaters, and collects centrifugal filter cake.Centrifugal filter cake is uniformly dispersed, and enters to carry out drying in the constant temperature blast drier 60～65 ℃ of constant temperature, dry 8～10 hours.Dried material enters micronizer and carries out micro mist, regulates grinding particle size to 160 order, collects the product barley diet fiber after pulverizing.The finished product sampling detects back packing warehouse-in.
Product highland barley young leaf green juice and barley diet fiber that the inventive method prepares contain nutritional labeling as shown in the following Table 1.
Embodiment 1
20～30 centimetres the tender seedling of highland barley in 1000 square metres of farmlands of harvesting gets highland barley tender leaf 243kg, transports to workshop in harvested 30 minutes.Reject impurity such as dead leaf weeds, with using pure water rinsing again behind the blue or green repeatedly wash clean of running water.
The highland barley tender leaf of cleaning is put into 80 ℃ of pure water and was soaked 3 minutes, kills the enzyme sterilization.Take out the back and use pure water rinsing, be cooled to room temperature rapidly, press dry with press drier then, must press dry material 123.3kg.Highland barley leaf after pressing dry enters and carries out supercritical extract in the SFE equipment, collects to such an extent that contain the extracted component 37.4kg of highland barley young leaf green juice and contains the extracted component 81.2kg of dietary fiber.
Open the refrigerated brine of colloid mill, in the extracted component that contains the highland barley young leaf green juice of 37.4kg, add the pure water of 16.8kg, grind, adjust the colloid mill fineness gradually, until being ground to more than 200 orders.Ground material is delivered to immediately and carries out spray-drying between spray-drying, keeps between 80 to 85 ℃ of the EATs below 172 ℃, leaving air temp, collect highland barley young leaf green juice 6.03kg.Finished product is detected back packing warehouse-in.
The extracted component 81.2kg that contains dietary fiber that supercritical extract is collected enters supercentrifuge and dewaters, collect centrifugal filter cake 61.6kg.Careful centrifugal filter cake is trembled is diffusing, and it is dispersed in the tray uniformly, enters and carries out drying in the constant temperature blast drier, 60～65 ℃ of dryings of constant temperature 8 hours.Get dry material 14.60kg after the drying, enter micronizer and carry out micro mist, regulate grinding particle size to 160 order, collect the material meter 14.03kg after pulverizing.The finished product sampling detects back packing warehouse-in.
Highland barley young leaf green juice, barley diet fiber that present embodiment prepares, its assay is as shown in table 2 below.
Embodiment 2
The farmland of once having gathered in is through fertilising and irrigate the back after about 20 days, the highland barley tender leaf of regeneration has reached the requirement of 20～30cm, the tender seedling of regeneration highland barley in 1000 square metres of farmlands of harvesting gets highland barley tender leaf 128kg, transports to workshop in harvested 30 minutes.Reject impurity such as dead leaf weeds, use pure water rinsing again after cleaning up repeatedly with running water.
The highland barley tender leaf of cleaning is put into 80 ℃ of pure water and was soaked 3 minutes, kills the enzyme sterilization.Take out the back and use pure water rinsing, be cooled to room temperature rapidly, press dry with press drier then, must press dry material 64.3kg.Highland barley leaf after pressing dry enters and carries out supercritical extract in the SFE equipment, collects to such an extent that contain the extracted component 19.6kg of highland barley young leaf green juice and contains the extracted component 41.2kg of dietary fiber.
Open the refrigerated brine of colloid mill, in the extracted component that contains the highland barley young leaf green juice of 19.6kg, add the pure water of 8.8kg, grind, adjust the colloid mill fineness gradually, until being ground to more than 200 orders.Ground material is delivered to immediately and carries out spray-drying between spray-drying, keeps between 80 to 85 ℃ of the EATs below 172 ℃, leaving air temp, collect highland barley young leaf green juice 3.19kg.Finished product is detected back packing warehouse-in.
The extracted component 41.2kg that contains dietary fiber that supercritical extract is collected enters supercentrifuge and dewaters, collect centrifugal filter cake 32.4kg.Careful centrifugal filter cake is trembled is diffusing, and it is dispersed in the tray uniformly, enters and carries out drying in the constant temperature blast drier, 60～65 ℃ of dryings of constant temperature 8 hours.Get dry material 7.68kg after the drying, enter micronizer and carry out micro mist, regulate grinding particle size to 160 order, collect the material meter 7.37kg after pulverizing.The finished product sampling detects back packing warehouse-in.
Product highland barley young leaf green juice, barley diet fiber that present embodiment prepares, its assay is as shown in table 3 below.
The above is preferred embodiment of the present invention only, is not to be used for limiting protection scope of the present invention.Be that all equivalences of doing according to content of the present invention change and modification, all should belong to category of the present invention.
Claims (6)
1. a preparation method who extracts highland barley young leaf green juice and barley diet fiber simultaneously is characterized in that, may further comprise the steps successively:
(1) highland barley tender leaf is placed to soak in the hot water and is killed the enzyme sterilization after cleaning, and press dry after cleaning once more;
(2) highland barley tender leaf after will pressing dry carries out supercritical extract, collects the extracted component that contains the highland barley young leaf green juice, the extracted component that contains dietary fiber respectively;
(3) the described extracted component that contains the highland barley young leaf green juice is carried out cryogrinding, spray-dried after, obtain Powdered highland barley young leaf green juice;
(4) the described extracted component that contains dietary fiber is carried out the high speed centrifugation dehydration, after freeze-day with constant temperature, ultramicro grinding, obtain Powdered barley diet fiber.
2. preparation method as claimed in claim 1 is characterized in that, described highland barley tender leaf is 20～30 centimetres the tender seedling of highland barley of growing to that derives from the Qinghai-Tibet Platean.
3. preparation method as claimed in claim 2 is characterized in that, described highland barley tender leaf is the secondary tender leaf that highland barley regrows after harvesting.
4. preparation method as claimed in claim 1 is characterized in that, in the described step (1) is to adopt 85 ℃ of pure water to soak.
5. preparation method as claimed in claim 1 is characterized in that, the powder in the described step (3) behind the cryogrinding is more than 200 orders.
6. preparation method as claimed in claim 1 is characterized in that, the powder in the described step (4) after the ultramicro grinding is the above homogeneous powder of 160 orders.
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| CN104171971A (en) * | 2014-08-11 | 2014-12-03 | 高勇 | Method for preparing organic highland barley green and organic highland barley seedling powder |
| CN105998105A (en) * | 2016-08-01 | 2016-10-12 | 昆明医科大学第附属医院 | Externally applied medicine for treating gout |
| CN108244207A (en) * | 2016-12-28 | 2018-07-06 | 西藏天麦力健康品有限公司 | A kind of biscuit for improving hyperglycemia and weight-reducing and preparation method thereof and purposes |
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| CN109527602A (en) * | 2018-12-07 | 2019-03-29 | 上海交通大学 | If the method for improving highland barley Ye Fenzhong soluble dietary fibre content |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104171971A (en) * | 2014-08-11 | 2014-12-03 | 高勇 | Method for preparing organic highland barley green and organic highland barley seedling powder |
| CN105998105A (en) * | 2016-08-01 | 2016-10-12 | 昆明医科大学第附属医院 | Externally applied medicine for treating gout |
| CN108244207A (en) * | 2016-12-28 | 2018-07-06 | 西藏天麦力健康品有限公司 | A kind of biscuit for improving hyperglycemia and weight-reducing and preparation method thereof and purposes |
| CN108260813A (en) * | 2016-12-30 | 2018-07-10 | 西藏天麦力健康品有限公司 | It is a kind of have the function of improve arthralgia, degenerative joint disease health food and its processing method |
| CN108260814A (en) * | 2016-12-30 | 2018-07-10 | 西藏天麦力健康品有限公司 | A kind of health food and its processing method for having the function of to improve injury gained in sports |
| US11634257B2 (en) | 2017-10-09 | 2023-04-25 | Terumo Bct Biotechnologies, Llc | Lyophilization container and method of using same |
| CN109527602B (en) * | 2018-12-07 | 2022-06-10 | 上海交通大学 | Method for improving content of soluble dietary fiber in highland barley young leaf powder |
| CN109527602A (en) * | 2018-12-07 | 2019-03-29 | 上海交通大学 | If the method for improving highland barley Ye Fenzhong soluble dietary fibre content |
| US11604026B2 (en) | 2019-03-14 | 2023-03-14 | Terumo Bct Biotechnologies, Llc | Lyophilization loading tray assembly and system |
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| US11609042B2 (en) | 2019-03-14 | 2023-03-21 | Terumo Bct Biotechnologies, Llc | Multi-part lyophilization container and method of use |
| US11740019B2 (en) | 2019-03-14 | 2023-08-29 | Terumo Bct Biotechnologies, Llc | Lyophilization loading tray assembly and system |
| US11747082B2 (en) | 2019-03-14 | 2023-09-05 | Terumo Bct Biotechnologies, Llc | Multi-part lyophilization container and method of use |
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Application publication date: 20110216 |