CN107568256A - The preparation method of one vegetative insecticide - Google Patents
The preparation method of one vegetative insecticide Download PDFInfo
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- CN107568256A CN107568256A CN201710873363.XA CN201710873363A CN107568256A CN 107568256 A CN107568256 A CN 107568256A CN 201710873363 A CN201710873363 A CN 201710873363A CN 107568256 A CN107568256 A CN 107568256A
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- 239000002917 insecticide Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 19
- IBFYXTRXDNAPMM-BVTMAQQCSA-N Geniposide Chemical compound O([C@@H]1OC=C([C@@H]2[C@H]1C(=CC2)CO)C(=O)OC)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O IBFYXTRXDNAPMM-BVTMAQQCSA-N 0.000 claims abstract description 10
- IBFYXTRXDNAPMM-FZEIBHLUSA-N Geniposide Natural products COC(=O)C1=CO[C@@H](O[C@H]2O[C@@H](CO)[C@H](O)[C@@H](O)[C@@H]2O)[C@H]2[C@@H]1CC=C2CO IBFYXTRXDNAPMM-FZEIBHLUSA-N 0.000 claims abstract description 10
- 244000068988 Glycine max Species 0.000 claims abstract description 10
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 10
- VGLLGNISLBPZNL-RBUKDIBWSA-N arborescoside Natural products O=C(OC)C=1[C@@H]2C([C@H](O[C@H]3[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O3)OC=1)=C(CO)CC2 VGLLGNISLBPZNL-RBUKDIBWSA-N 0.000 claims abstract description 10
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims description 56
- 239000000843 powder Substances 0.000 claims description 23
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
- 241000894006 Bacteria Species 0.000 claims description 18
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 16
- 238000004821 distillation Methods 0.000 claims description 14
- 235000013311 vegetables Nutrition 0.000 claims description 14
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 12
- 238000000605 extraction Methods 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 239000011780 sodium chloride Substances 0.000 claims description 8
- 241000512000 Asclepias curassavica Species 0.000 claims description 6
- 241000830536 Tripterygium wilfordii Species 0.000 claims description 6
- 239000001569 carbon dioxide Substances 0.000 claims description 6
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 239000012530 fluid Substances 0.000 claims description 6
- 238000007789 sealing Methods 0.000 claims description 6
- 235000015398 thunder god vine Nutrition 0.000 claims description 6
- 241000235342 Saccharomycetes Species 0.000 claims description 4
- 244000025254 Cannabis sativa Species 0.000 claims description 2
- 210000000003 hoof Anatomy 0.000 claims description 2
- 241001037822 Bacillus bacterium Species 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 abstract description 10
- 238000000855 fermentation Methods 0.000 abstract description 7
- 230000004151 fermentation Effects 0.000 abstract description 7
- 239000000575 pesticide Substances 0.000 abstract description 7
- 241000218208 Caltha Species 0.000 abstract description 6
- 235000008749 Caltha palustris Nutrition 0.000 abstract description 6
- 241000238631 Hexapoda Species 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 5
- 241000607479 Yersinia pestis Species 0.000 abstract description 4
- 239000003905 agrochemical Substances 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract description 4
- 239000000084 colloidal system Substances 0.000 abstract description 3
- 238000006555 catalytic reaction Methods 0.000 abstract description 2
- 244000005700 microbiome Species 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract description 2
- 235000016709 nutrition Nutrition 0.000 abstract description 2
- 230000035764 nutrition Effects 0.000 abstract description 2
- 239000000419 plant extract Substances 0.000 abstract description 2
- 239000003814 drug Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 244000063299 Bacillus subtilis Species 0.000 description 4
- 235000008216 herbs Nutrition 0.000 description 4
- 229940079593 drug Drugs 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 150000002611 lead compounds Chemical class 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 235000010576 Artemisia cina Nutrition 0.000 description 1
- 241000296609 Celastrus angulatus Species 0.000 description 1
- 244000281762 Chenopodium ambrosioides Species 0.000 description 1
- 235000000509 Chenopodium ambrosioides Nutrition 0.000 description 1
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 239000005906 Imidacloprid Substances 0.000 description 1
- CLEXYFLHGFJONT-DNMILWOZSA-N Jervine Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H](C(=O)C2=C3C)[C@@H]1[C@@H]2CC[C@@]13O[C@@H]2C[C@H](C)CN[C@H]2[C@H]1C CLEXYFLHGFJONT-DNMILWOZSA-N 0.000 description 1
- 240000000233 Melia azedarach Species 0.000 description 1
- 241000255969 Pieris brassicae Species 0.000 description 1
- 241000500437 Plutella xylostella Species 0.000 description 1
- VQXSOUPNOZTNAI-UHFFFAOYSA-N Pyrethrin I Natural products CC(=CC1CC1C(=O)OC2CC(=O)C(=C2C)CC=C/C=C)C VQXSOUPNOZTNAI-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229940056881 imidacloprid Drugs 0.000 description 1
- YWTYJOPNNQFBPC-UHFFFAOYSA-N imidacloprid Chemical compound [O-][N+](=O)\N=C1/NCCN1CC1=CC=C(Cl)N=C1 YWTYJOPNNQFBPC-UHFFFAOYSA-N 0.000 description 1
- CLEXYFLHGFJONT-UHFFFAOYSA-N jervine Natural products C1C=C2CC(O)CCC2(C)C(C(=O)C2=C3C)C1C2CCC13OC2CC(C)CNC2C1C CLEXYFLHGFJONT-UHFFFAOYSA-N 0.000 description 1
- QRXOCOSLDOPPKH-UHFFFAOYSA-N jervine sulfate Natural products CC1CNC2C(C1)OC3(CCC4=C(C3C)C(=O)C5C4CC=C6CC(O)CCC56C)C2C QRXOCOSLDOPPKH-UHFFFAOYSA-N 0.000 description 1
- KSURRTWGXADWNE-UHFFFAOYSA-N lead;3-(1-methylpyrrolidin-2-yl)pyridine Chemical compound [Pb].CN1CCCC1C1=CC=CN=C1 KSURRTWGXADWNE-UHFFFAOYSA-N 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 230000000361 pesticidal effect Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- HYJYGLGUBUDSLJ-UHFFFAOYSA-N pyrethrin Natural products CCC(=O)OC1CC(=C)C2CC3OC3(C)C2C2OC(=O)C(=C)C12 HYJYGLGUBUDSLJ-UHFFFAOYSA-N 0.000 description 1
- VJFUPGQZSXIULQ-XIGJTORUSA-N pyrethrin II Chemical compound CC1(C)[C@H](/C=C(\C)C(=O)OC)[C@H]1C(=O)O[C@@H]1C(C)=C(C\C=C/C=C)C(=O)C1 VJFUPGQZSXIULQ-XIGJTORUSA-N 0.000 description 1
- 229940080817 rotenone Drugs 0.000 description 1
- JUVIOZPCNVVQFO-UHFFFAOYSA-N rotenone Natural products O1C2=C3CC(C(C)=C)OC3=CC=C2C(=O)C2C1COC1=C2C=C(OC)C(OC)=C1 JUVIOZPCNVVQFO-UHFFFAOYSA-N 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention belongs to technical field of pesticide, and in particular to the preparation method of a vegetative insecticide.The present invention is run using pony and white bombys batryticatus provides source as nutrition; on the one hand nutriment is provided for fermentation; on the other hand plant surface is protected; prevent plant from being gnawed by insect; the mixing such as soybean are fermented using microorganism simultaneously; obtain colloid class material; improve the stickiness of insecticide, then by with the plant extract such as membranaceous marshmarigold herb, add insect resistant effect; then under the catalysis of titanium dioxide; by Geniposide, pest-resistant beneficial thing is crosslinked with colloid class material, makes slowly to discharge beneficial to thing; the term of validity is added, reduces the sprinkling number of agricultural chemicals.
Description
Technical field
The invention belongs to technical field of pesticide, and in particular to the preparation method of a vegetative insecticide.
Background technology
Medicine usage histories that insecticide is mainly used in preventing and treating agricultural pests and urban health insect are long-range, dosage is big, product
Kind is more.In twentieth century, agriculture develops rapidly, and insecticide makes farm output rise higher.But nearly all insecticide all can be tight
Important place changes the ecosystem, and most of harmful, others can be concentrated in food chain.We must be in agricultural development
With obtaining balance in environment and health.Biological source insecticide and the class of chemical synthesis insecticide two can be by sources divided into.Bt insecticides
Production method mainly have liquid deep layer fermenting and the class of semisolid fermentation two.Two-step method produces, and is in semisolid fermentation method
On the basis of improved, improved and created and sum up come effective, easy, practical Bt insecticide production technologies, its produce
Technique is simple, and scale is changeable, is particularly suitable for promoting in rural small enterprise, the production of insecticide can be greatly lowered
Cost, the development to microbial pesticide, plays a positive role.Particularly to the vegetable-crop pest-insect for eating leaf, such as cabbage caterpillar, diamondback moth
Prevention effect highly significant.
There are two purposes to botanical pesticide active matter Quality Research both at home and abroad.First, the new chemistry of synthesis is found from plant
The lead compound of agricultural chemicals, most successful example such as come from the lead compound of the pyrethrin pesticide of Dalmatian chrysanthemum, come from nicotine
Lead compound of imidacloprid pesticide etc..Second, directly plant resource explorationses new plant agriculture of the application with pesticidal active substance
Medicine.It is external mostly because resource shortage is then based on first purpose.Because vast territory and abundant resources, plant resources enriches in China, many plants
There is cultivation history.Therefore, most directly appliable plant resource, develops botanical pesticide.The plant agriculture that the country has developed at present
Medicine is mainly more using kuh-seng alkali preparation.It is other to also have chinaberry element, nicotine, Wormseed element, jervine, Celastrus angulatus, rotenone etc..These are planted
Material resource agricultural chemicals plays a good role for the production of crops non-polluted cultivation and green food.But current vegetable insecticide
Often, the term of validity is short, considerably increases the usage amount of medicine for spray.
The content of the invention
The technical problems to be solved by the invention：For current vegetable insecticide spray often, the problem of term of validity is short,
The invention provides the preparation method of a vegetative insecticide.
In order to solve the above technical problems, the present invention is using technical scheme as described below：
The preparation method of one vegetative insecticide, the preparation method comprise the following steps：
（1）Pony is run and white bombys batryticatus is put into pulverizer and crushed, collects crushed mixture, by crushed mixture, soybean,
Sodium chloride solution is put into container and stirred, and stands；
（2）After standing terminates, bacterium powder will be added into container, will be stirred, sealing container, be left to ferment, in collection vessel
Fermenting mixture；
（3）Count in parts by weight, take 70~80 parts of ethanol solutions, the fermenting mixture in 35~40 parts of containers, 15~17 portions of horses
Hoof grass, 11~14 parts of paniculate swallowworts and 7~9 portions of tripterygium wilfordiis, are put into bruisher and are smashed to pieces, and mixture is smashed in collection to pieces, then will be smash
Broken mixture carries out supercritical carbon dioxide extracting, collects extraction mixture；
（4）Extraction mixture is filtered, collects filtrate, and is distilled, collects distillation residue, then distillation is remaining
Thing, Geniposide and titanium dioxide are put into reactor, the stirring reaction at 90~95 DEG C, collect stirring mixture, and carried out
Filter, filtered fluid is collected, produces vegetable insecticide.
The step（1）Middle pony runs and the mass ratio of white bombys batryticatus is 4:6~9, crushed mixture, soybean, sodium chloride are molten
The mass ratio of liquid is 3~5:7:10~12.
The step（2）Middle bacterium powder is any one in bacillus subtilis bacterium powder, saccharomycete bacterium powder.
The step（2）The addition of middle bacterium powder is the 4~7% of white bombys batryticatus quality.
The step（4）Mass ratio in middle distillation residue, Geniposide and titanium dioxide is 15~17:0.9~1.1:2
~4.
Compared with other method, advantageous effects are the present invention：
The present invention is run using pony and white bombys batryticatus provides source as nutrition, on the one hand provides nutriment for fermentation, on the other hand right
Plant surface is protected, and prevents plant from being gnawed by insect, while the mixing such as soybean are fermented using microorganism, obtains glue
Matter class material, improves the stickiness of insecticide, then by with the plant extract such as membranaceous marshmarigold herb, insect resistant effect is added, then two
Under the catalysis of titanium oxide, by Geniposide, pest-resistant beneficial thing is crosslinked with colloid class material, makes slowly to discharge beneficial to thing,
The term of validity is added, reduces the sprinkling number of agricultural chemicals.
Embodiment
The selection of bacterium powder is：Any one in bacillus subtilis bacterium powder, saccharomycete bacterium powder.
The preparation method of one vegetative insecticide, the preparation method comprise the following steps：
（1）It is 4 in mass ratio:6~9, pony is run and white bombys batryticatus is put into pulverizer and crushed, collects crushed mixture,
It is 3~5 in mass ratio:7:10~12, crushed mixture, soybean, 0.8mol/L sodium chloride solutions are put into container and stirred
It is even, 5~8h is stood at 30 DEG C；
（2）After standing terminates, bacterium powder will be added into container, will be stirred, and sealing container, at 32~36 DEG C, stand hair
Ferment 1~3 day, the fermenting mixture in collection vessel；
（3）Count in parts by weight, take 70~80 parts of 1.3mol/L ethanol solutions, the fermenting mixture in 35~40 parts of containers, 15
~17 parts of membranaceous marshmarigold herbs, 11~14 parts of paniculate swallowworts and 7~9 portions of tripterygium wilfordiis, it is put into bruisher and carries out smashing 10 to pieces in 12000r/min
~15min, collection smash mixture to pieces, then will smash to pieces mixture carry out supercritical carbon dioxide extracting, extracting pressure be 10~
12MPa, temperature are 40~45 DEG C, and flow is 10~12kg/h, collect extraction mixture；
（4）Extraction mixture is filtered, collects filtrate, and is distilled, reclaims ethanol, collects distillation residue, then press
Mass ratio is 15~17:0.9~1.1:2~4, distillation residue, Geniposide and titanium dioxide are put into reactor, 90~
Stirring reaction at 95 DEG C, stirring mixture is collected, and filtered, collected filtered fluid, produce vegetable insecticide.
Example 1
The selection of bacterium powder is：Saccharomycete bacterium powder.
The preparation method of one vegetative insecticide, the preparation method comprise the following steps：
（1）It is 4 in mass ratio:7, pony is run and white bombys batryticatus is put into pulverizer and crushed, crushed mixture is collected, by matter
Amount is than being 4:7:11, crushed mixture, soybean, 0.8mol/L sodium chloride solutions are put into container and stirred, at 30 DEG C
Stand 6h；
（2）After standing terminates, bacterium powder will be added into container, will be stirred, sealing container, at 34 DEG C, standing for fermentation 2
My god, the fermenting mixture in collection vessel；
（3）Count in parts by weight, take 75 parts of 1.3mol/L ethanol solutions, the fermenting mixture in 38 parts of containers, 16 parts of membranaceous marshmarigold herbs,
12 parts of paniculate swallowworts and 8 portions of tripterygium wilfordiis, it is put into bruisher and carries out smashing 13min to pieces in 12000r/min, mixture is smashed in collection to pieces, then
Mixture will be smashed to pieces and carry out supercritical carbon dioxide extracting, extracting pressure 11MPa, temperature is 43 DEG C, flow 11kg/h, is received
Collection extraction mixture；
（4）Extraction mixture is filtered, collects filtrate, and is distilled, reclaims ethanol, collects distillation residue, then press
Mass ratio is 16:1.0:3, distillation residue, Geniposide and titanium dioxide are put into reactor, the stirring reaction at 93 DEG C,
Stirring mixture is collected, and is filtered, filtered fluid is collected, produces vegetable insecticide.
Example 2
The selection of bacterium powder is：Bacillus subtilis bacterium powder.
The preparation method of one vegetative insecticide, the preparation method comprise the following steps：
（1）It is 4 in mass ratio:9, pony is run and white bombys batryticatus is put into pulverizer and crushed, crushed mixture is collected, by matter
Amount is than being 5:7:12, crushed mixture, soybean, 0.8mol/L sodium chloride solutions are put into container and stirred, at 30 DEG C
Stand 8h；
（2）After standing terminates, bacterium powder will be added into container, will be stirred, sealing container, at 36 DEG C, standing for fermentation 3
My god, the fermenting mixture in collection vessel；
（3）Count in parts by weight, take 80 parts of 1.3mol/L ethanol solutions, the fermenting mixture in 40 parts of containers, 17 parts of membranaceous marshmarigold herbs,
14 parts of paniculate swallowworts and 9 portions of tripterygium wilfordiis, it is put into bruisher and carries out smashing 15min to pieces in 12000r/min, mixture is smashed in collection to pieces, then
Mixture will be smashed to pieces and carry out supercritical carbon dioxide extracting, extracting pressure 12MPa, temperature is 45 DEG C, flow 12kg/h, is received
Collection extraction mixture；
（4）Extraction mixture is filtered, collects filtrate, and is distilled, reclaims ethanol, collects distillation residue, then press
Mass ratio is 17:1.1:4, distillation residue, Geniposide and titanium dioxide are put into reactor, the stirring reaction at 95 DEG C,
Stirring mixture is collected, and is filtered, filtered fluid is collected, produces vegetable insecticide.
Example 3
The selection of bacterium powder is：Bacillus subtilis bacterium powder.
The preparation method of one vegetative insecticide, the preparation method comprise the following steps：
（1）It is 4 in mass ratio:6, pony is run and white bombys batryticatus is put into pulverizer and crushed, crushed mixture is collected, by matter
Amount is than being 3:7:10, crushed mixture, soybean, 0.8mol/L sodium chloride solutions are put into container and stirred, at 30 DEG C
Stand 5h；
（2）After standing terminates, bacterium powder will be added into container, will be stirred, sealing container, at 32 DEG C, standing for fermentation 1
My god, the fermenting mixture in collection vessel；
（3）Count in parts by weight, take 70 parts of 1.3mol/L ethanol solutions, the fermenting mixture in 35 parts of containers, 15 parts of membranaceous marshmarigold herbs,
11 parts of paniculate swallowworts and 7 portions of tripterygium wilfordiis, it is put into bruisher and carries out smashing 10min to pieces in 12000r/min, mixture is smashed in collection to pieces, then
Mixture will be smashed to pieces and carry out supercritical carbon dioxide extracting, extracting pressure 10MPa, temperature is 40 DEG C, flow 10kg/h, is received
Collection extraction mixture；
（4）Extraction mixture is filtered, collects filtrate, and is distilled, reclaims ethanol, collects distillation residue, then press
Mass ratio is 15:0.9:2, distillation residue, Geniposide and titanium dioxide are put into reactor, the stirring reaction at 90 DEG C,
Stirring mixture is collected, and is filtered, filtered fluid is collected, produces vegetable insecticide.
Comparative example：The vegetable insecticide of Hebei bio tech ltd production
Method：The farmland of 4 mu of sizes is chosen, is divided into 4 pieces, sprays medicine.
Pest controling effect situation such as table 1
Table 1
From the foregoing, it will be observed that the vegetable insecticide deinsectization ability that the present invention is produced is strong.Effective time is grown, and prevents and treats great efforts, is worth pushing away
Wide and use.
Claims (5)
1. the preparation method of a vegetative insecticide, it is characterised in that the preparation method comprises the following steps：
（1）Pony is run and white bombys batryticatus is put into pulverizer and crushed, collects crushed mixture, by crushed mixture, soybean,
Sodium chloride solution is put into container and stirred, and stands；
（2）After standing terminates, bacterium powder will be added into container, will be stirred, sealing container, be left to ferment, in collection vessel
Fermenting mixture；
（3）Count in parts by weight, take 70~80 parts of ethanol solutions, the fermenting mixture in 35~40 parts of containers, 15~17 portions of horses
Hoof grass, 11~14 parts of paniculate swallowworts and 7~9 portions of tripterygium wilfordiis, are put into bruisher and are smashed to pieces, and mixture is smashed in collection to pieces, then will be smash
Broken mixture carries out supercritical carbon dioxide extracting, collects extraction mixture；
（4）Extraction mixture is filtered, collects filtrate, and is distilled, collects distillation residue, then distillation is remaining
Thing, Geniposide and titanium dioxide are put into reactor, the stirring reaction at 90~95 DEG C, collect stirring mixture, and carried out
Filter, filtered fluid is collected, produces vegetable insecticide.
2. the preparation method of vegetable insecticide according to claim 1, it is characterised in that the step（1）Middle pony run and
The mass ratio of white bombys batryticatus is 4:6~9, crushed mixture, soybean, the mass ratio of sodium chloride solution are 3~5:7:10~12.
3. the preparation method of vegetable insecticide according to claim 1, it is characterised in that the step（2）Middle bacterium powder is withered
Any one in careless bacillus bacterium powder, saccharomycete bacterium powder.
4. the preparation method of vegetable insecticide according to claim 1, it is characterised in that the step（2）Middle bacterium powder adds
Enter 4~7% that amount is white bombys batryticatus quality.
5. the preparation method of vegetable insecticide according to claim 1, it is characterised in that the step（4）Middle distillation is remaining
Mass ratio in thing, Geniposide and titanium dioxide is 15~17:0.9~1.1:2~4.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107637611A (en) * | 2017-10-16 | 2018-01-30 | 江苏长龙国际贸易有限公司 | The preparation method of one vegetative insecticide |
| CN109168810A (en) * | 2018-09-25 | 2019-01-11 | 广西隆林金秋生态农业发展有限公司 | A method of preventing and treating fertile mandarin orange pest and disease damage |
| CN111387224A (en) * | 2020-05-09 | 2020-07-10 | 渠志灿 | Botanical insecticide prepared based on pepper leaves and preparation method thereof |
| CN111990416A (en) * | 2020-09-22 | 2020-11-27 | 河北农业大学 | Insecticidal substance, insecticide and preparation method and application thereof |
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